CN102018274A - Preparation method for regenerating tobacco leaves by using aromatic tobacco papermaking method - Google Patents

Preparation method for regenerating tobacco leaves by using aromatic tobacco papermaking method Download PDF

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CN102018274A
CN102018274A CN2010106159846A CN201010615984A CN102018274A CN 102018274 A CN102018274 A CN 102018274A CN 2010106159846 A CN2010106159846 A CN 2010106159846A CN 201010615984 A CN201010615984 A CN 201010615984A CN 102018274 A CN102018274 A CN 102018274A
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tobaccos
turkish tobaccos
tobacco
turkish
reconstituted
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CN102018274B (en
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邱晔
王建
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Yunnan Academy of Tobacco Science
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Yunnan Academy of Tobacco Science
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Abstract

The invention discloses a preparation method for regenerating tobacco leaves by using an aromatic tobacco papermaking method, belonging to the technical field of tobacco leaf regeneration by using a papermaking method in the tobacco industry. The preparation method is characterized by comprising the following steps of: extracting aromatic tobacco with an aqueous solution containing an organic solvent, separating solid and liquid, a concentrating extract into extractum, adding aromatic tobacco seed powder and a mixed solvent to the extractum to prepare coating fluid; mixing aromatic tobacco slag with tobacco cabo slag extracted through water to pulp into a film base through manufacturing and forming paper with pulp; coating the film base with the prepared coating liquid, drying, cutting and crushing into finished regenerating tobacco leaf products of aromatic tobacco type by using the aromatic tobacco papermaking method. The invention provides the tobacco regenerating method by using the papermaking method which can fully utilize the whole leaves, scraps, broken leaves and aromatic tobacco seed resources and have the characteristic of producing typical aromatic tobacco.

Description

A kind of production method of Turkish tobaccos type papermaking-method reconstituted tobaccos
Technical field
The present invention relates to a kind of production method of Turkish tobaccos type papermaking-method reconstituted tobaccos, belong to tobacco industry papermaking-method reconstituted tobaccos processing technique field.
Background technology
Turkish tobaccos are important raw tobacco materials of producing blended type cigarette, flue-cured tobacco an unusually sweet smell type cigarette, account for the usage ratio of 10-20% in the blended type cigarette prescription usually.Turkish tobaccos originate in Mediterranean coastwise contries, and big with the output of tradition countries such as Greece, Turkey, quality is good, on Thailand, the Chinese Baoshan and Xinjiang and other places not small-scale plantation are also arranged decades recently.Just lower because of its per mu yield, global annual output still is limited, and the gesture of anxiety is arranged during supply on the international market.Turkish tobaccos are easily made broken when modulation in addition, contain last rate height after the tobacco leaf chopping, filling capacity and flammability are also not as reasons such as other tobacco ingredients, cigarette industry is very low always to the practical efficiency of Turkish tobaccos raw material, and byproducts such as a large amount of fragments that produced in the process and broken end often can only be as waste disposal.In addition, Turkish tobaccos also have a large amount of cigarette seeds to produce in the later stage of field growing, though the feature that its cigarette seed is rich in several amino acids and Turkish tobaccos causes perfumery, but extract the tobacco aromatics using except seldom being used at present, most of Turkish tobaccos seed is still discarded in the field, even be used to extract spices, because of its production yield is not high, the solid slag of a large amount of extractions that produced still can't utilize.
With the best approach of tobacco waste comprehensive utilization and resource regeneration is to produce the reconstituted tobacco product, the processing of reconstituted tobacco mainly contains several technologies such as thick slurry method, roll-in method, paper process at present, wherein the highest with the technology content of paper process again, institute's product processed (papermaking-method reconstituted tobaccos) is best in quality, and this series products also has the releasing content of coke tar lower than natural tobacco leaf (be about tobacco leaf 50%), higher filling capacity (be about tobacco leaf 1.5 times), characteristics such as better flammability, and suction flavor is preferable.U.S. B﹠amp; The international monopoly PCT/US2005/027675 of W tobacco company application and just to relate to one to Chinese patents CN200580035343.0 serve as the production method of the burley tobaccos type reconstituted tobacco of a small amount of batching based on burley tobaccos raw material, Turkish tobaccos, it has adopted thick slurry method (belt flows and casts) technology.It is the method that body material is produced Turkish tobaccos type reconstituted tobacco with Turkish tobaccos that Korean Patent KR97064476-A also relates to one, but employing is roll-in method technology.In addition, these patents all also do not relate to a kind of whole leaf that can full price utilizes Turkish tobaccos, fragment, broken end and abundant cigarette seed resource and adopt the method for paper process explained hereafter typical perfumes cigarette type reconstituted tobacco.
Summary of the invention
The objective of the invention is to the problem that exists at existing processed flavors cigarette type reconstituted tobacco, provide a kind of and can full price utilize the Turkish tobaccos resource and be processed as the production method of typical perfumes cigarette type papermaking-method reconstituted tobaccos.
Purpose of the present invention is achieved by the following technical programs.
A kind of production method of Turkish tobaccos type papermaking-method reconstituted tobaccos, the step that method adopts is:
(1) Turkish tobaccos through Separation of Solid and Liquid, obtain Turkish tobaccos extract and spices scarp with containing the extraction with aqueous solution of organic solvent, become Turkish tobaccos medicinal extract standby wherein Turkish tobaccos extract evaporation and concentration;
(2) flue-cured tobacco offal water extracts, through Separation of Solid and Liquid and after discarding extract, and gained stalk slag and spices scarp mixed pulp, manufacturing paper with pulp in the paper machine portion of reconstituted tobacco production line is shaped to the sheet base;
(3) the Turkish tobaccos seed is finish-ground to fine powder, adds in the above-mentioned Turkish tobaccos medicinal extract, add the allotment solvent again and be deployed into coating fluid;
(4) deployed coating fluid is applied to the sheet base on the reconstituted tobacco production line, dries subsequently, divide and be cut to Turkish tobaccos type papermaking-method reconstituted tobaccos finished product.
Described Turkish tobaccos comprise that Turkish tobaccos put in order any one or more in leaf, Turkish tobaccos fragment and the broken end of Turkish tobaccos.
The described aqueous solution that contains organic solvent that is used to extract Turkish tobaccos is the aqueous solvent of ethanol or propane diols.
The described aqueous solution that contains organic solvent that is used for extracting Turkish tobaccos, the volume ratio of ethanol or propane diols and water is: 10~35: 90~65.
The mass ratio that feeds intake of described Turkish tobaccos and flue-cured tobacco offal is: 50~80: 50~20.
The powder that described Turkish tobaccos seed is finish-ground to is the above fine powders of 60 orders.
The ratio that described Turkish tobaccos seed fine powder joins in the Turkish tobaccos medicinal extract is 0.5~10% of a Turkish tobaccos medicinal extract quality.
Described coating fluid allotment solvent is that volume ratio is the mixed solvent of propane diols-glycerine-water of 1: 1: 1~4, and the solvent of this proportioning is the present invention through checking back the effect miscible agent and anticorrosion, the humectant of Turkish tobaccos medicinal extract, cigarette seed fine powder preferably.
The Turkish tobaccos medicinal extract that will add behind the Turkish tobaccos seed fine powder with the mixed solvent of described propane diols-glycerine-water is deployed into the coating fluid that density is 1.15~1.25g/ml.
Useful benefit of the present invention is:
1, full price has been utilized the Turkish tobaccos resource.The present invention adopts paper process technology, with atomatic tobacco and byproduct thereof, extracting, after the Separation of Solid and Liquid, be respectively applied for medicinal extract and reconstituted tobacco sheet base that coating fluid is produced in preparation, can fully utilize any one or more resource in the whole leaf, fragment, broken end of Turkish tobaccos fully.Particularly the present invention also is finish-ground to fine powder with the Turkish tobaccos seed, be deployed into coating fluid with Turkish tobaccos medicinal extract, mixed solvent again, mode by the coating of sheet base all is applied to it in reconstituted tobacco product, has more realized the full price utilization to abundant Turkish tobaccos seed resource.
2, improve product quality, strengthened the style and features of product.One aspect of the present invention selects for use the specific aqueous solution that contains organic solvent to extract Turkish tobaccos according to the characteristics of the contained chemical substance of Turkish tobaccos, causes perfumery and reverts to the reconstituted tobacco product by coating method with the feature of abundant extraction Turkish tobaccos; On the other hand, be rich in the characteristics that several amino acids and Turkish tobaccos feature cause perfumery, with its full price utilization and add in right amount in the reconstituted tobacco product according to the Turkish tobaccos seed.So practice both can improve the suction flavor of product, more can strengthen the style and features of product typical perfumes cigarette.
3, product yield height.Flue-cured tobacco stalk slag and spices scarp after the present invention will extract by certain rate of charge are mixed together slurrying, the sheet base of manufacturing paper with pulp then and being shaped to reconstituted tobacco, can guarantee under product quality and the rheobasic prerequisite of sheet, increase substantially the yield of reconstituted tobacco product, solve the general lower problem of pure Turkish tobaccos type reconstituted tobacco product yield.
The specific embodiment
Below in conjunction with specific embodiment technical scheme of the present invention is described further:
Embodiment 1
Get 50Kg Turkish tobaccos fragment and the broken end of 50Kg Turkish tobaccos, replacing water to carry out heat by known papermaking-method reconstituted tobaccos production technology with the aqueous solution that contains 35% ethanol extracts, carry out Separation of Solid and Liquid subsequently, resulting extract evaporation and concentration is become the Turkish tobaccos medicinal extract of 40Kg, add 4Kg again and worn into the above Turkish tobaccos seed fine powder of 60 orders, and be that the mixed solvent 6Kg of propane diols-glycerine-water of 1: 1: 1 is deployed into the coating fluid that density is 1.22g/ml with it with volume proportion.
Other get 45Kg flue-cured tobacco offal by known papermaking-method reconstituted tobaccos production technology with hot water extracting and Separation of Solid and Liquid after, discard extract, stay Turkish tobaccos scarp mixed pulp after stalk slag and the said extracted, manufacture paper with pulp in the paper machine portion of reconstituted tobacco production line again and be shaped to reconstituted tobacco sheet base, with above-mentioned deployed coating fluid it is coated with then, subsequently again drying, cut and finally obtain reconstituted tobacco finished product 106Kg.
Smoke panel test through the aesthetic quality, above-mentioned reconstituted tobacco finished product is distinguished the flavor of and is smelt in suction and all has tangible Turkish tobaccos style and features on the perfume (or spice), is a kind of typical Turkish tobaccos type papermaking-method reconstituted tobaccos product.After tested, the filling rate of this product reaches 6.1cm 3/ g is higher than 4.0~4.3cm of normal tobacco leaf pipe tobacco 3/ g; Releasing content of coke tar is that 5.8mg/ props up, and props up far below 11~15mg/ of normal tobacco leaf pipe tobacco; The production yield is calculated with total inventory of tobacco material, is 71.1%, and calculates with the raw material inventory of Turkish tobaccos, then is 101.9%.
Embodiment 2
Get the whole leaf of 100Kg Turkish tobaccos, replacing water to carry out heat by known papermaking-method reconstituted tobaccos production technology with the aqueous solution that contains 12% propane diols extracts, carry out Separation of Solid and Liquid subsequently, resulting extract evaporation and concentration is become the Turkish tobaccos medicinal extract of 43Kg, add 2Kg again and worn into the above Turkish tobaccos seed fine powder of 60 orders, and be that the mixed solvent 5Kg of propane diols-glycerine-water of 1: 1: 3 is deployed into the coating fluid that density is 1.18g/ml with it with volume proportion.
Other get 90Kg flue-cured tobacco offal by known papermaking-method reconstituted tobaccos production technology with hot water extracting and Separation of Solid and Liquid after, discard extract, stay Turkish tobaccos scarp mixed pulp after stalk slag and the said extracted, manufacture paper with pulp in the paper machine portion of reconstituted tobacco production line again and be shaped to reconstituted tobacco sheet base, with above-mentioned deployed coating fluid it is coated with then, subsequently again drying, cut and finally obtain reconstituted tobacco finished product 124Kg.
Smoke panel test through the aesthetic quality, above-mentioned reconstituted tobacco finished product is distinguished the flavor of and is smelt in suction and has tangible Turkish tobaccos style and features on the perfume (or spice), also is a kind of typical Turkish tobaccos type papermaking-method reconstituted tobaccos product.After tested, the filling rate of this product is 6.4cm 3/ g, releasing content of coke tar are that 5.5mg/ props up, and the production yield is calculated with total inventory of tobacco material, is 64.6%, and calculates with the raw material inventory of Turkish tobaccos, then up to 121.6%.
Embodiment 3
Get the whole leaf of Turkish tobaccos, fragment, each 33Kg of broken end, replacing water to carry out heat by known papermaking-method reconstituted tobaccos production technology with the aqueous solution that contains 25% ethanol extracts, carry out Separation of Solid and Liquid subsequently, resulting extract evaporation and concentration is become the Turkish tobaccos medicinal extract of 40Kg, add 0.25Kg again and worn into the above Turkish tobaccos seed fine powder of 60 orders, and be that the mixed solvent 5Kg of propane diols-glycerine-water of 1: 1: 4 is deployed into the coating fluid that density is 1.17g/ml with it with volume proportion.
Other get 60Kg flue-cured tobacco offal by known papermaking-method reconstituted tobaccos production technology with hot water extracting and Separation of Solid and Liquid after, discard extract, stay Turkish tobaccos scarp mixed pulp after stalk slag and the said extracted, manufacture paper with pulp in the paper machine portion of reconstituted tobacco production line again and be shaped to reconstituted tobacco sheet base, with above-mentioned deployed coating fluid it is coated with then, subsequently again drying, cut and finally obtain reconstituted tobacco finished product 110.5Kg.
Smoke panel test through the aesthetic quality, above-mentioned reconstituted tobacco finished product is distinguished the flavor of and smelt in suction tangible Turkish tobaccos style and features on the perfume (or spice), be a kind of typical Turkish tobaccos type papermaking-method reconstituted tobaccos product.After tested, the filling rate of this product is 6.2cm 3/ g, releasing content of coke tar are that 5.6mg/ props up, and the production yield is calculated with total inventory of tobacco material, is 69.4%, and calculates with the raw material inventory of Turkish tobaccos, then reaches 111.3%.
Embodiment 4
Get the whole leaf of Turkish tobaccos, each 50Kg of broken end, replacing water to carry out heat by known papermaking-method reconstituted tobaccos production technology with the aqueous solution that contains 18% propane diols extracts, carry out Separation of Solid and Liquid subsequently, resulting extract evaporation and concentration is become the Turkish tobaccos medicinal extract of 45Kg, add 1.5Kg again and worn into the above Turkish tobaccos seed fine powder of 60 orders, and be that the mixed solvent 3Kg of propane diols-glycerine-water of 1: 1: 4 is deployed into the coating fluid that density is 1.20g/ml with it with volume proportion.
Other get 50Kg flue-cured tobacco offal by known papermaking-method reconstituted tobaccos production technology with hot water extracting and Separation of Solid and Liquid after, discard extract, stay Turkish tobaccos scarp mixed pulp after stalk slag and the said extracted, manufacture paper with pulp in the paper machine portion of reconstituted tobacco production line again and be shaped to reconstituted tobacco sheet base, with above-mentioned deployed coating fluid it is coated with then, subsequently again drying, cut and finally obtain reconstituted tobacco finished product 108Kg.
Smoke panel test through the aesthetic quality, above-mentioned reconstituted tobacco finished product is distinguished the flavor of and smelt in suction tangible Turkish tobaccos style and features on the perfume (or spice), also be a kind of typical Turkish tobaccos type papermaking-method reconstituted tobaccos product.After tested, the filling rate of this product is 6.1cm 3/ g, releasing content of coke tar are that 5.7mg/ props up, and the production yield is calculated with total inventory of tobacco material, is 71.3%, and calculates with the raw material inventory of Turkish tobaccos, then reaches 106.4%.

Claims (9)

1. the production method of a Turkish tobaccos type papermaking-method reconstituted tobaccos is characterized in that method step is:
(1) Turkish tobaccos through Separation of Solid and Liquid, obtain Turkish tobaccos extract and spices scarp with containing the extraction with aqueous solution of organic solvent, become Turkish tobaccos medicinal extract standby wherein Turkish tobaccos extract evaporation and concentration;
(2) flue-cured tobacco offal water extracts, through Separation of Solid and Liquid and after discarding extract, and gained stalk slag and spices scarp mixed pulp, manufacturing paper with pulp in the paper machine portion of reconstituted tobacco production line is shaped to the sheet base;
(3) the Turkish tobaccos seed is finish-ground to fine powder, adds in the above-mentioned Turkish tobaccos medicinal extract, add the allotment solvent again and be deployed into coating fluid;
(4) deployed coating fluid is applied to the sheet base on the reconstituted tobacco production line, dries subsequently, divide and be cut to Turkish tobaccos type papermaking-method reconstituted tobaccos finished product.
2. the production method of Turkish tobaccos type papermaking-method reconstituted tobaccos according to claim 1 is characterized in that: described Turkish tobaccos comprise that Turkish tobaccos put in order any one or more in leaf, Turkish tobaccos fragment and the broken end of Turkish tobaccos.
3. the production method of Turkish tobaccos type papermaking-method reconstituted tobaccos according to claim 1 is characterized in that: the described aqueous solution that contains organic solvent that is used to extract Turkish tobaccos is the aqueous solvent of ethanol or propane diols.
4. according to the production method of claim 1 or 3 described Turkish tobaccos type papermaking-method reconstituted tobaccos, it is characterized in that: the described aqueous solution that contains organic solvent that is used for extracting Turkish tobaccos, the volume ratio of ethanol or propane diols and water is: 10~35: 90~65.
5. the production method of Turkish tobaccos type papermaking-method reconstituted tobaccos according to claim 1 is characterized in that: the mass ratio that feeds intake of described Turkish tobaccos and flue-cured tobacco offal is: 50~80: 50~20.
6. the production method of Turkish tobaccos type papermaking-method reconstituted tobaccos according to claim 1 is characterized in that: the powder that described Turkish tobaccos seed is finish-ground to is the above fine powders of 60 orders.
7. the production method of Turkish tobaccos type papermaking-method reconstituted tobaccos according to claim 1 is characterized in that: the ratio that described Turkish tobaccos seed fine powder joins in the Turkish tobaccos medicinal extract is 0.5~10% of a Turkish tobaccos medicinal extract quality.
8. the production method of Turkish tobaccos type papermaking-method reconstituted tobaccos according to claim 1 is characterized in that: described coating fluid allotment solvent is that volume ratio is the mixed solvent of propane diols-glycerine-water of 1: 1: 1~4.
9. according to the production method of claim 1 or 8 described Turkish tobaccos type papermaking-method reconstituted tobaccos, it is characterized in that: the Turkish tobaccos medicinal extract that will add behind the Turkish tobaccos seed fine powder with the mixed solvent of described propane diols-glycerine-water is deployed into the coating fluid that density is 1.15~1.25g/ml.
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CN102604740A (en) * 2012-03-08 2012-07-25 河南中烟工业有限责任公司 Tobacco extract, and extraction method and application thereof
CN102871212A (en) * 2012-10-08 2013-01-16 安徽中烟工业有限责任公司 Method for producing paper-making reconstituted tobacco
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CN102934837A (en) * 2012-11-09 2013-02-20 红云红河烟草(集团)有限责任公司 Preparation method for blended type reconstituted tobacco with burley tobacco style
CN102972862A (en) * 2012-12-20 2013-03-20 上海聚华科技股份有限公司 Process for improving tobacco materials and device thereof
CN103054156A (en) * 2012-12-18 2013-04-24 内蒙古昆明卷烟有限责任公司 Application of cordyceps sinensis extraction residues to reconstituted tobacco
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CN103263073A (en) * 2013-06-19 2013-08-28 云南烟草科学研究院 Method for reproducing tobacco leaves by paper-making method through bamboo pulp fibers instead of wood pulp fibers
CN103300464A (en) * 2013-06-28 2013-09-18 湖北中烟工业有限责任公司 Blended type cigarette processing method
CN103387875A (en) * 2013-07-31 2013-11-13 浙江中烟工业有限责任公司 Aromatic tobacco propylene glycol aqueous solution extract, and preparation method and application thereof
CN103393214A (en) * 2013-07-31 2013-11-20 浙江中烟工业有限责任公司 Aromatic tobacco ethyl alcohol and propylene glycol mixed solution extract and preparation method and application of aromatic tobacco ethyl alcohol and propylene glycol mixed solution extract
CN103462209A (en) * 2013-09-26 2013-12-25 云南烟草科学研究院 Method for preparing paper-making-method reconstituted tobacco with sun-cured red tobacco style characteristic
CN103462205A (en) * 2013-09-18 2013-12-25 浙江中烟工业有限责任公司 Reconstructed tobacco leaves containing basic incense substances in tobaccos prepared by water extraction method and ethanol extraction method and cigarettes produced by reconstructed tobacco leaves
CN103484245A (en) * 2013-09-18 2014-01-01 浙江中烟工业有限责任公司 Directed composite extraction method for tobacco endogenous original fragrant substance
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CN102604740A (en) * 2012-03-08 2012-07-25 河南中烟工业有限责任公司 Tobacco extract, and extraction method and application thereof
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CN102934837A (en) * 2012-11-09 2013-02-20 红云红河烟草(集团)有限责任公司 Preparation method for blended type reconstituted tobacco with burley tobacco style
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CN102972862A (en) * 2012-12-20 2013-03-20 上海聚华科技股份有限公司 Process for improving tobacco materials and device thereof
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