CN204409565U - A kind of destructive distillation room for heat tobacco and destructive distillation device - Google Patents

A kind of destructive distillation room for heat tobacco and destructive distillation device Download PDF

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Publication number
CN204409565U
CN204409565U CN201520096798.4U CN201520096798U CN204409565U CN 204409565 U CN204409565 U CN 204409565U CN 201520096798 U CN201520096798 U CN 201520096798U CN 204409565 U CN204409565 U CN 204409565U
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destructive distillation
room
heat
tobacco
heating
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CN201520096798.4U
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赵国玲
杨华武
尹新强
代远刚
卢红兵
黄建国
黎艳玲
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Abstract

The utility model relates to a kind of destructive distillation room for heat tobacco and destructive distillation device, belongs to electronic cigarette field.The described destructive distillation room for heat tobacco, comprises sample room, zone of heating and heat-insulation layer, and the surrounding of described sample room overlaps successively from the inside to the outside and has zone of heating and heat-insulation layer; One end of described sample room is provided with air inlet, and the other end is provided with gas outlet.The destructive distillation room for heat tobacco that the utility model provides and destructive distillation device, structure is simple, easy to operate, efficiently solves anaerobic heating still-process and produces black tobacco tar, the problem that smoke is overweight, can obtain the cigarette perfume similar to traditional combustion cigarette and mouthfeel.

Description

A kind of destructive distillation room for heat tobacco and destructive distillation device
Technical field
The utility model relates to a kind of destructive distillation room for heat tobacco and destructive distillation device, belongs to electronic cigarette field.
Background technology
In recent years, the novel tobacco such as low temperature cigarette, electronic cigarette goods are just in rapid rising.Electronic cigarette profile is similar to common cigarette, is the device that one can be vaporized into electronic cigarette liquid (actual is a kind of formula fragrance solution, also claims tobacco tar) fog, brings the sensation of similar smoking to smoker.
Electronic cigarette decreases the injury of the health to people while the custom meeting people's smoking.Generally, electronic cigarette has following principal characters: one is do not need burning, compares traditional cigarette harmfulness less; Two be PE is had an impact relatively little; Three is the needs that can adapt to and meet consumer to a certain extent.
But compare with traditional cigarette, electronic cigarette exists huge spread on the aesthetic quality sucked, to flavor quality satisfaction not when smoker sucks electronic cigarette, one is that electronic cigarette hay-scented is lightly seasoned thin; Two is the sensations lacking burning tobacco.
Utility model content
The utility model is for existing electronic cigarette liquid technical problem larger with the fragrant gap of the cigarette of traditional cigarette in the suction such as fragrance, mouthfeel sensation, provides a kind of destructive distillation room for heat tobacco and destructive distillation device.
The technical solution of the utility model is, a kind of destructive distillation room for heat tobacco, and described destructive distillation room comprises sample room, and the surrounding of described sample room overlaps successively from the inside to the outside and has zone of heating and heat-insulation layer; One end of described sample room is provided with air inlet, and the other end is provided with gas outlet.
Further, the air inlet of described sample room is provided with stainless steel gauze.
Further, described heat-insulation layer is heat-preservation cotton layer.
Further, the two ends of described zone of heating are provided with the pipeline connecting circular-pump.
Further, described pipeline is insulation stainless steel pipes.
The utility model is a kind of destructive distillation device for heat tobacco further, comprise connect successively above-mentioned destructive distillation room, condensing unit, absorption plant and vavuum pump.
Further, between absorption plant and vavuum pump, surge chamber is established.
Further, between absorption plant and vavuum pump, gas flowmeter is established.
The utility model utilizes destructive distillation device to add thermal distillation to pipe tobacco and/or offal, the material in pipe tobacco, offal with baking fragrance can be distilled, increase the sensation of similar traditional cigarette burning.
Current heating destructive distillation device mainly coal carbonization, publication number is patent discloses " a kind of external combustion internally heated coal carbonization furnace " of CN101691493, comprises dryer section, cooling section and cold flue gas pipeline.The high-temperature flue gas that this gas retort is produced by burning dry distillation gas carries out drying and destructive distillation to coal, and utilizes dry distillation gas to cool semicoke, and the heat smoke that cooling produces is used for the preheating of coal.
Publication number is the method that patent discloses one " low-temperature coal carbonization kiln " this gas retort of CN1966609A is that air sprays into interior pipe at a high speed, coal gas rotation under the insinuating of air sprays into and mixes with air, after entering body of heater, gas-fired becomes high-temperature gas, in furnace chamber, the coal charge of retort section contacts rear heat-shift with high-temperature gas, and coal charge pyrolysis discharges coal gas and tar.
The dry distillation of coal device of above-mentioned patent all adopts air heat to carry the mode of heating of internal heat type, and coal gas has combustion phenomena.The utility model is wished that offal or pipe tobacco only heat and is not burnt, deep fat is exported as circular-pump can be utilized, circulate between the zone of heating of deep fat in destructive distillation room and circular-pump, offal or pipe tobacco are placed in cylindrical sample indoor, the energy warms destructive distillation offal utilizing deep fat to transmit or pipe tobacco, one end of sample room is provided with the opening that can import oxygen-containing gas, enter for preventing the impurity such as dust, stainless gauze can be established at opening part, can ensure certain air enters sample room simultaneously, the sample room other end has the metal tube of rubber stopper to be connected with condensing unit by a cover, after pipe tobacco or offal heat, the flue gas volatilized condenses in condensing unit, the flue gas the do not condensed absorption plant that absorbing liquid is housed absorbs, absorption plant is connected with vavuum pump, surge flask is established between absorption plant and vavuum pump.In addition, can also establish the flow of vacuum testing flow meter air in whole destructive distillation device, vacuum-flow gauge is located between absorption plant and vavuum pump.
The center of destructive distillation room is the sample room of placing offal, and outside sample room, an interlayer passes into the deep fat from high-temperature circulator, is called zone of heating.Add the heat-preservation cotton layer that 2cm is thick around zone of heating, destructive distillation room and external environment are completely cut off, and heat loss is few.
The utility model utilizes vavuum pump to bring in destructive distillation room by certain air stream, by the fume collection that produces in retort process in condenser pipe and absorption bottle.By adjusting gas flow meter, the size of air draught in retort process can be controlled, the size of air draught has larger impact to destructive distillation effect, whole retort process is aerobic heating destructive distillation, and offal can not blackening in still-process, does not burn, just integral color is deepened, the tobacco tar of black can not be produced in retort process, there is the active ingredient of baking fragrance, closer to fragrance, the taste of traditional cigarette in the mainly tobacco that destructive distillation obtains.What traditional tobacco added that thermal distillation mainly adopts is anaerobic mode of heating, and offal is easy to blackening in high-temperature heating process, and is easy at still head the tobacco tar producing black, and the distillation smoke obtained can be heavier.
The utility model is containing under the air-flow of oxygen, the easiest is air, tobacco being heated to temperature is between 120 ~ 250 DEG C, preferably between 150 ~ 200 DEG C, heating is produced fragrant, air-flow will add thermogenetic fragrance matter importing condensing tube condensation simultaneously, collect the liquid that condensation produces, uncooled gas absorbs by taking over the tail after condenser pipe 2 bottles be connected, ethanol about 100-200 milliliter is housed in first bottle, the absorbing liquid based on glycerine about 300-400 milliliter is housed in absorption bottle below.The mode of air-flow with bubbling in absorption bottle produced is dissolved in absorbing liquid.What absorption bottle connected below is a surge flask, mainly prevents condensate from entering vavuum pump.Air draught outside system is entered destructive distillation device system by the effect of vavuum pump, is taken out of in condenser pipe by the gas produced in retort process simultaneously.-10 ~ 15 DEG C of cooling liquid coolings that condenser pipe exports with sub-cooled EGR, chilled liquid temperature preferably controls between-10 ~-5 DEG C.Absorbing liquid in the condensate liquid collected by condenser pipe after reaction terminates and absorption bottle merges, and must give the tobacco that electronic cigarette feels with burning tobacco and cause perfumery.
The destructive distillation room for heat tobacco that the utility model provides and destructive distillation device, structure is simple, easy to operate, efficiently solves anaerobic heating still-process and produces black tobacco tar, the problem that smoke is overweight, can obtain the cigarette perfume similar to traditional combustion cigarette and mouthfeel.
Accompanying drawing explanation
Fig. 1 represents the destructive distillation room schematic diagram for heat tobacco that the utility model provides.
Fig. 2 represents the destructive distillation device schematic diagram for heat tobacco that the utility model provides.
Detailed description of the invention
Below in conjunction with drawings and Examples, the utility model is described in further detail.
embodiment 1
Circular-pump is provided deep fat by the utility model, between the heat-insulation layer 3 of cylindrical destructive distillation room and sample room 1 is zone of heating 2 for the interlayer be connected with circular-pump, deep fat is circulated between zone of heating and circular-pump by the stainless steel tube 4 of two insulations, the heat-insulation layer 3 of zone of heating 2 periphery is the heat-preservation cotton that 2 cm are thick, sample room 1 is completely cut off with external environment, and heat loss is few.Offal or pipe tobacco are placed in columniform sample room 1, the stainless gauze 5 of to be diameter be in one end of sample room 18 cm ensures certain air and enters sample room, the sample room other end has the metal tube of rubber stopper to be connected with one end of condensing unit by a cover, the other end of condensing unit 6 is connected with the inlet end of absorption plant 7, absorption plant is the absorption bottle that absorbing liquid is housed, and absorbing liquid can absorb and dissolve the uncooled flue gas got off of condensing unit 6.Gas flowmeter 9, surge chamber 8 and vavuum pump 10 is connected successively in the outlet side of absorption plant 7.Under certain air draught, the high-temperature retorting thing of offal or pipe tobacco is condensate in the condensing unit 6 of-10 ~-5 DEG C, uncooled gas absorbing liquid absorbs, tobacco causes perfumery and is the flue gas distilled out, comprise condensation and uncooled flue gas, by the liquid of condensation and the absorbing liquid merging absorbing flue gas, i.e. electronic cigarette liquid, this electronic cigarette liquid must have cigarette burning cigarette perfume sensation.
embodiment 2
First by 20g Sangzhi B 3f offal is placed in the sample room of destructive distillation room, destructive distillation room and condensing unit, absorption plant, gas flowmeter, surge chamber and vavuum pump are connected, open circular-pump, the temperature of circular-pump is adjusted to 150 DEG C, vavuum pump is regulated to make air draught be 80 mL/min, absorbing liquid to be mass percent be 15% water, mass percent be 65% glycerine, mass percent be in the mixed liquor of the ethanol of 20%, distillation heating 1 h, merges the distillate in condenser pipe and absorbing liquid after distillation terminates and obtains the electronic cigarette liquid with cigarette burning cigarette perfume sensation.
Getting 1mL electronic cigarette liquid adds in atomizer, and the personnel that smoke panel test that please be professional smoke panel test, and electronic cigarette has obvious tobacco aroma, have the sensation of curing the tobacco calcination such as perfume (or spice), sootiness perfume and producing, but the sensation of sootiness is slighter.
embodiment 3
20g Zimbabwe offal is placed in the sample room of destructive distillation room, by destructive distillation room and condensing unit, absorption plant, gas flowmeter, surge chamber and vavuum pump connect, open heat cycles device, the temperature of heat cycles device is adjusted to 180 DEG C, air draught is regulated to be 100 mL/min, absorbing liquid to be mass percent be 10% water, mass percent is the glycerine of 70%, mass percent is in the mixed liquor of the ethanol of 20%, distillation heating 2h, after distillation terminates, the distillate in condenser pipe and absorbing liquid merged and obtain the electronic cigarette liquid with burning tobacco sensation.
Getting 1mL electronic cigarette liquid adds in atomizer, and the personnel that smoke panel test that please be professional smoke panel test, and electronic cigarette has tobacco aroma, but fragrance quality has decline, and have the sensation of curing the result of combustion of tobacco such as perfume (or spice), sootiness perfume and producing, the sensation of sootiness is stronger.
embodiment 4
By 20g U.S. SB 4f offal is placed in the sample room of destructive distillation room, destructive distillation room and condensing unit, absorption plant, gas flowmeter, surge chamber and vavuum pump are connected, open heat cycles device, the temperature of heat cycles device is adjusted to 200 DEG C, lower adjustment air draught is 200 mL/min, absorbing liquid to be mass percent be 15% water, mass percent be 65% glycerine, mass percent be in the mixed liquor of the ethanol of 20%, add thermal distillation 3h, after distillation terminates, the distillate in condenser pipe and absorbing liquid merged and obtain the electronic cigarette liquid with burning tobacco sensation.
Getting 1mL electronic cigarette liquid adds in atomizer, and the personnel that smoke panel test that please be professional smoke panel test, and electronic cigarette has tobacco aroma, have the sensation of curing the result of combustion of tobacco such as perfume (or spice), sootiness perfume and producing, but feeling of sootiness is stronger.

Claims (8)

1. the destructive distillation room for heat tobacco, it is characterized in that, described destructive distillation room comprises sample room (1), zone of heating (2) and heat-insulation layer (3), and the surrounding of described sample room (1) overlaps successively from the inside to the outside and has described zone of heating (2) and heat-insulation layer (3); One end of described sample room (1) is provided with air inlet, and the other end is provided with gas outlet.
2. destructive distillation room as claimed in claim 1, it is characterized in that, the air inlet of described sample room (1) is provided with stainless steel gauze (5).
3. destructive distillation room as claimed in claim 1, it is characterized in that, described heat-insulation layer (3) is heat-preservation cotton layer.
4. destructive distillation room as claimed in claim 1, is characterized in that, the two ends of described zone of heating (2) are provided with the pipeline (4) connecting circular-pump.
5. destructive distillation room as claimed in claim 4, is characterized in that, described pipeline (4) is insulation stainless steel pipes.
6. for a destructive distillation device for heat tobacco, it is characterized in that, comprise the described destructive distillation room of one of Claims 1 to 5 connected successively, condensing unit (6), absorption plant (7) and vavuum pump (10).
7. destructive distillation device as claimed in claim 6, is characterized in that, establish surge chamber (8) between absorption plant (7) and vavuum pump (10).
8. destructive distillation device as claimed in claims 6 or 7, is characterized in that, establish gas flowmeter (9) between absorption plant (7) and vavuum pump (10).
CN201520096798.4U 2015-02-11 2015-02-11 A kind of destructive distillation room for heat tobacco and destructive distillation device Active CN204409565U (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105661622A (en) * 2016-02-16 2016-06-15 中国农业科学院烟草研究所 Nicotine liquid raw material of electronic cigarette and preparation device and method of nicotine liquid raw material
CN105725265A (en) * 2016-04-28 2016-07-06 湖南中烟工业有限责任公司 Device and method for preparing tobacco source basic cigarette flavor material for novel tobacco products
CN107252135A (en) * 2017-06-28 2017-10-17 云南中烟工业有限责任公司 A kind of industrial abstract apparatus and method of tobacco pyrolytic cracking releaser
CN107699333A (en) * 2017-11-08 2018-02-16 江苏恒森烟草机械有限公司 A kind of high temperature extracts tobacco tar device
CN115161111A (en) * 2022-08-23 2022-10-11 云南中烟工业有限责任公司 Spices dry distillation extraction element

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105661622A (en) * 2016-02-16 2016-06-15 中国农业科学院烟草研究所 Nicotine liquid raw material of electronic cigarette and preparation device and method of nicotine liquid raw material
CN105661622B (en) * 2016-02-16 2018-03-23 中国农业科学院烟草研究所 A kind of tobacco juice for electronic smoke raw material and its preparation facilities and method
CN105725265A (en) * 2016-04-28 2016-07-06 湖南中烟工业有限责任公司 Device and method for preparing tobacco source basic cigarette flavor material for novel tobacco products
CN107252135A (en) * 2017-06-28 2017-10-17 云南中烟工业有限责任公司 A kind of industrial abstract apparatus and method of tobacco pyrolytic cracking releaser
CN107252135B (en) * 2017-06-28 2018-10-19 云南中烟工业有限责任公司 A kind of industrial abstract apparatus and method of tobacco pyrolytic cracking releaser
CN107699333A (en) * 2017-11-08 2018-02-16 江苏恒森烟草机械有限公司 A kind of high temperature extracts tobacco tar device
CN115161111A (en) * 2022-08-23 2022-10-11 云南中烟工业有限责任公司 Spices dry distillation extraction element

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