CN110150723A - It does not burn the application in cigarette for the tobacco compositions of papermaking-method reconstituted tobaccos and its in heating - Google Patents

It does not burn the application in cigarette for the tobacco compositions of papermaking-method reconstituted tobaccos and its in heating Download PDF

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Publication number
CN110150723A
CN110150723A CN201910538707.0A CN201910538707A CN110150723A CN 110150723 A CN110150723 A CN 110150723A CN 201910538707 A CN201910538707 A CN 201910538707A CN 110150723 A CN110150723 A CN 110150723A
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CN
China
Prior art keywords
papermaking
cigarette
stalk
reconstituted tobaccos
method reconstituted
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910538707.0A
Other languages
Chinese (zh)
Inventor
魏明文
李锐
陈宇超
吴建霖
张文军
冯涛
陈绍全
周俊
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Shi Weice (yunnan) Reconstituted Tobacco Co Ltd
Original Assignee
China Tobacco Shi Weice (yunnan) Reconstituted Tobacco Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Shi Weice (yunnan) Reconstituted Tobacco Co Ltd filed Critical China Tobacco Shi Weice (yunnan) Reconstituted Tobacco Co Ltd
Priority to CN201910538707.0A priority Critical patent/CN110150723A/en
Publication of CN110150723A publication Critical patent/CN110150723A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/186Treatment of tobacco products or tobacco substitutes by coating with a coating composition, encapsulation of tobacco particles
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00Cigars; Cigarettes
    • A24D1/002Cigars; Cigarettes with additives, e.g. for flavouring

Abstract

The invention discloses a kind of tobacco compositions for papermaking-method reconstituted tobaccos and its heating the application in the cigarette that do not burn, the present invention is divided into stalk group raw material and leaf group raw material, on conventional papermaking reconstituted tobacco Process ba- sis, stalk group tobacco powder wet end is made an addition into chip base before piece is base molded, leaf group tobacco powder makes an addition to coating fluid, the core material papermaking-method reconstituted tobaccos for being applied to heat the cigarette that do not burn are prepared, the addition requirement that papermaking-method reconstituted tobaccos chip base absorbent properties meet high-content smoke agent can be promoted using this kind of tobacco compositions, the perfect fragrance framework for heating the cigarette that do not burn, reach the quality pursuit for heating the cigarette that do not burn in terms of aesthetic quality, aroma quality is preferable, flue gas concentration is higher, strength is higher, exquisite in texture, miscellaneous gas is micro- to be had, pleasant impression is clean, hamony is preferable.

Description

For the tobacco compositions of papermaking-method reconstituted tobaccos and its in heating the cigarette that do not burn Application
Technical field
The present invention relates to tobacco leaf production technical fields, and in particular to for papermaking-method reconstituted tobaccos tobacco compositions and its Heating the application in the cigarette that do not burn.
Background technique
In terms of the research and development of new tobacco products and development, the more domestic early many decades of foreign countries' starting, and the side taken Formula is more various, 1970s, and transnational tobacco company begins to do preliminary preparation, has put into substantial contribution and has carried out city Field investigation, research and development of products, advertising.The main You Feimo of the higher product of temperature that current overseas market has occurred successively is international (PMI) iFuse glo, Ploom Tech of Japan Tobacco of IQOS, British American Tobacco etc., and achieve preferable sales volume and city Field degree of recognition, has good market prospects.And domestic development relatively lags behind, and three kinds of major type of new tobacco productses Developmental difference is larger, very unbalanced, and only electronics smoke product has occupied a small amount of market shares at present.Domestic heating is not burnt The research of cigarette products is still in the embryonic stage, although though Some Domestic Zhong Yan company and scientific research institution have lofty ideals for such product Research, but lay particular emphasis on basic theory and two aspect of utensil research and development mostly or still stay in the laboratory research stage, it forms small quantities of The smoking set of quantity research and a fairly large number of patent not yet form more mature product and large-scale industrial production.
Papermaking-method reconstituted tobaccos have mainly used for reference wet papermaking work as the maximum reconstituted tobacco product of yield, technique Skill, by extracting and developing, the processes such as slurrying, manufacture paper with pulp, be coated with by tobacco material processing molding reconstituted tobacco product.Its product is in Loose porous structure, have excellent Physical Processing performance and tobacco endogenous substance freely regulate and control, to the maximum extent improvement with Retain the effective component of tobacco material, aesthetic quality is preferable, and has good flexibility (adaptability) of operation.
Application of the reconstituted tobacco in heating not combustion products at present, mainly there is dry process reproduction tobacco leaf and reproduced by means of rolling cigarette Two kinds of leaf, wherein tobacco leaf reproduced by means of rolling has the advantage being integrally formed with high load amount, utilizes the reconstruction of this kind of technological forming Tobacco leaf application effect is best.But either dry process reproduction cigarette or tobacco leaf reproduced by means of rolling generally require in its forming process A large amount of adhesive assistant formation is added, the addition of the substance may affect the aesthetic quality of target product, together When there is also certain security risks;Simultaneously because the particularity of two kinds of technique, to the more demanding of tobacco material.
Summary of the invention
The purpose of the present invention is to provide a kind of tobacco compositions for papermaking-method reconstituted tobaccos and its heat it is non-ignitable The application in cigarette is burnt, solves the problems, such as to heat the effective tobacco material load capacity of cigarette papermaking-method reconstituted tobaccos of not burning low.
In order to solve the above technical problems, the invention adopts the following technical scheme:
A kind of tobacco compositions for papermaking-method reconstituted tobaccos, including stalk group raw material and/or leaf group raw material,
The stalk group raw material is obtained by the processing of at least one of short stalk, stalk label, long stalk;
The leaf group raw material is by fragment, offal, flue-cured tobacco piece cigarette, Sun cured tobacco piece cigarette, white rib cigarette sheet cigarette, fragrance smoked sheet cigarette At least one processing obtains.
Preferably, the stalk group raw material be by least one of short stalk, stalk label, long stalk after drying, broken It arrives;The leaf group raw material be by fragment, offal, flue-cured tobacco piece cigarette, Sun cured tobacco piece cigarette, white rib cigarette sheet cigarette, fragrance smoked sheet cigarette extremely It is few it is a kind of through drying, it is broken after obtain.
Preferably, the partial size of the stalk group raw material and leaf group raw material is 50-1000 mesh.
Preferably, the drying is microwave drying.
A kind of papermaking-method reconstituted tobaccos chip base, including stalk group raw material.
Preferably, by 80-90 parts by weight stalk group raw material and 10-20 part by weight of cellulose after hot water extracts separation, It is beaten by the beating degree of 50-60 ° of SR, into slurries, wet end addition stalk group raw material and then molding of quantitatively manufacturing paper with pulp are obtained.
A kind of papermaking-method reconstituted tobaccos coating fluid, including the leaf group raw material.
Preferably, including leaf group raw material 2-30 parts by weight, glycerol 12-18 parts by weight, propylene glycol 4-6 parts by weight, cigarette Careless concentrate 20-30 parts by weight
It is a kind of to heat the cigarette that do not burn, including the papermaking-method reconstituted tobaccos chip base and papermaking-method reconstituted tobaccos coating The papermaking-method reconstituted tobaccos coating fluid is coated in papermaking-method reconstituted tobaccos chip base by liquid.
Compared with prior art, beneficial effects of the present invention are at least one of following:
The internal voids structure of offal remains intact in stalk group raw material, can greatly increase paper process again after chip base is added Make the absorbability of tobacco leaf chip base.
Add tobacco compositions papermaking-method reconstituted tobaccos cigarette perfume is plentiful, aroma quality preferably, flue gas concentration is higher, strength compared with Height, exquisite in texture, miscellaneous gas is micro- to be had, pleasant impression is clean, hamony is preferable, can greatly improve the suction experience of user.
Detailed description of the invention
Fig. 1 is offal scanning electron microscope (SEM) photograph of the present invention.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to Limit the present invention.
Embodiment 1:
80 parts by weight tobacco materials and 20 part by weight of cellulose are extracted through hot water and are divided by a kind of papermaking-method reconstituted tobaccos chip base It from rear, is beaten by 50SR ° of beating degree, into slurries, then wet end addition stalk group raw material is quantitatively manufactured paper with pulp molding;
The stalk group raw material accounts for the 30% of slurries gross weight, passes through microwave drying by least one of short stalk, stalk label, long stalk Afterwards, it is crushed to partial size 50-100 mesh.
Embodiment 2:
90 parts by weight tobacco materials and 10 part by weight of cellulose are extracted through hot water and are divided by a kind of papermaking-method reconstituted tobaccos chip base It from rear, is beaten by the beating degree of 60 ° of SR, into slurries, then wet end addition stalk group raw material is quantitatively manufactured paper with pulp molding;
The stalk group raw material accounts for the 30% of slurries gross weight, passes through microwave drying by least one of short stalk, stalk label, long stalk Afterwards, it is crushed to partial size 900-1000 mesh.
Embodiment 3:
85 parts by weight tobacco materials and 15 part by weight of cellulose are extracted through hot water and are divided by a kind of papermaking-method reconstituted tobaccos chip base It from rear, is beaten by 55SR ° of beating degree, into slurries, then wet end addition stalk group raw material is quantitatively manufactured paper with pulp molding;
The stalk group raw material accounts for the 30% of slurries gross weight, passes through microwave drying by least one of short stalk, stalk label, long stalk Afterwards, it is crushed to partial size 200-300 mesh.
Embodiment 4:
The difference of the present embodiment and embodiment 3 is only that: the stalk group raw material accounts for the 20% of slurries gross weight.
Embodiment 5:
The difference of the present embodiment and embodiment 3 is only that: the stalk group raw material accounts for the 10% of slurries gross weight.
Control group 1:
The difference of the present embodiment and embodiment 3 is only that: stalk group raw material is added without in slurries.
The obtained papermaking-method reconstituted tobaccos chip base of control group 1 and embodiment 3-6 is tested, as a result as follows:
Sample classification Air permeability (ml/min/cm2) Cobb value (g/ ㎡) It adsorbs amounts of glycerol (%)
Control group 1 251 166 20
Embodiment 3 1028 289 75
Embodiment 4 675 255 60
Embodiment 5 480 185 35
According to upper table can be seen that papermaking-method reconstituted tobaccos chip base that embodiment 3 obtains no matter air permeability, cobb value also Be absorption amounts of glycerol on be all optimal.With the promotion of offal powder additional amount, piece rheobase is constantly being reduced, so offal powder Additional amount should not be excessive, the piece rheobase decline 30% or so if additional amount reaches 40%.
By a large amount of basic research, it is found by the applicant that there is the neat regular gap structure of a large amount of arrangements inside offal;Through Volume increases several times after crossing microwave expansion, and institutional framework is without obvious damaged and tearing, but the cavity organizations such as vascular bundle are swollen in microwave Volume change is unobvious after swollen processing, as shown in Figure 1, wherein left figure is the 200 mesh stalk group raw materials for amplifying 500 times, right figure is to put 200 mesh stalk group raw materials of big 500 times of microwave treatment.The complete of vascular tissue is proved according to lot of experimental data, favorably The absorption in chip base to coating feed liquid is made an addition in offal powder.
Embodiment 6:
The present embodiment provides a kind of papermaking-method reconstituted tobaccos coating fluids, including 20 parts by weight of leaf group raw material, 18 weight of glycerol Part, 6 parts by weight of propylene glycol, 30 parts by weight of tobacco concentrate of over dry.
Embodiment 7:
The present embodiment provides a kind of papermaking-method reconstituted tobaccos coating fluids, including 30 parts by weight of leaf group raw material, 12 weight of glycerol Part, 4 parts by weight of propylene glycol, over dry tobacco concentrate 20- parts by weight.
Embodiment 8:
The present embodiment provides a kind of papermaking-method reconstituted tobaccos coating fluids, including 25 parts by weight of leaf group raw material, 15 weight of glycerol Part, 5 parts by weight of propylene glycol, 25 parts by weight of tobacco concentrate of over dry.
Control group 2: 15 parts by weight of glycerol, 5 parts by weight of propylene glycol, 25 parts by weight of tobacco concentrate of over dry.
It is applied to the papermaking-method reconstituted tobaccos coating fluid that embodiment 6-8 and control group 2 obtain to be added to offal powder In chip base, and sensory evaluation carried out to product, obtained result such as following table, under equal conditions, most to the sensory evaluation of embodiment 8 It is good.
Sample classification Sensory quality assessment result
Control group Smoke amount it is moderate it is relatively low, cigarette perfume bottom rhythm is weaker, fragrance is coarse, strength is relatively low
Embodiment 6 Smoke amount it is moderate it is higher, cigarette perfume is still full, strength is moderate
Embodiment 7 The moderate relatively low, cigarette perfume of smoke amount it is full it is thick and solid, oral stimulation is larger, strength is moderate higher
Embodiment 8 Smoke amount is moderate, the full thick and solid, moderate concentration of cigarette perfume, strength is moderate, pleasant impression is completely comfortable
Embodiment 9:
The coating fluid that embodiment 8 is obtained is coated in the chip base that embodiment 3 obtains by 70% spreading rate
The control group of embodiment 9 is set:
Control group 2:
Difference with embodiment 9 is only that: not containing leaf group raw material in chip base without containing stalk group raw material, in coating fluid.
Control group 3:
Difference with embodiment 9 is only that: replacing paper process with dry process reproduction tobacco leaf using the cigarette that do not burn is heated.
Control group 4:
State's external heat not so cigarette core material.
Conventional preparation detection is carried out to embodiment 9 and control group 3-5, obtains following table:
Sample classification Hot-water solubles % Total reducing sugar % Reduced sugar % Nicotine %
Embodiment 9 61.28 13.20 12.21 1.62
Control group 3 35.89 5.20 4.50 0.60
Control group 4 56.80 12.90 11.70 1.00
Control group 5 63.69 12.70 12.05 --
Sensory quality assessment is carried out to the product that embodiment 9 and control group 3-5 obtain, obtains following table:
Sample classification Sense organ description
Embodiment 9 Smoke amount is moderate, cigarette perfume is plentiful, moderate concentration, strength are moderate higher
Control group 3 Smoke amount is relatively low, cigarette perfume is partially light, fragrance is coarse, oral stimulation
Control group 4 Smoke amount is moderate, cigarette perfume is partially light, moderate concentration is relatively low, strength is moderate
Control group 5 Smoke amount it is moderate it is higher, cigarette perfume is still plentiful, moderate concentration, strength are moderate higher
From upper table it can be clearly seen that under identical puffing regimens, the paper-making method reconstructed cigarette of tobacco compositions is added Although leaf does not have state's external heat in smoke amount, non-ignitable burning cigarette core material is high, compares in the plentiful degree of the distinctive fragrance of tobacco Control sample is high, while the papermaking-method reconstituted tobaccos strength impression for being added to this kind of tobacco compositions is more filled than dry process reproduction tobacco leaf Point.
Although reference be made herein to invention has been described for multiple explanatory embodiments of the invention, however, it is to be understood that Those skilled in the art can be designed that a lot of other modification and implementations, these modifications and implementations will fall in this Shen It please be within disclosed scope and spirit.It more specifically, within the scope of the present disclosure and claims, can be to master The building block and/or layout for inscribing composite configuration carry out a variety of variations and modifications.In addition to what is carried out to building block and/or layout Outside modification and improvement, to those skilled in the art, other purposes also be will be apparent.

Claims (9)

1. a kind of tobacco compositions for papermaking-method reconstituted tobaccos, it is characterised in that: including stalk group raw material and/or Ye Zuyuan Material, the stalk group raw material are obtained by the processing of at least one of short stalk, stalk label, long stalk;
The leaf group raw material by fragment, offal, flue-cured tobacco piece cigarette, Sun cured tobacco piece cigarette, white rib cigarette sheet cigarette, fragrance smoked sheet cigarette at least A kind of processing obtains.
2. the tobacco compositions according to claim 1 for papermaking-method reconstituted tobaccos, it is characterised in that: the stalk group is former Material be by least one of short stalk, stalk label, long stalk through drying, it is broken after obtain;The leaf group raw material be by fragment, offal, At least one of flue-cured tobacco piece cigarette, Sun cured tobacco piece cigarette, white rib cigarette sheet cigarette, fragrance smoked sheet cigarette through drying, it is broken after obtain.
3. the tobacco compositions according to claim 1 for papermaking-method reconstituted tobaccos, it is characterised in that: the stalk group is former The partial size of material and leaf group raw material is 50-1000 mesh.
4. the tobacco compositions according to claim 2 for papermaking-method reconstituted tobaccos, it is characterised in that: the drying is Microwave drying.
5. a kind of papermaking-method reconstituted tobaccos chip base, which is characterized in that including the original of stalk group described in claim 1-4 any one Material.
6. papermaking-method reconstituted tobaccos chip base according to claim 5, it is characterised in that: it is by 80-90 parts by weight tobacco Raw material and 10-20 part by weight of cellulose are beaten, into slurries after hot water extracts separation by the beating degree of 50-60 0SR Then wet end addition stalk group raw material quantitatively manufactures paper with pulp what molding obtained.
7. a kind of papermaking-method reconstituted tobaccos coating fluid, which is characterized in that including Ye Zuyuan described in claim 1-4 any one Material.
8. papermaking-method reconstituted tobaccos coating fluid according to claim 7, it is characterised in that: including leaf group raw material 2-30 weight Part, glycerol 12-18 parts by weight, propylene glycol 4-6 parts by weight, tobacco concentrate 20-30 parts by weight.
The cigarette 9. a kind of heating is not burnt, which is characterized in that it is to apply papermaking-method reconstituted tobaccos described in claim 7 or 8 Cloth liquid, which is coated on, to be obtained in papermaking-method reconstituted tobaccos chip base described in claim 5 or 6.
CN201910538707.0A 2019-06-20 2019-06-20 It does not burn the application in cigarette for the tobacco compositions of papermaking-method reconstituted tobaccos and its in heating Pending CN110150723A (en)

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CN110663986A (en) * 2019-11-15 2020-01-10 湖北中烟工业有限责任公司 Formula raw material of papermaking tobacco sheet and off-line treatment method thereof
CN110833201A (en) * 2019-11-28 2020-02-25 四川三联新材料有限公司 Dry-process reconstituted tobacco with adjustable air permeability and tightness as well as preparation method and application thereof
CN112716026A (en) * 2021-01-08 2021-04-30 中烟施伟策(云南)再造烟叶有限公司 Recombinant tobacco and preparation method thereof
CN112779818A (en) * 2021-01-08 2021-05-11 中烟施伟策(云南)再造烟叶有限公司 Heating tobacco cigarette paper and preparation method thereof
CN113115970A (en) * 2021-04-02 2021-07-16 中国烟草总公司郑州烟草研究院 Preparation method of reconstituted tobacco with low lignin content
CN113712239A (en) * 2021-09-07 2021-11-30 河北中烟工业有限责任公司 Preparation method of high-nicotine paper-making reconstituted tobacco with burley tobacco particles as filler

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Publication number Priority date Publication date Assignee Title
CN110663986A (en) * 2019-11-15 2020-01-10 湖北中烟工业有限责任公司 Formula raw material of papermaking tobacco sheet and off-line treatment method thereof
CN110833201A (en) * 2019-11-28 2020-02-25 四川三联新材料有限公司 Dry-process reconstituted tobacco with adjustable air permeability and tightness as well as preparation method and application thereof
CN110833201B (en) * 2019-11-28 2021-09-07 四川三联新材料有限公司 Dry-process reconstituted tobacco with adjustable air permeability and tightness as well as preparation method and application thereof
CN112716026A (en) * 2021-01-08 2021-04-30 中烟施伟策(云南)再造烟叶有限公司 Recombinant tobacco and preparation method thereof
CN112779818A (en) * 2021-01-08 2021-05-11 中烟施伟策(云南)再造烟叶有限公司 Heating tobacco cigarette paper and preparation method thereof
CN113115970A (en) * 2021-04-02 2021-07-16 中国烟草总公司郑州烟草研究院 Preparation method of reconstituted tobacco with low lignin content
CN113712239A (en) * 2021-09-07 2021-11-30 河北中烟工业有限责任公司 Preparation method of high-nicotine paper-making reconstituted tobacco with burley tobacco particles as filler
CN113712239B (en) * 2021-09-07 2022-11-25 河北中烟工业有限责任公司 Preparation method of high-nicotine paper-making reconstituted tobacco with burley tobacco particles as filler

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