CN104223346B - The method of functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass - Google Patents
The method of functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass Download PDFInfo
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- CN104223346B CN104223346B CN201410553399.6A CN201410553399A CN104223346B CN 104223346 B CN104223346 B CN 104223346B CN 201410553399 A CN201410553399 A CN 201410553399A CN 104223346 B CN104223346 B CN 104223346B
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Abstract
The invention discloses a kind of method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass, comprise the following steps: (1) by Nicotiana tabacum L. dead meal, account for Nicotiana tabacum L. dead meal gross weight 5% ~ 30% Fructus Citri tangerinae grass add mixing tank mixing, soaking, extract, solve fibre, solid-liquid separation obtains hybrid extraction liquid and mixing slag charge；(2) cabo is soaking, extract, solve fibre, separate after obtain obstruct liquid and stalk slag charge；(3) being mixed with stalk slag charge by mixing slag charge, defibrination, after being thickened by slurry, substrate is manufactured paper with pulp in online；(4) concentration of hybrid extraction liquid being allocated to obtain coating fluid, be applied on substrate, reconstituted tobacoo is made in drying, section.The present invention adds non-tobacco material Fructus Citri tangerinae grass in reconstituted tobacco, Fructus Citri tangerinae grass wide material sources, cheap, improve the utilization rate of plant resources, Fructus Citri tangerinae grass instead of the wood pulp cellulose in reconstituted tobacco paper substrate, reducing the production cost of Medicated cigarette, reconstituted tobacco prepared by the method has Fructus Citri tangerinae fragrance, improves the quality of reconstituted tobacoo.
Description
Technical field
The present invention relates to reconstituted tobacco technical field, particularly relate to a kind of method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass.
Background technology
Reconstituted tobacco is also known as recombination tobacco leaf, homogenizing Nicotiana tabacum L..Mainly by Nicotiana tabacum L. dead meal fragment, cabo or discarded tobacco leaf, additional Plant fiber, adhesive and other additive composition.In Medicated cigarette, dose appropriate reconstituted tobacoo, raw tobacco material can be saved to greatest extent, effectively reduce Medicated cigarette cost；Can also to a certain degree change the physicochemical property of Medicated cigarette, for improving the quality of tobacco product, reducing tar content, change smoke components, stablize Medicated cigarette interior quality and play a very important role.The addition of reconstituted tobacoo, for reducing tar and reducing harm important role, is the important technique measure reducing and improving Nicotiana tabacum L. harmful components.Reconstituted tobacoo originates from the 1950's, and at present, reconstituted tobacco mainly has three kinds of different production and processing methods: thick paste method, roll-in method and paper process.Papermaking-method reconstituted tobaccos owing to having that density is little, Filling power is high, the advantage such as filamentation rate is high, machining property is good and Modulatory character is good, it has also become the main method of domestic and international production reconstituted tobacco.Paper process is to utilize discarded cabo, tobacco leaf fragment, Nicotiana tabacum L. dead meal etc. for raw material, through extraction, concentration, perfuming, separate, pull an oar, manufacture paper with pulp, the technical process such as drying, make the Nicotiana tabacum L. substrate of function admirable, as Medicated cigarette implant, be back to production of cigarettes.
Reconstituted tobacco in order to make paper process prepare has suitable physical property, chemical composition content and abnormal smells from the patient, need to add the cigarette wood pulp cellulose of more than 5% in the formula of reconstituted tobacco, the price of this wood pulp cellulose, at 7000 ~ 8000 yuans/ton, increases the production cost of reconstituted tobacco.
Fructus Citri tangerinae grass is one of common Rhizoma et radix valerianae.Having Fructus Citri tangerinae fragrance, its fragrance can give people's freshness, recovers balance of body and spirit.Fructus Citri tangerinae grass has the advantages that trophophase is short, results are fast, yield is high, income is big.Fructus Citri tangerinae grass quintessence oil, is obtained through steam distillation by the herb of Fructus Citri tangerinae grass, is the quintessence oil that in aromatotherapy and therapy, purposes is the widest, is also commonly used for space deodorant.
Distillation extraction Fructus Citri tangerinae grass prepares quintessence oil, fresh leaf oil yield about 1 percent. two, and liquefaction process produces a large amount of Fructus Citri tangerinae grass slags, its main Land use systems is for burn as fuel at present, or use as fertilizer or covering, utilization rate is relatively low, causes the substantial amounts of wasting of resources and environmental pollution.Have no the correlation technique report that Fructus Citri tangerinae grass slag recycles at present.
Summary of the invention
The technical problem to be solved is to provide a kind of method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass, by increasing capacitance it is possible to increase reconstituted tobacco distinctive Orange flavor fragrance, effectively reduces the production cost of reconstituted tobacco.
For solving above-mentioned technical problem, the technical scheme that the present invention uses is: a kind of method providing Fructus Citri tangerinae grass to prepare functional type reconstituted tobacco, comprises the following steps:
(1) by Nicotiana tabacum L. dead meal, account for Nicotiana tabacum L. dead meal gross weight 5% ~ 30% Fructus Citri tangerinae grass add mixing tank mixing, add the hot water of 50 ~ 80 DEG C by amount that solid-to-liquid ratio is 1:4 ~ 8, extract 20 ~ 60min, fine to the compound solution after extraction, solving fine beating degree is 10 ~ 15》SR, obtains hybrid extraction liquid and mixing slag charge to the compound solid-liquid separation after solving fibre；
(2) cabo being added mixing tank, add the hot water of 50 ~ 80 DEG C by the amount that solid-to-liquid ratio is 1:4 ~ 8, extract 20 ~ 60min, fine to the cabo solution after extraction, solving fine beating degree is 10 ~ 15》SR, obtains the cabo solid-liquid separation after solving fibre obstructing liquid and stalk slag charge；
(3) successively carrying out middle concentrated jordaning and low dense defibrination after being mixed by the stalk slag charge in the mixing slag charge in step (1) and step (2), the beating degree of slurry is 20 ~ 30》SR, the slurry mix homogeneously that will obtain, after thickening, upper paper machine is copied into substrate；
(4) the hybrid extraction liquid obtained in step (1) concentration being allocated to obtain coating fluid, be applied to step (3) and manufacture paper with pulp on the substrate obtained, reconstituted tobacoo is made in drying, section.
In a preferred embodiment of the present invention, Fructus Citri tangerinae grass described in step (1) is the fresh Fructus Citri tangerinae grass after solving fibre or Fructus Citri tangerinae grass slag.
In a preferred embodiment of the present invention, in step (1), the water bath heat preservation temperature of mixing tank is 50 ~ 80 DEG C, makes Nicotiana tabacum L. dead meal and Fructus Citri tangerinae grass fully soak.
In a preferred embodiment of the present invention, in step (4), hybrid extraction liquid purifies through rectangular mesh screen and centrifuge, hybrid extraction liquid after purification concentrates through MVR falling film type evaporation, concentrated solution concentration after concentration is 40% ~ 50%, under this spreading rate, the organoleptic quality of the final reconstituted tobacoo prepared is optimum.
In a preferred embodiment of the present invention, described Nicotiana tabacum L. dead meal is offal or tobacco leaf fragment.
The reconstituted tobacoo prepared by said method is made sample cigarette according to different design proportion together with blank sample and is carried out sensory evaluating smoking, and contrast, its empty sample is the sample with Fructus Citri tangerinae grass, smoking result shows, the present invention prepare the method gained of Fructus Citri tangerinae grass functional type reconstituted tobacoo reconstituted tobacoo there is delicate fragrance and fragrant and sweet feature, xylon gas is relatively small, inhales taste softer.
The invention has the beneficial effects as follows: the present invention adds non-tobacco material Fructus Citri tangerinae grass in reconstituted tobacco, Fructus Citri tangerinae grass wide material sources, cheap, on the one hand improve the utilization rate of plant resources, on the other hand the reconstituted tobacco that prepared by the method has Fructus Citri tangerinae fragrance, improves the quality of reconstituted tobacoo；And Fructus Citri tangerinae grass instead of the wood pulp cellulose in reconstituted tobacco paper substrate, significantly reduce the production cost of Medicated cigarette, be suitable to industrialized production.
Accompanying drawing explanation
Fig. 1 is the process chart that method one preferred embodiment of functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass of the present invention.
Detailed description of the invention
Below in conjunction with the accompanying drawings presently preferred embodiments of the present invention is described in detail, so that advantages and features of the invention can be easier to be readily appreciated by one skilled in the art, thus protection scope of the present invention is made apparent clear and definite defining.
Embodiment 1:
A. the method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass, comprises the following steps:
(1) by Nicotiana tabacum L. dead meal, account for Nicotiana tabacum L. dead meal gross weight 5% Fructus Citri tangerinae grass add mixing tank mixing, add the hot water of 50 DEG C by the amount that solid-to-liquid ratio is 1:8, mixing tank water bath heat preservation temperature is 50 DEG C, extracts 20min, fine by fiber uncoiling machine solution to the compound after extraction, solving fine beating degree is 10》SR, obtains hybrid extraction liquid and mixing slag charge to the compound solid-liquid separation after solving fibre；
(2) cabo being added mixing tank, add the hot water of 60 DEG C by the amount that solid-to-liquid ratio is 1:8, mixing tank water bath heat preservation temperature is 60 DEG C, extracts 20min, fine by fiber uncoiling machine solution to the cabo after extraction, and solving fine beating degree is 10》SR, obtains the cabo solid-liquid separation after solving fibre obstructing liquid and stalk slag charge；
(3) successively carrying out middle concentrated jordaning and low dense defibrination after being mixed by the stalk slag charge in the mixing slag charge in step (1) and step (2), the beating degree of slurry is 20》SR, the slurry mix homogeneously that will obtain, after thickening, upper paper machine is copied into substrate；
(4) the hybrid extraction liquid obtained in step (1) is purified through rectangular mesh screen and centrifuge, hybrid extraction liquid after purification concentrates through MVR falling film type evaporation, concentrated solution concentration after concentration is 40%, concentrated solution is deployed into coating fluid, being applied to step (3) and manufacture paper with pulp on the substrate obtained, reconstituted tobacoo is made in drying, section.
B. smoke panel test experiment
By the reconstituted tobacco shredding of preparation, put into climatic chamber inner equilibrium 24h, make Medicated cigarette, as sample sets, and to be not added with the prepared Medicated cigarette of the reconstituted tobacco of Fructus Citri tangerinae grass as a control group.By sample sets and matched group random number, the group of smokeing panel test being made up of the member of smoking possessing qualification of smokeing panel test carries out sensory evaluating smoking.
C. effect assessment
Smoking result shows: compared with matched group, and the reconstituted tobacco prepared with Fructus Citri tangerinae grass has a feature that Fructus Citri tangerinae is fragrant, and zest and xylon gas relatively small, infiltration sense increases.
Embodiment 2:
A. the method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass, comprises the following steps:
(1) by Nicotiana tabacum L. dead meal, account for Nicotiana tabacum L. dead meal gross weight 15% Fructus Citri tangerinae grass add mixing tank mixing, add the hot water of 65 DEG C by the amount that solid-to-liquid ratio is 1:6, mixing tank water bath heat preservation temperature is 65 DEG C, extracts 40min, fine by fiber uncoiling machine solution to the compound after extraction, solving fine beating degree is 13》SR, obtains hybrid extraction liquid and mixing slag charge to the compound solid-liquid separation after solving fibre；
(2) cabo being added mixing tank, add the hot water of 65 DEG C by the amount that solid-to-liquid ratio is 1:6, mixing tank water bath heat preservation temperature is 65 DEG C, extracts 40min, fine by fiber uncoiling machine solution to the cabo after extraction, and solving fine beating degree is 13》SR, obtains the cabo solid-liquid separation after solving fibre obstructing liquid and stalk slag charge；
(3) successively carrying out middle concentrated jordaning and low dense defibrination after being mixed by the stalk slag charge in the mixing slag charge in step (1) and step (2), the beating degree of slurry is 25》SR, the slurry mix homogeneously that will obtain, after thickening, upper paper machine is copied into substrate；
(4) the hybrid extraction liquid obtained in step (1) is purified through rectangular mesh screen and centrifuge, hybrid extraction liquid after purification concentrates through MVR falling film type evaporation, concentrated solution concentration after concentration is 45%, concentrated solution is deployed into coating fluid, being applied to step (3) and manufacture paper with pulp on the substrate obtained, reconstituted tobacoo is made in drying, section.
B. smoke panel test experiment
By the reconstituted tobacco shredding of preparation, put into climatic chamber inner equilibrium 24h, make Medicated cigarette, as sample sets, and to be not added with the prepared Medicated cigarette of the reconstituted tobacco of Fructus Citri tangerinae grass as a control group.By sample sets and matched group random number, the group of smokeing panel test being made up of the member of smoking possessing qualification of smokeing panel test carries out sensory evaluating smoking.
C. effect assessment
Smoking result shows: compared with matched group, and the reconstituted tobacco prepared with Fructus Citri tangerinae grass has the feature that Fructus Citri tangerinae is fragrant, and wherein Fructus Citri tangerinae fragrance is obvious, and zest and xylon gas relatively small, infiltration sense increases.
Embodiment 3:
A. the method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass, comprises the following steps:
(1) by Nicotiana tabacum L. dead meal, account for Nicotiana tabacum L. dead meal gross weight 30% Fructus Citri tangerinae grass add mixing tank mixing, add the hot water of 80 DEG C by the amount that solid-to-liquid ratio is 1:4, mixing tank water bath heat preservation temperature is 80 DEG C, extracts 60min, fine by fiber uncoiling machine solution to the compound after extraction, solving fine beating degree is 15》SR, obtains hybrid extraction liquid and mixing slag charge to the compound solid-liquid separation after solving fibre；
(2) cabo being added mixing tank, add the hot water of 80 DEG C by the amount that solid-to-liquid ratio is 1:4, mixing tank water bath heat preservation temperature is 80 DEG C, extracts 60min, fine by fiber uncoiling machine solution to the cabo after extraction, and solving fine beating degree is 15》SR, obtains the cabo solid-liquid separation after solving fibre obstructing liquid and stalk slag charge；
(3) successively carrying out middle concentrated jordaning and low dense defibrination after being mixed by the stalk slag charge in the mixing slag charge in step (1) and step (2), the beating degree of slurry is 30》SR, the slurry mix homogeneously that will obtain, after thickening, upper paper machine is copied into substrate；
(4) the hybrid extraction liquid obtained in step (1) is purified through rectangular mesh screen and centrifuge, hybrid extraction liquid after purification concentrates through MVR falling film type evaporation, concentrated solution concentration after concentration is 50%, concentrated solution is deployed into coating fluid, being applied to step (3) and manufacture paper with pulp on the substrate obtained, reconstituted tobacoo is made in drying, section.
B. smoke panel test experiment
By the reconstituted tobacco shredding of preparation, put into climatic chamber inner equilibrium 24h, make Medicated cigarette, as sample sets, and to be not added with the prepared Medicated cigarette of the reconstituted tobacco of Fructus Citri tangerinae grass as a control group.By sample sets and matched group random number, the group of smokeing panel test being made up of the member of smoking possessing qualification of smokeing panel test carries out sensory evaluating smoking.
C. effect assessment
Smoking result shows: compared with matched group, and the reconstituted tobacco prepared with Fructus Citri tangerinae grass has the feature that Fructus Citri tangerinae is fragrant, and wherein Fructus Citri tangerinae fragrance is notable, and zest and xylon gas relatively small, infiltration sense increases.
The non-tobacco material Fructus Citri tangerinae grass that patent of the present invention uses, wide material sources, cheap, improve the utilization rate of plant resources, and the addition of Fructus Citri tangerinae grass can also increase reconstituted tobacco peculiar Orange flavor fragrance.When with the Fructus Citri tangerinae soluble material slag of grass, offal soluble material slurry material, cabo soluble material slurry material and wood pulp cellulose mixing, Fructus Citri tangerinae grass slag part instead of the wood pulp cellulose in reconstituted tobacco paper substrate, significantly reduces production of cigarettes cost, but obtains equal paper substrate performance.
The method of the invention is simple to operate, and material source is extensive, it is easy to production practices, is suitable to industrialized production.
The foregoing is only embodiments of the invention; not thereby the scope of the claims of the present invention is limited; every equivalent structure utilizing description of the invention and accompanying drawing content to be made or equivalence flow process conversion; or directly or indirectly it is used in other relevant technical fields, the most in like manner it is included in the scope of patent protection of the present invention.
Claims (6)
1. the method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass, comprises the following steps:
(1) by Nicotiana tabacum L. dead meal, account for Nicotiana tabacum L. dead meal gross weight 5% ~ 30% Fructus Citri tangerinae grass add mixing tank mixing, add the hot water of 50 ~ 80 DEG C by amount that solid-to-liquid ratio is 1:4 ~ 8, extract 20 ~ 60min, fine to the compound solution after extraction, solving fine beating degree is 10 ~ 15》SR, obtains hybrid extraction liquid and mixing slag charge to the compound solid-liquid separation after solving fibre；
(2) cabo being added mixing tank, add the hot water of 50 ~ 80 DEG C by the amount that solid-to-liquid ratio is 1:4 ~ 8, extract 20 ~ 60min, fine to the cabo solution after extraction, solving fine beating degree is 10 ~ 15》SR, obtains the cabo solid-liquid separation after solving fibre obstructing liquid and stalk slag charge；
(3) successively carrying out middle concentrated jordaning and low dense defibrination after being mixed by the stalk slag charge in the mixing slag charge in step (1) and step (2), the beating degree of slurry is 20 ~ 30》SR, the slurry mix homogeneously that will obtain, after thickening, upper paper machine is copied into substrate；
(4) the hybrid extraction liquid obtained in step (1) concentration being allocated to obtain coating fluid, be applied to step (3) and manufacture paper with pulp on the substrate obtained, reconstituted tobacoo is made in drying, section.
The method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass the most according to claim 1, it is characterised in that Fructus Citri tangerinae grass described in step (1) is the fresh Fructus Citri tangerinae grass after solving fibre or Fructus Citri tangerinae grass slag.
The method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass the most according to claim 1, it is characterised in that in step (1), the water bath heat preservation temperature of mixing tank is 50 ~ 80 DEG C.
The method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass the most according to claim 1, it is characterized in that, in step (4), hybrid extraction liquid purifies through rectangular mesh screen and centrifuge, hybrid extraction liquid after purification concentrates through MVR falling film type evaporation, and the concentrated solution concentration after concentration is 40% ~ 50%.
The method that functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass the most according to claim 1, it is characterised in that described Nicotiana tabacum L. dead meal is offal or tobacco leaf fragment.
6. the reconstituted tobacco that the preparation method described in any one of claim 1 ~ 5 prepares.
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| CN104687233B (en) * | 2014-12-30 | 2017-10-10 | 广东中烟工业有限责任公司 | The preparation method and orange flavor reconstituted tobacco of a kind of orange flavor reconstituted tobacco |
| CN104738810B (en) * | 2015-02-11 | 2016-08-17 | 云南瑞升烟草技术（集团）有限公司 | A kind of preparation method of high bulk papermaking-method reconstituted tobaccos |
| CN108338399A (en) * | 2017-12-18 | 2018-07-31 | 中科国思生物科技研究（广州）有限公司 | A kind of health care tobacco preparation of sections method |
| CN108378409B (en) * | 2018-03-29 | 2021-12-17 | 河南中烟工业有限责任公司 | Method for improving quality of reconstituted tobacco by using bacterial cellulose |
| CN108783562B (en) * | 2018-07-02 | 2021-08-31 | 云南拓宝科技有限公司 | Preparation method of tobacco shreds suitable for novel cigarettes |
| CN110150727B (en) * | 2019-05-05 | 2023-07-21 | 贵州中烟工业有限责任公司 | Preparation method of dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes |
| CN110025036A (en) * | 2019-05-10 | 2019-07-19 | 湖北中烟工业有限责任公司 | A kind of preparation method of sweet orange odor type reconstituted tobacco |
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