CN103263072B - Preparation method of medium-temperature tobacco material for non-combustion cigarette - Google Patents
Preparation method of medium-temperature tobacco material for non-combustion cigarette Download PDFInfo
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- CN103263072B CN103263072B CN201310195250.0A CN201310195250A CN103263072B CN 103263072 B CN103263072 B CN 103263072B CN 201310195250 A CN201310195250 A CN 201310195250A CN 103263072 B CN103263072 B CN 103263072B
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- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 36
- 239000000463 material Substances 0.000 title claims abstract description 31
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 241000208125 Nicotiana Species 0.000 title abstract description 33
- 238000002485 combustion reaction Methods 0.000 title abstract 2
- 239000012530 fluid Substances 0.000 claims abstract description 15
- 238000000605 extraction Methods 0.000 claims abstract description 11
- 238000000199 molecular distillation Methods 0.000 claims abstract description 11
- 241001579180 Matthiola longipetala Species 0.000 claims abstract description 9
- 238000004537 pulping Methods 0.000 claims abstract description 5
- 239000011248 coating agent Substances 0.000 claims description 19
- 238000000576 coating method Methods 0.000 claims description 19
- 239000000284 extract Substances 0.000 claims description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 9
- 239000002002 slurry Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 240000004784 Cymbopogon citratus Species 0.000 claims description 4
- 235000017897 Cymbopogon citratus Nutrition 0.000 claims description 4
- 240000001812 Hyssopus officinalis Species 0.000 claims description 4
- 235000010650 Hyssopus officinalis Nutrition 0.000 claims description 4
- 101000905241 Mus musculus Heart- and neural crest derivatives-expressed protein 1 Proteins 0.000 claims description 4
- 235000010676 Ocimum basilicum Nutrition 0.000 claims description 4
- 240000007926 Ocimum gratissimum Species 0.000 claims description 4
- 244000178231 Rosmarinus officinalis Species 0.000 claims description 4
- 238000010009 beating Methods 0.000 claims description 4
- 239000008367 deionised water Substances 0.000 claims description 4
- 229910021641 deionized water Inorganic materials 0.000 claims description 4
- 239000000835 fiber Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 244000061176 Nicotiana tabacum Species 0.000 claims 3
- 239000003205 fragrance Substances 0.000 abstract description 7
- 239000000126 substance Substances 0.000 abstract description 5
- 235000009508 confectionery Nutrition 0.000 abstract description 4
- 238000009835 boiling Methods 0.000 abstract description 2
- 210000000697 sensory organ Anatomy 0.000 abstract description 2
- 239000000779 smoke Substances 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract 2
- 241000196324 Embryophyta Species 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 235000013599 spices Nutrition 0.000 abstract 1
- 230000001953 sensory effect Effects 0.000 description 5
- 230000000391 smoking effect Effects 0.000 description 5
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- 239000003546 flue gas Substances 0.000 description 3
- 239000000470 constituent Substances 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
- Paper (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a preparation method of a medium-temperature tobacco material for a non-combustion cigarette. Directly pulping tobacco raw material to prepare sheet base, and taking natural perfume plant to utilize supercritical CO2Extracting the aroma components by fluid extraction-molecular distillation, and extracting the aroma componentsThe aromatic component is coated on the base sheet to obtain the required medium-temperature tobacco material. The invention furthest reserves the aroma substances contained in the tobacco raw materials; by using supercritical CO2The selectivity of the fluid extraction-molecular distillation method realizes the directional extraction of chemical components with the boiling point of 300-400 ℃ in natural spice plants, thereby realizing the regulation and control of the chemical components of the medium-temperature tobacco material; the prepared moderate-temperature tobacco material has rich fragrance, harmonious smoke, better sense organ comfort, obvious sweet feeling and outstanding faint scent characteristic.
Description
Technical field
The invention belongs to without burning technical field of cigarettes, specifically relate to a kind of for the preparation method without warm tobacco-containing material in burning cigarette.
Background technology
Development of new without burning cigarette as present stage tobacco business research emphasis and focus, although achieve more achievement in correlative study, the research of targeted release flavor matter is also in blank at a certain temperature.For traditional cigarette, because it burns under about 800 DEG C of conditions, create a large amount of tar and multiple aroma component, the health of fractions to smoker produced of simultaneously burning is harmful.Therefore, exploitation can discharge the similar tobacco-containing material normally burning and sucking cigarette smoke by destructive distillation at a lower temperature, and the development for cigarette has important practical significance.Relevant report prepared by middle temperature tobacco-containing material is there is not yet in prior art.
Summary of the invention
The object of the invention is to, for without the single of cigarette tobacco product type of burning, provide a kind of for the preparation method without warm tobacco-containing material in burning cigarette.In this, warm tobacco-containing material can enrich fragrance and the taste type of nothing burning cigarette, meets the needs of consumer better.
Object of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage of the present invention is percetage by weight, and number is weight portion.
For the preparation method without warm tobacco-containing material in burning cigarette, comprise the following steps:
(1) get tobacco 10 ~ 20 parts, soak after 0.5 ~ 2 hour and discongest the fibre stuff into beating degree 20 ~ 40 ° of SR with pulping equipment;
(2) be 0.5 ~ 1.2% by deionized water diluted slurry to concentration expressed in percentage by weight, manufacture paper with pulp base in blocks with paper making equipment;
(3) get natural perfume plant 1 ~ 5 part, be placed in extraction equipment, in extracting pressure 25 ~ 30MPa, extraction temperature 40 ~ 60 DEG C, resolve pressure 5.5 ~ 7.2MPa, resolution temperature 40 ~ 60 DEG C, CO
2flow velocity is under 25kg/h condition, obtained supercritical extract liquid after constant temperature and pressure extracts 3 hours;
(4) get supercritical extract liquid, be placed in molecular distillation equipment, under vacuum 30 ~ 60Pa, heating-up temperature 100 ~ 200 DEG C, rotor knifing rotating speed 270 ~ 300 turns/min, flow velocity 2 ~ 4mL/min condition, must thing be reserved;
(5) thing will be reserved and be heated to 150 DEG C, be placed in molecular distillation equipment, at vacuum 5 ~ 10Pa, under heating-up temperature 300 ~ 400 DEG C, rotor knifing rotating speed 270 ~ 300 turns/min, flow velocity 2 ~ 3mL/min condition, must thing be steamed;
(6) get and steam thing 1 ~ 5 part, ethanol 5 ~ 50 parts, mixing jolting 10min is prepared into coating fluid;
(7) coating fluid is pressed the coating weight even spread of 40 ~ 60% on sheet base, dry under 70 ~ 90 DEG C of temperature conditions, obtain required middle temperature tobacco-containing material.
Described natural perfume plant is selected from a kind of in rosemary, sweet basil, lemon-grass, Hyssopus officinalis or their mixture.
Relative to prior art, the present invention has the following advantages:
(1) the present invention's tobacco material is directly pulled an oar and is prepared sheet base, remains the flavor matter that tobacco material itself is contained to greatest extent;
(2) the present invention utilizes supercritical CO
2fluid extraction-molecularly distilled selective, achieves natural perfume plant mid-boiling point and extracts between the orientation of the chemical constituent of 300 ~ 400 DEG C, thus achieve the regulation and control of middle temperature tobacco-containing material chemical constituent;
(3) the middle temperature tobacco-containing material fragrance that prepared by the present invention enriches, flue gas is coordinated, better, the sweet sense of sense organ comfort level is obvious, delicate fragrance feature is given prominence to.
Detailed description of the invention
Below by embodiment, the present invention is described in further detail, but embodiment is not limited to the technical solution.
Embodiment 1
Get tobacco material 10 parts, soak after 0.5 hour and discongest with pulping equipment the fibre stuff that beating degree is 20 ° of SR; Be 1.2% by deionized water diluted slurry to concentration expressed in percentage by weight, manufacture paper with pulp base in blocks with paper making equipment; Get rosemary 5 parts, be placed in extraction equipment, in extracting pressure 28MPa, extraction temperature 50 DEG C, resolve pressure 7.0MPa, resolution temperature 60 DEG C, CO
2flow velocity is under 25kg/h condition, obtained supercritical extract liquid after constant temperature and pressure extracts 3 hours; Get supercritical extract liquid, be placed in molecular distillation equipment, under vacuum 30Pa, heating-up temperature 150 DEG C, rotor knifing rotating speed 280 turns/min, flow velocity 2mL/min condition, must thing be reserved; Thing will be reserved and be heated to 150 DEG C, be placed in molecular distillation equipment, at vacuum 5Pa, under heating-up temperature 350 DEG C, rotor knifing rotating speed 280 turns/min, flow velocity 2mL/min condition, must thing be steamed; Get and steam thing 5 parts, ethanol 50 parts, mixing jolting 10min is prepared into coating fluid; Coating fluid is pressed the coating weight even spread of 50% on sheet base, dry under 90 DEG C of temperature conditions, obtain low temperature tobacco-containing material 1.
The obtained middle temperature tobacco-containing material 1 of this law adds to without after in burning cigarette, through sensory evaluating smoking, compared with blank, fragrant and sweet and delicate fragrance obviously, flue gas mouthfeel better, few, the comfortableness of assorted gas promotes to some extent.
Embodiment 2
Get tobacco material 20 parts, soak after 2 hours and discongest with pulping equipment the fibre stuff that beating degree is 40 ° of SR; Be 0.5% by deionized water diluted slurry to concentration expressed in percentage by weight, manufacture paper with pulp base in blocks with paper making equipment; Get lemon-grass 1 part, be placed in extraction equipment, in extracting pressure 25MPa, extraction temperature 40 DEG C, resolve pressure 5.5MPa, resolution temperature 60 DEG C, CO
2flow velocity is under 25kg/h condition, obtained supercritical extract liquid after constant temperature and pressure extracts 3 hours; Get supercritical extract liquid, be placed in molecular distillation equipment, under vacuum 50Pa, heating-up temperature 180 DEG C, rotor knifing rotating speed 300 turns/min, flow velocity 2.4mL/min condition, must thing be reserved; Thing will be reserved and be heated to 180 DEG C, be placed in molecular distillation equipment, at vacuum 10Pa, under heating-up temperature 400 DEG C, rotor knifing rotating speed 300 turns/min, flow velocity 2.4mL/min condition, must thing be steamed; Get and steam thing 1 part, ethanol 5 parts, mixing jolting 10min is prepared into coating fluid; Coating fluid is pressed the coating weight even spread of 45% on sheet base, dry under 80 DEG C of temperature conditions, obtain low temperature tobacco-containing material 2.
The obtained middle temperature tobacco-containing material 2 of this law adds to without after in burning cigarette, through sensory evaluating smoking, compared with blank, perfume quantity increases to some extent, stimulate reduce, sweet sense enhancing, flue gas be comparatively soft.
Embodiment 3
Repeat embodiment 1, have following difference: slurry weight percentage concentration is 1.0%, natural perfume plant is sweet basil; Coating fluid presses the coating weight even spread of 40% on sheet base, dries, obtain low temperature tobacco-containing material 3 under 70 DEG C of temperature conditions.
The middle temperature tobacco-containing material 3 that this law obtains adds to after in nothing burning cigarette, and through sensory evaluating smoking, compared with blank, full aroma, moisture feeling are better, excitant reduces.
Embodiment 4
Repeat embodiment 2, have following difference: slurry weight percentage concentration is 0.8%, natural perfume plant is Hyssopus officinalis; Coating fluid presses the coating weight even spread of 50% on sheet base, dries, obtain low temperature tobacco-containing material 4 under 75 DEG C of temperature conditions.
The middle temperature tobacco-containing material 4 that this law obtains adds to after in nothing burning cigarette, and through sensory evaluating smoking, compared with blank, delicate fragrance is obvious, comfortableness promotes to some extent.
Embodiment 5
Repeat embodiment 2, have following difference: natural perfume plant is the mixture of rosemary, sweet basil, lemon-grass, Hyssopus officinalis, extraction conditions is extracting pressure 30MPa, extraction temperature 55 DEG C, parsing pressure 7.2MPa, resolution temperature 55 DEG C, CO
2flow velocity is under 25kg/h condition, obtained supercritical extract liquid after constant temperature and pressure extracts 3 hours; Under molecular clock condition vacuum 30Pa, heating-up temperature 300 DEG C, rotor knifing rotating speed 290 turns/min, flow velocity 4.0mL/min condition, thing must be reserved; Thing will be reserved and be heated to 200 DEG C, be placed in molecular distillation equipment, at vacuum 5Pa, under heating-up temperature 400 DEG C, rotor knifing rotating speed 290 turns/min, flow velocity 2.5mL/min condition, must thing be steamed; Get and steam thing 1 part, ethanol 5 parts, mixing jolting 10min is prepared into coating fluid; Coating fluid is pressed the coating weight even spread of 50% on sheet base, dry under 90 DEG C of temperature conditions, obtain low temperature tobacco-containing material 5.
The obtained middle temperature tobacco-containing material 5 of this law adds to without after in burning cigarette, through sensory evaluating smoking, compared with blank, delicate fragrance and fragrant and sweetly to promote to some extent, comfortableness obviously, moisture feeling strengthens, assorted gas reduces.
Claims (1)
1., for the preparation method without warm tobacco-containing material in burning cigarette, comprise the following steps:
(1) get tobacco 10 ~ 20 parts, soak after 0.5 ~ 2 hour and discongest the fibre stuff into beating degree 20 ~ 40 ° of SR with pulping equipment;
(2) be 0.5 ~ 1.2% by deionized water diluted slurry to concentration expressed in percentage by weight, manufacture paper with pulp base in blocks with paper making equipment;
(3) get natural perfume plant 1 ~ 5 part, be placed in extraction equipment, in extracting pressure 25 ~ 30MPa, extraction temperature 40 ~ 60 DEG C, resolve pressure 5.5 ~ 7.2MPa, resolution temperature 40 ~ 60 DEG C, CO
2flow velocity is under 25kg/h condition, obtained supercritical extract liquid after constant temperature and pressure extracts 3 hours; Described natural perfume plant is selected from a kind of in rosemary, sweet basil, lemon-grass, Hyssopus officinalis or their mixture;
(4) get supercritical extract liquid, be placed in molecular distillation equipment, under vacuum 30 ~ 60Pa, heating-up temperature 100 ~ 200 DEG C, rotor knifing rotating speed 270 ~ 300 turns/min, flow velocity 2 ~ 4mL/min condition, obtain distillate;
(5) distillate is heated to 150 DEG C, is placed in molecular distillation equipment, at vacuum 5 ~ 10Pa, under heating-up temperature 300 ~ 400 DEG C, rotor knifing rotating speed 270 ~ 300 turns/min, flow velocity 2 ~ 3mL/min condition, must thing be steamed;
(6) get and steam thing 1 ~ 5 part, ethanol 5 ~ 50 parts, mixing jolting 10min is prepared into coating fluid;
(7) coating fluid is pressed the coating weight even spread of 40 ~ 60% on sheet base, dry under 70 ~ 90 DEG C of temperature conditions, obtain required middle temperature tobacco-containing material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310195250.0A CN103263072B (en) | 2013-05-23 | 2013-05-23 | Preparation method of medium-temperature tobacco material for non-combustion cigarette |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310195250.0A CN103263072B (en) | 2013-05-23 | 2013-05-23 | Preparation method of medium-temperature tobacco material for non-combustion cigarette |
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| Publication Number | Publication Date |
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| CN103263072A CN103263072A (en) | 2013-08-28 |
| CN103263072B true CN103263072B (en) | 2015-05-27 |
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| CN201310195250.0A Active CN103263072B (en) | 2013-05-23 | 2013-05-23 | Preparation method of medium-temperature tobacco material for non-combustion cigarette |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6860345B2 (en) * | 2013-10-14 | 2021-04-14 | フィリップ・モーリス・プロダクツ・ソシエテ・アノニム | Heated aerosol-generating articles containing improved rods |
| CN103919269B (en) * | 2014-03-28 | 2016-01-20 | 广东中烟工业有限责任公司 | A kind of electronic cigarette |
| CN103892437B (en) * | 2014-03-28 | 2016-03-30 | 广东中烟工业有限责任公司 | A kind of production method of novel tobacco goods |
| CN104223346B (en) * | 2014-10-17 | 2016-08-24 | 安徽中烟再造烟叶科技有限责任公司 | The method of functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass |
| CN105768191B (en) * | 2016-04-29 | 2018-03-27 | 河南中烟工业有限责任公司 | A kind of reconstituted tobacco and do not burnt cigarette using the heating prepared by it |
| CN106307606B (en) * | 2016-11-22 | 2018-02-23 | 中国烟草总公司郑州烟草研究院 | A kind of preparation method of high fragrance tobacco extract |
| CN108936791B (en) * | 2018-08-28 | 2022-03-15 | 云南恒罡科技有限公司 | Method for preparing flue gas condensate by high-temperature thermal cracking |
| GB201817557D0 (en) | 2018-10-29 | 2018-12-12 | Nerudia Ltd | Smoking substitute consumable |
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|---|---|---|---|---|
| US5435325A (en) * | 1988-04-21 | 1995-07-25 | R. J. Reynolds Tobacco Company | Process for providing tobacco extracts using a solvent in a supercritical state |
| CN101926508A (en) * | 2010-08-10 | 2010-12-29 | 广东中烟工业有限责任公司 | Application of blackberrykiky rhizome in cigarette |
| CN102018274A (en) * | 2010-12-31 | 2011-04-20 | 云南烟草科学研究院 | Preparation method for regenerating tobacco leaves by using aromatic tobacco papermaking method |
| CN102041174A (en) * | 2011-01-07 | 2011-05-04 | 江苏中烟工业有限责任公司 | Preparation method of moss-scented tobacco flavor and application of moss-scented cigarette flavor in cigarette flavoring |
| CN103045371A (en) * | 2012-12-13 | 2013-04-17 | 大兴安岭林格贝有机食品有限责任公司 | Preparation method for purifying essential oil and ursolic acid from wild ledum palustre in great khingan |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8887737B2 (en) * | 2005-07-29 | 2014-11-18 | Philip Morris Usa Inc. | Extraction and storage of tobacco constituents |
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2013
- 2013-05-23 CN CN201310195250.0A patent/CN103263072B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5435325A (en) * | 1988-04-21 | 1995-07-25 | R. J. Reynolds Tobacco Company | Process for providing tobacco extracts using a solvent in a supercritical state |
| CN101926508A (en) * | 2010-08-10 | 2010-12-29 | 广东中烟工业有限责任公司 | Application of blackberrykiky rhizome in cigarette |
| CN102018274A (en) * | 2010-12-31 | 2011-04-20 | 云南烟草科学研究院 | Preparation method for regenerating tobacco leaves by using aromatic tobacco papermaking method |
| CN102041174A (en) * | 2011-01-07 | 2011-05-04 | 江苏中烟工业有限责任公司 | Preparation method of moss-scented tobacco flavor and application of moss-scented cigarette flavor in cigarette flavoring |
| CN103045371A (en) * | 2012-12-13 | 2013-04-17 | 大兴安岭林格贝有机食品有限责任公司 | Preparation method for purifying essential oil and ursolic acid from wild ledum palustre in great khingan |
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| CN103263072A (en) | 2013-08-28 |
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