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CN103263073A - Method for reproducing tobacco leaves by paper-making method through bamboo pulp fibers instead of wood pulp fibers - Google Patents

Method for reproducing tobacco leaves by paper-making method through bamboo pulp fibers instead of wood pulp fibers Download PDF

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CN103263073A
CN103263073A CN 201310244008 CN201310244008A CN103263073A CN 103263073 A CN103263073 A CN 103263073A CN 201310244008 CN201310244008 CN 201310244008 CN 201310244008 A CN201310244008 A CN 201310244008A CN 103263073 A CN103263073 A CN 103263073A
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pulp
tobacco
method
step
bamboo
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CN 201310244008
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Chinese (zh)
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向海英
刘晶
王保兴
张娜
王建
简彬
孔宁川
王浩雅
马迅
殷艳飞
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云南烟草科学研究院
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Abstract

The invention relates to a method for reproducing tobacco leaves by a paper-making method through bamboo pulp fibers instead of wood pulp fibers and belongs to the field of tobacco leaf reproduction. The method comprises a step a of preparing the bamboo pulp fibers, a step b of preparing a coating solution, a step c of manufacturing paper with pulp on a film base and a step d of preparing the reproduced tobacco leaves by the paper-making method, and particularly comprises the following steps of: boiling aired large dendrocalamus giganteus to prepare bamboo slurry, and carrying out deoxidization treatment to obtain deoxidized bamboo pulp; uniformly mixing 40% of a tobacco stem extract, 55% of fragment/tobacco powder mixed extract and 5% of flavors and fragrances in mass percentage to obtain the coating solution; mixing 45% by mass of tobacco stem residual dreg initially-milled pulp with the beating degree of 8-degree SR and 45% by mass of fragment and tobacco powder mixed residual dregs to obtain the film base; adding 10% by mass of deoxidized bamboo pulp fibers, and mixing uniformly and grinding; preparing the film base after the beating degree is 35-48-degree SR; carrying out conventional coating on the film base prepared by the step c by utilizing the coating solution prepared by the step b, and drying; controlling the water content of a finished product to 10-12%; and slicing for future use. The method disclosed by the invention has the advantages of simple and feasible method and stable quality of the reproduced tobacco leaves.

Description

一种用竹浆纤维代替木浆纤维的造纸法再造烟叶的方法 A method of reconstituted tobacco paper-making pulp fiber bamboo fiber was replaced with

技术领域: FIELD:

[0001] 本发明涉及一种用竹浆纤维代替木浆纤维的造纸法再造烟叶的方法,属于再造烟叶领域。 [0001] The present invention relates to a method of reconstituted tobacco paper-making with an alternative to wood pulp fibers bamboo fiber, belonging to the field of reconstituted tobacco.

背景技术: Background technique:

[0002] 作为卷烟重要的组成部分,造纸法再造烟叶在卷烟中扮演着重要的角色,既能起到降焦减害的作用,又能提高卷烟的经济效益。 [0002] As an important part of the cigarette, paper and reconstituted tobacco in cigarettes play an important role, both play a role in reducing tar harm reduction, but also improve the economic benefits of cigarettes.

[0003] 造纸法再造烟叶是由烟梗、烟叶碎片和烟末加水进行萃取,固液分离,所得的残渣进行磨浆,并加入一定的外加纤维进行抄片制成片基,液体进行浓缩并加料加香后,涂布于片基上而制成。 Reconstituted tobacco [0003] paper making process is extraction, solid-liquid separation, from the resulting residue stems, tobacco scrap and tobacco dust by adding water for refining, and adding some additional handsheet fibers formed into a sheet-yl, and the liquid was concentrated after the addition perfuming, coated on a base sheet made. 在再造烟叶生产中,外加纤维的作用是增加片基的物理强度,且便于后续加工。 In the production of reconstituted tobacco, the applied effect is to increase the physical strength of the fiber sheet of the group, and to facilitate subsequent processing. 目前,国内企业绝大部分再造烟叶的生产过程中所添加的外加纤维均为木浆纤维,包括阔叶木和针叶木纤维。 Currently, domestic enterprises most of reconstituted tobacco manufacturing process plus the added fibers are wood pulp fibers, including hardwood and softwood fibers.

[0004] 木浆纤维一般是在造纸行业中使用,近年来国内的木材资源本身就缺乏,加上环保方面的压力,开发更多新的浆料纤维代替木浆纤维势在必行。 [0004] wood pulp fibers are generally used in the paper industry, in recent years, the timber itself is the lack of domestic resources, coupled with the pressure of environmental protection, the development of more new pulp fiber instead of wood pulp fibers imperative.

[0005] 本发明旨研究竹浆纤维代替木浆纤维作为外加纤维用于造纸法再造烟叶的生产的可行性,缓解国内木材资源匮乏的现状,且为竹浆纤维拓展新的用途。 [0005] aims to study bamboo fiber instead of wood pulp fibers of the present invention as an external fiber recycling feasibility of the production of tobacco paper method is used to ease the shortage of domestic timber resources the status quo, and to develop new uses for bamboo fiber.

[0006] 经文献检索,未见与本发明相同的公开报道。 [0006] literature search, no disclosure of the present invention, the same report.

发明内容: SUMMARY:

[0007] 本发明的目的在于提供一种简单、可行、质量稳定的用竹浆纤维代替木浆纤维的造纸法再造烟叶的方法。 [0007] The object of the present invention is to provide a simple, practical, stable quality reconstituted tobacco paper-making method in place of wood pulp fibers with the bamboo fiber.

[0008] 本发明的用竹浆纤维代替木浆纤维的造纸法再造烟叶的方法,具体步骤如下: [0008] bamboo fiber with the inventive method instead of reconstituted tobacco paper-making pulp fibers, the following steps:

[0009] a.竹浆纤维的制备 [0009] a. Preparation of bamboo fiber

[0010] 将风干后的大龙竹进行切片,在蒸煮锅中以温度165°C,升温120 min,保温60 min条件进行蒸煮,制成竹浆,再在温度90°C,时间60 min,氧压0.6 Mpa,MgS04用量0.5%, NaOH用量2.5%,浆浓10%条件进行氧脱处理,得到氧脱竹浆; [0010] Lung large bamboo dried after slicing, the cooker at a temperature of 165 ° C, temperature increase 120 min, 60 min incubation conditions for cooking, made of bamboo, and then at a temperature of 90 ° C, time 60 min, oxygen pressure 0.6 Mpa, MgS04 amount of 0.5%, NaOH 2.5% dosage, the conditions of 10% pulp consistency oxygen delignification treatment to obtain oxygen delignification of bamboo;

[0011] b.涂布液的制备 b Preparation [0011] The coating liquid

[0012] 以复烤烟梗、碎片与烟末为原料,其中烟梗单独用水萃取60min,碎片与烟末按质量比70: 30混合以水为溶剂进行萃取60min。 [0012] In the end of the complex flue-cured tobacco stems, tobacco scrap and raw materials, wherein the end of the stems was extracted with water alone 60min, debris and smoke mass ratio of 70: 30 were mixed to water as a solvent for extraction 60min. 原料萃取后分别进行固液分离,液体置于旋转蒸发仪中45°C条件下浓缩成密度为1.25 g/cm3膏状;取质量比40%的烟梗浸膏和60%的碎片/烟末混合浸膏,添加质量比5%的香精香料,混合均匀后即制成涂布液; After the raw materials were extracted with solid-liquid separation, the liquid was placed in a rotary evaporator at 45 ° C was concentrated to a density of 1.25 g / cm3 paste; take mass ratio of 40% at the end of the tobacco stem extract and 60% of the debris / smoke mixed extract, the mass ratio of 5% was added flavors and fragrances, after uniformly mixed to prepare a coating solution;

[0013] c.片基的抄造 [0013] c. Group papermaking sheet

[0014] 将步骤b的烟梗残渣先进行初磨浆,打浆度为8。 [0014] The residue of step b tobacco stems to be First refining, freeness 8. SR ;取质量比45%的烟梗残渣初磨浆,与质量比45%的碎片和烟末混合残渣混合,添加质量比10%的的氧脱竹浆纤维,混合均匀后进行磨浆,打浆度打浆度为35-48° SR,后制成片基; The SR; 45% taking the mass ratio of early stem residue refining, and the residue was mixed in the mixing quality of 45% at the end of the debris and smoke than the added mass ratio of oxygen of 10% off the bamboo fiber, for refining uniformly mixed beating degree of freeness of 35-48 ° SR, the base sheet is made;

[0015] d.造纸法再造烟叶的制备[0016] 用步骤b制备的涂布液对步骤c制备的片基进行常规的涂布、烘干,控制成品的水分在10-12%,切片备用。 [0015] d. Preparation of reconstituted tobacco [0016] The coating solution prepared in step b of the base sheet prepared in step c conventional coating and drying, the finished papermaking process to control the moisture 10-12%, cut back .

[0017] 本发明所用设备均为标准化产品,市场购买。 [0017] The present invention used equipment are standardized products, market purchase.

[0018] 本发明的优点在于:方法简单、可行,再造烟叶的质量稳定。 [0018] The advantage of the present invention is that: the method is simple, feasible and stable quality reconstituted tobacco.

具体实施方式: detailed description:

[0019] 本发明的具体步骤如下: [0019] In particular steps of the present invention are as follows:

[0020] a.竹浆纤维的制备 [0020] a. Preparation of bamboo fiber

[0021] 将风干后的大龙竹进行切片,在蒸煮锅中以温度165°C,升温120 min,保温60 min条件进行蒸煮,制成竹浆,再温度900C,时间60 min,氧压0.6 Mpa, MgSO4用量0.5%,NaOH用量2.5%,浆浓10%条件进行氧脱处理,得到氧脱竹浆; [0021] Lung large bamboo dried after slicing, the cooker at a temperature of 165 ° C, temperature increase 120 min, 60 min incubation conditions for cooking, made of bamboo, and then the temperature of 900C, time 60 min, oxygen pressure 0.6 mpa, MgSO4 amount of 0.5%, NaOH 2.5% dosage, the conditions of 10% pulp consistency oxygen delignification treatment to obtain oxygen delignification of bamboo;

[0022] b.涂布液的制备 b Preparation [0022] The coating liquid

[0023] 以复烤烟梗、碎片与烟末为原料,其中烟梗单独用水萃取60min,碎片与烟末按70: 30混合以水为溶剂进行萃取60min。 [0023] In the end of the complex flue-cured tobacco stems, tobacco chips as raw material and extraction 60min, the end pieces and wherein tobacco stems by water alone 70: 30 mixed solvent of water and extracted 60min. 原料萃取后分别进行固液分离,液体置于旋转蒸发仪中45°C温度下浓缩成密度为1.25 g/cm3膏状;取质量比40%的烟梗浸膏和55%的碎片/烟末混合浸膏,添加质量比5%的香精香料,混合均匀后即制成涂布液; After the raw materials were extracted with solid-liquid separation, the liquid was placed under a rotary evaporator and concentrated to a temperature of 45 ° C a density of 1.25 g / cm3 paste; take mass ratio of 40% at the end of the tobacco stem extract and 55% of the debris / smoke mixed extract, the mass ratio of 5% was added flavors and fragrances, after uniformly mixed to prepare a coating solution;

[0024] c.片基的抄造 [0024] c. Group papermaking sheet

[0025] 将步骤b的烟梗残渣先进行初磨浆,打浆度为8。 [0025] The residue of step b tobacco stems to be First refining, freeness 8. SR ;取质量比45%的烟梗残渣初磨浆,与质量比45%的碎片和烟末混合残渣混合,添加质量比10%的的氧脱竹浆纤维,混合均匀后进行磨浆,打浆度为35-48° SR,后制成片基; [0026] 制备的氧脱竹浆纤维,混合均匀后进行磨浆,到打浆度为35° SR或40° SR或48° SR时,进行抄造,制成片基。 The SR; 45% taking the mass ratio of early stem residue refining, and the residue was mixed in the mixing quality of 45% at the end of the debris and smoke than the added mass ratio of oxygen of 10% off the bamboo fiber, for refining uniformly mixed beating degree of 35-48 ° SR, the base sheet is made; when oxygen delignification bamboo fiber [0026] preparation of mixed uniformly for grinding, to a beating degree of 35 ° SR or 40 ° SR or 48 ° SR, for papermaking, to form a sheet group.

[0027] d.造纸法再造烟叶的制备 [0027] d. Preparation of reconstituted tobacco paper-making

[0028] 用步骤b制备的涂布液对步骤c制备的片基进行常规的涂布、烘干,控制成品的水分在10%或11%或12%,并切片。 [0028] The coating solution prepared in the step b to step c sheet substrate prepared in conventional coating, drying, controlling moisture in the finished product 10% or 11% or 12%, and sectioned.

[0029] 根据上述方法制造的造纸法再造烟叶产品,经专家进行感官质量评价,结果见表I。 [0029] The paper-making reconstituted tobacco products produced as described above, a sensory quality evaluation by experts, the results are shown in Table I. 由表I看出,竹浆纤维制成的再造烟叶产品口腔刺激较小,木质气较轻。 From Table I, reconstituted tobacco product made from bamboo fiber small mouth irritation, wood gas lighter.

[0030] 表I添加木浆纤维和竹浆纤维前、后的再造烟叶的感官评价结果 Before [0030] Table I added bamboo fiber and wood pulp fibers, results of sensory evaluation after the reconstituted tobacco

Figure CN103263073AD00041

Claims (1)

  1. 1.一种用竹浆纤维代替木浆纤维的造纸法再造烟叶的方法,其特征在于该方法的具体步骤如下: a.竹浆纤维的制备将风干后的大龙竹进行切片,在蒸煮锅中以温度165°C,升温120 min,保温60 min条件进行蒸煮,制成竹浆,再温度900C,时间60 min,氧压0.6 Mpa, MgSO4用量0.5%,NaOH用量2.5%,浆浓10%条件进行氧脱处理,得到氧脱竹浆; b.涂布液的制备以复烤烟梗、碎片与烟末为原料,其中烟梗单独用水萃取60min,碎片与烟末按质量比70: 30混合以水为溶剂进行萃取60min。 1. A method of reconstituted tobacco used in place of wood pulp fibers of the bamboo fiber paper method, characterized in that the specific steps of the method are as follows:. A large preparing bamboo fiber after air drying Bamboo slicing, cooking pot in at a temperature of 165 ° C, temperature increase 120 min, 60 min incubation conditions for cooking, made of bamboo, and then the temperature of 900C, time 60 min, an oxygen pressure of 0.6 Mpa, MgSO4 amount of 0.5%, NaOH 2.5% dosage, pulp consistency 10% conditions for oxygen delignification treatment to obtain oxygen delignification of bamboo; preparation of coating solution B in the complex flue-cured tobacco stems, tobacco as the raw material and the end pieces, wherein the end of the stems was extracted with water alone 60min, debris and smoke mass ratio 70: 30 mixing water as a solvent for extraction 60min. 原料萃取后分别进行固液分离,液体置于旋转蒸发仪中45°C温度下浓缩成密度为1.25 g/cm3膏状;取质量比40%的烟梗浸膏和55%的碎片/烟末混合浸膏,添加质量比5%的香精香料,混合均匀后即制成涂布液; c.片基的抄造将步骤b的烟梗残渣先进行初磨浆,打浆度为8° SR ;取质量比45%的烟梗残渣初磨浆,与质量比45%的碎片和烟末混合残渣混合,添加质量比10%的的氧脱竹浆纤维,混合均匀后进行磨浆,打浆度为35-48° SR,后制成片基; d.造纸法再造烟叶的制备用步骤b制备的涂布液对步骤c制备的片基进行常规的涂布、烘干,控制成品的水分在10-12%,切片备用。 After the raw materials were extracted with solid-liquid separation, the liquid was placed under a rotary evaporator and concentrated to a temperature of 45 ° C a density of 1.25 g / cm3 paste; take mass ratio of 40% at the end of the tobacco stem extract and 55% of the debris / smoke mixed extract, the mass ratio of 5% was added flavors and fragrances, after uniformly mixed to prepare a coating solution;. c group papermaking sheet tobacco stems step b for the beginning of the first refining residue, beating degree of 8 ° SR; taken 45% of the mass ratio of early stem residue refining, and the residue was mixed in the mixing quality of 45% at the end of the debris and smoke than the added mass ratio of oxygen of 10% off the bamboo fiber mixed performed after refining, a freeness of 35 -48 ° SR, the base sheet is made;. d papermaking process for preparing a coating solution of step b prepared reconstituted tobacco sheet substrate prepared in the step c for conventional coating, drying, controlling moisture in the finished 10- 12%, cut back.
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CN103478886A (en) * 2013-10-12 2014-01-01 云南烟草科学研究院 Method for using expansion stems for preparing paper-making process reconstituted tobacco leaves
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CN104213458A (en) * 2014-07-24 2014-12-17 四川省西龙生物质材料科技有限公司 Original-color bamboo fiber pulp, preparation method thereof and an application of the bamboo fiber pulp as tobacco additive
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CN104738808A (en) * 2015-02-11 2015-07-01 云南瑞升烟草技术(集团)有限公司 Preparing method for paper-making process reconstituted tobacco with novel surface physical structure
CN104988780A (en) * 2015-07-28 2015-10-21 湖北中烟工业有限责任公司 Method for preparing recombinant tobacco cigarette paper by replacing wood pulp with bamboo pulp
CN106418651A (en) * 2016-11-09 2017-02-22 湖北中烟工业有限责任公司 Method for improving flexibility of tobacco reconstituted through paper-making process
CN106858699A (en) * 2017-03-30 2017-06-20 浙江中烟工业有限责任公司 Method for increasing padding retention rate of paper process reconstituted tobacco product with diatomite
CN106880076A (en) * 2017-03-30 2017-06-23 浙江中烟工业有限责任公司 Method for improving retention rate of paper-making process reconstituted tobacco product filler by adopting diatomite and titanium dioxide composite filler
CN106901397A (en) * 2017-03-30 2017-06-30 浙江中烟工业有限责任公司 Method for improving filler retention rate of a papermaking-method reconstituted tobacco product by employing ternary composite filler
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CN103535850B (en) * 2013-09-30 2016-04-27 上海烟草集团有限责任公司 Application of the coating solution, an acid and its recycling in the tobacco
CN103535850A (en) * 2013-09-30 2014-01-29 上海烟草集团有限责任公司 Acid coating liquid and application of acid coating liquid in reconstituted tobacco
CN103478886A (en) * 2013-10-12 2014-01-01 云南烟草科学研究院 Method for using expansion stems for preparing paper-making process reconstituted tobacco leaves
CN103829364A (en) * 2014-03-05 2014-06-04 上海烟草集团有限责任公司 Salt coating liquid and application thereof in reconstituted tobacco
CN104213458A (en) * 2014-07-24 2014-12-17 四川省西龙生物质材料科技有限公司 Original-color bamboo fiber pulp, preparation method thereof and an application of the bamboo fiber pulp as tobacco additive
CN104213458B (en) * 2014-07-24 2017-04-19 四川环龙新材料有限公司 Bamboo fiber qualities of pulp preparation and its application as an additive in tobacco
CN104256881A (en) * 2014-08-06 2015-01-07 云南中烟工业有限责任公司 Method for preparing reconstituted tobacco by replacing wood pulp fibers with bamboo leaf fiber parts
CN104256881B (en) * 2014-08-06 2016-02-24 云南中烟工业有限责任公司 A method of making reconstituted tobacco substitute wood pulp fibers in bamboo fiber portions
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CN106418651A (en) * 2016-11-09 2017-02-22 湖北中烟工业有限责任公司 Method for improving flexibility of tobacco reconstituted through paper-making process
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CN106858699A (en) * 2017-03-30 2017-06-20 浙江中烟工业有限责任公司 Method for increasing padding retention rate of paper process reconstituted tobacco product with diatomite
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