CN109602074A - A kind of cigarette Alevaire and the method for improving traditional tobacco leaf Alevaire uptake - Google Patents

A kind of cigarette Alevaire and the method for improving traditional tobacco leaf Alevaire uptake Download PDF

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Publication number
CN109602074A
CN109602074A CN201811558960.4A CN201811558960A CN109602074A CN 109602074 A CN109602074 A CN 109602074A CN 201811558960 A CN201811558960 A CN 201811558960A CN 109602074 A CN109602074 A CN 109602074A
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China
Prior art keywords
alevaire
tobacco leaf
cigarette
steam
leaf
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Pending
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CN201811558960.4A
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Chinese (zh)
Inventor
杨俊鹏
王昊
庞哲
张耀华
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Priority to CN201811558960.4A priority Critical patent/CN109602074A/en
Publication of CN109602074A publication Critical patent/CN109602074A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances

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  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The present invention provides a kind of cigarette Alevaire and improves the method that traditional tobacco leaf Alevaire absorbs.The cigarette is to be mixed by D-sorbite, glycerol, glycerine, triethylene-glycol diacetate, methyl stearate, dodecanedioic acid dimethyl ester according to mass ratio 1:10~20:10~20:5~10:2~6:0.6~1.0 ratio with Alevaire.Will be formulated tobacco leaf after mixing in 30 DEG C~50 DEG C, steam blasting time less than 0.01 second, steam pressure in 0.4MPa~0.8Mpa, pressure retention time is Steam explosion treatment under conditions of 10~60 seconds, prepared Alevaire is spread in tobacco leaf rapidly after the completion of processing, it is then sent to leaf storing cabinet, equilibrium water conten takes out after fully absorbing and carries out preparation silk.The present invention can greatly improve the Alevaire additive amount of traditional tobacco leaf, allow to for heating in the cigarette that do not burn.

Description

A kind of cigarette Alevaire and the method for improving traditional tobacco leaf Alevaire uptake
Technical field
The invention belongs to heat tobacco product technical field of not burning, and in particular to a kind of cigarette Alevaire and improve tradition The method of tobacco leaf Alevaire uptake.
Background technique
Low temperature cigarette also makes heating not burn cigarette (heat-not-burn cigarette), by external heat source to cigarette Careless substance is heated, and the atomizing medium, flavor component and outer flavoring in tobacco material are generated by heating and be similar to conventional roll The smog that cigarette is burnt and sucked makes consumer obtain physiology satisfaction.
Incombustible characteristic is only heated due to having when its suction, heating temperature is generally below 350 DEG C, therefore amount of smoke It is small, fragrance is insufficient, poor sensory experience is that existing heating is not burnt tobacco product common problem.Usually added by improving Heat does not burn the Alevaire ratio in tobacco product to promote amount of smoke.The most common method is incited somebody to action based on tobacco component Reconstituted tobacco is made after crushing in it, while loading Alevaire of the large dosage based on glycerol and propylene glycol, and then pass through cigarette Cigarette of not burning is heated in technique processing preparation.
In recent years, deeply many patents also expand research for this direction with research.Patent CN 105768191 A are manufactured paper with pulp by paper process prepares tobacco chip base, is then coated flavoring and dry be prepared into can smoking products.Specially It is compound that propylene glycol, glycerol, curing agent, sodium benzoate, essence spice for cigarette and water are mixed into colloidal by sharp CN 104824830A Alevaire is allowed to be adhered to tobacco product surface, to improve the amount of smoke that the tobacco product does not burn on smoking set in heating.Specially Sharp CN 106723282A by using the porous tobacco stem shred uptake improved to Alevaire in the feed, to improve product Smoke yields.But above-mentioned patent and in the prior art raw tobacco material are under normal conditions to the absorbability of Alevaire Poor, traditional raw tobacco material can not improve the absorption or load capacity of Alevaire.Therefore, it is former in traditional tobacco leaf how to solve Alevaire The assimilation ratio of material is allowed to that big amount of smoke and existing production technology can be generated in heating the smoking set that do not burn, is still The insoluble problem of the prior art.
Summary of the invention
In order to solve the above technical problems, the present invention provide a kind of cigarette Alevaire dedicated in traditional raw tobacco material and The method for improving traditional tobacco leaf Alevaire uptake, the present invention form a kind of atomization by the way that many kinds of substance is optimized compounding Agent guarantees that Alevaire is heated under conditions of smoke, reduces the viscosity of Alevaire, is allowed to be easier to absorb for tobacco leaf, quick-fried using steam Broken technology pre-processes tobacco leaf, under high temperature, high steam effect, expands the gas play in tobacco leaf internal void, utilizes Tobacco leaf rises again rapidly and quickly absorbs Alevaire when being in structure swelling state, allows Alevaire well into tobacco leaf surface In stomata, realize that tobacco leaf largely absorbs the purpose of Alevaire.
In order to achieve the above objects and other related objects, a kind of cigarette Alevaire provided by the invention, it is characterised in that: institute It is by D-sorbite, glycerol, glycerine, triethylene-glycol diacetate, methyl stearate, dodecanedioic acid diformazan that cigarette, which is stated, with Alevaire Ester is that 1:10~20:10~20:5~10:2~6:0.6~1.0 ratio is mixed according to mass ratio.
A kind of method improving traditional tobacco leaf Alevaire uptake provided by the invention, it is characterised in that specific steps are such as Under:
(1) Alevaire is prepared: by D-sorbite, glycerol, glycerine, triethylene-glycol diacetate, methyl stearate, dodecane Acid dimethyl is that 1:10~20:10~20:5~10:2~6:0.6~1.0 ratio is uniformly mixed obtained cigarette use in mass ratio Alevaire;
(2) pre-treatment of tobacco leaf: formula tobacco leaf is uniformly mixed by belt and vibration slot, is delivered in steam blasting equipment Steam explosion treatment is carried out, the temperature of steam blasting is 30 DEG C~50 DEG C, the steam blasting time was less than 0.01 second, steam pressure In 0.4MPa~0.8Mpa, pressure retention time is 10~60 seconds;
(3) preparation absorbs the formula tobacco leaf of Alevaire: the cigarette Alevaire prepared in step (1) is fitted into charging bucket, When being formulated tobacco leaf after Steam explosion treatment, Alevaire is sprayed at rapidly tobacco leaf surface, rises again and locates rapidly using tobacco leaf When structure swelling state, Alevaire is fully absorbed;Wherein the application ratio of the Alevaire is the 15%- of tobacco leaf weight 40%;
(4) the formula tobacco leaf that Alevaire is absorbed in step (3) formula tobacco leaf post-processing: is sent to leaf storing cabinet, equilibrium water Point, fully absorb after take out, and then subsequent routine can be carried out and prepare wire process.
The present invention preferably technical solution: in the step (2), steam blasting working media is saturated steam.
The present invention preferably technical solution: enter its equilibrium temperature in leaf storing cabinet in the step (4) and be 15~25 DEG C, put down The humidity that weighs is 8~12%, equilibration time is 2h~4h.
The use ratio of single variety Alevaire is greatly lowered by the formula composition of optimization Alevaire in the present invention, Guarantee that Alevaire is heated under conditions of smoke, reduce the viscosity of Alevaire, absorbs Alevaire convenient for tobacco leaf;And pass through steam blasting Technology handles traditional tobacco leaf, under high temperature, high steam effect, expands the gas play in tobacco leaf internal void, generates " explosion " effect generates destruction to tobacco leaf internal microstructure, is risen again rapidly using tobacco leaf and is in quick when structure swelling state Alevaire is absorbed, allows Alevaire well into the stomata of tobacco leaf surface, improves the adsorption effect to Alevaire, then lead to Spray plus the excellent atomization feed liquid matched are crossed to increase tobacco leaf Alevaire adsorbance, and passes through the tobacco leaf micro-structure after destroying for tobacco leaf surface Alevaire sucking is intracellular, makes to obtain homogeneous immersion inside and outside tobacco leaf.
Beneficial effects of the present invention:
1. in preferred Alevaire used in this programme, by optimizing the formula composition of Alevaire, single variety is greatly lowered The use ratio of Alevaire reduces the viscosity of Alevaire, absorbs mist convenient for tobacco leaf under conditions of guarantee Alevaire is heated smoke Agent;
2. carrying out pre-treatment to tobacco leaf using steam explosion technology, tobacco leaf internal microstructure can be effectively destroyed;Utilize cigarette Leaf rises again and is in structure swelling state, the Alevaire for being sprayed at surface effectively can be absorbed into tobacco leaf inside configuration;
3. the provided application method of this programme can be avoided and be generallyd use at present effective for existing tobacco leaf processing link The problem of tobacco leaf to be processed into powder and then is prepared into complex procedures present in reconstituted tobacco, waste larger, higher cost.
The present invention utilizes special atomization agent prescription, in conjunction with the steam blasting pre-treatment work to tobacco leaf, substantially increases The uptake of tobacco leaf Alevaire can largely be added to and heat in the cigarette that do not burn, that is, solve the preparation of reconstituted tobacco The problem of at high cost, complex process, and substantially increase heating and do not burn the aesthetic quality of cigarette.
Specific embodiment
In order to better explain the present invention, below in conjunction with specific experiment room embodiment the present invention is furture elucidated it is main in Hold, but the contents of the present invention are not limited solely to following embodiment.
A kind of cigarette provided by the invention is by D-sorbite, glycerol, glycerine, triethylene-glycol diacetate, hard with Alevaire Resin acid methyl esters, dodecanedioic acid dimethyl ester are 1:10~20:10~20:5~10:2~6:0.6~1.0 ratio according to mass ratio Example is mixed.
Below with reference to embodiment, the present invention is further described:
A kind of method for improving traditional tobacco leaf Alevaire of embodiment 1, detailed process is as follows:
(1) Alevaire is prepared first, in accordance with formula as below: weighing sorbose according to mass ratio 1:10:10:7.5:3.5:0.7 Alcohol, glycerol, glycerine, triethylene-glycol diacetate, methyl stearate, dodecanedioic acid dimethyl ester are uniformly mixed and are configured to cigarette use Alevaire A;
(2) 150g tobacco leaf is placed in steam blasting equipment, 40 DEG C of Yu Wendu, pressure 0.6MPa, pressure retention time 15 Steam blasting is carried out under conditions of second;The steam blasting time, pressure retention time was 10~60 seconds less than 0.01 second;Steam blasting Working media is saturated steam;
(3) cigarette prepared in 30g step (1) is taken to be put into charging bucket with Alevaire A, in step (2) at steam blasting After reason, tobacco leaf surface after the cigarette in charging bucket is all sprayed at explosion treatment with Alevaire A rapidly is fast using tobacco leaf When speed rises again and is in structure swelling state, Alevaire is fully absorbed;After fully absorbing Alevaire A, taking-up is placed in constant temperature In constant humidity cabinet, 2h is balanced under conditions of 15 DEG C of Yu Wendu and humidity 9%, then chopping, which rolls into, heats the cigarette A that do not burn.
A kind of method for raising tradition tobacco leaf Alevaire that embodiment 2 provides, detailed process is as follows:
(1) D-sorbite, glycerol, glycerine, 7g triethylene glycol oxalic acid are weighed according to mass ratio 1:15:15:7:3:0.6 Ester, methyl stearate, dodecanedioic acid dimethyl ester are uniformly mixed obtained cigarette Alevaire B;
(2) 100g tobacco leaf is placed in steam blasting equipment, in temperature 45 C, pressure 0.6MPa, pressure retention time 30 Steam blasting is carried out under conditions of second, the steam blasting time, pressure retention time was 10~60 seconds less than 0.01 second;Steam blasting Working media is saturated steam;
(3) cigarette prepared in 30g step (1) is taken to be put into charging bucket with Alevaire B, in step (2) at steam blasting After reason, tobacco leaf surface after the cigarette in charging bucket is all sprayed at explosion treatment with Alevaire B rapidly is fast using tobacco leaf When speed rises again and is in structure swelling state, Alevaire is fully absorbed;After fully absorbing Alevaire B, taking-up is placed in constant temperature In constant humidity cabinet, 3h is balanced under conditions of 18 DEG C of Yu Wendu and humidity 10%, then chopping, which rolls into, heats the cigarette B that do not burn.
A kind of method for raising tradition tobacco leaf Alevaire that embodiment 3 provides, detailed process is as follows:
(1) according to mass ratio 1:20:20:7:3:0.5 weigh D-sorbite, glycerol, glycerine, triethylene-glycol diacetate, Methyl stearate, dodecanedioic acid dimethyl ester are uniformly mixed obtained Alevaire C;
(2) 100g tobacco leaf is placed in steam blasting equipment, in temperature 45 C, pressure 0.8MPa, pressure retention time 40 Steam blasting is carried out under second, the steam blasting time, pressure retention time was 10~60 seconds less than 0.01 second;Steam blasting work is situated between Matter is saturated steam;
(3) cigarette prepared in 35g step (1) is taken to be put into charging bucket with Alevaire C, in step (2) at steam blasting After reason, tobacco leaf surface after the cigarette in charging bucket is all sprayed at explosion treatment with Alevaire C rapidly is fast using tobacco leaf When speed rises again and is in structure swelling state, Alevaire is fully absorbed;After fully absorbing Alevaire C, taking-up is placed in constant temperature In constant humidity cabinet, 3.5h is balanced under conditions of 22 DEG C of Yu Wendu and humidity 10%, then chopping, which rolls into, heats the cigarette C that do not burn.
Reference examples 1: it weighs after 15g glycerol, 15g mixed with propylene glycol uniformly, obtains Alevaire D;Then after 100g tobacco leaf crushes Reconstituted tobacco is conventionally prepared, and Alevaire D is added in process of production, and completes reconstituted tobacco production, in turn Chopping rolls cigarette.
Reference examples 2: it weighs after 20g glycerol, 20g mixed with propylene glycol uniformly, obtains Alevaire E;It is pressed after 100g tobacco leaf is crushed The method of more solito prepares reconstituted tobacco, and Alevaire E is added in process of production, and completes reconstituted tobacco production, and then chopping, Roll cigarette.
Reference examples 3: weighing the Alevaire A in 30g embodiment 1, and conventionally makes after taking 100g tobacco leaf to crush Standby reconstituted tobacco, is added Alevaire A in process of production, and completes reconstituted tobacco production, and then chopping, rolls cigarette.
Reference examples 4: Alevaire E processed is prepared according to the formula of reference examples 2,100g tobacco leaf is then placed in steam blasting equipment In, steam blasting is carried out under conditions of temperature 45 C, pressure 0.6MPa, pressure retention time 30 seconds, the steam blasting time is small In 0.01 second, pressure retention time was 10~60 seconds;Steam blasting working media is saturated steam;At tobacco leaf steam blasting After reason, the tobacco leaf surface for taking 40g cigarette to be placed in charging bucket and be all sprayed at after explosion treatment with Alevaire E rapidly, When rising again rapidly using tobacco leaf and being in structure swelling state, Alevaire is fully absorbed;After fully absorbing Alevaire C, take out It is placed in climatic chamber, balances 3.5h under conditions of 22 DEG C of Yu Wendu and humidity 10%, then chopping rolls into heating not Burn cigarette E.
For the pipe tobacco obtained after three embodiments and four comparative example processing, Alevaire inspection is carried out by gas-chromatography It surveys, theoretical application ratio of the Alevaire on tobacco leaf and actual measurement assimilation ratio are as shown in table 1.
Application ratio of 1 Alevaire of table on tobacco leaf
As shown in Table 1, in reference examples 1 and reference examples 2, raw material is prepared using existing reconstituted tobacco technology, to Alevaire D Poor with the assimilation effect of Alevaire E, the uptake for surveying Alevaire is only 17% or so of tobacco leaf weight, is existed with design object Larger difference.And in embodiment 1-3, the uptake for surveying Alevaire at most can be 32% or so of tobacco leaf weight, much higher than control Example 1 and reference examples 2.Reference examples 1 and reference examples 3 prepare raw material using identical existing reconstituted tobacco technology, phase have been respectively adopted With two kinds of dosage, different Alevaires, assimilation effect of the Alevaire A in current art are substantially better than Alevaire E.2 He of reference examples Reference examples 4 are apparently higher than using the assimilation effect of the Alevaire E pipe tobacco obtained by the treatment process through the invention of same amount Existing reconstituted tobacco technology.
By the pipe tobacco obtained after three embodiments and the processing of four comparative examples be made heating do not burn cigarette finished cigarettes into Row aesthetic quality's overall evaluation, the results are shown in Table 2.
Tobacco leaf is heating the overall evaluation in the smoking set that do not burn after table 2 applies Alevaire
As shown in Table 2, in heating the smoking set that do not burn, cigarette prepared by reference examples is because Alevaire uptake is few, cigarette The amount of smoke generated after Zhi Shoure is medium, demand of the consumer to big smog is unable to satisfy, simultaneously as adding using reconstituted tobacco Work technology can introduce a small amount of wood pulp cellulose and bring uncoordinated wooden miscellaneous gas.In embodiment 1-3, the excellent Alevaire matched, engagement is steamed The use of vapour blasting technique improves the uptake of Alevaire, guarantees that a large amount of Alevaires are atomized rapidly when cigarette is heated, generates a large amount of Smog meets the use demand of consumer, while using conventional smoke filament processing process, and product quality is more preferably.

Claims (4)

1. a kind of cigarette Alevaire, it is characterised in that: the cigarette is by D-sorbite, glycerol, glycerine, triethylene glycol with Alevaire Diacetate esters, methyl stearate, dodecanedioic acid dimethyl ester are 1:10~20:10~20:5~10:2~6 according to mass ratio: 0.6~1.0 ratio is mixed.
2. a kind of method for improving traditional tobacco leaf Alevaire uptake, it is characterised in that specific step is as follows:
(1) Alevaire is prepared: by D-sorbite, glycerol, glycerine, triethylene-glycol diacetate, methyl stearate, dodecanedioic acid Dimethyl ester is that 1:10~20:10~20:5~10:2~6:0.6~1.0 ratio is uniformly mixed obtained cigarette atomization in mass ratio Agent;
(2) pre-treatment of tobacco leaf: formula tobacco leaf is uniformly mixed by belt and vibration slot, is delivered in steam blasting equipment and carries out Steam explosion treatment, the temperature of steam blasting is 30 DEG C~50 DEG C, the steam blasting time existed less than 0.01 second, steam pressure 0.4MPa~0.8Mpa, pressure retention time are 10~60 seconds;
(3) preparation absorbs the formula tobacco leaf of Alevaire: the cigarette Alevaire prepared in step (1) being fitted into charging bucket, when matching Square tobacco leaf is sprayed at rapidly tobacco leaf surface after Steam explosion treatment, by Alevaire, is risen again rapidly using tobacco leaf and in knot When structure swelling state, Alevaire is fully absorbed;Wherein the application ratio of the Alevaire is the 15%-40% of tobacco leaf weight;
(4) formula tobacco leaf post-processing: the formula tobacco leaf that Alevaire is absorbed in step (3) is sent to leaf storing cabinet, equilibrium water conten fills Divide after absorbing and take out, and then subsequent routine can be carried out and prepare wire process.
3. a kind of method for improving traditional tobacco leaf Alevaire uptake according to claim 2, it is characterised in that: the step Suddenly in (2), steam blasting working media is saturated steam.
4. a kind of method for improving traditional tobacco leaf Alevaire uptake according to claim 2, it is characterised in that: the step Suddenly its equilibrium temperature is 15~25 DEG C in entrance leaf storing cabinet in (4), equilibrium humidity is 8~12%, equilibration time is 2h~4h.
CN201811558960.4A 2018-12-19 2018-12-19 A kind of cigarette Alevaire and the method for improving traditional tobacco leaf Alevaire uptake Pending CN109602074A (en)

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Cited By (7)

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Publication number Priority date Publication date Assignee Title
CN110150710A (en) * 2019-04-30 2019-08-23 安徽中烟工业有限责任公司 A method of cigarette pipe tobacco is prepared by tobacco leaf or raw material pipe tobacco
CN110292192A (en) * 2019-07-03 2019-10-01 深圳市长能汇科科技有限公司 A kind of preparation method of the hot type smoking article without binder
CN110693069A (en) * 2019-11-13 2020-01-17 湖北中烟工业有限责任公司 Method for improving absorption of traditional tobacco leaf atomizing agent
CN110833202A (en) * 2019-11-13 2020-02-25 湖北中烟工业有限责任公司 Method for improving absorption of tobacco stem atomizing agent
CN111802687A (en) * 2020-07-27 2020-10-23 湖北中烟工业有限责任公司 Atomizing agent containing conjugated linoleic acid and saponin and cigarette without burning during heating
CN113693261A (en) * 2021-09-01 2021-11-26 深圳市真味生物科技有限公司 Atomizing agent, preparation method thereof and application of atomizing agent in heating non-combustion smoking set
CN114711450A (en) * 2022-04-13 2022-07-08 湖北中烟工业有限责任公司 Method for improving fragrance release amount of heating non-combustible tobacco product

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110150710A (en) * 2019-04-30 2019-08-23 安徽中烟工业有限责任公司 A method of cigarette pipe tobacco is prepared by tobacco leaf or raw material pipe tobacco
CN110292192A (en) * 2019-07-03 2019-10-01 深圳市长能汇科科技有限公司 A kind of preparation method of the hot type smoking article without binder
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CN110833202A (en) * 2019-11-13 2020-02-25 湖北中烟工业有限责任公司 Method for improving absorption of tobacco stem atomizing agent
CN111802687A (en) * 2020-07-27 2020-10-23 湖北中烟工业有限责任公司 Atomizing agent containing conjugated linoleic acid and saponin and cigarette without burning during heating
CN113693261A (en) * 2021-09-01 2021-11-26 深圳市真味生物科技有限公司 Atomizing agent, preparation method thereof and application of atomizing agent in heating non-combustion smoking set
CN114711450A (en) * 2022-04-13 2022-07-08 湖北中烟工业有限责任公司 Method for improving fragrance release amount of heating non-combustible tobacco product
CN114711450B (en) * 2022-04-13 2022-12-02 湖北中烟工业有限责任公司 Method for improving fragrance release amount of heating non-combustible tobacco product

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