CN108783562A - A kind of pipe tobacco preparation method suitable for new cigarette - Google Patents
A kind of pipe tobacco preparation method suitable for new cigarette Download PDFInfo
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- CN108783562A CN108783562A CN201810708972.4A CN201810708972A CN108783562A CN 108783562 A CN108783562 A CN 108783562A CN 201810708972 A CN201810708972 A CN 201810708972A CN 108783562 A CN108783562 A CN 108783562A
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- tobacco
- pipe tobacco
- fiber
- method suitable
- new cigarette
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- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 156
- 241000208125 Nicotiana Species 0.000 title claims abstract description 149
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 239000000835 fiber Substances 0.000 claims abstract description 67
- 239000000284 extract Substances 0.000 claims abstract description 21
- 238000000605 extraction Methods 0.000 claims abstract description 17
- 238000001035 drying Methods 0.000 claims abstract description 16
- 239000002904 solvent Substances 0.000 claims abstract description 14
- 239000002131 composite material Substances 0.000 claims abstract description 13
- 241000196324 Embryophyta Species 0.000 claims abstract description 10
- 239000012454 non-polar solvent Substances 0.000 claims abstract description 8
- 239000000853 adhesive Substances 0.000 claims abstract description 6
- 230000001070 adhesive effect Effects 0.000 claims abstract description 6
- 238000011084 recovery Methods 0.000 claims abstract description 4
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 82
- 238000000034 method Methods 0.000 claims description 26
- 239000007788 liquid Substances 0.000 claims description 23
- 239000000686 essence Substances 0.000 claims description 22
- 239000000376 reactant Substances 0.000 claims description 21
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 238000010494 dissociation reaction Methods 0.000 claims description 11
- 230000005593 dissociations Effects 0.000 claims description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000002304 perfume Substances 0.000 claims description 10
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- 229920001282 polysaccharide Polymers 0.000 claims description 9
- 239000005017 polysaccharide Substances 0.000 claims description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 8
- 244000061176 Nicotiana tabacum Species 0.000 claims description 8
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 8
- 235000000346 sugar Nutrition 0.000 claims description 8
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical group COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims description 6
- 235000019441 ethanol Nutrition 0.000 claims description 6
- 229920000881 Modified starch Polymers 0.000 claims description 5
- 150000004676 glycans Chemical class 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 5
- 235000012907 honey Nutrition 0.000 claims description 5
- 235000019426 modified starch Nutrition 0.000 claims description 5
- 238000004806 packaging method and process Methods 0.000 claims description 5
- 150000005846 sugar alcohols Polymers 0.000 claims description 5
- 244000144730 Amygdalus persica Species 0.000 claims description 4
- 229920000742 Cotton Polymers 0.000 claims description 4
- 244000241257 Cucumis melo Species 0.000 claims description 4
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims description 4
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 claims description 4
- 235000016623 Fragaria vesca Nutrition 0.000 claims description 4
- 240000009088 Fragaria x ananassa Species 0.000 claims description 4
- 235000011363 Fragaria x ananassa Nutrition 0.000 claims description 4
- 240000006240 Linum usitatissimum Species 0.000 claims description 4
- 235000004431 Linum usitatissimum Nutrition 0.000 claims description 4
- YKVWPZJHENXDAJ-VOTSOKGWSA-N Megastigmatrienone Chemical compound CC1=CC(=O)CC(C)(C)C1\C=C\C=C YKVWPZJHENXDAJ-VOTSOKGWSA-N 0.000 claims description 4
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 4
- 244000061458 Solanum melongena Species 0.000 claims description 4
- 235000002597 Solanum melongena Nutrition 0.000 claims description 4
- 244000299461 Theobroma cacao Species 0.000 claims description 4
- 235000009470 Theobroma cacao Nutrition 0.000 claims description 4
- 244000290333 Vanilla fragrans Species 0.000 claims description 4
- 235000009499 Vanilla fragrans Nutrition 0.000 claims description 4
- 235000012036 Vanilla tahitensis Nutrition 0.000 claims description 4
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims description 4
- 229920006221 acetate fiber Polymers 0.000 claims description 4
- RHDGNLCLDBVESU-UHFFFAOYSA-N but-3-en-4-olide Chemical compound O=C1CC=CO1 RHDGNLCLDBVESU-UHFFFAOYSA-N 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 229940093503 ethyl maltol Drugs 0.000 claims description 4
- 235000011187 glycerol Nutrition 0.000 claims description 4
- 238000003475 lamination Methods 0.000 claims description 4
- 229920001277 pectin Polymers 0.000 claims description 4
- 239000001814 pectin Substances 0.000 claims description 4
- 235000010987 pectin Nutrition 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- 230000001360 synchronised effect Effects 0.000 claims description 4
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical group COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 claims description 4
- 239000004368 Modified starch Substances 0.000 claims description 3
- 229920001131 Pulp (paper) Polymers 0.000 claims description 3
- 229920002678 cellulose Polymers 0.000 claims description 3
- 239000001913 cellulose Substances 0.000 claims description 3
- 150000002576 ketones Chemical class 0.000 claims description 3
- 238000010030 laminating Methods 0.000 claims description 3
- 239000003208 petroleum Substances 0.000 claims description 2
- 238000001291 vacuum drying Methods 0.000 claims description 2
- 238000009777 vacuum freeze-drying Methods 0.000 claims description 2
- 244000269722 Thea sinensis Species 0.000 claims 1
- 235000009508 confectionery Nutrition 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 6
- 239000002994 raw material Substances 0.000 abstract description 3
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- 239000007921 spray Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 description 9
- 150000008163 sugars Chemical class 0.000 description 4
- 235000019505 tobacco product Nutrition 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 238000004108 freeze drying Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000006200 vaporizer Substances 0.000 description 2
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 description 1
- 241001474374 Blennius Species 0.000 description 1
- 244000303965 Cyamopsis psoralioides Species 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical compound ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- AJAZMOFONMJGNP-WMZOPIPTSA-N n-[(2s)-4-methyl-1-oxo-1-[[(2s)-3-oxo-4-(pyridin-2-ylsulfonylamino)butan-2-yl]amino]pentan-2-yl]-1-benzofuran-2-carboxamide Chemical group O=C([C@H](C)NC(=O)[C@@H](NC(=O)C=1OC2=CC=CC=C2C=1)CC(C)C)CNS(=O)(=O)C1=CC=CC=N1 AJAZMOFONMJGNP-WMZOPIPTSA-N 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
- 239000011122 softwood Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/04—Humidifying or drying tobacco bunches or cut tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
A kind of pipe tobacco preparation method suitable for new cigarette is the tobacco extract that tobacco leaf is extracted to using nonpolar solvent, concentrated distillation and solvent recovery formation concentration.The direct low temperature drying of tobacco leaf after extraction is simultaneously milled to offal, and offal detaches to form tobacco stalk fibre.Tobacco leaf powder, tobacco stalk fibre and plant fiber are mixed to form composite fibre silk jointly, by the way of layer stack, fibrous raw material is successively laid on web forming, and tobacco extraction concentrat is mixed a certain amount of adhesive and as the stacking of fiber synchronizes spray and is added, so that fibres bond is dried at smoked sheet and using microwave mode, by dried smoked sheet chopping.The present invention can selectively carry out the enrichment and application of fragrance component according to the odor characteristic of tobacco leaf, effectively improve the interior quality of pipe tobacco, solve the drawbacks of traditional pipe tobacco can not carry out interior quality adjustment.
Description
Technical field
The present invention relates to tobacco preparation method technical fields, and in particular to is mainly used for heating the cigarette that the cigarette that do not burn uses
Silk preparation method.
Background technology
Burning tobacco is carried out to tobacco-containing material with a relatively low temperature (generally below 350 degrees Celsius) for heating
Baking, makes toasted tobacco-containing material give out tobacco aroma in the case that incombustible, to meet the sense organ need of tobacco suction
It asks, simultaneously as heating temperature is relatively low, not will produce numerous harmful substances that regular-size cigarette is formed by burning, also effectively subtract
The harmfulness of low tobacco suction.It is the cigarette prepared based on roll-in method to be currently used in the tobacco-containing material that low temperature does not burn in cigarette
Careless thin slice, the form and quality of material cannot all fully meet the quality requirements of low temperature tobacco, it is also necessary to it is further improved, and
Since roll-in method thin slice is easy to absorb moisture in low temperature tobacco processing course, stability and processing to the processing of low temperature tobacco are just
Profit all there is a problem of larger.
Invention content
The purpose of the present invention is the practical application requests based on new cigarette, provide a kind of pipe tobacco suitable for new cigarette
Preparation method.
The technical solution adopted by the present invention is as follows：
A kind of pipe tobacco preparation method suitable for new cigarette, method and step are as follows：
(1) tobacco extract is prepared：Tobacco leaf is extracted with nonpolar solvent, the mass ratio of tobacco leaf and nonpolar solvent
It is 1:5-1:25, extraction temperature is 30-50 DEG C, extraction time 1-5 hours, is separated by solid-liquid separation after the completion of extraction, by liquid in 40-80
DEG C, carry out solvent recovery under the conditions of the concentrations of 0.02-0.06MPa vacuum degrees and concentrated after tobacco extract；
(2) baccy fiber is prepared：After the tobacco leaf low temperature drying that step (1) is isolated ball mill grinding at 80-150 mesh cigarette
End；In addition offal is taken, mill be used in combination that offal is carried out fiber dissociation, the tobacco stalk fibre after dissociation is dried at 80-120 DEG C again
It is dry；
(3) pipe tobacco is prepared：According to mass ratio, 1-10 part tobacco stalk fibre silks and 1-10 parts of offals prepared by step (2) into
Row mixing, and tobacco stalk fibre silk and the common mixing of plant fiber of offal gross mass 5-20% is added, obtain composite fibre silk；It takes
30-50 parts of tobacco extracts, 20-50 parts of adhesives, 5-15 parts of polyalcohols, feed liquid is formed after being mixed evenly at normal temperatures；
Composite fibre silk is stacked on using the method for layer stack on forming net, and synchronous addition feed liquid, makes fiberizing, contained
The wet smoked sheet of water rate 20-30%；Wet smoked sheet is sent into microwave dryer drying under the conditions of 60-100 DEG C, obtains moisture content 13-
15% smoked sheet；Smoked sheet is cut into the width of 0.8-1.0mm, then is dried to moisture content 9-11%, obtains pipe tobacco.
The present invention mixes 1-5 parts of natural essences, 1-10 parts of reduced sugars, 1-10 parts of natural perfume material reactants, by mixture
It is added in pipe tobacco according to the ratio of tobacco quality 1-5%, improves the quality of pipe tobacco and abundant cigarette perfume.The cigarette that will be prepared again
Silk was put into container balance after 2 hours, carried out vacuumizing packaging.
Nonpolar solvent described in the method for the present invention is in ethyl alcohol, petroleum ether, dimethyl ether, No. 6 solvents, dichloromethane
It is one or more of.The tobacco leaf low temperature drying method is vacuum drying or freeze-drying.Prepare adhesive used by feed liquid
For one or more of starch-polysaccharides, modified starch, fibrous polysaccharaide, algal polysaccharides, pectin.Used polyalcohol is sorb
One or more of alcohol, propylene glycol, glycerine, diethylene glycol (DEG), plant polyose.The plant fiber be flax fiber, cotton fiber,
One or more of acetate fiber, wood pulp cellulose, Herbaceous Fiber.The layer stack method of the composite fibre silk is folded for electrostatic
One kind in layer, vacuum lamination, natural laminating method.The natural essence be vanillic aldehyde, ethylmaltol, Megastigmatrienone,
One or more of eggplant Buddhist nun ketone, furanone, furfural, strawberry essence, honey peach essence, melon essence, plum essence, it is described natural
Fragrance reactant is in cocoa reactant, flue-cured tobacco maillard reaction thing, burley tobaccos reactant, Radix Glycyrrhizae reactant, vanilla reactant
One or more.
Beneficial effects of the present invention are as follows：
1. preparation method of the present invention is the new method dramatically different with the preparation method of traditional pipe tobacco, tradition can be effectively solved
Pipe tobacco can not carry out the drawbacks of interior quality adjustment, and the enrichment of fragrance component can be selectively carried out according to the odor characteristic of tobacco leaf
And application, effectively improve the interior quality of pipe tobacco.
2. the present invention, which is formed by pipe tobacco product, can improve that the heating cigarette flavor that do not burn at present is single, and taste is inhaled not in inherence
Ideal state re-starts moulding for flavouring essence quality, substantially increases the use value of pipe tobacco product.
3. using microwave heating and subsequent flavoring humectation treatment process, being conducive to the quality for improving tobacco aroma and enriching
Property, provide quality higher, fragrance more rich raw material for cigarette and the heating tobacco product that do not burn.
4. pipe tobacco prepared by the method for the present invention is applied widely, especially suitable for heating the cigarette that do not burn, it is also used as
A kind of tobacco raw material of unique style make an addition to it is existing traditional burn and suck in formula cigarette shreds, play and effectively promote cigarette filling
Value reduces harmful components, improves the effect of flavor quality of cigarette.Meanwhile being prepared using the method for the present invention in traditional cigarette
Pipe tobacco, since it is directly at silk, moreover it is possible to which the additive amount for effectively reducing common pipe tobacco, reaching reduces tobacco leaf consumption, improves production effect
The purpose of energy.
Specific implementation mode
Embodiment 1
A kind of pipe tobacco preparation method suitable for new cigarette, method and step are as follows：
(1) tobacco extract is prepared：By tobacco leaf (flue-cured tobacco, burley tobaccos, drying cigarette, in Turkish tobaccos any one or it is several
Kind) extracted with dimethyl ether and No. 6 solvents, the mass ratio of tobacco leaf and nonpolar solvent is 1:5, extraction temperature is 40 DEG C, leaching
It carries the time 5 hours, is separated by solid-liquid separation after the completion of extraction, liquid is subjected to solvent under the conditions of 80 DEG C, the concentrations of 0.02MPa vacuum degrees
Tobacco extract after recycling and being concentrated；
(2) baccy fiber is prepared：The tobacco leaf that step (1) is isolated after 10 DEG C of low temperature dryings ball mill grinding at 150 mesh
Offal；In addition take offal, mill be used in combination that offal is carried out fiber dissociation, tobacco stalk fibre after dissociation again at 80-120 DEG C into
Row drying；
(3) pipe tobacco is prepared：According to mass ratio, 1-10 part tobacco stalk fibre silks and 1-10 parts of offals prepared by step (2) into
Row mixing, the present embodiment is to mix 1 part of tobacco stalk fibre silk with 10 parts of offals, and tobacco stalk fibre silk and the total matter of offal is added
The cotton fiber and acetate fiber of amount 20%, common mixing obtain composite fibre silk；Take 50 parts of tobacco extracts, 10 parts of starch more
Sugar, 10 portions of modified starches, 20 parts of algal polysaccharides, 10 parts of pectin, 5 parts of sorbierites, 5 portions of diethylene glycol (DEG)s are mixed equal at normal temperatures
Feed liquid is formed after even；Composite fibre silk is stacked on using the method for the laminated electrostatic of the prior art on forming net, and synchronizes and adds
Feed liquid, makes fiberizing, obtains the wet smoked sheet of moisture content 30%；It is dry under the conditions of 70 DEG C that wet smoked sheet is sent into microwave dryer
It is dry, keep tobacco aroma stronger using microwave heating, enhance the satisfaction of fragrance, obtains the smoked sheet of moisture content 15%；
Smoked sheet is cut into the width of 0.8-1.0mm, then is dried to moisture content 9%, obtains pipe tobacco；
(4) 1 part of vanillic aldehyde, 1 part of Megastigmatrienone, 3 parts of plum essence, 10 parts of reduced sugars, 3 parts of cocoa reactants are mixed
It closes, mixture is added to according to the ratio of tobacco quality 5% in pipe tobacco, the quality of pipe tobacco and abundant cigarette perfume are improved.
(5) it after the pipe tobacco being prepared being put into container balance 2 hours, carries out vacuumizing packaging.
Embodiment 2
A kind of pipe tobacco preparation method suitable for new cigarette, method and step are as follows：
(1) tobacco extract is prepared：Drying cigarette tobacco leaf is extracted with ethyl alcohol, the mass ratio of tobacco leaf and ethyl alcohol is 1:
15, extraction temperature is 45 DEG C, extraction time 4 hours, is separated by solid-liquid separation after the completion of extraction, by liquid in 60 DEG C, 0.05MPa vacuum degrees
Concentration under the conditions of carry out solvent recovery and the tobacco extract after being concentrated；
(2) baccy fiber is prepared：After the tobacco leaf freeze-drying that step (1) is isolated ball mill grinding at 100 mesh offal；
In addition offal is taken, mill be used in combination that offal is carried out fiber dissociation, the tobacco stalk fibre after dissociation is dried at 80-120 DEG C again；
(3) pipe tobacco is prepared：According to mass ratio, 1 part of tobacco stalk fibre silk prepared by step (2) is mixed with 6 parts of offals,
And the Herbaceous Fiber of tobacco stalk fibre silk and offal gross mass 16% is added, common mixing obtains composite fibre silk；Take 40 portions of tobaccos
Extract, 25 parts of algal polysaccharides, 2 parts of sorbierites, 5 parts of plant polyoses, feed liquid is formed after being mixed evenly at normal temperatures；It will mix
Condensating fiber silk is stacked on using vacuum lamination method on forming net, and synchronous addition feed liquid, is made fiberizing, is obtained moisture content
28% wet smoked sheet；Wet smoked sheet is sent into microwave dryer drying under the conditions of 80 DEG C, keeps tobacco fragrant using microwave heating
Gas is stronger, enhances the satisfaction of fragrance, obtains the smoked sheet of moisture content 14%；Smoked sheet is cut into the width of 0.8-1.0mm,
It is dried to moisture content 10% again, obtains pipe tobacco；
(4) by 1 part of ethylmaltol, 1 part of furfural, 1 part of eggplant Buddhist nun ketone, 1 part of strawberry essence or melon essence, 6 parts of reduction
Sugar, 5 parts of burley tobaccos reactant mixing, mixture is added to according to the ratio of tobacco quality 5% in pipe tobacco, the product of pipe tobacco are improved
Matter and abundant cigarette perfume.
(5) it after the pipe tobacco being prepared being put into container balance 2 hours, carries out vacuumizing packaging.
Embodiment 3
A kind of pipe tobacco preparation method suitable for new cigarette, method and step are as follows：
(1) tobacco extract is prepared：It takes Domestic Flue-cured Tobacco C3F in 1 part to be put into extraction vessel, 15 parts of stones is then added
Oily ether or 95% alcohol solvent, after 30 DEG C of extractions in confined conditions 2 hours, using 60 DEG C, the cryogenic vaporizer of 0.04mpa
The concentration for carrying out the collection and extracting solution of solvent, after removing solvent to be evaporated, the tobacco extract after being concentrated；
(2) baccy fiber is prepared：Ball mill grinding after the tobacco leaf that step (1) is isolated is dried in vacuo in a low temperature of 30 DEG C
At the offal of 100 mesh；In addition 1 part of flue-cured tobacco stalk is taken, mill be used in combination that offal is carried out fiber dissociation, fibre stuff is formed, after dissociation
Tobacco stalk fibre at 80-120 DEG C using drying dehydration process dry, obtain tobacco stalk fibre silk；
(3) pipe tobacco is prepared：
A. according to mass ratio, 1 part of tobacco stalk fibre silk prepared by step (2) is mixed with 1 part of offal, and offal is added
Filament and the common mixing of the flax fiber of offal gross mass 10%, obtain composite fibre silk；
B. by weight, take 45 parts of tobacco extracts, 20 portions of modified starches, 10 parts of guar gums, 5 parts of propylene glycol, 10 part third
Triol is sufficiently mixed is mixing uniformly to form feed liquid at normal temperatures；
C. by composite fibre silk using the vacuum lamination method of the prior art by fiber stack on forming net, and synchronize and add
Feed liquid, makes fiberizing, obtains the wet smoked sheet of moisture content 25%；
D. wet smoked sheet is sent into microwave dryer drying under the conditions of 60-70 DEG C by conveyer belt, obtains moisture content
14.5% smoked sheet；
E., smoked sheet is cut into the width of 0.8-1.0mm, then is dried to moisture content 10%, obtains pipe tobacco；
(4) 1 part of honey peach essence, 5 parts of reduced sugars, 10 parts of flue-cured tobacco maillard reaction things are mixed, by mixture according to pipe tobacco
The ratio of quality 1% is added in pipe tobacco, with the quality for further increasing pipe tobacco and abundant cigarette perfume.
(5) it after the pipe tobacco being prepared being put into container balance 2 hours, is packed by the way of vacuumizing.
Embodiment 4
A kind of pipe tobacco preparation method suitable for new cigarette, method and step are as follows：
(1) tobacco extract is prepared：Take Domestic Flue-cured Tobacco C3F in 3 parts, 1 part of U.S.'s production burley tobaccos tobacco leaf, 1 part of native ear
Its atomatic tobacco produced is put into extraction vessel, then presses solid-to-liquid ratio 1：25 add methylene chloride solvent, 50 DEG C in confined conditions
After extraction 1 hour, the concentration of the collection and extracting solution of solvent is carried out using the cryogenic vaporizer of 40 DEG C, 0.06mpa, it is to be evaporated to remove
After removing solvent, the tobacco extract that is concentrated；
(2) baccy fiber is prepared：The tobacco leaf that step (1) is isolated is dried and is volatilized molten using freeze-drying mode
After agent, the offal of 80 mesh is milled into ball mill；In addition 3 parts of flue-cured tobacco stalks, 2 parts of Burley Stems are taken, mill is used in combination to carry out offal
Fiber dissociates, and technique drying is dried and dehydrated in the tobacco stalk fibre after dissociation at 80-120 DEG C again, obtains tobacco stalk fibre silk.
(3) pipe tobacco is prepared：
A. according to mass ratio, 3 parts of tobacco stalk fibre silks prepared by step (2) are mixed with 1 part of offal, and offal is added
The common mixing of softwood pulp fiber of filament and offal gross mass 5%, obtains composite fibre silk；
B. by weight, take 30 parts of tobacco extracts, 10 parts of starch-polysaccharides, 5 parts of algal polysaccharides, 5 parts of fibrous polysaccharaides, 3 parts
Glycerine, 2 parts of honey, are sufficiently mixed are mixing uniformly to form feed liquid at normal temperatures；
C. it utilizes nature laminating method by fiber stack on forming net composite fibre silk, and synchronous addition feed liquid, makes
Fiberizing obtains the wet smoked sheet of moisture content 20%；
D. wet smoked sheet is sent into microwave dryer drying under the conditions of 80-100 DEG C by conveyer belt, obtains moisture content 13%
Smoked sheet；
E., smoked sheet is cut into the width of 0.8-1.0mm with filament cutter, then is dried to moisture content 11%, obtains pipe tobacco；
(4) by 1 part of furanone, 2 parts of reduced sugars, 1 part of vanilla reactant or Radix Glycyrrhizae reactant mix, by mixture according to
The ratio of tobacco quality 2% is added in pipe tobacco, further increases the quality of pipe tobacco and abundant cigarette perfume.
(5) it after the pipe tobacco after flavoring being put into container balance 2 hours, carries out vacuumizing packaging.
(starch-polysaccharides, modified starch, fibrous polysaccharaide, seaweed are more for tobacco extract used in the method for the present invention, adhesive
Sugar, pectin), polyalcohol (sorbierite, propylene glycol, glycerine, diethylene glycol (DEG), plant polyose), (flax fiber, cotton are fine for plant fiber
Dimension, acetate fiber, wood pulp cellulose, Herbaceous Fiber), natural essence (vanillic aldehyde, ethylmaltol, Megastigmatrienone, eggplant Buddhist nun ketone,
Furanone, furfural, strawberry essence, honey peach essence, melon essence, plum essence), natural perfume material reactant it is (cocoa reactant, roasting
Cigarette maillard reaction thing, burley tobaccos reactant, Radix Glycyrrhizae reactant, vanilla reactant) etc. it is commercially available, also voluntarily can extract or match
System.
Claims (10)
1. a kind of pipe tobacco preparation method suitable for new cigarette, which is characterized in that method and step is as follows：
(1) tobacco extract is prepared：Tobacco leaf is extracted with nonpolar solvent, the mass ratio of tobacco leaf and nonpolar solvent is 1:
5-1:25, extraction temperature be 30-50 DEG C, extraction time 1-5 hour, extraction after the completion of separation of solid and liquid, by liquid 40-80 DEG C,
Tobacco extract after carrying out solvent recovery under the conditions of the concentration of 0.02-0.06MPa vacuum degrees and being concentrated；
(2) baccy fiber is prepared：After the tobacco leaf low temperature drying that step (1) is isolated ball mill grinding at 80-150 mesh offal；
In addition offal is taken, mill be used in combination that offal is carried out fiber dissociation, the tobacco stalk fibre after dissociation is dried at 80-120 DEG C again；
(3) pipe tobacco is prepared：According to mass ratio, 1-10 part tobacco stalk fibre silks prepared by step (2) are mixed with 1-10 parts of offals
It closes, and tobacco stalk fibre silk and the common mixing of plant fiber of offal gross mass 5-20% is added, obtain composite fibre silk；Take 30-
50 parts of tobacco extracts, 20-50 parts of adhesives, 5-15 parts of polyalcohols, feed liquid is formed after being mixed evenly at normal temperatures；It will mix
Condensating fiber silk is stacked on using the method for layer stack on forming net, and synchronous addition feed liquid, is made fiberizing, is obtained moisture content
The wet smoked sheet of 20-30%；Wet smoked sheet is sent into microwave dryer drying under the conditions of 60-100 DEG C, obtains moisture content 13-15%
Smoked sheet；Smoked sheet is cut into the width of 0.8-1.0mm, then is dried to moisture content 9-11%, obtains pipe tobacco.
2. a kind of pipe tobacco preparation method suitable for new cigarette according to claim 1, which is characterized in that by 1-5 parts
Natural essence, 1-10 part reduced sugar, 1-10 parts of natural perfume material reactant mixing, by mixture according to the ratio of tobacco quality 1-5%
Example is added in pipe tobacco, improves the quality of pipe tobacco and abundant cigarette perfume.
3. a kind of pipe tobacco preparation method suitable for new cigarette according to claim 1 or 2, which is characterized in that will make
Standby obtained pipe tobacco was put into container balance after 2 hours, carried out vacuumizing packaging.
4. a kind of pipe tobacco preparation method suitable for new cigarette according to claim 1 or 2, which is characterized in that described
Nonpolar solvent is one or more of ethyl alcohol, petroleum ether, dimethyl ether, No. 6 solvents, dichloromethane.
5. a kind of pipe tobacco preparation method suitable for new cigarette according to claim 1 or 2, which is characterized in that described
Tobacco leaf low temperature drying method be vacuum drying or freeze-drying.
6. a kind of pipe tobacco preparation method suitable for new cigarette according to claim 1 or 2, which is characterized in that prepare
Adhesive used by feed liquid is one or more of starch-polysaccharides, modified starch, fibrous polysaccharaide, algal polysaccharides, pectin.
7. a kind of pipe tobacco preparation method suitable for new cigarette according to claim 1 or 2, which is characterized in that adopted
Polyalcohol is one or more of sorbierite, propylene glycol, glycerine, diethylene glycol (DEG), plant polyose.
8. a kind of pipe tobacco preparation method suitable for new cigarette according to claim 1 or 2, which is characterized in that described
Plant fiber is one or more of flax fiber, cotton fiber, acetate fiber, wood pulp cellulose, Herbaceous Fiber.
9. a kind of pipe tobacco preparation method suitable for new cigarette according to claim 1 or 2, which is characterized in that described
The layer stack method of composite fibre silk is one kind in laminated electrostatic, vacuum lamination, natural laminating method.
10. a kind of pipe tobacco preparation method suitable for new cigarette according to claim 2, which is characterized in that the day
Right essence is vanillic aldehyde, ethylmaltol, Megastigmatrienone, eggplant Buddhist nun ketone, furanone, furfural, strawberry essence, honey peach essence, sweet tea
One or more of melon essence, plum essence, the natural perfume material reactant are cocoa reactant, flue-cured tobacco Maillard reaction
One or more of object, burley tobaccos reactant, Radix Glycyrrhizae reactant, vanilla reactant.
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| CN201810708972.4A CN108783562B (en) | 2018-07-02 | 2018-07-02 | Preparation method of tobacco shreds suitable for novel cigarettes |
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| CN109793255A (en) * | 2019-01-25 | 2019-05-24 | 安徽中烟工业有限责任公司 | A kind of pipe tobacco and preparation method thereof that cool taste is soft |
| CN110279137A (en) * | 2019-06-27 | 2019-09-27 | 云南瑞升烟草技术（集团）有限公司 | A kind of compound reconstruction stem |
| CN110432533A (en) * | 2019-08-22 | 2019-11-12 | 河南中烟工业有限责任公司 | A kind of heating using micro-wave drying method preparation is not burnt tobacco slice |
| CN110693061A (en) * | 2019-11-20 | 2020-01-17 | 湖北中烟工业有限责任公司 | Treatment feed liquid and treatment method for yellow sun-cured tobacco |
| CN111184248A (en) * | 2020-03-19 | 2020-05-22 | 中国烟草总公司郑州烟草研究院 | Preparation and application of additive capable of improving sensory quality of cut stems |
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| CN110693061A (en) * | 2019-11-20 | 2020-01-17 | 湖北中烟工业有限责任公司 | Treatment feed liquid and treatment method for yellow sun-cured tobacco |
| CN111184248A (en) * | 2020-03-19 | 2020-05-22 | 中国烟草总公司郑州烟草研究院 | Preparation and application of additive capable of improving sensory quality of cut stems |
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