CN109349677A - A kind of ultra micro tobacco powder reconstituted tobacco and preparation method thereof - Google Patents

A kind of ultra micro tobacco powder reconstituted tobacco and preparation method thereof Download PDF

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Publication number
CN109349677A
CN109349677A CN201811476687.0A CN201811476687A CN109349677A CN 109349677 A CN109349677 A CN 109349677A CN 201811476687 A CN201811476687 A CN 201811476687A CN 109349677 A CN109349677 A CN 109349677A
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China
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tobacco
ultra micro
weight
tobacco powder
preparation
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CN201811476687.0A
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CN109349677B (en
Inventor
杨紫刚
杨涛
王晓耕
雷连龙
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Yunnan Bazi Biotechnology Co ltd
Yunnan Chunxu Biotechnology Co ltd
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Yunnan Bagu Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products

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  • Manufacture Of Tobacco Products (AREA)
  • Paper (AREA)

Abstract

The present invention relates to a kind of ultra micro tobacco powder reconstituted tobaccos and preparation method thereof.The preparation method includes that external source fiber cuts fine, thick slurry liquid preparation and reconstituted tobacco molding.Reconstituted tobacco prepared by the present invention is suitable for heating the fragrant section of incombustible production, with big smoke amount, fragrance is abundant and physiology meets by force, it inhales taste and natural tobacco is close, close to natural tobacco, machining property is good for product density and Filling power, generates in production without waste water, raw material availability is high, meet energy conservation and environmental protection requirement, simple production process is suitble to industrialized production.

Description

A kind of ultra micro tobacco powder reconstituted tobacco and preparation method thereof
[technical field]
The invention belongs to tobacco leaf production technical fields.More particularly it relates to a kind of ultra micro tobacco powder reconstituted tobacco, also It is related to the preparation method of the ultra micro tobacco powder reconstituted tobacco.
[background technique]
It is generated largely in tobacco processing course, such as in beating and double roasting, loosening and gaining moisture, Primary Processing, seaming operation Tobacco cut, offal, offal, tobacco business often recycles processing to improve these raw material availabilities and economic benefit, is made Widely known reconstituted tobacco, the reconstituted tobacco technique being currently known have roll-in method, thick slurry method, wet papermaking, the dry method of paper-making.
Currently, the heating of commercial type is not burnt, cigarette produces fragrant section material and mainly uses paper process thin slice, dry method thin slice Equal materials, this fragrant section raw material availability of classification production is low, and raw material is unstable, and the fragrance of product and style is caused to change, and And the fragrant material fumes amount of these productions is small, fragrance is weak, and satisfaction is weaker, and technique is cumbersome;Thick slurry method is to crush raw material, mix Afterwards, a certain proportion of efficient binder is added, is equably sprayed on stainless steel band after being sufficiently stirred, forms reconstituted tobacoo. Raw material effective rate of utilization is increased to 90.3% from 52.7%, and reconstituted tobacoo fragrance, suction taste and the natural tobacco of thick slurry method production connect Closely, close to natural tobacco, machining property is good for product density and Filling power, releasing content of coke tar lower than natural tobacco 25%.
Therefore, for many technological deficiencies of the prior art, tobacco leaf formulation of the present inventor by adjusting thick slurry method, smoke Formula has carried out a large amount of test and analysis, has completed the present invention finally.
[summary of the invention]
[technical problems to be solved]
The object of the present invention is to provide a kind of ultra micro tobacco powder reconstituted tobaccos.
It is a further object to provide the preparation methods of the ultra micro tobacco powder reconstituted tobacco.
[technical solution]
The present invention is achieved through the following technical solutions.
The present invention relates to a kind of ultra micro tobacco powder reconstituted tobacco preparation methods.
The step of ultra micro tobacco powder reconstituted tobacco preparation method, is as follows:
A, external source fiber cuts fibre
According to weight ratio 2~8:200~500 of external source fiber and water, external source fiber is added in water, then with cutting fine machine It carries out cutting fibre, obtains a kind of fiber slurry, using the measurement standard method measurement of GB3332-1982 slurry pulping degree, the fibre The beating degree for tieing up slurry is 25~30 ° of SR;
B, prepared by thick slurry liquid
Weigh 70~90 parts by weight ultra micro tobacco powder, 2~5 parts by weight binders, 10~30 parts by weight smoke agents, 0.1~2.0 Parts by weight of phosphoric acid hydrogen diammonium and 0.05~1.0 parts by weight amino acid are uniformly mixed, are then added to the external source fiber obtained in step A To be stirred 15~20min in the fiber slurry of 2~8 parts by weight, obtained thick slurry liquid is deaerated under vacuum until not going out again Existing bubble;
C, reconstituted tobacco forms
The degassing thick slurry liquid that step B is obtained uniformly is spread and is dispersed on steel band, is then heated to 40 DEG C of temperature, and in this temperature Degree is lower to keep 5~8min, its thick slurry liquid that deaerates is made to be shaped to thin slice;Then the thin slice is heated to 80 DEG C of temperature, until thin Heating stops when piece water content is by weight 8%, is cooled to room temperature, allows the thin slice resurgence of heat treatment to reach water content and is By weight 12~14%, resurgence thin slice is removed with scraper, obtains the ultra micro tobacco powder reconstituted tobacco.
A preferred embodiment of the invention, in step, the external source fiber are one or more are selected from The external source fiber of bamboo pulp fiber, wood pulp cellulose or sugarcane fibre.
According to another preferred method of implementation of the present invention, in step, the external source fiber revolving speed 200~ 20~40min of fibre is cut under conditions of 400r/min.
According to another preferred method of implementation of the present invention, in stepb, the ultra micro tobacco powder is one or more choosings From flue-cured tobacco raw material, Turkish tobaccos, burley tobaccos or the ultra micro tobacco powder for drying cigarette that granularity is 80~300 mesh.
According to another preferred method of implementation of the present invention, in stepb, the binder is one or more is selected from Guar gum, chitosan, CMC, converted starch, sodium alginate or shellac binder.
According to another preferred method of implementation of the present invention, in stepb, the smoke agent is one or more is selected from Propylene glycol, glycerine, single triacetin, two acetoglycerides or triacetyl glycerine smoke agent.
According to another preferred method of implementation of the present invention, in stepb, the amino acid be alanine, leucine, Phenylalanine, proline, tryptophan, tyrosine, asparagine, lysine or histidine.
According to another preferred method of implementation of the present invention, in stepb, the thick slurry liquid obtained is -0.1 in vacuum degree It is de-gassed under conditions of~-0.01MPa.
The invention further relates to the ultra micro tobacco powder reconstituted tobaccos that the ultra micro tobacco powder reconstituted tobacco preparation method is prepared.
A preferred embodiment of the invention, the ultra micro tobacco powder reconstituted tobacco have following physical characteristics:
0.2~0.4mm of thickness;
100~300g/m of grammes per square metre2
300~700N/m of tensile strength.
The present invention is described in more detail below.
The present invention relates to a kind of ultra micro tobacco powder reconstituted tobacco preparation methods.
The step of ultra micro tobacco powder reconstituted tobacco preparation method, is as follows:
A, external source fiber cuts fibre
According to weight ratio 2~8:200~500 of external source fiber and water, external source fiber is added in water, then with cutting fine machine It carries out cutting fibre, obtains a kind of fiber slurry, using the measurement standard method measurement of GB3332-1982 slurry pulping degree, the fibre The beating degree for tieing up slurry is 25~30 ° of SR;
According to the present invention, the external source fiber is one or more selected from bamboo pulp fiber, wood pulp cellulose or sugarcane fibre External source fiber.Bamboo pulp fiber, wood pulp cellulose or the sugarcane fibre is all current market sales of bamboo pulp, wood pulp or sweet Sugarcane slurry product is cut obtained by fibre by cutting fine machine.
In the present invention, the dosage of water be 200~500 when, if the dosage of external source fiber less than 2, fiber in thin slice Less, tensile strength reduces;If the dosage of external source fiber is greater than 8, fiber disperses unevenness in water, causes the thickness of thin slice Homogeneity is poor;Therefore, it is reasonably preferably 3~6 that the dosage of external source fiber, which is 2~8,;
Similarly, when the dosage of external source fiber is 2~8, if the dosage of water is less than 200, slurry concentration is higher, unfavorable Slurry is laid in steel band;If the dosage of water is greater than 500, slurry concentration is reduced, and is easy out during thin slice drying forming It splits, influences thin slice appearance and quality;Therefore, it is suitably preferably 300~400 that the dosage of water, which is 200~500,;
In the present invention, the external source fiber is carried out using cutting fine machine under conditions of 200~400r/min of revolving speed Cut 20~40min of fibre.In the present invention, if the revolving speed for cutting fine machine is lower than 200r/min, long fibre ratio is higher, and length is fine It is poor to tie up uniformity, influences the physical property of thin slice;If the revolving speed for cutting fine machine is higher than 400r/min, staple fiber ratio is higher, Long and short fiber uniformity is poor, influences the physical property of thin slice;Then cut fine machine revolving speed be 200~400r/min be it is feasible, Preferably 260~340r/min;Herein, if cutting the fine time lower than 20min, there is fiber flocculation, it is difficult to uniformly divide It dissipates in slurry, influences thin slice physical qualities;If cutting the fine time is longer than 40min, fibre debris can be made to increase, be unfavorable for thin slice Molding;Cut so the fine time be 20~40min be appropriate, preferably 25~35min;
Beating degree is to measure the index of pulp suspension performance in water.It is measured and is marked using GB3332-1982 slurry pulping degree Quasi- method measurement, the beating degree of fiber slurry of the present invention are 25~30 ° of SR.If the beating degree of fiber slurry of the present invention is less than 25 ° of SR, then fiber water retention property is poor, has cracked in drying course;If the beating degree of fiber slurry of the present invention is higher than 30 ° SR, then fiber water retention property is preferable, and drying time is elongated;Therefore, it is to close that the beating degree of fiber slurry of the present invention, which is 25~30 ° of SR, Suitable;
It is current market sales of product that the present invention used, which cuts fine machine, for example, by Dongguan City clean brook Ge Tai machinery plant with The product of trade name fiber dispersion machine sale.
B, prepared by thick slurry liquid
Weigh 70~90 parts by weight ultra micro tobacco powder, 2~5 parts by weight binders, 10~30 parts by weight smoke agents, 0.1~2.0 Parts by weight of phosphoric acid hydrogen diammonium and 0.05~1.0 parts by weight amino acid are uniformly mixed, are then added to the external source fiber obtained in step A To be stirred 15~20min in the fiber slurry of 2~8 parts by weight, obtained thick slurry liquid is deaerated under vacuum until not going out again Existing bubble;
In the present invention, the ultra micro tobacco powder is one or more flue-cured tobacco raw material, perfume (or spice) selected from granularity for 80~300 mesh Expect cigarette, burley tobaccos or the ultra micro tobacco powder for drying cigarette.
In the present invention, the flue-cured tobacco raw material is it should be understood that the tobacco leaf through overbaking, such as Qujing flue-cured tobacco;Described Turkish tobaccos it should be understood that safflower tobacco (Nicotianatobacum) a kind of special tobacco type.Since Turkish tobaccos are with dense Yu Fangxiang and pure jealous quality characteristic, there is special application value in tobacco product, are production mixed types, outer odor type With one of oriental type cigarette and the important source material of pipe tobacco.Especially blended type cigarette is sufficient with strength, taste is dense, materials are extensive, can Tar content is effectively reduced to mitigate smoking to the harmful characteristics of human health, the deep favor by smoker becomes and works as this life The cigarette type of boundary's prevalence, such as Baoshan Turkish tobaccos;The burley tobaccos are it should be understood that tobacco leaf passes through made of Air-curing Cigarette, such as American Burley tobacco;The sunning cigarette dries in the air it should be understood that shining system, system of drying in the air or solarization under field conditions (factors) and combines method The tobacco leaf of modulation, such as Shaanxi dry cigarette.
In the present invention, using disintegrating apparatus and screening plant usually used in the art by these raw material tobacco powder It is broken to obtain the ultra micro tobacco powder that granularity is 80~300 mesh.The granularity of this ultra micro tobacco powder is more than that the particle size range is undesirable , because tobacco powder granularity is less than 80 mesh, sheet surface is relatively rough, and granularity is greater than 300 mesh, then will increase the dosage of tobacco powder.
In the present invention, binder is to increase slurry preparing the main function in ultra micro tobacco powder reconstituted tobacco of the present invention Viscosity improves the tensile strength of thin slice.
The binder that the present invention uses is one or more selected from guar gum, chitosan, CMC, converted starch, sodium alginate Or the binder of shellac.They are all current market sales of products, for example, by Jinan Guo Shi great achievement Chemical Co., Ltd. with Trade name height glues the guar gum of guar gum sale, the carboxymethyl sold by the municipal day Chemical Co., Ltd. of Renqiu with trade name CMC Cellulose, the converted starch sold by Shandong Ya Heng Biotechnology Co., Ltd with trade name starch.
In the present invention, smoke agent is to provide amount of smoke in the main function prepared in ultra micro tobacco powder reconstituted tobacco of the present invention With elution flue gas.
The smoke agent that the present invention uses is one or more sweet selected from propylene glycol, glycerine, single triacetin, two acetic acid The smoke agent of grease or triacetyl glycerine.They are all current market sales of products, such as close mesophytization by Wuhan City Single triacetin that Manufacturing Co., Ltd is sold with trade name monoglyceride, by Yixing City Yong Jia Chemical Co., Ltd. with trade name The triacetyl glycerine of triglyceride sale.
In the present invention, amino acid is and ultra micro tobacco powder in the main function prepared in ultra micro tobacco powder reconstituted tobacco of the present invention Carry out Maillard reaction.
The amino acid that the present invention uses is alanine, leucine, phenylalanine, proline, tryptophan, tyrosine, asparagus fern Amide, lysine or histidine.They are all current market sales of products.
In the present invention, when the dosage of other raw materials is in the range, if the dosage of ultra micro tobacco powder is lower than 70 weight Part, then when thin slice aspirates, cigarette perfume is weak;If the dosage of ultra micro tobacco powder is higher than 90 parts by weight, slurry concentration increases, is unfavorable for Uniformly paving dissipates in steel band;Therefore, it is feasible that the dosage of ultra micro tobacco powder, which is 70~90 parts by weight,;Preferably 76~84 weight Part.
When the dosage of other raw materials is in the range, if the dosage of binder is lower than 2 parts by weight, the anti-tensile of thin slice Strength reduction is unfavorable for upper machine;If the dosage of binder is higher than 5 parts by weight, slurry concentration is increased, and is unfavorable for uniformly spreading scattered In steel band;Therefore, it is appropriate, preferably 2.6~4.2 parts by weight that the dosage of binder, which is 2~5 parts by weight,.
When the dosage of other raw materials is in the range, if the dosage of smoke agent be lower than 10 parts by weight, smoke amount compared with It is few;If the dosage of smoke agent is higher than 30 parts by weight, water mist sense is stronger in flue gas, influences to aspirate mouthfeel;Therefore, smoke agent Dosage is that 10~30 parts by weight are suitable, preferably 15~24 parts by weight.
When the dosage of other raw materials is in the range, if the dosage of diammonium hydrogen phosphate is lower than 0.1 parts by weight, thin slice Pectin breath is serious when suction;If the dosage of diammonium hydrogen phosphate is higher than 2.0 parts by weight, chemistry breath is tight when thin slice aspirates Weight;Then, it is appropriate, preferably 0.6~1.4 parts by weight that the dosage of diammonium hydrogen phosphate, which is 0.1~2.0 parts by weight,.
When the dosage of other raw materials is in the range, if the dosage of amino acid is lower than 0.05 parts by weight, U.S. ladd Reaction is incomplete;If the dosage of amino acid is higher than 1.0 parts by weight, protein breath is serious in flue gas;Therefore, amino acid Dosage is that 0.05~1.0 parts by weight are appropriate, preferably 0.12~0.84 parts by weight.
It is thin if the dosage of step A fiber slurry is lower than 2 parts by weight when the dosage of other raw materials is in the range Fiber is less in piece, and tensile strength reduces;If the dosage of step A fiber slurry is higher than 8 parts by weight, then fiber divides in water Unevenness is dissipated, causes the caliper uniformity of thin slice poor;Therefore, the dosage of step A fiber slurry be 2~8 parts by weight be it is suitable, Preferably 3~7 parts by weight.
In this step, by ultra micro tobacco powder, binder, smoke agent, diammonium hydrogen phosphate, amino acid and step A fiber pulp The thick slurry liquid that body obtains is de-gassed until there is not bubble under conditions of vacuum degree is -0.1~-0.01MPa, and purpose exists Stomatal number during reducing slice forming.
C, reconstituted tobacco forms
The degassing thick slurry liquid that step B is obtained uniformly is spread and is dispersed on steel band, is then heated to 40 DEG C of temperature, and in this temperature Degree is lower to keep 5~8min, its thick slurry liquid that deaerates is made to be shaped to thin slice;Then the thin slice is heated to 80 DEG C of temperature, until thin Heating stops when piece water content is by weight 8%, is cooled to room temperature, allows the thin slice resurgence of heat treatment to reach water content and is By weight 12~14%, resurgence thin slice is removed with scraper, obtains the ultra micro tobacco powder reconstituted tobacco.
In this step, the heat treatment thin slice being cooled to room temperature is in cold wind blast apparatus in 22 ± 1 DEG C of temperature and phase To carrying out resurgence processing under conditions of humidity 60 ± 3%.The thin slice water content of resurgence processing is according to GBT 23357-2009 cigarette What the measurement Karl_Fischer method standard method of grass and tobacco product moisture measured.The thin slice water content control of resurgence processing exists It 12~14% is very important by weight, because thin slice is easy to process within the scope of this moisture.
The invention further relates to the ultra micro tobacco powder reconstituted tobaccos that the ultra micro tobacco powder reconstituted tobacco preparation method is prepared.
It is analyzed according to YCT 16.2-2002 reconstituted tobacco part 2 thick slurry method standard method, the ultra micro tobacco powder reproduces cigarette Leaf has following physical characteristics:
0.2~0.4mm of thickness;
100~300g/m of grammes per square metre2
300~700N/m of tensile strength.
[beneficial effect]
The beneficial effects of the present invention are:
Reconstituted tobacco prepared by the present invention is suitable for heating the fragrant section of incombustible productions, have big smoke amount, fragrance enrich and Physiology meets by force, inhales taste and natural tobacco is close, close to natural tobacco, machining property is good for product density and Filling power, raw It is generated in production without waste water, raw material availability is high, meets energy conservation and environmental protection requirement, and simple production process is suitble to industrialized production.
[specific embodiment]
It will be better understood that the present invention by following embodiments.
Embodiment 1: ultra micro tobacco powder reconstituted tobacco is prepared
The ultra micro tobacco powder reconstituted tobacco preparation step is as follows:
A, external source fiber cuts fibre
According to the weight ratio 4:400 of external source fiber and water, bamboo pulp fiber external source fiber is added in water, then with by Dongguan Fibre is cut under conditions of revolving speed 300r/min with the fine machine of cutting that trade name fiber dispersion machine is sold by city clean brook Ge Tai machinery plant 30min obtains a kind of fiber slurry, using the measurement standard method measurement of GB3332-1982 slurry pulping degree, the fiber pulp The beating degree of body is 25 ° of SR;
B, prepared by thick slurry liquid
Weigh flue-cured tobacco raw material ultra micro tobacco powder, the 4 parts by weight guar gum binders, 26 weight that 78 parts by weight granularities are 200 mesh Part propylene glycol smoke agent, 0.1 parts by weight of phosphoric acid hydrogen diammonium and 0.8 parts by weight alanine amino acid, are uniformly mixed, are then added in step The external source fiber that rapid A is obtained is to be stirred 15min, obtained thick slurry liquid is again in vacuum degree in the fiber slurry of 6 parts by weight It is degassing under conditions of -0.1MPa until there is not bubble;
C, reconstituted tobacco forms
The degassing thick slurry liquid that step B is obtained uniformly is spread and is dispersed on steel band, is then heated to 40 DEG C of temperature, and in this temperature Degree is lower to keep 6min, its thick slurry liquid that deaerates is made to be shaped to thin slice;Then
The thin slice is heated to 80 DEG C of temperature, until heating stops when thin slice water content is by weight 8%, then is cooled down To room temperature, allowing the thin slice resurgence of heat treatment to reach water content is by weight 12.0%, removes resurgence thin slice with scraper, obtains The ultra micro tobacco powder reconstituted tobacco.
Using the standard method detection of this specification description, the ultra micro tobacco powder reconstituted tobacco of embodiment preparation has following Physical characteristic:
Thickness 0.2mm;
Grammes per square metre 230g/m2
Tensile strength 620N/m.
Embodiment 2: ultra micro tobacco powder reconstituted tobacco is prepared
The ultra micro tobacco powder reconstituted tobacco preparation step is as follows:
A, external source fiber cuts fibre
According to the weight ratio 6:300 of external source fiber and water, wood pulp cellulose external source fiber is added in water, then with by Dongguan Fibre is cut under conditions of revolving speed 250r/min with the fine machine of cutting that trade name fiber dispersion machine is sold by city clean brook Ge Tai machinery plant 35min obtains a kind of fiber slurry, using the measurement standard method measurement of GB3332-1982 slurry pulping degree, the fiber pulp The beating degree of body is 26 ° of SR;
B, prepared by thick slurry liquid
Weigh Turkish tobaccos ultra micro tobacco powder, the 2 parts by weight chitosan binders, 14 parts by weight third that 82 parts by weight granularities are 80 mesh Triol smoke agent, 2.0 parts by weight of phosphoric acid hydrogen diammoniums and 1.0 parts by weight leucine amino acid are uniformly mixed, are then added in step A Obtained external source fiber be 4 parts by weight fiber slurry in, be stirred 18min, obtained thick slurry liquid again vacuum degree be- Degassing is not until there is bubble under conditions of 0.02MPa;
C, reconstituted tobacco forms
The degassing thick slurry liquid that step B is obtained uniformly is spread and is dispersed on steel band, is then heated to 40 DEG C of temperature, and in this temperature Degree is lower to keep 8min, its thick slurry liquid that deaerates is made to be shaped to thin slice;Then
The thin slice is heated to 80 DEG C of temperature, until heating stops when thin slice water content is by weight 8%, then is cooled down To room temperature, allowing the thin slice resurgence of heat treatment to reach water content is by weight 12.5%, removes resurgence thin slice with scraper, obtains The ultra micro tobacco powder reconstituted tobacco.
Using the standard method detection of this specification description, the ultra micro tobacco powder reconstituted tobacco of embodiment preparation has following Physical characteristic:
Thickness 0.3mm;
Grammes per square metre 100g/m2
Tensile strength 580N/m.
Embodiment 3: ultra micro tobacco powder reconstituted tobacco is prepared
The ultra micro tobacco powder reconstituted tobacco preparation step is as follows:
A, external source fiber cuts fibre
According to the weight ratio 2:200 of external source fiber and water, sugarcane fibre external source fiber is added in water, then with by Dongguan Fibre is cut under conditions of revolving speed 200r/min with the fine machine of cutting that trade name fiber dispersion machine is sold by city clean brook Ge Tai machinery plant 40min obtains a kind of fiber slurry, using the measurement standard method measurement of GB3332-1982 slurry pulping degree, the fiber pulp The beating degree of body is 30 ° of SR;
B, prepared by thick slurry liquid
Weigh burley tobaccos ultra micro tobacco powder, 3 parts by weight CMC binders, the 18 parts by weight list vinegar that 70 parts by weight granularities are 100 mesh Acid glyceride smoke agent, 1.0 parts by weight of phosphoric acid hydrogen diammoniums and 0.05 parts by weight phenylalanine amino acid, are uniformly mixed, are then added to In the fiber slurry that the external source fiber that step A is obtained is 2 parts by weight, it is stirred 20min, obtained thick slurry liquid is again in vacuum Degassing is not until there is bubble under conditions of degree is -0.04MPa;
C, reconstituted tobacco forms
The degassing thick slurry liquid that step B is obtained uniformly is spread and is dispersed on steel band, is then heated to 40 DEG C of temperature, and in this temperature Degree is lower to keep 5min, its thick slurry liquid that deaerates is made to be shaped to thin slice;Then
The thin slice is heated to 80 DEG C of temperature, until heating stops when thin slice water content is by weight 8%, then is cooled down To room temperature, allowing the thin slice resurgence of heat treatment to reach water content is by weight 12.8%, removes resurgence thin slice with scraper, obtains The ultra micro tobacco powder reconstituted tobacco.
Using the standard method detection of this specification description, the ultra micro tobacco powder reconstituted tobacco of embodiment preparation has following Physical characteristic:
Thickness 0.2mm;
Grammes per square metre 120g/m2
Tensile strength 300N/m.
Embodiment 4: ultra micro tobacco powder reconstituted tobacco is prepared
The ultra micro tobacco powder reconstituted tobacco preparation step is as follows:
A, external source fiber cuts fibre
According to the weight ratio 8:200 of external source fiber and water, wood pulp cellulose external source fiber is added in water, then with by Dongguan Fibre is cut under conditions of revolving speed 350r/min with the fine machine of cutting that trade name fiber dispersion machine is sold by city clean brook Ge Tai machinery plant 25min obtains a kind of fiber slurry, using the measurement standard method measurement of GB3332-1982 slurry pulping degree, the fiber pulp The beating degree of body is 28 ° of SR;
B, prepared by thick slurry liquid
Weigh sunning cigarette ultra micro tobacco powder, the 5 parts by weight converted starch binders, 10 weight that 74 parts by weight granularities are 300 mesh Two acetoglyceride smoke agents of part, 0.6 parts by weight of phosphoric acid hydrogen diammonium and 0.2 parts by weight tryptophan amino acid, are uniformly mixed, then plus To in the fiber slurry that the external source fiber that step A is obtained is 8 parts by weight, it is stirred 15min, obtained thick slurry liquid is again true Degassing is not until there is bubble under conditions of reciprocal of duty cycle is -0.06MPa;
C, reconstituted tobacco forms
The degassing thick slurry liquid that step B is obtained uniformly is spread and is dispersed on steel band, is then heated to 40 DEG C of temperature, and in this temperature Degree is lower to keep 6min, its thick slurry liquid that deaerates is made to be shaped to thin slice;Then
The thin slice is heated to 80 DEG C of temperature, until heating stops when thin slice water content is by weight 8%, then is cooled down To room temperature, allowing the thin slice resurgence of heat treatment to reach water content is by weight 13.2%, removes resurgence thin slice with scraper, obtains The ultra micro tobacco powder reconstituted tobacco.
Using the standard method detection of this specification description, the ultra micro tobacco powder reconstituted tobacco of embodiment preparation has following Physical characteristic:
Thickness 0.4mm;
Grammes per square metre 180g/m2
Tensile strength 700N/m.
Embodiment 5: ultra micro tobacco powder reconstituted tobacco is prepared
The ultra micro tobacco powder reconstituted tobacco preparation step is as follows:
A, external source fiber cuts fibre
According to the weight ratio 5:300 of external source fiber and water, bamboo pulp fiber external source fiber is added in water, then with by Dongguan Fibre is cut under conditions of revolving speed 400r/min with the fine machine of cutting that trade name fiber dispersion machine is sold by city clean brook Ge Tai machinery plant 20min obtains a kind of fiber slurry, using the measurement standard method measurement of GB3332-1982 slurry pulping degree, the fiber pulp The beating degree of body is 27 ° of SR;
B, prepared by thick slurry liquid
Weigh the Turkish tobaccos and burley tobaccos mixture (weight ratio 2:1) ultra micro tobacco powder, 3 weights that 90 parts by weight granularities are 150 mesh Measure part sodium alginate binder, 30 parts by weight triacetyl glycerine smoke agents, 1.2 parts by weight of phosphoric acid hydrogen diammoniums and 0.4 parts by weight Amino acid asparagine is uniformly mixed, and is then added in the fiber slurry that the external source fiber that step A is obtained is 5 parts by weight, stirring 18min is mixed, obtained thick slurry liquid deaerates under conditions of vacuum degree is -0.08MPa until there is not bubble again;
C, reconstituted tobacco forms
The degassing thick slurry liquid that step B is obtained uniformly is spread and is dispersed on steel band, is then heated to 40 DEG C of temperature, and in this temperature Degree is lower to keep 7min, its thick slurry liquid that deaerates is made to be shaped to thin slice;Then
The thin slice is heated to 80 DEG C of temperature, until heating stops when thin slice water content is by weight 8%, then is cooled down To room temperature, allowing the thin slice resurgence of heat treatment to reach water content is by weight 13.6%, removes resurgence thin slice with scraper, obtains The ultra micro tobacco powder reconstituted tobacco.
Using the standard method detection of this specification description, the ultra micro tobacco powder reconstituted tobacco of embodiment preparation has following Physical characteristic:
Thickness 0.3mm;
Grammes per square metre 260g/m2
Tensile strength 410N/m.
Embodiment 6: ultra micro tobacco powder reconstituted tobacco is prepared
The ultra micro tobacco powder reconstituted tobacco preparation step is as follows:
A, external source fiber cuts fibre
According to the weight ratio 7:500 of external source fiber and water, outside bamboo pulp fiber and wood pulp cellulose mixture (weight ratio 1:1) Source fiber is added in water, is then being turned with by Dongguan City clean brook Ge Tai machinery plant with the fine machine of cutting that trade name fiber dispersion machine is sold Fine 30min is cut under conditions of fast 300r/min, obtains a kind of fiber slurry, is measured and is marked using GB3332-1982 slurry pulping degree Quasi- method measurement, the beating degree of the fiber slurry are 28 ° of SR;
B, prepared by thick slurry liquid
Weigh the flue-cured tobacco raw material and sunning cigarette mixture (weight ratio 1:1) ultra micro tobacco powder, 4 that 86 parts by weight granularities are 250 mesh Parts by weight shellac binder, 22 parts by weight triacetyl glycerine smoke agents, 1.5 parts by weight of phosphoric acid hydrogen diammoniums and 0.6 parts by weight group Valine amino acid is uniformly mixed, and is then added in the fiber slurry that the external source fiber that step A is obtained is 7 parts by weight, is stirred 20min, obtained thick slurry liquid deaerate under conditions of vacuum degree is -0.01MPa until there is not bubble again;
C, reconstituted tobacco forms
The degassing thick slurry liquid that step B is obtained uniformly is spread and is dispersed on steel band, is then heated to 40 DEG C of temperature, and in this temperature Degree is lower to keep 8min, its thick slurry liquid that deaerates is made to be shaped to thin slice;Then
The thin slice is heated to 80 DEG C of temperature, until heating stops when thin slice water content is by weight 8%, then is cooled down To room temperature, allowing the thin slice resurgence of heat treatment to reach water content is by weight 14.0%, removes resurgence thin slice with scraper, obtains The ultra micro tobacco powder reconstituted tobacco.
Using the standard method detection of this specification description, the ultra micro tobacco powder reconstituted tobacco of embodiment preparation has following Physical characteristic:
Thickness 0.4mm;
Grammes per square metre 300g/m2
Tensile strength 360N/m.

Claims (10)

1. a kind of ultra micro tobacco powder reconstituted tobacco preparation method, it is characterised in that the step of preparation method is as follows
A, external source fiber cuts fibre
According to weight ratio 2~8:200~500 of external source external source fiber and water, external source fiber is added in water, then with cutting fine machine It carries out cutting fibre, obtains a kind of fiber slurry, using the measurement standard method measurement of GB3332-1982 slurry pulping degree, the fibre The beating degree for tieing up slurry is 25~30 ° of SR;
B, prepared by thick slurry liquid
Weigh 70~90 parts by weight ultra micro tobacco powder, 2~5 parts by weight binders, 10~30 parts by weight smoke agents, 0.1~2.0 weight Part diammonium hydrogen phosphate and 0.05~1.0 parts by weight amino acid are uniformly mixed, be then added to the external source fiber that obtains in step A for 2~ In the fiber slurry of 8 parts by weight, it is stirred 15~20min, obtained thick slurry liquid is deaerated under vacuum until there is not gas again Bubble
C, reconstituted tobacco forms
The degassing thick slurry liquid that step B is obtained uniformly is spread and is dispersed on steel band, is then heated to 40 DEG C of temperature, and at this temperature 5~8min is kept, its thick slurry liquid that deaerates is made to be shaped to thin slice;Then
The thin slice is heated to 80 DEG C of temperature, until heating stops when thin slice water content is by weight 8%, is cooled to room Temperature, allowing the thin slice resurgence of heat treatment to reach water content is by weight 12~14%, removes resurgence thin slice with scraper, obtains institute The ultra micro tobacco powder reconstituted tobacco stated.
2. ultra micro tobacco powder reconstituted tobacco preparation method according to claim 1, it is characterised in that in step, described External source fiber is one or more a variety of external source fibers selected from bamboo pulp fiber, wood pulp cellulose or sugarcane fibre.
3. ultra micro tobacco powder reconstituted tobacco preparation method according to claim 1, it is characterised in that in step, described External source fiber cuts 20~40min of fibre under conditions of 200~400r/min of revolving speed.
4. ultra micro tobacco powder reconstituted tobacco preparation method according to claim 1, it is characterised in that in stepb, described Ultra micro tobacco powder is one or more selected from flue-cured tobacco raw material, Turkish tobaccos, burley tobaccos or the ultra micro for drying cigarette that granularity is 80~300 mesh Tobacco powder.
5. ultra micro tobacco powder reconstituted tobacco preparation method according to claim 1, it is characterised in that in stepb, described Binder is one or more binders selected from guar gum, chitosan, CMC, converted starch, sodium alginate or shellac.
6. ultra micro tobacco powder reconstituted tobacco preparation method according to claim 1, it is characterised in that in stepb, described Smoke agent is one or more selected from propylene glycol, glycerine, single triacetin, two acetoglycerides or triacetyl glycerine Smoke agent.
7. ultra micro tobacco powder reconstituted tobacco preparation method according to claim 1, it is characterised in that in stepb, described Amino acid is alanine, leucine, phenylalanine, proline, tryptophan, tyrosine, asparagine, lysine or histidine.
8. ultra micro tobacco powder reconstituted tobacco preparation method according to claim 1, it is characterised in that in stepb, obtain Thick slurry liquid is de-gassed under conditions of vacuum degree is -0.1~-0.01MPa.
9. what ultra micro tobacco powder reconstituted tobacco preparation method described in any one of -8 claims was prepared according to claim 1 is super Micro- tobacco powder reconstituted tobacco.
10. ultra micro tobacco powder reconstituted tobacco according to claim 9, it is characterised in that the ultra micro tobacco powder reconstituted tobacco has Following physical characteristics:
0.2~0.4mm of thickness;
100~300g/m of grammes per square metre2
300~700N/m of tensile strength.
CN201811476687.0A 2018-12-05 2018-12-05 Ultramicro tobacco powder reconstituted tobacco and preparation method thereof Active CN109349677B (en)

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CN110680024A (en) * 2019-10-10 2020-01-14 黑龙江黑科科技有限责任公司 Preparation method of cannabis electronic tobacco shreds and cannabis electronic cigarette cartridge
CN110742295A (en) * 2019-10-10 2020-02-04 黑龙江黑科科技有限责任公司 Preparation method of hemp cut tobacco and hemp cigarette thereof
CN110839935A (en) * 2019-11-28 2020-02-28 江苏中烟工业有限责任公司 Production method of reconstituted tobacco special for heating cigarettes
CN112641125A (en) * 2021-01-08 2021-04-13 中烟施伟策(云南)再造烟叶有限公司 Paper filter tip rod of reconstituted tobacco and preparation method of filter tip rod

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CN101011182A (en) * 2007-02-16 2007-08-08 湖南中烟工业公司 Method for producing tobacco sheets by improved papermaking method
CN107647468A (en) * 2017-10-13 2018-02-02 浙江泽源植物科技有限公司 A kind of method that reconstituted tobacoo is prepared using fennel seeds stalk as raw material
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CN1043184C (en) * 1997-03-13 1999-05-05 开封汽车配件厂 Method and equipment of blending moistening fibre into rolled tobacco sheet
DE10355394A1 (en) * 2003-11-25 2005-06-30 Hauni Primary Gmbh Rutscheinrichtung for a tobacco cache
CN101011182A (en) * 2007-02-16 2007-08-08 湖南中烟工业公司 Method for producing tobacco sheets by improved papermaking method
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CN110680024A (en) * 2019-10-10 2020-01-14 黑龙江黑科科技有限责任公司 Preparation method of cannabis electronic tobacco shreds and cannabis electronic cigarette cartridge
CN110742295A (en) * 2019-10-10 2020-02-04 黑龙江黑科科技有限责任公司 Preparation method of hemp cut tobacco and hemp cigarette thereof
CN110839935A (en) * 2019-11-28 2020-02-28 江苏中烟工业有限责任公司 Production method of reconstituted tobacco special for heating cigarettes
CN112641125A (en) * 2021-01-08 2021-04-13 中烟施伟策(云南)再造烟叶有限公司 Paper filter tip rod of reconstituted tobacco and preparation method of filter tip rod

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