CN105167170A - Method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis - Google Patents
Method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis Download PDFInfo
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- CN105167170A CN105167170A CN201510580910.6A CN201510580910A CN105167170A CN 105167170 A CN105167170 A CN 105167170A CN 201510580910 A CN201510580910 A CN 201510580910A CN 105167170 A CN105167170 A CN 105167170A
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Abstract
The invention relates to electronic cigarettes, in particular to a method for applying tobacco subjected to dry distillation pyrolysis to a novel tobacco product to obtain an extract with sensual pleasures and psychological intensity similar to those of traditional cigarettes. The method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis comprises the steps of weighing tobacco, placing tobacco in a heating furnace, increasing temperature to 150-1000 DEG C, introducing carrier gas, introducing smoke generated from pyrolysis into an absorption bottle, placing the absorption bottle in a cold trap, conducting smoke collection with an electronic cigarette solvent, washing smoke condensation products in a pipeline out by means of collection liquid, and obtaining smoke extraction solution. The electronic cigarette nicotine liquid has the advantage that sensual pleasures and psychological intensity similar to those of traditional cigarettes are obtained.
Description
Technical field
The present invention relates to electronic cigarette, especially relate to a kind of by carbonization method process tobacco use in novel tobacco goods, make to obtain the method for treatment of tobacco of the extract close to traditional cigarette pleasure of the senses and physiological strength.
Background technology
Smoking is harmful to your health, and second-hand-cigarette harm is larger, and form secondary pollution and public harm, therefore smoke-free tobacco product is urgently developed, and electronic cigarette, heats the not novel tobacco goods such as burning tobacco goods, buccal cigarette and become the domestic and international industry focus of attention.Result of combustion of tobacco process has the complicated reaction such as thermal cracking, Mei Lade, and different temperatures and atmosphere affect huge on product.Research shows that tobacco discharges fragrance component kind and reaches maximum when being heated to 600 DEG C, but the novel tobacco form such as electronic cigarette and heating non-combustion-type cigarette, its aspiration procedure cannot reach this heating-up temperature, thus with the essential oil of tobaccos that traditional tobacco processing mode extracts, be applied to the rich and relative traditional cigarette Shortcomings of physiological strength of its smoke perfume in novel tobacco, consumer cannot be brought corresponding satisfaction, the novel tobaccos such as electronic cigarette are squeezed into the market, replace cigarette conventional consumption mode to cause obstruction.
Summary of the invention
For overcoming the existing deficiency being applied to the tobacco processing mode of novel tobacco, and make up the shortcoming such as existing electronic cigarette liquid tobacco aroma and physiological strength deficiency, the object of the present invention is to provide a kind of tobacco of carbonization process to prepare the method for tobacco juice for electronic smoke, extract the method for treatment of tobacco of the essential oil of tobaccos close to traditional cigarette flue gas sense organ.
In order to realize above-mentioned object, present invention employs following technical scheme:
A kind of tobacco of carbonization process prepares the method for tobacco juice for electronic smoke, the method comprises the following steps: claim tobacco to put into heating furnace, be heated to 150-1000 DEG C, pass into carrier gas, flue gas pyrolysis produced brings absorption bottle into, is placed in cold-trap, carries out flue gas trapping with electronic cigarette solvent, and wash out ducted smoke condensate with trapping solution, obtain tobacco extract.
As preferably, described tobacco is offal, or traditional cigarette pipe tobacco, or tobacco leaf.
As preferably, described carrier gas is nitrogen or air, or the mist of different oxygen content.Different carrier gas can conditioning tobacco cracking atmosphere, changes gained smoke components, thus changes flue gas sense organ.
As preferably, described electronic cigarette solvent adopts one or more mixing in ethanol, propane diols, glycerine, D-sorbite and xylitol.The electronic cigarette liquid solvents such as direct propane diols are as absorbing liquid, propane diols has good dissolution to nicotine and most flavor component, regulate sense organ through later stage flavoring and casing and inhale taste, taste can be obtained comparatively ripe and close to the electronic cigarette liquid formula of traditional cigarette sense organ.
Heating-up temperature can carry out set temperature according to taste demand, and temperature is higher, and physiological strength is larger, can set a certain heating-up temperature, also can carry out temperature programming.As preferably, described heating-up temperature is 400-600 DEG C.At this temperature, the release of tobacco flavor composition is comparatively abundant, and harmful substance release not yet rolls up.
The present invention also discloses a kind of tobacco juice for electronic smoke in addition, and the method described in this electronic cigarette prepares.Can certainly sense organ be regulated to obtain with suction taste by flavoring and casing on this basis.
The present invention is by the mode of pyrogenation and carbonization, in tobacco processing procedure, carry out reaching the complex reaction process such as cracking, Mei Lade that traditional cigarette local flavor has to pass through in advance, the tobacco extract obtained at utmost can reduce traditional cigarette flue gas, make up the shortcomings such as the insufficient fragrance such as existing electronic cigarette, new cigarette, style be fuzzy, minimizing cigarette smoke can be reached on the basis not affecting cigarette sense organ, avoid the effect of second-hand-cigarette and environmental pollution.Tobacco juice for electronic smoke of the present invention has the advantage close to traditional cigarette pleasure of the senses and physiological strength.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1: take 4g pipe tobacco and put into tube furnace, be heated to 200 DEG C, pass into nitrogen, flue gas pyrolysis produced brings the absorption bottle being placed in cold-trap into, absorb with 25mL propane diols, and wash out ducted smoke condensate with 40mL propane diols, obtain tobacco extract.
Embodiment 2: take 4g pipe tobacco and put into tube furnace, be heated to 400 DEG C, pass into nitrogen, flue gas pyrolysis produced brings the absorption bottle being placed in cold-trap into, absorb with 25mL propane diols, and wash out ducted smoke condensate with 40mL propane diols, obtain tobacco extract.
Embodiment 3: take 4g pipe tobacco and put into tube furnace, be heated to 600 DEG C, pass into nitrogen, flue gas pyrolysis produced brings the absorption bottle being placed in cold-trap into, absorb with 25mL propane diols, and wash out ducted smoke condensate with 40mL propane diols, obtain tobacco extract.
Embodiment 4: take 1g pipe tobacco and put into tube furnace, be heated to 200 DEG C, pass into air, flue gas pyrolysis produced brings the absorption bottle being placed in cold-trap into, absorb with 25mL propane diols, and wash out ducted smoke condensate with 30mL propane diols, obtain tobacco extract.
Above experimental result shows, under nitrogen atmosphere, within the scope of 200-600 DEG C, increase with temperature, tobacco extract fragrance is rich to be increased with physiological strength.And under same heating-up temperature, the tobacco extract relative nitrogen atmosphere obtained under air atmosphere, its physiological strength is stronger, and sense organ is closer to traditional cigarette.
Above the tobacco processing mode of carbonization method extraction essential oil of tobaccos of the present invention is set forth; the present invention is understood for helping; but embodiments of the present invention are not restricted to the described embodiments; any do not deviate from the principle of the invention under do change, modification, substitute, combination, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (7)
1. the tobacco of a carbonization process prepares the method for tobacco juice for electronic smoke, it is characterized in that the method comprises the following steps: claim tobacco to put into heating furnace, be heated to 150-1000 DEG C, pass into carrier gas, flue gas pyrolysis produced brings absorption bottle into, is placed in cold-trap, carries out flue gas trapping with electronic cigarette solvent, and wash out ducted smoke condensate with trapping solution, obtain tobacco extract.
2. the tobacco of a kind of carbonization process according to claim 1 prepares the method for tobacco juice for electronic smoke, it is characterized in that: described tobacco is offal, or traditional cigarette pipe tobacco, or tobacco leaf.
3. the tobacco of a kind of carbonization process according to claim 1 prepares the method for tobacco juice for electronic smoke, it is characterized in that: carrier gas is nitrogen or air, or the mist of different oxygen content.
4. the tobacco of a kind of carbonization process according to claim 1 prepares the method for tobacco juice for electronic smoke, it is characterized in that: electronic cigarette solvent adopts one or more mixing in ethanol, propane diols, glycerine, D-sorbite and xylitol.
5. the tobacco of a kind of carbonization process according to claim 1 prepares the method for tobacco juice for electronic smoke, it is characterized in that: heating-up temperature is 400-600 DEG C.
6. a tobacco juice for electronic smoke, is characterized in that this tobacco juice for electronic smoke is prepared by the method described in claim 1 ~ 5 any one claim.
7. a tobacco juice for electronic smoke, is characterized in that this regulates sense organ to obtain with suction taste by a kind of tobacco juice for electronic smoke flavoring and casing according to claim 6.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510580910.6A CN105167170A (en) | 2015-09-14 | 2015-09-14 | Method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis |
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| CN201510580910.6A CN105167170A (en) | 2015-09-14 | 2015-09-14 | Method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis |
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| CN105167170A true CN105167170A (en) | 2015-12-23 |
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Cited By (20)
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|---|---|---|---|---|
| CN105661622A (en) * | 2016-02-16 | 2016-06-15 | 中国农业科学院烟草研究所 | Nicotine liquid raw material of electronic cigarette and preparation device and method of nicotine liquid raw material |
| CN105686070A (en) * | 2016-04-28 | 2016-06-22 | 湖南中烟工业有限责任公司 | Preparation method for tobacco source raw material with basic cigarette smell |
| CN105725266A (en) * | 2016-04-28 | 2016-07-06 | 湖南中烟工业有限责任公司 | Preparation method of basic cigarette-smell raw material deriving from tobacco |
| CN105852200A (en) * | 2016-04-28 | 2016-08-17 | 湖南中烟工业有限责任公司 | Preparation method of tobacco-sourced basic cigarette-smell raw material |
| CN105852199A (en) * | 2016-04-28 | 2016-08-17 | 湖南中烟工业有限责任公司 | Preparation method of tobacco-sourced basic cigarette-smell raw material |
| CN106418664A (en) * | 2016-12-08 | 2017-02-22 | 江苏中烟工业有限责任公司 | Method for preparing electronic tobacco juice from tobacco raw material by using alkali type low-temperature dry distillation process |
| CN107744710A (en) * | 2017-09-07 | 2018-03-02 | 浙江中烟工业有限责任公司 | The method of aroma component and application in a kind of selective absorption tobacco Pintsch process flue gas using solid adsorption material |
| CN108601390A (en) * | 2016-02-25 | 2018-09-28 | 菲利普莫里斯生产公司 | The method of composite before evaporation of the manufacture comprising volatile matter |
| CN110747058A (en) * | 2019-09-27 | 2020-02-04 | 云南中烟工业有限责任公司 | Method for extracting special plant spice for heating non-combustible cigarettes |
| CN110959896A (en) * | 2018-09-26 | 2020-04-07 | 浙江中烟工业有限责任公司 | Tobacco shred added with functional fragrant raw material and heating non-combustible cigarette |
| CN111296886A (en) * | 2019-12-10 | 2020-06-19 | 颐中（青岛）实业有限公司 | Dry distillation spice and application thereof in novel tobacco products |
| CN113349405A (en) * | 2021-06-30 | 2021-09-07 | 四川三联新材料有限公司 | Preparation method of tobacco source fragrance raw material for heating cigarettes |
| CN113712241A (en) * | 2021-09-14 | 2021-11-30 | 中国烟草总公司郑州烟草研究院 | Tobacco tar prepared by heating herbal raw materials with assistance of atomizing agent |
| CN113727615A (en) * | 2019-06-05 | 2021-11-30 | 菲利普莫里斯生产公司 | Improved method for producing liquid tobacco extract |
| CN113905621A (en) * | 2019-06-05 | 2022-01-07 | 菲利普莫里斯生产公司 | Method of producing blended liquid tobacco extracts from two or more tobaccos |
| CN114073326A (en) * | 2021-11-12 | 2022-02-22 | 刘虎 | Preparation method of tobacco tar |
| CN114343232A (en) * | 2022-03-03 | 2022-04-15 | 云南中烟工业有限责任公司 | Method for trapping substances in flue gas by using high-temperature distillation method |
| CN114451576A (en) * | 2022-03-03 | 2022-05-10 | 云南中烟工业有限责任公司 | Method for trapping substances in flue gas by using smoldering method |
| CN114554876A (en) * | 2019-11-14 | 2022-05-27 | 菲利普莫里斯生产公司 | Improved tobacco-flavored dry powder formulations |
| JP2022534865A (en) * | 2019-06-05 | 2022-08-04 | フィリップ・モーリス・プロダクツ・ソシエテ・アノニム | Concentration of wet tobacco extract |
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Cited By (26)
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| CN105661622B (en) * | 2016-02-16 | 2018-03-23 | 中国农业科学院烟草研究所 | A kind of tobacco juice for electronic smoke raw material and its preparation facilities and method |
| CN105661622A (en) * | 2016-02-16 | 2016-06-15 | 中国农业科学院烟草研究所 | Nicotine liquid raw material of electronic cigarette and preparation device and method of nicotine liquid raw material |
| CN108601390A (en) * | 2016-02-25 | 2018-09-28 | 菲利普莫里斯生产公司 | The method of composite before evaporation of the manufacture comprising volatile matter |
| CN108601390B (en) * | 2016-02-25 | 2022-05-10 | 菲利普莫里斯生产公司 | Method of making pre-evaporation formulations containing volatiles |
| CN105686070A (en) * | 2016-04-28 | 2016-06-22 | 湖南中烟工业有限责任公司 | Preparation method for tobacco source raw material with basic cigarette smell |
| CN105725266A (en) * | 2016-04-28 | 2016-07-06 | 湖南中烟工业有限责任公司 | Preparation method of basic cigarette-smell raw material deriving from tobacco |
| CN105852200A (en) * | 2016-04-28 | 2016-08-17 | 湖南中烟工业有限责任公司 | Preparation method of tobacco-sourced basic cigarette-smell raw material |
| CN105852199A (en) * | 2016-04-28 | 2016-08-17 | 湖南中烟工业有限责任公司 | Preparation method of tobacco-sourced basic cigarette-smell raw material |
| CN106418664A (en) * | 2016-12-08 | 2017-02-22 | 江苏中烟工业有限责任公司 | Method for preparing electronic tobacco juice from tobacco raw material by using alkali type low-temperature dry distillation process |
| CN107744710B (en) * | 2017-09-07 | 2020-06-19 | 浙江中烟工业有限责任公司 | Method for selectively adsorbing aroma components in tobacco pyrolysis smoke and application |
| CN107744710A (en) * | 2017-09-07 | 2018-03-02 | 浙江中烟工业有限责任公司 | The method of aroma component and application in a kind of selective absorption tobacco Pintsch process flue gas using solid adsorption material |
| CN110959896A (en) * | 2018-09-26 | 2020-04-07 | 浙江中烟工业有限责任公司 | Tobacco shred added with functional fragrant raw material and heating non-combustible cigarette |
| CN113905621B (en) * | 2019-06-05 | 2023-09-12 | 菲利普莫里斯生产公司 | Method of producing blended liquid tobacco extract from two or more tobaccos |
| CN113727615A (en) * | 2019-06-05 | 2021-11-30 | 菲利普莫里斯生产公司 | Improved method for producing liquid tobacco extract |
| CN113905621A (en) * | 2019-06-05 | 2022-01-07 | 菲利普莫里斯生产公司 | Method of producing blended liquid tobacco extracts from two or more tobaccos |
| CN113727615B (en) * | 2019-06-05 | 2023-09-05 | 菲利普莫里斯生产公司 | Improved method for producing liquid tobacco extract |
| JP2022534865A (en) * | 2019-06-05 | 2022-08-04 | フィリップ・モーリス・プロダクツ・ソシエテ・アノニム | Concentration of wet tobacco extract |
| CN110747058A (en) * | 2019-09-27 | 2020-02-04 | 云南中烟工业有限责任公司 | Method for extracting special plant spice for heating non-combustible cigarettes |
| CN114554876A (en) * | 2019-11-14 | 2022-05-27 | 菲利普莫里斯生产公司 | Improved tobacco-flavored dry powder formulations |
| CN114554876B (en) * | 2019-11-14 | 2024-03-01 | 菲利普莫里斯生产公司 | Improved tobacco flavor dry powder formulations |
| CN111296886A (en) * | 2019-12-10 | 2020-06-19 | 颐中（青岛）实业有限公司 | Dry distillation spice and application thereof in novel tobacco products |
| CN113349405A (en) * | 2021-06-30 | 2021-09-07 | 四川三联新材料有限公司 | Preparation method of tobacco source fragrance raw material for heating cigarettes |
| CN113712241A (en) * | 2021-09-14 | 2021-11-30 | 中国烟草总公司郑州烟草研究院 | Tobacco tar prepared by heating herbal raw materials with assistance of atomizing agent |
| CN114073326A (en) * | 2021-11-12 | 2022-02-22 | 刘虎 | Preparation method of tobacco tar |
| CN114451576A (en) * | 2022-03-03 | 2022-05-10 | 云南中烟工业有限责任公司 | Method for trapping substances in flue gas by using smoldering method |
| CN114343232A (en) * | 2022-03-03 | 2022-04-15 | 云南中烟工业有限责任公司 | Method for trapping substances in flue gas by using high-temperature distillation method |
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Application publication date: 20151223 |
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