CN109793255A - A kind of pipe tobacco and preparation method thereof that cool taste is soft - Google Patents
A kind of pipe tobacco and preparation method thereof that cool taste is soft Download PDFInfo
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- CN109793255A CN109793255A CN201910072086.1A CN201910072086A CN109793255A CN 109793255 A CN109793255 A CN 109793255A CN 201910072086 A CN201910072086 A CN 201910072086A CN 109793255 A CN109793255 A CN 109793255A
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Abstract
The invention discloses a kind of pipe tobaccos and preparation method thereof that cool taste is soft, it is that dried peppermint leaf, loguat leaf and sweet basil leaf are mixed and added into deionized water, extracting solution is prepared in such a way that heating is boiled, it is transferred to the ethereal oil in dried peppermint leaf, loguat leaf and sweet basil leaf in extracting solution, to assign extracting solution a kind of refrigerant mouthfeel；Then extracting solution and tobacco leaf concentration are prepared into tobacco extract, tobacco leaf and tobacco extract are formed by addition natural essence, acetate fiber, modified starch and propylene glycol monomethyl ether later, pipe tobacco is made, pipe tobacco surface is set to contain the ethereal oil in extracting solution, to make pipe tobacco that there is refrigerant soft mouthfeel.Pipe tobacco unique style prepared by the present invention, effectively improves the Filling power of cigarette, improves flavor quality of cigarette.
Description
Technical field
The invention belongs to technology field of tobacco preparation, specially a kind of pipe tobacco and preparation method thereof that cool taste is soft.
Background technique
Pipe tobacco, which refers to, is cut into Filamentous, granular, sheet, last shape or other shapes for tobacco leaf, adds auxiliary material, through everfermentation,
Storage, can the tobacco product that smokes of sale without rolling.Such as pipe tobacco, Mo He tobacco, offal, shredded tobacco for water pipes, yellow red pipe tobacco.Pipe tobacco
Application method there are many, can directly be taken out with cigarette paper roll at arbitrary shape, also pipe tobacco is rolled by useful dedicated cigarette-roller
Cigarette-like to use the method that the smoking sets such as more useful tobacco pipe are used cooperatively.Pipe tobacco is that tobacco leaf is formed after processing, according to the place of production
The taste of difference, cigarette is also very different.The pipe tobacco of genuine piece cigarette is mainly by cut tobacco, stem and tobacco thin filament etc. at grouping
At.
Cigarette flavouring humectation is to promote Chinese-style cigarette quality, increase perfume quantity, mention Yang Xiangyun, set off nature fragrance, reduce
The key of gas drying sense.The demand for sense that current existing cigarette is not able to satisfy increase fragrance, enhancing flue gas promotes the production of body fluid, and can not
The refrigerant soft mouthfeel of cigarette is provided from the angle of pipe tobacco.
Summary of the invention
In order to overcome above-mentioned technical problem, the present invention provides a kind of soft pipe tobacco of cool taste and preparation method thereof.
The purpose of the present invention is achieved through the following technical solutions:
The present invention discloses a kind of pipe tobacco that cool taste is soft first, is made of following raw material: 15-30
Part dried peppermint leaf, 15-25 parts of loguat leaves, 5-10 parts of sweet basil leafs, 50-70 parts of deionized waters, 80% ethyl alcohol (volume fraction of 50-70 part
For 80%), 35-55 parts of tobacco leaves, 55-70 parts of propylene glycol monomethyl ethers, 5-10 parts of natural essences, 8-15 portions of modified starches, 15-20 portions of vinegar
Sour fiber.The preparation method of the soft pipe tobacco of cool taste of the present invention is: dried peppermint leaf, loguat leaf and sweet basil leaf are mixed simultaneously
Deionized water is added, prepares extracting solution in such a way that heating is boiled, makes the volatility in dried peppermint leaf, loguat leaf and sweet basil leaf
Oil is transferred in extracting solution, to assign extracting solution a kind of refrigerant mouthfeel；80% second will be added after extracting solution and tobacco leaf concentration
Tobacco extract is made in alcohol, later by adding natural essence, acetate fiber, modified starch and propylene glycol monomethyl ether for tobacco leaf and cigarette
Careless extract molding, is made pipe tobacco, pipe tobacco surface is made to contain the ethereal oil in extracting solution, so that it is refrigerant soft to have pipe tobacco
Mouthfeel.
Further, the modified starch is made by the following method:
(1) 20g cornstarch is poured into beaker, 100mL deionized water is added, be put into water-bath and heat and stir for 80 DEG C
20min is mixed, starch milk is formed；Starch milk is transferred in 60 DEG C of thermostat water bath, keeps the temperature 30min, 1g sodium bicarbonate is added
And stir evenly, 15mL vinylacetate is added, 5h is stirred by the blender of 200r/min, mass concentration, which is then added, is
10% sodium hydroxide solution adjusts pH, until pH=9, stands 1h；
(2) sodium chloride solution that 10mL mass concentration is 5%, at the uniform velocity stirring 15min is added, 0.1g acetic acid is then added
Zinc reacts 2h, adds the dilute hydrochloric acid solution that mass concentration is 10% and adjusts pH, until deionization is used in pH=7, centrifugal dehydration
It is dry after water washing, obtain modified starch.
The anti -precipitability of starch emulsion can be poor, is easy to happen the case where mutually separating as adhesive, but starch emulsion
With good wet colloidality energy and environment-protecting and non-poisonous, will not cause damages to human body and environment, so needing to change starch
Property.The present invention is during preparing pipe tobacco, using modified starch as adhesive, during starch conversion using zinc acetate as
Crosslinking agent carries out multiple elements design to starch by sodium bicarbonate, vinylacetate and sodium chloride solution and is modified, on vinylacetate
Double bond disconnection be grafted on starch backbone, increase the branchedness of starch chain, zinc acetate is as crosslinking agent, by vinylacetate
It is crosslinked with starch molecule, cross-linking effect is much larger than the hydrogen bond formed, and vinylacetate and starch molecule formation one is whole
Body, structure is tighter, and property stabilization will not there is a situation where mutually separate.
Further, the natural essence is one or more of ethylmaltol, strawberry essence and chinese cymbidium rope.
Further, the acetate fiber is CAFM9002.
The invention also discloses the preparation methods of the soft pipe tobacco of the cool taste, include the following steps:
Step S1, extracting solution is prepared:
S11, dried peppermint leaf, loguat leaf and sweet basil leaf are mixed, is ground into powder, cross 50 meshes；
S12, the powder after grinding is put into decoction vessel, deionized water is added, then heating is boiled, it is cooked by slow fire 1h,
It is filtered after standing 15min, extracting solution is made；
Step S2, tobacco extract is prepared:
It is added in extracting solution after tobacco leaf is ground, is heated to 60 DEG C, impregnate 2h, then heat to 80 DEG C, impregnated simultaneously
It is spare to collect tobacco leaf for ultrasonic 3h, filtering；30min is concentrated in filtrate by inspissator, the temperature for controlling inspissator is 60 DEG C, true
Reciprocal of duty cycle is 0.06MPa；80% ethyl alcohol is added into the filtrate after concentration, is carried out after standing 1h by the centrifuge of 5000r/min
Tobacco extract is made in centrifugation, filtering；
Step S3, pipe tobacco is prepared:
S31, the tobacco leaf and natural essence collected in step S2 are mixed, adds acetate fiber, it is spare after mixing；
S32, modified starch and the tobacco extract are added in propylene glycol monomethyl ether, are warming up to 40 DEG C, at the uniform velocity stir
30min then heats to 50 DEG C, stirs 10min, and mixed liquor is made, spare；
S33, mixture obtained by step S31 is placed on forming net, wet smoked sheet is made in mixed liquor obtained by addition step S32；
Wet smoked sheet is dried by 80 DEG C of drying box, cuts smoked sheet after drying, obtains the soft pipe tobacco of cool taste.
Further, in step S33, the moisture content after wet smoked sheet drying is 10-13%, and the width of pipe tobacco is 0.6-
0.8mm。
The beneficial effects of the present invention are embodied in:
(1) present invention mixes dried peppermint leaf, loguat leaf and sweet basil leaf, prepares extracting solution in such a way that heating is boiled,
It is transferred to the ethereal oil in dried peppermint leaf, loguat leaf and sweet basil leaf in extracting solution, to assign extracting solution a kind of refrigerant mouth
Sense；Then extracting solution and tobacco leaf concentration are prepared into tobacco extract, passes through addition natural essence, acetate fiber, modified shallow lake later
Powder and propylene glycol monomethyl ether form tobacco leaf and tobacco extract, and pipe tobacco is made, pipe tobacco surface is made to contain the volatility in extracting solution
Oil, to make pipe tobacco that there is refrigerant soft mouthfeel.
(2) present invention is during preparing pipe tobacco, using modified starch as adhesive, using propylene glycol monomethyl ether as solvent,
In pipe tobacco forming process, modified starch can adequately be bonded tobacco extract and tobacco leaf, can be by pipe tobacco and cigarette
Careless extract is crosslinked more thorough, so that the refrigerant soft mouthfeel of pipe tobacco is more comprehensive, and can be by natural essence more
It merges well, greatly improves the quality of cigarette；
(3) the soft pipe tobacco unique style of cool taste prepared by the present invention, it is applied widely, effectively improve cigarette
Filling power improves flavor quality of cigarette；And the present invention is mixed by acetate fiber and tobacco leaf, can both promote tobacco leaf at
Silk improves into silk efficiency, and can reduce the consumption of tobacco leaf, saves production cost.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, all other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Modified starch used in following embodiments is made as follows:
(1) 20g cornstarch is poured into beaker, 100mL deionized water is added, be put into water-bath and heat and stir for 80 DEG C
20min is mixed, starch milk is formed；Starch milk is transferred in 60 DEG C of thermostat water bath, keeps the temperature 30min, 1g sodium bicarbonate is added
And stir evenly, 15mL vinylacetate is added, 5h is stirred by the blender of 200r/min, mass concentration, which is then added, is
10% sodium hydroxide solution adjusts pH, until pH=9, stands 1h；
(2) sodium chloride solution that 10mL mass concentration is 5%, at the uniform velocity stirring 15min is added, 0.1g acetic acid is then added
Zinc reacts 2h, adds the dilute hydrochloric acid solution that mass concentration is 10% and adjusts pH, until deionization is used in pH=7, centrifugal dehydration
Water washing is dried afterwards three times, obtains modified starch.
Embodiment 1
The soft pipe tobacco of the present embodiment cool taste, is made of following raw material: 15 parts of dried peppermint leaves, 15 portions of loquats
Leaf, 5 parts of sweet basil leafs, 50 parts of deionized waters, 50 part of 80% ethyl alcohol, 35 parts of tobacco leaves, 55 parts of propylene glycol monomethyl ethers, 5 parts of ethylmaltols,
8 portions of modified starches, 15 parts of acetate fibers；
The soft pipe tobacco of the present embodiment cool taste is made of following steps:
Step S1, extracting solution is prepared:
S11, dried peppermint leaf, loguat leaf and sweet basil leaf are mixed, is ground into powder, cross 50 meshes；
S12, the powder after grinding is put into decoction vessel, deionized water is added, then heating is boiled, it is cooked by slow fire 1h,
It is filtered after standing 15min, extracting solution is made；
Step S2, tobacco extract is prepared:
It is added in extracting solution after tobacco leaf is ground, is heated to 60 DEG C, impregnate 2h, then heat to 80 DEG C, impregnated simultaneously
It is spare to collect tobacco leaf for ultrasonic 3h, filtering；30min is concentrated in filtrate by inspissator, the temperature for controlling inspissator is 60 DEG C, true
Reciprocal of duty cycle is 0.06MPa；80% ethyl alcohol is added into the filtrate after concentration, is carried out after standing 1h by the centrifuge of 5000r/min
Tobacco extract is made in centrifugation, filtering；
Step S3, pipe tobacco is prepared:
S31, the tobacco leaf and natural essence collected in step S2 are mixed, adds acetate fiber, it is spare after mixing；
S32, modified starch and the tobacco extract are added in propylene glycol monomethyl ether, are warming up to 40 DEG C, at the uniform velocity stir
30min then heats to 50 DEG C, stirs 10min, and mixed liquor is made, spare；
S33, mixture obtained by step S31 is placed on forming net, wet smoked sheet is made in mixed liquor obtained by addition step S32；
Wet smoked sheet is dried by 80 DEG C of drying box, cuts smoked sheet after drying, obtains the soft pipe tobacco of cool taste.
Embodiment 2
The soft pipe tobacco of the present embodiment cool taste, is made of following raw material: 20 parts of dried peppermint leaves, 18 portions of loquats
Leaf, 7 parts of sweet basil leafs, 55 parts of deionized waters, 55 part of 80% ethyl alcohol, 40 parts of tobacco leaves, 58 parts of propylene glycol monomethyl ethers, 7 parts of ethylmaltols,
10 portions of modified starches, 16 parts of acetate fibers.
The soft pipe tobacco of the present embodiment cool taste is made by the identical step of embodiment 1.
Embodiment 3
The soft pipe tobacco of the present embodiment cool taste, is made of following raw material: 25 parts of dried peppermint leaves, 22 portions of loquats
Leaf, 9 parts of sweet basil leafs, 65 parts of deionized waters, 65 part of 80% ethyl alcohol, 50 parts of tobacco leaves, 65 parts of propylene glycol monomethyl ethers, 8 parts of ethylmaltols,
12 portions of modified starches, 18 parts of acetate fibers.
The soft pipe tobacco of the present embodiment cool taste is made by the identical step of embodiment 1.
Embodiment 4
The soft pipe tobacco of the present embodiment cool taste, is made of following raw material: 30 parts of dried peppermint leaves, 25 portions of loquats
Leaf, 10 parts of sweet basil leafs, 70 parts of deionized waters, 70 part of 80% ethyl alcohol, 55 parts of tobacco leaves, 70 parts of propylene glycol monomethyl ethers, 10 parts of ethyl malt
Phenol, 15 portions of modified starches, 20 parts of acetate fibers.
The soft pipe tobacco of the present embodiment cool taste is made by the identical step of embodiment 1.
Comparative example 1
Compared with Example 1, difference is only that replaces modified starch with starch to this comparative example.
Comparative example 2
This comparative example is a kind of pipe tobacco that mouthfeel is soft in market.
The embodiment 1-4 and comparative example 1-2 pipe tobacco surface volatile oil content prepared is detected, as a result such as the following table 1
It is shown:
Table 1
50 professionals are selected, the mouthfeel of the embodiment 1-4 and comparative example 1-2 pipe tobacco prepared is tested, is made
Sensory evaluation, gets score, full marks very, as a result as shown in table 2 below:
Table 2
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Comparative example 1 | Comparative example 2 | |
| Mouthfeel | 8.5 | 8.7 | 8.8 | 9.0 | 7.5 | 7.0 |
From upper table 1-2 as can be seen that embodiment 1-4 preparation pipe tobacco surface ethereal oil content 37-51% it
Between, the content of the soft pipe tobacco surface ethereal oil of cool taste of comparative example 1-2 preparation is within the scope of 0-38%；Embodiment 1-4
Score 8.5-9.0/, the score of comparative example 1-2 is between 7.0-7.5.So cool taste prepared by the present invention is soft
Not only there is refrigerant soft mouthfeel with pipe tobacco, also improve cigarette quality, receive an acclaim.
Above content is only citing made for the present invention and explanation, affiliated those skilled in the art are to being retouched
The specific embodiment stated does various modifications or additions or is substituted in a similar manner, and without departing from invention or surpasses
More range defined in the claims, is within the scope of protection of the invention.
Claims (7)
1. a kind of pipe tobacco that cool taste is soft, which is characterized in that be made of following raw material: 15-30 parts of dried peppermint leaves,
15-25 parts of loguat leaves, 5-10 parts of sweet basil leafs, 50-70 parts of deionized waters, 80% ethyl alcohol of 50-70 part, 35-55 parts of tobacco leaves, 55-70
Part propylene glycol monomethyl ether, 5-10 parts of natural essences, 8-15 portions of modified starches, 15-20 parts of acetate fibers.
2. a kind of soft pipe tobacco of cool taste according to claim 1, which is characterized in that the cool taste is soft
The preparation method of pipe tobacco is: dried peppermint leaf, loguat leaf and sweet basil leaf being mixed and added into deionized water, in such a way that heating is boiled
Extracting solution is prepared, is transferred to the ethereal oil in dried peppermint leaf, loguat leaf and sweet basil leaf in extracting solution, to assign extracting solution
A kind of refrigerant mouthfeel；Tobacco extract is made by 80% ethyl alcohol is added after extracting solution and tobacco leaf concentration, passes through addition day later
Right essence, acetate fiber, modified starch and propylene glycol monomethyl ether form tobacco leaf and tobacco extract, and pipe tobacco is made, makes pipe tobacco table
The ethereal oil in extracting solution is contained in face, so that pipe tobacco be made to have refrigerant soft mouthfeel.
3. the soft pipe tobacco of a kind of cool taste according to claim 1 or 2, which is characterized in that the modified starch is by such as
Lower section method is made:
(1) 20g cornstarch is poured into beaker, 100mL deionized water is added, be put into water-bath and heat and stir for 80 DEG C
20min forms starch milk；Starch milk is transferred in 60 DEG C of thermostat water bath, keeps the temperature 30min, 1g sodium bicarbonate is added simultaneously
It stirs evenly, adds 15mL vinylacetate, 5h is stirred by the blender of 200r/min, mass concentration, which is then added, is
10% sodium hydroxide solution adjusts pH, until pH=9, stands 1h；
(2) sodium chloride solution that 10mL mass concentration is 5%, at the uniform velocity stirring 15min is added, 0.1g zinc acetate is then added, instead
2h is answered, the dilute hydrochloric acid solution that mass concentration is 10% is added and adjusts pH, until pH=7, centrifugal dehydration are washed with deionized
After dry, obtain modified starch.
4. a kind of soft pipe tobacco of cool taste according to claim 1 or 2, it is characterised in that: the natural essence is
One or more of ethylmaltol, strawberry essence and chinese cymbidium rope.
5. a kind of soft pipe tobacco of cool taste according to claim 1 or 2, it is characterised in that: the acetate fiber is
CAFM9002。
6. the preparation method of the soft pipe tobacco of cool taste described in a kind of any one of Claims 1 to 5, feature exist
In including the following steps:
Step S1, extracting solution is prepared:
S11, dried peppermint leaf, loguat leaf and sweet basil leaf are mixed, is ground into powder, cross 50 meshes；
S12, the powder after grinding is put into decoction vessel, deionized water is added, then heating is boiled, and is cooked by slow fire 1h, is stood
It is filtered after 15min, extracting solution is made；
Step S2, tobacco extract is prepared:
It is added in extracting solution after tobacco leaf is ground, is heated to 60 DEG C, impregnate 2h, then heat to 80 DEG C, impregnated and ultrasonic
It is spare to collect tobacco leaf for 3h, filtering；30min is concentrated in filtrate by inspissator, the temperature for controlling inspissator is 60 DEG C, vacuum degree
For 0.06MPa；80% ethyl alcohol is added into the filtrate after concentration, is centrifuged after standing 1h by the centrifuge of 5000r/min,
Tobacco extract is made in filtering；
Step S3, pipe tobacco is prepared:
S31, the tobacco leaf and natural essence collected in step S2 are mixed, adds acetate fiber, it is spare after mixing；
S32, modified starch and the tobacco extract are added in propylene glycol monomethyl ether, are warming up to 40 DEG C, at the uniform velocity stirring 30min,
50 DEG C are then heated to, 10min is stirred, mixed liquor is made, it is spare；
S33, mixture obtained by step S31 is placed on forming net, wet smoked sheet is made in mixed liquor obtained by addition step S32；It will be wet
Smoked sheet is dried by 80 DEG C of drying box, cuts smoked sheet after drying, obtains the soft pipe tobacco of cool taste.
7. preparation method according to claim 6, which is characterized in that in step S33, the moisture content after wet smoked sheet drying is
10-13%, the width of pipe tobacco are 0.6-0.8mm.
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| CN201910072086.1A CN109793255A (en) | 2019-01-25 | 2019-01-25 | A kind of pipe tobacco and preparation method thereof that cool taste is soft |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115005493A (en) * | 2022-06-08 | 2022-09-06 | 吉林烟草工业有限责任公司 | Bean-flavor characteristic extract, preparation method thereof and cigarette |
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