CN106036982B - A kind of preparation method and applications of cigarette bay leaf extract - Google Patents
A kind of preparation method and applications of cigarette bay leaf extract Download PDFInfo
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- CN106036982B CN106036982B CN201610578804.9A CN201610578804A CN106036982B CN 106036982 B CN106036982 B CN 106036982B CN 201610578804 A CN201610578804 A CN 201610578804A CN 106036982 B CN106036982 B CN 106036982B
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- leaf extract
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- 229940021973 bay leaf extract Drugs 0.000 title claims abstract description 66
- 239000001883 pimenta racemosa mill. fruit leaf extract Substances 0.000 title claims abstract description 66
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 39
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 108090000790 Enzymes Proteins 0.000 claims abstract description 23
- 102000004190 Enzymes Human genes 0.000 claims abstract description 23
- 229940088598 enzyme Drugs 0.000 claims abstract description 23
- 241000208125 Nicotiana Species 0.000 claims abstract description 21
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000004062 sedimentation Methods 0.000 claims abstract description 14
- 239000002131 composite material Substances 0.000 claims abstract description 13
- 239000000284 extract Substances 0.000 claims abstract description 13
- 238000000605 extraction Methods 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 11
- 108010059892 Cellulase Proteins 0.000 claims abstract description 7
- 229940106157 cellulase Drugs 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims abstract 2
- 239000012141 concentrate Substances 0.000 claims description 10
- 238000005352 clarification Methods 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 6
- 108010084185 Cellulases Proteins 0.000 claims description 5
- 102000005575 Cellulases Human genes 0.000 claims description 5
- 239000000706 filtrate Substances 0.000 claims description 5
- 238000007654 immersion Methods 0.000 claims description 5
- 239000000919 ceramic Substances 0.000 claims description 3
- 239000012528 membrane Substances 0.000 claims description 3
- 238000007865 diluting Methods 0.000 claims 1
- 239000002304 perfume Substances 0.000 abstract description 9
- 210000000214 mouth Anatomy 0.000 abstract description 3
- 230000000638 stimulation Effects 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 abstract description 2
- 238000005096 rolling process Methods 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 abstract description 2
- 238000001914 filtration Methods 0.000 abstract 3
- 230000007071 enzymatic hydrolysis Effects 0.000 abstract 1
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 15
- 230000000694 effects Effects 0.000 description 9
- 239000000126 substance Substances 0.000 description 8
- 125000003118 aryl group Chemical group 0.000 description 7
- 150000001875 compounds Chemical class 0.000 description 5
- 238000001816 cooling Methods 0.000 description 4
- 230000006837 decompression Effects 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 4
- 230000007062 hydrolysis Effects 0.000 description 4
- 238000006460 hydrolysis reaction Methods 0.000 description 4
- 238000010790 dilution Methods 0.000 description 3
- 239000012895 dilution Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- SCCDQYPEOIRVGX-UHFFFAOYSA-N Acetyleugenol Chemical compound COC1=CC(CC=C)=CC=C1OC(C)=O SCCDQYPEOIRVGX-UHFFFAOYSA-N 0.000 description 2
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 2
- ZYEMGPIYFIJGTP-UHFFFAOYSA-N O-methyleugenol Chemical compound COC1=CC=C(CC=C)C=C1OC ZYEMGPIYFIJGTP-UHFFFAOYSA-N 0.000 description 2
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 description 2
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 description 1
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 description 1
- 239000001169 1-methyl-4-propan-2-ylcyclohexa-1,4-diene Substances 0.000 description 1
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- WEEGYLXZBRQIMU-UHFFFAOYSA-N Eucalyptol Chemical compound C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 description 1
- 239000005770 Eugenol Substances 0.000 description 1
- 239000005792 Geraniol Substances 0.000 description 1
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- 235000019082 Osmanthus Nutrition 0.000 description 1
- 241000333181 Osmanthus Species 0.000 description 1
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 108010047754 beta-Glucosidase Proteins 0.000 description 1
- 102000006995 beta-Glucosidase Human genes 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229960005233 cineole Drugs 0.000 description 1
- RFFOTVCVTJUTAD-UHFFFAOYSA-N cineole Natural products C1CC2(C)CCC1(C(C)C)O2 RFFOTVCVTJUTAD-UHFFFAOYSA-N 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 229960002217 eugenol Drugs 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 229940113087 geraniol Drugs 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- 229930007744 linalool Natural products 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229940116837 methyleugenol Drugs 0.000 description 1
- PRHTXAOWJQTLBO-UHFFFAOYSA-N methyleugenol Natural products COC1=CC=C(C(C)=C)C=C1OC PRHTXAOWJQTLBO-UHFFFAOYSA-N 0.000 description 1
- 150000007875 phellandrene derivatives Chemical class 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- RBNWAMSGVWEHFP-UHFFFAOYSA-N trans-p-Menthane-1,8-diol Chemical compound CC(C)(O)C1CCC(C)(O)CC1 RBNWAMSGVWEHFP-UHFFFAOYSA-N 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Abstract
The invention discloses a kind of preparation method and applications of cigarette with bay leaf extract.The dry basyleave of this method, which is crushed, to be soaked in water, and then carries out filtering after ultrasonic wave extraction, obtains bay leaf extract；Filtered after again dissolving cellulase and β glucuroide complex enzyme water, by obtained composite enzyme solution, composite enzyme solution is added to above-mentioned bay leaf extract by 5 15g/L, adjust the enzymatic hydrolysis condition of mixed liquor, digested, its relative density will be concentrated under reduced pressure into after enzymolysis liquid sedimentation filtration afterwards for after 1.05 1.25, then carries out sedimentation filtration and obtains cigarette bay leaf extract.The bay leaf extract prepared using the method for the present invention with cigarette perfume harmony is good, can improve aroma quality, abundant cigarette perfume, have a wide range of application, can directly feed and use and use in composition；The extract is used as tobacco aromaticss, and stability is strong, overcomes the residual that the extract that common solvent refluxing extraction obtains comes to tobacco rolling belt, can obviously reduce stimulation, oral cavity pleasant impression is clean.
Description
Technical field
The invention belongs to technical field of extraction of perfume extraction, and in particular to a kind of cigarette preparation method of bay leaf extract, area
The compound method of the other bay leaf extract in fields such as medicinal, food and its application.
Background technology
In tobacco product, the fragrance and suction taste of tobacco are most important, therefore addition spices is to improve product style and carry
One of effective means of high cigarette flavor quality.The leaf of many natural plants contains abundant aromatic substance, has distinctive pungent
Fragrance, is processed to tobacco aromaticss.Wherein, linalool, Eugenol, Geraniol, 1,8- are mainly contained in basyleave
Cineole, terpinol, acetyleugenol, methyleugenol, australene, the aromatic substance, these aromatic substances such as phellandrene
Spicy fragrance and preferable elegant sense with feature.And the aromatic substance of leaf class is mostly with cellulose family and glycoside link state shape
Formula is present, it is difficult to discharge.Be not added with enzyme the conventional steam way of distillation extract basyleave aromatic substance, recovery rate compared with
Low, the aromatic substance of acquisition is more single so that cigarette perfume effect of the bay leaf extract in cigarette be not obvious, so as to limit the moon
Application of the osmanthus leaf extract in cigarette.
The content of the invention
The purpose of the present invention is to provide a kind of preparation method of cigarette bay leaf extract according to the deficiencies in the prior art, should
Method can improve the aroma quality and recovery rate of basyleave aromatic substance, cigarette perfume effect of the enhancing bay leaf extract in cigarette
Really.
The technical scheme that the present invention is provided：A kind of preparation method of cigarette bay leaf extract, it is characterised in that tool
Body step includes：
(1) dry bay leaf powder is broken into bay leaf coarse powder, then bay leaf coarse powder with the water of 5-15 times of its weight is soaked into 1-3
Hour, it is put into afterwards in ultrasonic container in supersonic frequency 50-70KHz, at 40 DEG C -60 DEG C, extraction 60-180 minutes, then
It is filtered to remove filter residue and obtains bay leaf extract；
(2) by cellulase and beta-glucosidase according to 1:It is water-soluble with 2-10 times of its weight after 1-5 ratio mixing
0.8 μm of ceramic membrane filter is used after solution, composite enzyme solution is obtained；
(3) composite enzyme solution of step (2) is added in 5-15g/L ratio in the bay leaf extract of step (1),
The pH value for adjusting mixed liquor is 3-7, digests 10-30h under the conditions of 25-40 DEG C, after enzymolysis is finished, under the conditions of 3 DEG C at sedimentation
Manage after 24-48h, be filtered to remove filter residue, the bay leaf extract clarified；
(4) the bay leaf extract of step (3) is concentrated under reduced pressure into its relative density for after 1.05-1.25, in 3 DEG C of conditions
Filter residue is filtered to remove after lower sedimentation 24-48h, cigarette bay leaf extract is obtained.
The present invention preferably technical scheme：The addition of water described in step (1) is 8 times of dry basyleave weight, institute
The time for stating ultrasonic extraction is 1-3h.
The present invention preferably technical scheme：Filter type in step (1), step (3) and step (4) uses 0.8 μ
M ceramic membrane filter.
The present invention preferably technical scheme：In step (2), the addition of water is 6 times of complex enzyme weight.
The present invention preferably technical scheme：In step (4), thickening temperature is 50-80 DEG C, and concentration pressure is 0.01-
0.2Mpa。
The addition of complex enzyme has a certain impact to enzymolysis activity in the present invention, and relatively low and higher amount has to enzymolysis
Influence, complex enzyme 5-15g/L addition can reach maximum extracted rate.The pH value for adjusting mixed liquor is 3-7.It can ensure to be combined
The active highest of enzyme.
The present invention provides another technical scheme：Bay leaf extract prepared by a kind of use above method should
With, it is characterised in that：Bay leaf extract prepared by the above method directly sprays after using concentration for 60-80% ethanol dilution
It is spread across on pipe tobacco and perfuming is carried out to pipe tobacco, the addition of bay leaf extract is that the ratio of pipe tobacco weight is 1 ‰ -8 ‰.
The method have the advantages that：
(1) preparation method for the bay leaf extract that the present invention is provided has high aroma quality, recovery rate height, safe operation letter
Single the advantages of.
(2) extraction raw material basyleave is cheap and easy to get, and raw material sources are also without limitations.
(3) extraction process is simple, it is abundant to extract, do not destroy active ingredient, and simple excellent with easily operated, post processing
Point, is converted beneficial to production.
(4) the bay leaf extract for preparing the present invention is added in pipe tobacco as perfuming material, can be with cigarette perfume harmony
Well, aroma quality, abundant cigarette perfume can be improved, is had a wide range of application, can directly be fed and use and use in composition.
(5) extract prepared using the method for the present invention is used as tobacco aromaticss, and stability is strong, overcomes common solvent and returns
Stream extracts the residual that obtained extract comes to tobacco rolling belt, can obviously reduce stimulation, oral cavity pleasant impression is clean.
(6) present invention be prepared for it is a kind of can be natural harmless and with low cost with the spices of General Promotion cigarette quality,
Open the new way for preparing tobacco aromaticss.
Embodiment
The present invention is further described with reference to embodiment.
Embodiment 1, the preparation method of a kind of cigarette bay leaf extract, it is characterised in that comprise the following steps that：Weigh
The dry basyleaves of 1000g are crushed, and are added 12000mL water immersion, are carried out ultrasonic wave extraction 2h, extract solution is stood into mistake after cooling
Filter, collects filtrate and obtains bay leaf extract；Take after 10g cellulase and the mixing of 20g beta-glucosidases, add 300mL
Water, after dissolving filter, obtain composite enzyme solution；300g composite enzyme solution is added to above-mentioned bay leaf extract, adjusted
The pH value of mixed liquor is saved to 7,30h is digested under the conditions of 25 DEG C, after enzymolysis is finished, filters, obtains after sedimentation 36h under the conditions of 3 DEG C
To the bay leaf extract of clarification；By the bay leaf extract of clarification temperature be 80 DEG C, pressure be decompression under the conditions of 0.01MPa
Concentration, obtains the concentrate that relative density is 1.15, concentrate is filtered after sedimentation 36h under the conditions of 3 DEG C, you can obtain cigarette use
Bay leaf extract.The effect that the basyleave of the more unused compound ferment treatment of bay leaf extract extracted after complex enzyme hydrolysis is extracted
Rate improves 25%.
Embodiment 2, the preparation method of a kind of cigarette bay leaf extract, it is characterised in that comprise the following steps that：Weigh
The dry basyleaves of 1000g are crushed, and are added 15000mL water immersion, are carried out ultrasonic wave extraction 3h, extract solution is stood into mistake after cooling
Filter, collects filtrate and obtains bay leaf extract；Take after 10g cellulase and the mixing of 25g beta-glucosidases, add 300mL
Water, after dissolving filter, obtain composite enzyme solution；300g composite enzyme solution is added to above-mentioned bay leaf extract, adjusted
The pH value of mixed liquor is saved to 6,25h is digested under the conditions of 25 DEG C, after enzymolysis is finished, filters, obtains after sedimentation 36h under the conditions of 3 DEG C
To the bay leaf extract of clarification；By the bay leaf extract of clarification temperature be 70 DEG C, pressure be decompression under the conditions of 0.01MPa
Concentration, obtains the concentrate that relative density is 1.15, concentrate is filtered after sedimentation 36h under the conditions of 3 DEG C, you can obtain cigarette use
Bay leaf extract.The effect that the basyleave of the more unused compound ferment treatment of bay leaf extract extracted after complex enzyme hydrolysis is extracted
Rate improves 30%.
Embodiment 3, the preparation method of a kind of cigarette bay leaf extract, it is characterised in that comprise the following steps that：Weigh
The dry basyleaves of 1000g are crushed, and are added 10000mL water immersion, are carried out ultrasonic wave extraction 2.5h, extract solution is stood into mistake after cooling
Filter, collects filtrate and obtains bay leaf extract；Take after 10g cellulase and the mixing of 40g beta-glucosidases, add 400mL
Water, after dissolving filter, obtain composite enzyme solution；400g composite enzyme solution is added to above-mentioned bay leaf extract, adjusted
The pH value of mixed liquor is saved to 7,20h is digested under the conditions of 25 DEG C, after enzymolysis is finished, filters, obtains after sedimentation 48h under the conditions of 3 DEG C
To the bay leaf extract of clarification；By the bay leaf extract of clarification temperature be 65 DEG C, pressure be decompression under the conditions of 0.01MPa
Concentration, obtains the concentrate that relative density is 1.20, concentrate is filtered after sedimentation 36h under the conditions of 3 DEG C, you can obtain cigarette use
Bay leaf extract.The effect that the basyleave of the more unused compound ferment treatment of bay leaf extract extracted after complex enzyme hydrolysis is extracted
Rate improves 28%.
Embodiment 4, the preparation method of a kind of cigarette bay leaf extract, it is characterised in that comprise the following steps that：Weigh
The dry basyleaves of 1000g are crushed, and are added 8000mL water immersion, are carried out ultrasonic wave extraction 1.5h, extract solution is stood into mistake after cooling
Filter, collects filtrate and obtains bay leaf extract；Take after 10g cellulase and the mixing of 50g beta-glucosidases, add 300mL
Water, after dissolving filter, obtain composite enzyme solution；300g composite enzyme solution is added to above-mentioned bay leaf extract, adjusted
The pH value of mixed liquor is saved to 7,30h is digested under the conditions of 25 DEG C, after enzymolysis is finished, filters, obtains after sedimentation 48h under the conditions of 3 DEG C
To the bay leaf extract of clarification；By the bay leaf extract of clarification temperature be 70 DEG C, pressure be decompression under the conditions of 0.01MPa
Concentration, obtains the concentrate that relative density is 1.25, concentrate is filtered after sedimentation 48h under the conditions of 3 DEG C, you can obtain cigarette use
Bay leaf extract.The effect that the basyleave of the more unused compound ferment treatment of bay leaf extract extracted after complex enzyme hydrolysis is extracted
Rate improves 35%.
Contrast test：Directly sprayed after the bay leaf extract prepared in the present invention is used into concentration for 70% ethanol dilution
It is spread across on pipe tobacco and perfuming is carried out to pipe tobacco, the addition of bay leaf extract is that the ratio of pipe tobacco weight is 5 ‰, then by perfuming
Cigarette is made in pipe tobacco afterwards, allows the professional cigarette personnel that smoke panel test to be smoked panel test；The bay extract prepared simultaneously using common process
It is sprayed onto after concentration is used for 70% ethanol dilution on pipe tobacco and perfuming is carried out to pipe tobacco, the addition of bay leaf extract is cigarette
The ratio of silk weight is 5 ‰, and the pipe tobacco after perfuming is made into cigarette, allows the professional cigarette personnel that smoke panel test to be smoked panel test；And by two kinds
The smoking result of cigarette is contrasted, specific as follows：
Cigarette Contrast on effect
As seen from the above table, act on, make by being combined the cause perfume for the small-molecule substance that the bay leaf extract of ferment treatment is produced
Bay leaf extract possesses abundant cigarette perfume, is improved the effect of fragrance texture, meanwhile, it can obviously reduce stimulation, oral cavity pleasant impression
Totally.
Claims (3)
1. a kind of cigarette preparation method of bay leaf extract, it is characterised in that specific steps include：
(1) the dry basyleaves of 1000g are weighed to crush, 8000mL water immersion is added, ultrasonic wave extraction 1.5h is carried out, extract solution is quiet
Cooled and filtered is put, filtrate is collected and obtains bay leaf extract；The supersonic frequency 50-70KHz, 40 DEG C -60 DEG C of temperature；
(2) take after 10g cellulase and the mixing of 50g beta-glucosidases, add 300mL water, filter, answered after dissolving
Synthase solution；
(3) composite enzyme solution prepared in (2) the step of 300g is added to the bay leaf extract in step (1), regulation is mixed
The pH value of liquid is closed to 7,30h is digested under the conditions of 25 DEG C, after enzymolysis is finished, is filtered after sedimentation 48h under the conditions of 3 DEG C, obtains clear
Clear bay leaf extract；
(4) by the bay leaf extract of clarification in step (3) temperature be 70 DEG C, pressure be to be concentrated under reduced pressure under the conditions of 0.01MPa,
The concentrate that relative density is 1.25 is obtained, concentrate is filtered after sedimentation 48h under the conditions of 3 DEG C, you can obtain cigarette and use bay
Leaf extract.
2. a kind of preparation method of cigarette bay leaf extract according to claim 1, it is characterised in that：Step (1),
Filter type in step (3) and step (4) uses 0.8 μm of ceramic membrane filter.
3. the application of cigarette bay leaf extract prepared by method described in a kind of usage right requirement 1, it is characterised in that：Will be upper
The bay leaf extract for stating method preparation uses concentration to be directly sprayed onto on pipe tobacco to enter pipe tobacco after diluting for 60-80% ethanol
Row perfuming, the addition of bay leaf extract is that the ratio of pipe tobacco weight is 1 ‰ -8 ‰.
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| CN201610578804.9A CN106036982B (en) | 2016-07-20 | 2016-07-20 | A kind of preparation method and applications of cigarette bay leaf extract |
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|---|---|---|---|
| CN201610578804.9A CN106036982B (en) | 2016-07-20 | 2016-07-20 | A kind of preparation method and applications of cigarette bay leaf extract |
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| CN107510091B (en) * | 2017-08-16 | 2019-11-08 | 湖北中烟工业有限责任公司 | A kind of preparation method of the quick-fried pearl essential oil of cigarette |
| WO2020155058A1 (en) * | 2019-01-31 | 2020-08-06 | 邦泰生物工程(深圳)有限公司 | Method for preparing radix codonopsis extract from radix codonopsis leftover material |
| CN112189875A (en) * | 2020-10-23 | 2021-01-08 | 湖北中烟工业有限责任公司 | Polysweet fruit refined extract for cigarettes as well as preparation method and application thereof |
| CN114874855A (en) * | 2022-06-15 | 2022-08-09 | 河南省新郑金叶香料有限公司 | Preparation method of grape extract essence and application of grape extract essence in cigarettes |
| CN115104754B (en) * | 2022-07-11 | 2023-07-07 | 湖北中烟工业有限责任公司 | Dried longan extract for cigarettes and preparation method and application thereof |
| CN115606779A (en) * | 2022-09-27 | 2023-01-17 | 南通奥凯生物技术开发有限公司 | Method for preparing edible essence by deep processing of bay leaf extract |
| CN115820341B (en) * | 2022-10-28 | 2024-02-02 | 延边天翊科技有限公司 | Essence for costustoot charm cigarettes, and preparation method and application thereof |
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| JP2005013138A (en) * | 2003-06-27 | 2005-01-20 | Kiyomitsu Kawasaki | Method for producing spice flavor |
| CN102150948B (en) * | 2011-05-19 | 2012-10-03 | 湖北中烟工业有限责任公司 | Method for preparing jasmine extract for tobacco |
| CN104164454A (en) * | 2014-08-19 | 2014-11-26 | 云南中烟工业有限责任公司 | Magnolia liliiflora fermentation broth extract as well as preparation method and application thereof |
| CN104178517A (en) * | 2014-08-19 | 2014-12-03 | 云南中烟工业有限责任公司 | Lonicera japonica fermented extract and preparation method and application thereof |
| CN104862075A (en) * | 2015-06-03 | 2015-08-26 | 湖北中烟工业有限责任公司 | Preparation method of mullein extract for cigarette |
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