CN107156904B - Preparation method of kudzu vine root particles for cigarette filter, particles and cigarette filter - Google Patents

Preparation method of kudzu vine root particles for cigarette filter, particles and cigarette filter Download PDF

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Publication number
CN107156904B
CN107156904B CN201710459458.7A CN201710459458A CN107156904B CN 107156904 B CN107156904 B CN 107156904B CN 201710459458 A CN201710459458 A CN 201710459458A CN 107156904 B CN107156904 B CN 107156904B
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China
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kudzu root
particles
cigarette filter
powder
root powder
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CN107156904A (en
Inventor
何沛
凌军
向能军
刘志华
杨光宇
王晋
韦克毅
申钦鹏
刘春波
朱瑞芝
司晓喜
张凤梅
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China Tobacco Yunnan Industrial Co Ltd
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China Tobacco Yunnan Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/14Use of materials for tobacco smoke filters of organic materials as additive
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/18Mouthpieces for cigars or cigarettes; Manufacture thereof

Abstract

The invention relates to a preparation method of kudzu vine root particles for a cigarette filter, the particles and a cigarette filter, and belongs to the field of filter materials. The method comprises the following steps: (1) dividing the kudzu root powder into two parts, wherein one part is added with water for gelatinization, and the gelatinized kudzu root powder accounts for 8-20% of the total mass of the kudzu root powder; the remaining one part is used as granulated dry powder; (2) adding water into the kudzu root powder for gelatinization, heating for gelatinization, wherein the amount of the added water is 5-10 times of the mass of the gelatinized kudzu root powder, and obtaining gelatinized kudzu root powder colloidal solution; (3) granulating with conventional fluidized bed granulator, and sieving to obtain 20-80 mesh granules. The method can improve yield, avoid interference of external adhesive on sensory quality of radix Puerariae, improve material utilization rate, save product cost, and further improve product quality.

Description

Preparation method of kudzu vine root particles for cigarette filter, particles and cigarette filter
Technical Field
The invention discloses a preparation method of kudzu vine root particles for a cigarette filter, the particles and a cigarette filter, and belongs to the field of filter materials.
Background
The filter tip is used as a bridge between a smoker and the mainstream smoke, can filter partial harmful components in the smoke, is connected with the filter tip on the cigarette, can effectively intercept total particulate matters in the mainstream smoke of the cigarette, reduces the tar content and reduces the harm of the smoke to the human health and the environment.
Kudzu root is a perennial plant of Pueraria of Leguminosae, is a common vegetable in some provinces of south China, is sweet, cool and delicious in taste, and is often used as soup. Can also be used as medicine. The flavone extracted from radix Puerariae can increase blood flow of brain and coronary blood vessel, and reduce vascular resistance. The soybean flavone has multiple functions of spasmolysis, blood sugar reduction and the like. Radix Puerariae itself also has effects of promoting fluid production to quench thirst, etc. China has 14 species of Pueraria plants, is the most abundant in germplasm resources and is the top of the world.
With the increasing requirements of consumers on the cigarette quality, how to enhance the smoke comfort and improve the cigarette quality becomes a hot point for research and development of various cigarette production enterprises. The industrial application of the kudzu root granular material to the cigarette filter is already realized in the past. However, the current application methods mainly include two methods, namely, the kudzu root is directly crushed into particles of 20-80 meshes, or a certain amount of adhesive is added into the kudzu root powder, and the particles are prepared by various forming methods. However, both methods have drawbacks: the kudzu root is directly crushed into particles, the particle shapes are uneven, the physical properties are unstable, the particles are easy to crush during the forming of the cigarette filter stick, so that a large amount of dust is generated, and the material utilization rate is not high; the granules prepared by the additional adhesive easily cause certain negative influence on the sense of the radix puerariae granules. Aiming at the defects, how to adopt a proper process technology to improve the yield of the product and avoid the negative influence is a problem to be solved urgently for the application of the kudzuvine root particles in the cigarette filter.
Disclosure of Invention
The invention aims to provide a kudzu root granular material for a cigarette filter and a preparation method thereof, wherein a kudzu root method colloidal solution pasted under certain process conditions is used as an adhesive, and fluidized bed granulation is carried out in a top spraying mode.
The specific technical scheme of the invention is as follows:
a preparation method of kudzu vine root particles for cigarette filter tips is characterized by comprising the following steps: the method comprises the following steps:
(1) dividing the kudzu root powder into two parts, wherein one part is added with water for gelatinization, and the gelatinized kudzu root powder accounts for 8-20% of the total mass of the kudzu root powder; the remaining one part is used as granulated dry powder;
(2) adding water into the kudzu root powder for gelatinization, heating for gelatinization, wherein the amount of the added water is 5-10 times of the mass of the gelatinized kudzu root powder, and obtaining gelatinized kudzu root powder colloidal solution;
(3) granulating with conventional fluidized bed granulator, and sieving to obtain 20-80 mesh granules.
Further, in the step (3), a boiling fluidized bed granulation machine is adopted for granulation, and the gelatinized pueraria powder colloidal solution is sprayed on the top.
Further, heating for gelatinization is specifically stirring heating, and under the condition of vigorous stirring, water is heated to boiling and kept for 5-30 minutes. The hot water brewing mode is not adopted. The requirement of the kudzu root granules is controlled by the proportion of gelatinized kudzu root powder, the added water quantity and the boiling retention time. The larger the proportion of the gelatinized pueraria powder is, the smaller the mesh number of the prepared particles is; the larger the added water amount is, the larger the mesh number of the prepared particles is, the longer the process granulation needs, and the better the product stability is; the longer the boiling hold time, the higher the sweetness of the resulting granules.
Further, the method also comprises a step (4), after the granulation is finished, the moisture in the fluidized bed is humidified or heated, the moisture balance is carried out on the granules, and the moisture is controlled to be 7-10%.
The invention relates to cigarette filter tip kudzu root particles obtained by the preparation method.
The cigarette filter tip obtained by adopting the cigarette filter tip kudzu root particles has the additive amount of 20-40mg per cigarette filter tip kudzu root particles.
Compared with the prior art, the invention has the advantages that:
(1) compared with a direct crushing granulation method, the method has the advantages that the yield is high (the yield of the direct crushing method is only about 20%, and the yield of the method can reach more than 90%), the particle shape is uniform, the physical property is stable and uniform, the sweetness of the particle can be obviously improved, and the sensory quality of subsequent cigarette products is improved;
(2) compared with the traditional granulation method with the additional adhesive, the method does not add any additional component, does not cause any negative influence on the sensory quality of the radix puerariae granules, can also increase sweetness and has high product safety.
Detailed Description
The technical solutions in the embodiments are clearly and completely described below, and it is obvious that the described embodiments are only a part of examples of the present invention, and not all examples. All other embodiments, which can be obtained by a person skilled in the art without inventive effort based on the embodiments of the present invention, are within the scope of the present invention. The granulation process is a conventional fluidized bed granulation process. The filter stick forming process is a conventional process.
Example 1
(1) Dividing the kudzu root powder into two parts, wherein 8% of the kudzu root powder is used for gelatinization, and the other 92% of the kudzu root powder is used as granulated dry powder;
(2) adding 10 times of water by mass into the kudzu root powder for gelatinization, heating the water to boiling under the condition of vigorous stirring, and keeping for 5 minutes to obtain gelatinized kudzu root powder colloidal solution;
(3) granulating in fluidized bed granulator, spraying gelatinized radix Puerariae powder colloidal solution, and sieving to obtain 50-80 mesh granules with yield of 94%.
(4) After granulation is finished, humidifying or heating in the fluidized bed, balancing the moisture of the granules, controlling the moisture to be 7-10%, and then sieving and packaging according to requirements.
Compared with the kudzu root particles manufactured by a direct crushing method, the product uniformity is better, and the yield is greatly improved (the yield is obtained by dividing the quality of the obtained qualified particles by the total quality of the kudzu root powder (including the dry kudzu root powder and the kudzu root powder for preparing the colloidal solution).
And (3) putting the finally obtained radix puerariae particles into a filter tip forming device for production, wherein the adding amount is 20 mg/cigarette, so as to obtain the cigarette filter containing the filter tip particles, and manufacturing cigarettes. Compared with cigarettes made of the kudzu root particles by using an additional adhesive granulation method, the cigarette has the advantages that the sweet and moist smoke feeling is remarkably improved, no additional miscellaneous gas is generated, the product quality is obviously improved, and the sensory evaluation score is increased by 1 point.
Example 2
(1) Dividing the kudzu root powder into two parts, wherein 20% of the kudzu root powder is used for gelatinization, and the other 80% of the kudzu root powder is used as granulated dry powder;
(2) adding 10 times of water by mass into the kudzu root powder for gelatinization, heating the water to boiling under the condition of vigorous stirring, and keeping for 30 minutes to obtain gelatinized kudzu root powder colloidal solution;
(3) granulating in fluidized bed granulator, spraying gelatinized radix Puerariae powder colloidal solution, and sieving to obtain 40-60 mesh granules with yield of 96%.
(4) After granulation is finished, humidifying or heating in the fluidized bed, balancing the moisture of the granules, controlling the moisture to be 7-10%, and then sieving and packaging according to requirements.
Compared with the kudzuvine root particles prepared by a direct crushing method, the kudzuvine root particles have better product uniformity and greatly improved yield.
And (3) putting the finally obtained radix puerariae particles into a filter tip forming device for production, wherein the adding amount is 40 mg/cigarette, so as to obtain the cigarette filter containing the filter tip particles, and manufacturing cigarettes. Compared with cigarettes made of the kudzu root particles by using an additional adhesive granulation method, the cigarette has the advantages that the sweet and moist smoke feeling is remarkably improved, no additional miscellaneous gas is generated, the product quality is obviously improved, and the sensory evaluation score is increased by 0.5.
Example 3
(1) Dividing the kudzu root powder into two parts, wherein 10% of the kudzu root powder is used for gelatinization, and the other 90% of the kudzu root powder is used as granulated dry powder;
(2) adding 5 times of water by mass into the kudzu root powder for gelatinization, heating the water to boiling under the condition of vigorous stirring, and keeping for 10 minutes to obtain gelatinized kudzu root powder colloidal solution;
(3) granulating in fluidized bed granulator, spraying gelatinized radix Puerariae powder colloidal solution, and sieving to obtain 30-50 mesh granules with yield of 95%.
(4) After granulation is finished, humidifying or heating in the fluidized bed, balancing the moisture of the granules, controlling the moisture to be 7-10%, and then sieving and packaging according to requirements.
Compared with the kudzuvine root particles prepared by a direct crushing method, the kudzuvine root particles have better product uniformity and greatly improved yield.
And (3) putting the finally obtained radix puerariae particles into a filter tip forming device for production, wherein the adding amount is 36 mg/cigarette, so as to obtain the cigarette filter containing the filter tip particles, and manufacturing cigarettes. Compared with cigarettes made of the kudzu root particles by using an additional adhesive granulation method, the cigarette has the advantages that the sweet and moist smoke feeling is remarkably improved, no additional miscellaneous gas is generated, the product quality is obviously improved, and the sensory evaluation score is increased by 0.5.
Example 4
(1) Dividing the kudzu root powder into two parts, wherein 5% of the kudzu root powder is used for gelatinization, and the other 95% of the kudzu root powder is used as granulated dry powder;
(2) adding 8 times of water by mass into the kudzu root powder for gelatinization, heating the water to boiling under the condition of vigorous stirring, and keeping for 10 minutes to obtain gelatinized kudzu root powder colloidal solution;
(3) granulating in conventional fluidized bed granulator, spraying gelatinized radix Puerariae powder colloidal solution in top spray mode, and sieving to obtain 20-50 mesh granules with yield of 98%.
(4) After granulation is finished, humidifying or heating in the fluidized bed, balancing the moisture of the granules, controlling the moisture to be 7-10%, and then sieving and packaging according to requirements.
Compared with the kudzuvine root particles prepared by a direct crushing method, the kudzuvine root particles have better product uniformity and greatly improved yield.
And (3) putting the finally obtained radix puerariae particles into a filter tip forming device for production, wherein the adding amount is 25 mg/cigarette, obtaining the cigarette filter containing the filter tip particles, and manufacturing cigarettes. Compared with cigarettes made of the kudzu root particles by using an additional adhesive granulation method, the cigarette has the advantages that the sweet and moist smoke feeling is remarkably improved, no additional miscellaneous gas is generated, the product quality is obviously improved, and the sensory evaluation score is increased by 1 point.
Example 5
(1) Dividing the kudzu root powder into two parts, wherein 15% of the kudzu root powder is used for gelatinization, and the other 85% of the kudzu root powder is used as granulated dry powder;
(2) adding 7 times of water by mass into the kudzu root powder for gelatinization, heating the water to boiling under the condition of vigorous stirring, and keeping for 10 minutes to obtain gelatinized kudzu root powder colloidal solution;
(3) granulating radix Puerariae powder as dry powder in conventional fluidized bed, spraying gelatinized radix Puerariae powder colloidal solution in top spray mode, and sieving to obtain 40-60 mesh granules with yield of 91%.
(4) After granulation is finished, humidifying or heating in the fluidized bed, balancing the moisture of the granules, controlling the moisture to be 7-10%, and then sieving and packaging according to requirements.
Compared with the kudzuvine root particles prepared by a direct crushing method, the kudzuvine root particles have better product uniformity and greatly improved yield.
And (3) putting the finally obtained radix puerariae particles into a filter tip forming device for production, wherein the adding amount is 30 mg/cigarette, so as to obtain the cigarette filter containing the filter tip particles, and manufacturing cigarettes. Compared with cigarettes made of the kudzu root particles by using an additional adhesive granulation method, the cigarette has the advantages that the sweet and moist smoke feeling is remarkably improved, no additional miscellaneous gas is generated, the product quality is obviously improved, and the sensory evaluation score is increased by 0.5.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.

Claims (5)

1. A preparation method of kudzu vine root particles for cigarette filter tips is characterized by comprising the following steps: the method comprises the following steps:
(1) dividing the kudzu root powder into two parts, wherein one part is added with water for gelatinization, and the gelatinized kudzu root powder accounts for 8-20% of the total mass of the kudzu root powder; the remaining one part is used as granulated dry powder;
(2) adding water into the kudzu root powder for gelatinization, heating for gelatinization, wherein the amount of the added water is 5-10 times of the mass of the gelatinized kudzu root powder, and obtaining gelatinized kudzu root powder colloidal solution; heating gelatinization is specifically stirring heating, and under the condition of vigorous stirring, water is heated to boiling and kept for 5-30 minutes;
(3) granulating by using a conventional fluidized bed granulator, and sieving the prepared granules to obtain granules with 20-80 meshes, wherein the granules have uniform shapes and stable and uniform physical properties, and can remarkably improve the sweetness of the granules.
2. The preparation method of the kudzu root particles for the cigarette filter according to claim 1, wherein the preparation method comprises the following steps: and (3) granulating by adopting a fluidized bed granulation machine, and top-spraying the gelatinized pueraria powder colloidal solution.
3. The preparation method of the kudzu root particles for the cigarette filter according to claim 2, wherein the preparation method comprises the following steps: and (4) humidifying or heating in the fluidized bed after granulation is finished, and balancing the moisture of the granules, wherein the moisture is controlled to be 7-10%.
4. A kudzu root particle for cigarette filter obtained by the preparation method of any one of claims 1 to 3.
5. A cigarette filter obtained by using the cigarette filter kudzu root particles as claimed in claim 4, wherein: the addition amount of the kudzu root particles for the cigarette filter is 20-40 mg/cigarette.
CN201710459458.7A 2017-06-16 2017-06-16 Preparation method of kudzu vine root particles for cigarette filter, particles and cigarette filter Active CN107156904B (en)

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CN113287784B (en) * 2021-06-25 2022-09-30 云南中烟工业有限责任公司 Cigarette filter particles capable of reducing release amount of hydrogen sulfide in smoke, preparation method and filter

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