CN104323423A - Application of Pu'er tea polysaccharide in cigarette filter stick - Google Patents
Application of Pu'er tea polysaccharide in cigarette filter stick Download PDFInfo
- Publication number
- CN104323423A CN104323423A CN201410513893.XA CN201410513893A CN104323423A CN 104323423 A CN104323423 A CN 104323423A CN 201410513893 A CN201410513893 A CN 201410513893A CN 104323423 A CN104323423 A CN 104323423A
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- China
- Prior art keywords
- tea polysaccharide
- powder
- tea
- filter stick
- cigarette
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0229—Filter rod forming processes
Abstract
The invention discloses application of Pu'er tea polysaccharide in a cigarette filter stick. The extracted Pu'er tea polysaccharide powder and the optimized plant powder are uniformly mixed, are uniformly dispersed in filter stick strands in the form of particles with the size of 20-40 meshes through a granulating process, and are rolled to a composite functional filter stick through a filter stick forming machine; or the extracted Pu'er tea polysaccharide is prepared to a solution for dip coating of a center line of an axis of the filter stick and is prepared to the filter stick containing the functional center line through the filter stick forming machine after drying. The sensory evaluation shows that that after the Pu'er tea polysaccharide is applied to the cigarette filter stick, the cigarette smoke is fresh, saturated, moisturized and mellow, the smoke irritation and the bitter and spicy taste can be remarkably reduced, the sensory quality of the cigarette is improved and the cigarette smoking quality is improved.
Description
Technical field
The invention belongs to cigarette additive technical field, be specifically related to the embody rule of Pu ' er Tea Polysaccharide in cigarette filter rod.
Background technology
Containing abundant glucide in natural plants, be added into cigarette after the glucide in natural plants is extracted, effectively can promote the sweet sense in Tianjin of flue gas.Such as: make sweet taste dripping pill after Song Xuyan, Luo Chenghao etc. (essence and flavoring agent cosmetics, 2012,2,1) are composite in proportion by perillartine and menthyl lactate and add in cigarette filter rod, the fresh and sweet sense of cigarette can be increased; Algal polysaccharides and derivative thereof as additive for filter tip of cigarette, effectively can be reduced the alkoxy free group in cigarette smoke by patent CN 1682614 A.
Tea polysaccharide is the macromolecular compound of a kind of similar GL-B and panaxan, is have bioactive complex polysaccharide in tealeaves.The composition of tea polysaccharide comprises the water-soluble polysaccharides such as Arabic tree sugar, wood sugar, glucose galactose, galactolipin glycan, and molecular weight is about 1 × 10
4~ 5 × 10
4, to human body, there is important physiological function.Research shows, tea polysaccharide has hypoglycemic, reducing blood lipid, develop immunitypty and the multiple biological function such as radiation proof and anticoagulation.The antioxidation activity of tea polysaccharide and vitamin C are substantially close, and this may be that it can one of the mechanism strengthening immunization.As a kind of natural products having application and DEVELOPMENT PROSPECT, tea polysaccharide has been widely used in the fields such as food, medicine, health care.
Simultaneously, the polyhydroxy structure that tea polysaccharide has makes it to become a kind of natural humectation material, be applied to the humectation effect obviously can improving cigarette in cigarette, the dry sensation of cigarette is reduced, sweet degree increases, simultaneously also can effectively reduce the harmful components such as free radical in flue gas, nitrosamine, aldehydes matter.In Pu'er tea, the content of tea polysaccharide and pectin teas more typical in other is all high, except zymotechnique, kind be not both important influence factor, the raw material of Pu'er tea are the large leaf tea in Yunnan, its content material is more abundant, and composition activity is also eager to excel than other teas.
In prior art, relate generally to about the application of tea polysaccharide in cigarette and be made into feed liquid and be sprayed in pipe tobacco; Tea polysaccharide and water, adhesive etc. are made water paint and is applied to cigarette forming paper; And tea polysaccharide is prepared tobacco aromatics etc. as the sugared source of mailland reaction.But there is not yet relevant report for the Pu ' er Tea Polysaccharide application in cigarette, the particularly Pu ' er Tea Polysaccharide application in cigarette filter rod.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, the embody rule of Pu ' er Tea Polysaccharide in cigarette filter rod is provided, using Pu ' er Tea Polysaccharide as a kind of filter stick additive, to improve the suction quality of cigarette.
Object of the present invention is achieved by following technical proposals.
Except as otherwise noted, percentage of the present invention is mass percent.
The application of Pu ' er Tea Polysaccharide in cigarette filter rod.
The application of described Pu ' er Tea Polysaccharide in cigarette filter rod, is specially: first make Pu ' er Tea Polysaccharide powder by after concentrated for Pu'er tea leaching liquor, drying, then mixes with plant powder, obtains Pu ' er Tea Polysaccharide composite particles after granulation; Then, when filter stick formation, described Pu ' er Tea Polysaccharide composite particles is evenly dispersed in filter stick tow by the addition of 1 ~ 3mg/mm, makes functional form cigarette filter rod.
Wherein, described Pu ' er Tea Polysaccharide composite particles, is prepared by following method:
(1) Pu'er tea is pulverized, cross 80 mesh sieves, add the distilled water of 8 ~ 10 times, 60 ~ 75 DEG C of lixiviates 2 ~ 3 times, each 2h; Merge leaching liquor, filter, filtrate is reduced pressure concentration 2h under 0.02 ~ 0.05Mpa, 70 DEG C of conditions;
(2) filtrate after concentrating adds 95% ethanol of 3 ~ 5 times, and in 0 DEG C of standing 8h, centrifugal 40min, filtration, freeze drying obtain Pu ' er Tea Polysaccharide powder;
(3) mixed with the mass ratio of plant powder according to 0.5 ~ 3:1 by Pu ' er Tea Polysaccharide powder, described plant powder is balloonflower powder, dendrobe powder or aloe powder; Add binder through granulation, sieve obtained 20 ~ 40 object Pu ' er Tea Polysaccharide composite particles.
Described binder is any combination of one or more in edible gelatin, dextrin, Arabic gum, polyethylene glycol.
The application of described Pu ' er Tea Polysaccharide in cigarette filter rod, is specially: first make Pu ' er Tea Polysaccharide powder by after concentrated for Pu'er tea leaching liquor, drying; Water and propane diols are mixed as solvent by the volume ratio of 2 ~ 3:1; Be dissolved in by Pu ' er Tea Polysaccharide powder in described solvent, in solution, the mass fraction of Pu ' er Tea Polysaccharide powder is 20 ~ 40%; Then this solution is used for dip-coating filter stick center line, after drying, is shaped to central line filter stick by filter-stick forming device.
Wherein, described Pu ' er Tea Polysaccharide powder, is prepared by following method:
(1) Pu'er tea is pulverized, cross 80 mesh sieves, add the distilled water of 8 ~ 10 times, 60 ~ 75 DEG C of lixiviates 2 ~ 3 times, each 2h; Merge leaching liquor, filter, filtrate is reduced pressure concentration 2h under 0.02 ~ 0.05Mpa, 70 DEG C of conditions;
(2) filtrate after concentrating adds 95% ethanol of 3 ~ 5 times, and in 0 DEG C of standing 8h, centrifugal 40min, filtration, freeze drying obtain Pu ' er Tea Polysaccharide powder.
Relative to prior art, the present invention has the following advantages:
1, Pu ' er Tea Polysaccharide composite particles adds in cigarette filter rod the hardship alleviating tobacco, peppery, puckery sensation to, play improve cigarette suction comfortableness, reduce irritating effect, scavenging free radicals and oxidation resistant effect is played when cigarette smoking, and can tar adsorption to a certain extent; Functional components in the plant powder of preferred interpolation is understood some and is entered absorption of human body with main flume in aspiration procedure, can play it and strengthen immunity of organisms, anti-oxidant and radiation-resistant physiological function.
2, by the dip-coating of Pu ' er Tea Polysaccharide solution on filter stick center line, the stimulus to the sense organ brought after can weakening reducing cigarette tar and reducing, reaches the effect promoting cigarette flavor and suction quality, improves cigarette filter rod to the filter effect of main flume harmful components simultaneously.
3, present invention process is simple, is convenient to carry out suitability for industrialized production, has good development prospect under the prerequisite not changing existing Cigarette processing technique.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, be described in further detail below in conjunction with embodiment.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
Embodiment 1
Pulverized by Pu'er tea, cross 80 mesh sieves, add the water of 8 times, 70 DEG C of lixiviates 3 times, each 2h, merge water extract, filter, filtrate is at 0.04Mpa, 70 DEG C, reduced pressure concentration under 2h condition.Filtrate after concentrated is added 95% ethanol of 5 times, in 0 DEG C of standing 8h, centrifugal 40min, filter, freeze drying obtains Pu ' er Tea Polysaccharide powder.By balloonflower root raw material through the broken obtained Platycodon Root of washing-drying-coarse crushing-low-temperature submicron powder.After Pu ' er Tea Polysaccharide powder and Platycodon Root in mass ratio 1:1 Homogeneous phase mixing, carry out mist projection granulating with the edible gelatin aqueous solution of 3% through fluidized bed spray granulation machine, sieving obtains 20 ~ 40 object Pu ' er Tea Polysaccharide composite particles.In filter stick formation operation, described Pu ' er Tea Polysaccharide composite particles is evenly dispersed in filter stick tow by the addition of 3mg/mm, makes 1# functional form cigarette filter rod.
Embodiment 2
Pulverized by Pu'er tea, cross 80 mesh sieves, add the water of 10 times, 60 DEG C of lixiviates 3 times, each 2h, merge water extract, filter, filtrate is at 0.02Mpa, 70 DEG C, reduced pressure concentration under 2h condition.Filtrate after concentrated is added 95% ethanol of 3 times, in 0 DEG C of standing 8h, centrifugal 40min, filter, freeze drying obtains Pu ' er Tea Polysaccharide powder.By stem of noble dendrobium raw material through the broken obtained Dendrobium of washing-drying-coarse crushing-low-temperature submicron powder.After Pu ' er Tea Polysaccharide powder and Dendrobium in mass ratio 2:1 Homogeneous phase mixing, the dextrin in aqueous solution of 3% carries out mist projection granulating through fluidized bed spray granulation machine, sieving obtains 20 ~ 40 object Pu ' er Tea Polysaccharide composite particles.In filter stick formation operation, described Pu ' er Tea Polysaccharide composite particles is evenly dispersed in filter stick tow by the addition of 2mg/mm, makes 2# functional form cigarette filter rod.
Embodiment 3
Pulverized by Pu'er tea, cross 80 mesh sieves, add the water of 9 times, 75 DEG C of lixiviates 3 times, each 2h, merge water extract, filter, filtrate is at 0.05Mpa, 70 DEG C, reduced pressure concentration under 2h condition.Filtrate after concentrated is added 95% ethanol of 4 times, in 0 DEG C of standing 8h, centrifugal 40min, filter, freeze drying obtains Pu ' er Tea Polysaccharide powder.By aloe raw material through the broken obtained Alose of washing-drying-coarse crushing-low-temperature submicron powder.After Pu ' er Tea Polysaccharide powder and Alose in mass ratio 2:1 Homogeneous phase mixing, the Arabic gum aqueous solution of 2% carries out mist projection granulating through fluidized bed spray granulation machine, sieving obtains 20 ~ 40 object Pu ' er Tea Polysaccharide composite particles.In filter stick formation operation, described Pu ' er Tea Polysaccharide composite particles is evenly dispersed in filter stick tow by the addition of 1mg/mm, makes 3# functional form cigarette filter rod.
Embodiment 4
Pulverized by Pu'er tea, cross 80 mesh sieves, add the water of 8 times, 70 DEG C of lixiviates 3 times, each 2h, merge water extract, filter, filtrate is at 0.04Mpa, 70 DEG C, reduced pressure concentration under 2h condition.Filtrate after concentrated is added 95% ethanol of 5 times, in 0 DEG C of standing 8h, centrifugal 40min, filter, freeze drying obtains Pu ' er Tea Polysaccharide powder.By wiring solution-forming in the mixed solvent of water-soluble for Pu ' er Tea Polysaccharide powder and propane diols (v/v=2:1), the mass fraction of solution is 40%, for dip-coating filter stick center line, after drying, be shaped to central line filter stick (4# filter stick) by filter-stick forming device.When aspirating, most of flow of main flume can be concentrated and pass through-the cross section in vertical filter stick axle center, and this cross section is centered by filter stick axle center, larger the closer to centralized traffic.
Application Example
Filter stick obtained by embodiment 1 ~ 4 is used for cigarette, and to use the cigarette sample in contrast of common cigarette acetate tow filter stick, transfer to 10 experts that smoke panel test to smoke panel test, result is as follows:
As seen from the above table: the functional form filter stick obtained by embodiment 1 ~ 4, the harmful components in flue gas can be reduced while improving cigarette smoking quality.Tool improves significantly Sensory Quality of Cigarette, reduces flue gas drying sense, promotes the effect of sweet degree and comfort level.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (6)
1. the application of Pu ' er Tea Polysaccharide in cigarette filter rod.
2. the application of Pu ' er Tea Polysaccharide according to claim 1 in cigarette filter rod, is characterized in that: first make Pu ' er Tea Polysaccharide powder by after concentrated for Pu'er tea leaching liquor, drying, then mixes with plant powder, obtains Pu ' er Tea Polysaccharide composite particles after granulation; Then, when filter stick formation, described Pu ' er Tea Polysaccharide composite particles is evenly dispersed in filter stick tow by the addition of 1 ~ 3mg/mm, makes functional form cigarette filter rod.
3. the application of Pu ' er Tea Polysaccharide according to claim 2 in cigarette filter rod, is characterized in that: described Pu ' er Tea Polysaccharide composite particles, is prepared by following method:
(1) Pu'er tea is pulverized, cross 80 mesh sieves, add the distilled water of 8 ~ 10 times, 60 ~ 75 DEG C of lixiviates 2 ~ 3 times, each 2h; Merge leaching liquor, filter, filtrate is reduced pressure concentration 2h under 0.02 ~ 0.05Mpa, 70 DEG C of conditions;
(2) filtrate after concentrating adds 95% ethanol of 3 ~ 5 times, and in 0 DEG C of standing 8h, centrifugal 40min, filtration, freeze drying obtain Pu ' er Tea Polysaccharide powder;
(3) mixed with the mass ratio of plant powder according to 0.5 ~ 3:1 by Pu ' er Tea Polysaccharide powder, described plant powder is balloonflower powder, dendrobe powder or aloe powder; Add binder through granulation, sieve obtained 20 ~ 40 object Pu ' er Tea Polysaccharide composite particles.
4. the application of Pu ' er Tea Polysaccharide according to claim 3 in cigarette filter rod, is characterized in that: described binder is any combination of one or more in edible gelatin, dextrin, Arabic gum, polyethylene glycol.
5. the application of Pu ' er Tea Polysaccharide according to claim 1 in cigarette filter rod, is characterized in that: first make Pu ' er Tea Polysaccharide powder by after concentrated for Pu'er tea leaching liquor, drying; Water and propane diols are mixed as solvent by the volume ratio of 2 ~ 3:1; Be dissolved in by Pu ' er Tea Polysaccharide powder in described solvent, in solution, the mass fraction of Pu ' er Tea Polysaccharide powder is 20 ~ 40%; Then this solution is used for dip-coating filter stick center line, after drying, is shaped to central line filter stick by filter-stick forming device.
6. the application of Pu ' er Tea Polysaccharide according to claim 5 in cigarette filter rod, is characterized in that: described Pu ' er Tea Polysaccharide powder, is prepared by following method:
(1) Pu'er tea is pulverized, cross 80 mesh sieves, add the distilled water of 8 ~ 10 times, 60 ~ 75 DEG C of lixiviates 2 ~ 3 times, each 2h; Merge leaching liquor, filter, filtrate is reduced pressure concentration 2h under 0.02 ~ 0.05Mpa, 70 DEG C of conditions;
(2) filtrate after concentrating adds 95% ethanol of 3 ~ 5 times, and in 0 DEG C of standing 8h, centrifugal 40min, filtration, freeze drying obtain Pu ' er Tea Polysaccharide powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410513893.XA CN104323423A (en) | 2014-09-29 | 2014-09-29 | Application of Pu'er tea polysaccharide in cigarette filter stick |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410513893.XA CN104323423A (en) | 2014-09-29 | 2014-09-29 | Application of Pu'er tea polysaccharide in cigarette filter stick |
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| CN104323423A true CN104323423A (en) | 2015-02-04 |
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| CN201410513893.XA Pending CN104323423A (en) | 2014-09-29 | 2014-09-29 | Application of Pu'er tea polysaccharide in cigarette filter stick |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104705442A (en) * | 2015-03-31 | 2015-06-17 | 吴绍平 | Dendrobium officinale tea and preparation method thereof |
| CN104839886A (en) * | 2015-04-30 | 2015-08-19 | 湖北中烟工业有限责任公司 | Anti-microbial cigarette filter tip and manufacturing method thereof |
| CN106617286A (en) * | 2017-01-16 | 2017-05-10 | 河北中烟工业有限责任公司 | Preparation method of lotus leaf-type composite filter rods of cigarettes |
| CN108251216A (en) * | 2018-01-18 | 2018-07-06 | 云南中烟工业有限责任公司 | A kind of preparation method and application of the Pu'er tea absolute oil containing the fragrant component of Viscμm articulatum Burm f cause |
| CN111000288A (en) * | 2019-12-30 | 2020-04-14 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
| CN111035061A (en) * | 2019-12-30 | 2020-04-21 | 福建中烟工业有限责任公司 | Composition for cigarettes, preparation method and application thereof |
| CN111117768A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Composition for cigarette, preparation method thereof and application of composition in tobacco products |
| CN111117767A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
| CN111109653A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
-
2014
- 2014-09-29 CN CN201410513893.XA patent/CN104323423A/en active Pending
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| 罗玲 等: "普洱茶茶多糖的提取工艺的响应面分析研究", 《中国农学通报》 * |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104705442A (en) * | 2015-03-31 | 2015-06-17 | 吴绍平 | Dendrobium officinale tea and preparation method thereof |
| CN104839886A (en) * | 2015-04-30 | 2015-08-19 | 湖北中烟工业有限责任公司 | Anti-microbial cigarette filter tip and manufacturing method thereof |
| CN106617286A (en) * | 2017-01-16 | 2017-05-10 | 河北中烟工业有限责任公司 | Preparation method of lotus leaf-type composite filter rods of cigarettes |
| CN108251216A (en) * | 2018-01-18 | 2018-07-06 | 云南中烟工业有限责任公司 | A kind of preparation method and application of the Pu'er tea absolute oil containing the fragrant component of Viscμm articulatum Burm f cause |
| CN111000288A (en) * | 2019-12-30 | 2020-04-14 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
| CN111035061A (en) * | 2019-12-30 | 2020-04-21 | 福建中烟工业有限责任公司 | Composition for cigarettes, preparation method and application thereof |
| CN111117768A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Composition for cigarette, preparation method thereof and application of composition in tobacco products |
| CN111117767A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
| CN111109653A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
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