CN104783323A - Electronic cigarette solution containing dry-distilled perfume - Google Patents
Electronic cigarette solution containing dry-distilled perfume Download PDFInfo
- Publication number
- CN104783323A CN104783323A CN201510246335.6A CN201510246335A CN104783323A CN 104783323 A CN104783323 A CN 104783323A CN 201510246335 A CN201510246335 A CN 201510246335A CN 104783323 A CN104783323 A CN 104783323A
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- CN
- China
- Prior art keywords
- tobacco
- dry distillated
- distillated flavor
- dry
- glycerine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Abstract
The invention discloses an electronic cigarette solution containing a dry-distilled perfume. The electronic cigarette solution is prepared by uniformly mixing 15-50% of the dry-distilled perfume and 30-60% of glycerinum and propylene glycol, wherein the dry-distilled perfume is prepared by dry distilling tobaccos in a nitrogen atmosphere at a proper temperature. Due to use of the dry-distilled perfume disclosed by the invention, the sensory quality of electronic cigarettes is obviously improved, so that the electronic cigarette is very close to the traditional cigarette on the aspects of fragrance and taste.
Description
Technical field
The present invention relates to a kind of tobacco juice for electronic smoke containing Dry distillated flavor, belong to electronic cigarette technical field.
Background technology
Electronic cigarette has another name called atomizer for electric, generally by the means of electrons heat, the nicotine-containing atomization of liquid is formed aerosol and is transmitted to respiratory system.As cigarette substitute, the outward appearance of its simulated cigarette and taste, but without burning, can not produce cigarette ash and stub, avoid disaster hidden-trouble; Also can not produce second-hand-cigarette, can not have an impact to PE; Also not containing harmful substances such as tar, CO, hydrogen cyanide, methacrylaldehyde, lead, arsenic.These advantages can break through the restriction of global Tobacco Control campaign, obtain huge growing space, have attracted the eyeball of numerous consumer at short notice.
But, compared with real cigarette, mostly there is the shortcoming that organoleptic quality is not good in current commercially available electronic cigarette, the development of the electronic cigarette of serious restriction.For this reason, the work promoting electronic cigarette aesthetic quality is extensively launched.Wherein, one of effective means be added with in tobacco juice for electronic smoke suitable means extract tobacco and/or non-tobacco class plant in active ingredient.Patent CN103054172A, CN103054171A and CN103070473A all adopt ultrasonic wave to extract Luzhou-flavor, flat-flavor and delicate fragrance type tobacco leaf respectively, prepare the electronic cigarette that fragrance, mouthfeel and traditional cigarette are more close.Patent CN103989244A and CN103720030A adopts supercritical CO
2extract non-tobacco natural plants and cigarette foam, the electronic cigarette aesthetic quality obtained and traditional cigarette are more close.Patent CN103054173A adopts 65 DEG C of gas bath shaking table succusions to extract discarded tobacco leaf, the method that patent CN103919274A utilizes 80 DEG C of refluxing extraction and molecular clock to combine is extracted Zimbabwe's tobacco leaf, American Burley tobacco leaf, Turkey's atomatic tobacco, Xinjiang tobacco leaf etc., large for Yunnan safflower gold dollar tobacco leaf is soaked in ethanol by patent CN103070472A, desolventize obtain leaf tobacco extract by centrifugal, steaming, these work all improve the aesthetic quality of electronic cigarette.But at present, there is not yet the relevant report promoting electronic cigarette organoleptic quality by adding Dry distillated flavor in prior art.
Summary of the invention
The present invention is the weak point for avoiding existing for above-mentioned prior art, and provide a kind of tobacco juice for electronic smoke containing Dry distillated flavor, to further promoting the aesthetic quality of electronic cigarette, make electronic cigarette closer to traditional cigarette, more consumer accepted.
The present invention is that technical solution problem adopts following technical scheme:
The present invention contains the tobacco juice for electronic smoke of Dry distillated flavor, and its feature is: each raw material formation by mass percentage of described tobacco juice for electronic smoke is:
Dry distillated flavor 15 ~ 50%;
Glycerine 30 ~ 60%;
Surplus is propane diols.
The present invention contains the tobacco juice for electronic smoke of Dry distillated flavor, and its feature is also: described Dry distillated flavor is at least one that condensation Dry distillated flavor and glycerine trap in Dry distillated flavor.
Described condensation Dry distillated flavor is prepared as follows: in a nitrogen atmosphere, and tobacco is carried out destructive distillation at 200 DEG C-400 DEG C, and distillate flows in receiving bottle through running water condensation and collects, and obtains condensation Dry distillated flavor.
Described glycerine trapping Dry distillated flavor is prepared as follows: in a nitrogen atmosphere, tobacco is carried out destructive distillation at 200 DEG C-400 DEG C, distillate directly imports in glycerine, obtains glycerine trapping Dry distillated flavor.The mass ratio of described tobacco and described glycerine is 0.5-4:1.
Described tobacco is at least one in flue-cured tobacco, burley tobaccos and Turkish tobaccos, the form of described tobacco be sheet, thread and Powdered at least one.
Compared with the prior art, advantage applies of the present invention exists:
(1) tobacco juice for electronic smoke of the present invention with the Dry distillated flavor of tobacco for main component, provide not only nicotine, additionally provide abundant tobacco characteristic aroma substance, obviously improve the aesthetic quality of electronic cigarette, make the fragrance of itself and traditional cigarette, mouthfeel more close.
(2) tobacco juice for electronic smoke of the present invention is used for the atomization of electronic cigarette, and harmful components are few, greatly reduces, and can not produce the harm of second-hand-cigarette to consumer's harm.
Detailed description of the invention
Below by way of detailed description of the invention, the invention will be further described, but embodiment is not the restriction to content of the present invention.
Embodiment 1:
The formula of the present embodiment tobacco juice for electronic smoke is (mass percent): 10% condensation Dry distillated flavor A, 50% glycerine, 40% propane diols.Above-mentioned raw materials is proportionally weighed rear mixing, and is stirred to evenly, namely obtain the tobacco juice for electronic smoke containing condensation Dry distillated flavor A, directly can be added on atomization in electronic cigarette device and suck.
The present embodiment condensation Dry distillated flavor A preparation process is as follows: under nitrogen protection; 900g Anhui south flue-cured tobacco pipe tobacco and 100g Greece spices offal are carried out destructive distillation at 220 DEG C; distillate flows in receiving bottle through running water condensation, the obtained condensation Dry distillated flavor A that can improve electronic cigarette organoleptic quality.
Embodiment 2:
The formula of the present embodiment tobacco juice for electronic smoke is (mass percent): 50% glycerine trapping Dry distillated flavor B, 40% glycerine, 10% propane diols.Above-mentioned raw materials is proportionally weighed rear mixing, and is stirred to evenly, namely obtain the tobacco juice for electronic smoke containing glycerine trapping Dry distillated flavor B, directly can be added on atomization in electronic cigarette device and suck.
The present embodiment glycerine trapping Dry distillated flavor B preparation process is as follows: under nitrogen protection; 1000g Yunnan Flue-cured Tobacco pipe tobacco is carried out destructive distillation at 320 DEG C; distillate directly imports in 800g glycerine without condensation; the obtained glycerine trapping Dry distillated flavor B that can improve electronic cigarette organoleptic quality, its main chemical compositions through GC-MS analysis result in table 1.
Table 1 Dry distillated flavor chemical composition
| Compound title | Condensation Dry distillated flavor C (μ g/mL) | Glycerine trapping Dry distillated flavor B (μ g/mL) |
| Pyridine | 286.35 | 69.57 |
| Pyrazine | 5.19 | 1.11 |
| Geranyl acetone | 519.78 | 172.47 |
| 3-methyl-2-cyclopentene-1-one | 63.87 | 15.65 |
| 4-cyclopentene-1,3-diketone | 73.12 | 20.31 |
| 3-furfural | 302.45 | 110.13 |
| 2-furfuryl alcohol | 594.60 | 224.67 |
| 5 hydroxymethyl furfural | 66.54 | 17.79 |
| 2,3-dimethyl indole | 24.34 | 6.79 |
| 2 methyl indole | 74.69 | 29.42 |
| 2-cyclopentene-Isosorbide-5-Nitrae-diketone | 56.86 | 17.07 |
| Valeric acid | 83.24 | 20.95 |
| Oleic acid | 39.80 | 11.09 |
| Acetic acid | 1519.84 | 514.78 |
| Nicotine | 3134.71 | 1648.37 |
Embodiment 3:
The formula of the present embodiment tobacco juice for electronic smoke is (mass percent): 5% condensation Dry distillated flavor C, 40% glycerine trapping Dry distillated flavor B, 40% glycerine, 15% propane diols.Above-mentioned raw materials is proportionally weighed rear mixing, and is stirred to evenly, namely obtain, containing the tobacco juice for electronic smoke of condensation Dry distillated flavor C and glycerine trapping Dry distillated flavor B, to be directly added on atomization in electronic cigarette device and to suck.
The present embodiment condensation Dry distillated flavor C preparation process is as follows: under nitrogen protection; 900g Anhui south flue-cured tobacco pipe tobacco and 100g Greece spices offal are carried out destructive distillation at 350 DEG C; distillate flows in receiving bottle through running water condensation; the obtained condensation Dry distillated flavor C that can improve electronic cigarette organoleptic quality, its main chemical compositions through GC-MS analysis result in table 1.
Embodiment 4:
The formula of the present embodiment tobacco juice for electronic smoke is (mass percent): 10% condensation Dry distillated flavor C, 20% glycerine trapping Dry distillated flavor B, 40% glycerine, 20% propane diols.Above-mentioned raw materials is proportionally weighed rear mixing, and is stirred to evenly, namely obtain, containing the tobacco juice for electronic smoke of condensation Dry distillated flavor C and glycerine trapping Dry distillated flavor B, to be directly added on atomization in electronic cigarette device and to suck.
Tobacco juice prepared by embodiment 1, embodiment 2, embodiment 3 and embodiment 4 is added in electronic cigarette and carries out sensory evaluation, evaluation result is in table 2, known, in the present invention, the consumption of Dry distillated flavor and different Dry distillated flavor ratio have impact to electronic cigarette organoleptic quality, be specially Dry distillated flavor lower than 15% time (embodiment 1), cigarette sense is more weak, and when consumption is between 15 ~ 50% (embodiment 2,3 and 4), integrated sensory's quality is better.
Table 2 electronic cigarette sensory quality assessment result
| Sample number into spectrum | Aesthetic quality describes |
| Embodiment 1 | Cigarette sense is weak, pleasant impression is low |
| Embodiment 2 | Fragrance is better, cigarette sense is moderate, good after-taste |
| Embodiment 3 | Fragrance is good, mouthfeel is full, cigarette sense enhancing, good after-taste |
| Embodiment 4 | Fragrance better, cigarette sense by force, slightly Ipomoea batatas burnt odor, good after-taste |
Claims (6)
1. the tobacco juice for electronic smoke containing Dry distillated flavor, is characterized in that: each raw material formation by mass percentage of described tobacco juice for electronic smoke is:
Dry distillated flavor 15 ~ 50%;
Glycerine 30 ~ 60%;
Surplus is propane diols.
2. the tobacco juice for electronic smoke containing Dry distillated flavor according to claim 1, is characterized in that: described Dry distillated flavor is at least one that condensation Dry distillated flavor and glycerine trap in Dry distillated flavor.
3. the tobacco juice for electronic smoke containing Dry distillated flavor according to claim 2, it is characterized in that: described condensation Dry distillated flavor is prepared as follows: in a nitrogen atmosphere, tobacco is carried out destructive distillation at 200 DEG C-400 DEG C, distillate flows in receiving bottle through running water condensation and collects, and obtains condensation Dry distillated flavor.
4. the tobacco juice for electronic smoke containing Dry distillated flavor according to claim 2, it is characterized in that: described glycerine trapping Dry distillated flavor is prepared as follows: in a nitrogen atmosphere, tobacco is carried out destructive distillation at 200 DEG C-400 DEG C, distillate directly imports in glycerine, obtains glycerine trapping Dry distillated flavor.
5. the tobacco juice for electronic smoke containing Dry distillated flavor according to claim 4, is characterized in that: the mass ratio of described tobacco and described glycerine is 0.5-4:1.
6. the tobacco juice for electronic smoke according to claim 3 and 4, is characterized in that: described tobacco is at least one in flue-cured tobacco, burley tobaccos and Turkish tobaccos, the form of described tobacco be sheet, thread and Powdered at least one.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510246335.6A CN104783323B (en) | 2015-05-14 | 2015-05-14 | A kind of tobacco juice for electronic smoke containing Dry distillated flavor |
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|---|---|---|---|
| CN201510246335.6A CN104783323B (en) | 2015-05-14 | 2015-05-14 | A kind of tobacco juice for electronic smoke containing Dry distillated flavor |
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| CN104783323A true CN104783323A (en) | 2015-07-22 |
| CN104783323B CN104783323B (en) | 2016-08-17 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105167170A (en) * | 2015-09-14 | 2015-12-23 | 浙江中烟工业有限责任公司 | Method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis |
| CN105249518A (en) * | 2015-09-25 | 2016-01-20 | 安徽中烟工业有限责任公司 | Porous tobacco material for heating non-combustion type cigarettes and preparation method of porous tobacco material |
| CN105595411A (en) * | 2016-02-01 | 2016-05-25 | 湖北中烟工业有限责任公司 | Method for preparing tobacco-characteristic-taste tobacco flavor material and electronic cigarette fluid containing tobacco flavor material |
| CN105725265A (en) * | 2016-04-28 | 2016-07-06 | 湖南中烟工业有限责任公司 | Device and method for preparing tobacco source basic cigarette flavor material for novel tobacco products |
| CN113142643A (en) * | 2021-02-08 | 2021-07-23 | 广东中烟工业有限责任公司 | Cigarette essence for heating non-combustible cigarettes and preparation method and application thereof |
Citations (4)
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| US5235992A (en) * | 1991-06-28 | 1993-08-17 | R. J. Reynolds Tobacco Company | Processes for producing flavor substances from tobacco and smoking articles made therewith |
| CN1742636A (en) * | 2004-09-02 | 2006-03-08 | 邹宝安 | Technology for producing pollution-free liquid cigarette |
| CN104041935A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese-style flue-cured tobacco fragrance cigarette juice for electronic cigarette |
| CN104041936A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese style mixed-fragrance cigarette juice for electronic cigarette |
-
2015
- 2015-05-14 CN CN201510246335.6A patent/CN104783323B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5235992A (en) * | 1991-06-28 | 1993-08-17 | R. J. Reynolds Tobacco Company | Processes for producing flavor substances from tobacco and smoking articles made therewith |
| CN1742636A (en) * | 2004-09-02 | 2006-03-08 | 邹宝安 | Technology for producing pollution-free liquid cigarette |
| CN104041935A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese-style flue-cured tobacco fragrance cigarette juice for electronic cigarette |
| CN104041936A (en) * | 2014-06-06 | 2014-09-17 | 山东中烟工业有限责任公司 | Method for extracting Chinese style mixed-fragrance cigarette juice for electronic cigarette |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105167170A (en) * | 2015-09-14 | 2015-12-23 | 浙江中烟工业有限责任公司 | Method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis |
| CN105249518A (en) * | 2015-09-25 | 2016-01-20 | 安徽中烟工业有限责任公司 | Porous tobacco material for heating non-combustion type cigarettes and preparation method of porous tobacco material |
| CN105249518B (en) * | 2015-09-25 | 2017-10-03 | 安徽中烟工业有限责任公司 | A kind of preparation method for heating the porous tobacco-containing material of non-combustion-type cigarette |
| CN105595411A (en) * | 2016-02-01 | 2016-05-25 | 湖北中烟工业有限责任公司 | Method for preparing tobacco-characteristic-taste tobacco flavor material and electronic cigarette fluid containing tobacco flavor material |
| CN105595411B (en) * | 2016-02-01 | 2017-05-17 | 湖北中烟工业有限责任公司 | Method for preparing tobacco-characteristic-taste tobacco flavor material and electronic cigarette fluid containing tobacco flavor material |
| CN105725265A (en) * | 2016-04-28 | 2016-07-06 | 湖南中烟工业有限责任公司 | Device and method for preparing tobacco source basic cigarette flavor material for novel tobacco products |
| CN113142643A (en) * | 2021-02-08 | 2021-07-23 | 广东中烟工业有限责任公司 | Cigarette essence for heating non-combustible cigarettes and preparation method and application thereof |
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| Publication number | Publication date |
|---|---|
| CN104783323B (en) | 2016-08-17 |
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