CN104041935B - A kind of extracting method of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice - Google Patents
A kind of extracting method of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice Download PDFInfo
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- CN104041935B CN104041935B CN201410249421.8A CN201410249421A CN104041935B CN 104041935 B CN104041935 B CN 104041935B CN 201410249421 A CN201410249421 A CN 201410249421A CN 104041935 B CN104041935 B CN 104041935B
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Abstract
The invention discloses the extracting method of a kind of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice, comprise the following steps: 1) fire-cured tobacco type Nicotiana tabacum L., tobacco shred or the mixture of offal；2) cigarette feed liquid or the high material of sugar content put on Nicotiana tabacum L., tobacco shred or offal；3) temperature section dry distilling Nicotiana tabacum L., tobacco shred or offal are divided；4) collection of fraction.The fraction that this inventive method is collected can use directly as tobacco juice for electronic smoke, also can add essence spice for cigarette or the edible essence spice with special flavor, with abundant tobacco juice for electronic smoke style.This inventive method collect tobacco juice for electronic smoke possess style and features and the taste being similar to Chinese-style cigarette, gratification is good, fragrance coordinate, inhale taste alcohol and.
Description
Technical field
The present invention relates to the extracting method of a kind of electronic cigarette atomizing tobacco juice, particularly to a kind of electronic cigarette Chinese style flue-cured tobacco odor type style
The extracting method of tobacco juice.
Background technology
There is extremely complex chemistry, physical change in Medicated cigarette during burning, cigarette mainstream flue gas composition is extremely complex, cigarette
The compound identified in gas just has kind more than 5000, there is harmful and/or poisonous component in these compounds.
Along with the countries in the world control to Medicated cigarette, tobacco business will face many difficulties.Owing to smoking property of cigarette person has and depends on sucking Medicated cigarette
Lai Xing, mandatory successful quitting rate is the lowest, and therefore novel tobacco goods arise at the historic moment as the transition product of smoking cessation.
Electronic cigarette is the one in novel tobacco goods, and electronic cigarette has another name called virtual medicated cigarette, electronic cigarette, is mainly used in smoking cessation and replaces
For medicated cigarette.It has with particularly for tobacco items as outward appearance, also like medicated cigarette the same can sucking-off cigarette, sucking-off taste with sensation come.It is a kind of logical
Cross electronics heater means and transmit the electronic installation of nicotine to respiratory system.Therefore tobacco juice formula is to affect electronic cigarette taste profile
Deciding factor, is directly connected to the Consumer acceptance of product.Owing to electronic cigarette is to make electronic cigarette liquid mist by electronics heating
Changing, and Medicated cigarette is to produce flue gas by burning tobacco, both are essentially different, but electronic cigarette smoker always wishes electronic cigarette
There is " taste " of medicated cigarette, and without hope there is " evil " of medicated cigarette.
The extraction of existing tobacco juice is usually through CO2Supercritical extraction or by Nicotiana tabacum L. through one or more levels dry distilling process after again
Adding seasoning class material, modulate the tobacco juice of required taste, it is fragrant that Chinese patent CN1742636A discloses a kind of nuisanceless liquid
The production technology of cigarette, tobacco shred processes through dehydrating kettle, the second retort, the 3rd retort etc., and retorting step herein is complicated,
It is difficult to operation, and after 430 DEG C of dry distilling, tobacco shred the most carbonization, after 555 DEG C, tobacco shred seriously carbonization, carbonization
Rear tobacco shred is only as garbage, and tobacco shred is when glowing, and the temperature of combustion cone is at 400～550 DEG C, and in side-stream smoke, part has
The content that the content of evil composition is higher than in main flume.Utilize Maillard reaction to prepare flavouring essence for tobacco etc. be in prior art
Know, but Maillard reaction is combined with dry distilling the electronic cigarette liquid that can directly use of preparation and there is techniques below problem: Mei La
Moral reaction is temperature required relatively low, and the temperature of dry distilling is of a relatively high, if carrying out according to the temperature needed for unified Maillard reaction,
Tobacco juice extracts insufficient, reacts according to the temperature of dry distilling if unified, may produce impurity, even in Maillard reaction
Poisonous material, so not being unified in carrying of electronic cigarette fire-cured tobacco type style tobacco juice by Maillard reaction and dry distilling in prior art
In access method, the extracting method that can use directly as the tobacco juice of electronic cigarette with preparation.
Summary of the invention
It is an object of the invention to provide the extracting method of a kind of electronic cigarette fire-cured tobacco type style tobacco juice, the extracting solution that the method obtains can
With the tobacco juice directly as electronic cigarette, and remain the tobacco flavor that medicated cigarette is dense.
For reaching above-mentioned technical purpose, the present invention is achieved through the following technical solutions:
The extracting method of a kind of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice, comprises the following steps: fire-cured tobacco type Nicotiana tabacum L., tobacco shred or
The material that the mixture of offal, cigarette feed liquid or sugar content are high puts on Nicotiana tabacum L., tobacco shred or offal, point temperature section dry distilling Nicotiana tabacum L., cigarette
Silk or offal, the collection of fraction.
The extracting method of a kind of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice, specifically includes following steps:
1) fire-cured tobacco type Nicotiana tabacum L., tobacco shred or offal 70-100 part, cigarette feed liquid 1-5 part or sugary material 1-30 part load dry distilling
Tank；
2) heating dry distilling tank is to 60-120 DEG C (preferably 80 DEG C), insulation 0.5-2h (preferably 1h)；
3) after, temperature is increased to 180-240 DEG C (preferably 220 DEG C), keeps 0.5-2h (preferably 1h)；
4) fraction is collected after reaction terminates.
Above-mentioned sugary material is one or more the mixture in Mel, dried Fructus Vitis viniferae, Fructus Jujubae, Radix Glycyrrhizae, Fructus Fragariae Ananssae or Caulis Sacchari sinensis.
The solvent of above-mentioned collection fraction is followed successively by ethanol, water, propylene glycol and glycerol.
The fraction of above-mentioned collection both can be individually directly as the tobacco juice of electronic cigarette, it is also possible to make after the fraction mixing collected five kinds
For the tobacco juice of electronic cigarette, the mouthfeel of combination is more rich.
Tobacco juice obtained by said extracted method and the application in electronic cigarette of this tobacco juice.
The invention has the beneficial effects as follows: the fraction collected by the extracting method of the present invention can directly as the tobacco juice of electronic cigarette,
The cigarette tobacco taste of tobacco juice is dense, is suitable for consumer demand.This inventive method collect tobacco juice for electronic smoke possess be similar to Chinese style volume
The style and features of cigarette and taste, gratification is good, fragrance coordinate, inhale taste alcohol and, also can add the flavouring essence for tobacco with special flavor
Spice or edible essence spice, with abundant tobacco juice for electronic smoke style.
Maillard reaction that tobacco juice spice additive is extracted by the present invention and the dry distilling that tobacco juice extracts are unified in the extraction of tobacco juice for electronic smoke
In method, by the effective control to dry distilling condition of the present invention, both avoided tobacco juice carbonization in common dry distilling and be harmful to
The generation of material, makes tobacco juice additive directly mix with tobacco juice simultaneously, simplifies step, reduce cost.
Detailed description of the invention
Embodiment 1
Yunnan Flue-cured Tobacco 20g, Flue-cured tobacco in Fujian 15g, Hunan Flue-cured Tobacco 25g, Henan flue cured tobacco 15g, properties of flue-cured tobacco in Sichuan Province 15g and Shandong are baked
Cigarette 10g adds dry distilling tank；
Add the cigarette feed liquid of 3g；
Rotate dry distilling tank, make the material mix homogeneously of addition dry distilling tank；
Heating dry distilling tank so that it is temperature is maintained at 110 DEG C, constant temperature time 0.5h；
Rise high-temperature, be maintained at 220 DEG C, constant temperature time 0.5h；
After having reacted, collect fraction with ethanol, water, propylene glycol successively.
Embodiment 2
By Yunnan Flue-cured Tobacco 10g, Flue-cured tobacco in Fujian 10g, Hunan Flue-cured Tobacco 20g, Henan flue cured tobacco 5g, properties of flue-cured tobacco in Sichuan Province 15g and Shandong flue-cured tobacco
10g adds dry distilling tank；
Add the Mel of 1g；
Rotate dry distilling tank, make the material mix homogeneously of addition dry distilling tank；
Heating dry distilling tank so that it is temperature is maintained at 80 DEG C, constant temperature time 2h；
Rise high-temperature, keep 180 DEG C, constant temperature time 2h；
Fraction is collected successively with ethanol, water, propylene glycol.
Embodiment 3
Yunnan Flue-cured Tobacco 20g, Flue-cured tobacco in Fujian 15g, Hunan Flue-cured Tobacco 25g, Henan flue cured tobacco 15g, properties of flue-cured tobacco in Sichuan Province 15g and Shandong are baked
Cigarette 10g adds dry distilling tank；
Add the cigarette feed liquid of 1g；
Add 6g dried Fructus Vitis viniferae, 4g Fructus Jujubae；
Rotate dry distilling tank, make the material mix homogeneously of addition dry distilling tank；
Heating dry distilling tank so that it is temperature is maintained between 100 DEG C, constant temperature time 0.5～2h；
Pyrolysis temperature so that it is temperature is maintained between 240 DEG C, constant temperature time 0.5～2h；
Fraction is collected successively with ethanol, water, propylene glycol, glycerol.
Embodiment 4
Weigh Yunnan Flue-cured Tobacco tobacco shred 100g；
Add 10g dried Fructus Vitis viniferae, 15g Fructus Jujubae；
Rotate dry distilling tank, make the material mix homogeneously of addition dry distilling tank；
Heating dry distilling tank so that it is temperature is maintained between 100 DEG C, constant temperature time 1h；
Rise high-temperature, between keeping 240 DEG C, constant temperature time 0.5h；
Fraction is collected successively with ethanol, water, propylene glycol, glycerol.
Embodiment 5
The offal 100g produced during weighing Flue-cured tobacco in Fujian cigarette primary processing adds agitator tank；
Add 15g Caulis Sacchari sinensis, 10g Fructus Fragariae Ananssae；
Rotate dry distilling tank, make the material mix homogeneously of addition dry distilling tank；
Heating dry distilling tank so that it is temperature is maintained at 120 DEG C, constant temperature time 2h；
Rise high-temperature, keep 240 DEG C, constant temperature time 1h；
Fraction is collected successively with ethanol, water, propylene glycol, glycerol.
The detailed description of the invention of the present invention is described although above-mentioned in conjunction with the embodiments, but not to scope
Limiting, one of ordinary skill in the art should be understood that, on the basis of technical scheme, those skilled in the art need not
Pay various amendments or deformation that creative work can make still within protection scope of the present invention.
Claims (7)
1. the electronic cigarette extracting method of Chinese style flue-cured tobacco odor type style tobacco juice, it is characterised in that comprise the following steps:
1) fire-cured tobacco type Nicotiana tabacum L., tobacco shred or offal 70-100 part mixture altogether, cigarette loads dry distilling tank with feed liquid 1-5 part or containing sugar substance 1-30 part；
2) when using containing sugar substance 1-30 part: heating dry distilling tank, to 60-120 DEG C, is incubated 0.5-2h；Maybe when using cigarette with feed liquid 1-5 part: heating dry distilling tank, to 60-80 DEG C, is incubated 0.5-2h；；
3) when using containing sugar substance 1-30 part: afterwards temperature is increased to 180-240 DEG C, it is incubated 0.5-2h；Maybe when using cigarette feed liquid 1-5 part: afterwards temperature is increased to 180-220 DEG C, it is incubated 0.5-2h；
4) fraction is collected after reaction terminates；
Described sugary material is one or more the mixture in Mel, dried Fructus Vitis viniferae, Fructus Jujubae, Radix Glycyrrhizae, Fructus Fragariae Ananssae or Caulis Sacchari sinensis.
2. extracting method as claimed in claim 1, it is characterised in that described step 4) is collected the solvent of fraction and is followed successively by ethanol, water, propylene glycol and glycerol.
3. the extracting method as described in claim 1, it is characterised in that described step 2) in heating dry distilling tank to 80 DEG C.
4. the extracting method as described in claim 1, it is characterised in that in described step 3), temperature is increased to 220 DEG C.
5. extracting method as claimed in claim 1, it is characterised in that described step 2), 3) in insulation 1h.
6. the tobacco juice that the extracting method as described in claim 1-5 is arbitrary obtains.
7. tobacco juice application in electronic cigarette as claimed in claim 6.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410249421.8A CN104041935B (en) | 2014-06-06 | 2014-06-06 | A kind of extracting method of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice |
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| CN201410249421.8A CN104041935B (en) | 2014-06-06 | 2014-06-06 | A kind of extracting method of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice |
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| CN104041935A CN104041935A (en) | 2014-09-17 |
| CN104041935B true CN104041935B (en) | 2016-08-24 |
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| CN104432489B (en) * | 2014-10-22 | 2016-03-30 | 浙江中烟工业有限责任公司 | A kind ofly utilize the tobacco juice for electronic smoke solvent of polyglycerol and the tobacco juice for electronic smoke of preparation thereof and electronic cigarette |
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| CN104585860B (en) * | 2015-01-15 | 2016-11-30 | 中国烟草总公司郑州烟草研究院 | There is the preparation method of the tobacco juice for electronic smoke of the fragrant feature of baking |
| CN104687240B (en) * | 2015-01-20 | 2016-11-30 | 川渝中烟工业有限责任公司 | There is electronic cigarette liquid of Ambra Grisea fragrance and preparation method thereof |
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| CN104783323B (en) * | 2015-05-14 | 2016-08-17 | 安徽中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke containing Dry distillated flavor |
| CN105011355B (en) * | 2015-06-05 | 2016-07-06 | 浙江中烟工业有限责任公司 | A kind of essential oil of tobaccos and extracting method thereof and application |
| CN106418660B (en) * | 2015-08-13 | 2020-03-24 | 上海烟草集团有限责任公司 | Preparation method and application of electronic cigarette liquid |
| CN105167170A (en) * | 2015-09-14 | 2015-12-23 | 浙江中烟工业有限责任公司 | Method for preparing electronic cigarette nicotine liquid by means of tobacco subjected to dry distillation pyrolysis |
| CN105725266A (en) * | 2016-04-28 | 2016-07-06 | 湖南中烟工业有限责任公司 | Preparation method of basic cigarette-smell raw material deriving from tobacco |
| CN105852200A (en) * | 2016-04-28 | 2016-08-17 | 湖南中烟工业有限责任公司 | Preparation method of tobacco-sourced basic cigarette-smell raw material |
| CN105852199A (en) * | 2016-04-28 | 2016-08-17 | 湖南中烟工业有限责任公司 | Preparation method of tobacco-sourced basic cigarette-smell raw material |
| CN105725265A (en) * | 2016-04-28 | 2016-07-06 | 湖南中烟工业有限责任公司 | Device and method for preparing tobacco source basic cigarette flavor material for novel tobacco products |
| CN105686070A (en) * | 2016-04-28 | 2016-06-22 | 湖南中烟工业有限责任公司 | Preparation method for tobacco source raw material with basic cigarette smell |
| CN106307602A (en) * | 2016-09-12 | 2017-01-11 | 三峡大学 | Electronic cigarette liquid for freshening breath |
| CN109393568B (en) * | 2018-11-09 | 2021-02-02 | 湖北中烟工业有限责任公司 | Burley tobacco extract for heating non-combustible cigarettes and preparation method thereof |
| CN113142643A (en) * | 2021-02-08 | 2021-07-23 | 广东中烟工业有限责任公司 | Cigarette essence for heating non-combustible cigarettes and preparation method and application thereof |
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