CN110982625A - Licorice-flavored dried beads for cigarette filter tips and preparation method thereof - Google Patents
Licorice-flavored dried beads for cigarette filter tips and preparation method thereof Download PDFInfo
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- CN110982625A CN110982625A CN201911386833.5A CN201911386833A CN110982625A CN 110982625 A CN110982625 A CN 110982625A CN 201911386833 A CN201911386833 A CN 201911386833A CN 110982625 A CN110982625 A CN 110982625A
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- 239000011324 bead Substances 0.000 title claims abstract description 49
- 238000002360 preparation method Methods 0.000 title abstract description 15
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- 239000002826 coolant Substances 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 3
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- 230000008569 process Effects 0.000 description 3
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- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- VTAJIXDZFCRWBR-UHFFFAOYSA-N Licoricesaponin B2 Natural products C1C(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2)C(O)=O)C)(C)CC2)(C)C2C(C)(C)CC1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O VTAJIXDZFCRWBR-UHFFFAOYSA-N 0.000 description 2
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- 239000001685 glycyrrhizic acid Substances 0.000 description 2
- 229960004949 glycyrrhizic acid Drugs 0.000 description 2
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- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 1
- OCKGFTQIICXDQW-ZEQRLZLVSA-N 5-[(1r)-1-hydroxy-2-[4-[(2r)-2-hydroxy-2-(4-methyl-1-oxo-3h-2-benzofuran-5-yl)ethyl]piperazin-1-yl]ethyl]-4-methyl-3h-2-benzofuran-1-one Chemical compound C1=C2C(=O)OCC2=C(C)C([C@@H](O)CN2CCN(CC2)C[C@H](O)C2=CC=C3C(=O)OCC3=C2C)=C1 OCKGFTQIICXDQW-ZEQRLZLVSA-N 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Abstract
The invention discloses a licorice-flavored dry bead for a cigarette filter and a preparation method thereof, wherein the licorice-flavored dry bead for the cigarette filter comprises carrier microspheres, a licorice flavoring agent and a licorice sweetening agent are adsorbed on the carrier microspheres, the licorice flavoring agent accounts for 0.5-8% of the mass of the carrier microspheres, and the licorice sweetening agent accounts for 0.02-0.5% of the mass of the carrier microspheres. The liquorice-flavored dried beads for the cigarette filter can be directly added into the cigarette filter, have the characteristic styles of enriching the baked sweetness and fragrance of cigarettes and highlighting the sweet and moist feeling of liquorice, cover up miscellaneous gas, increase the smooth feeling of smoke and have comfortable aftertaste. The invention has simple preparation process, is easy to add into cigarette filters, is easy to realize mass production, can avoid the surface aroma loss of the tobacco shred flavoring link, and is beneficial to reducing the cost.
Description
Technical Field
The invention relates to the technical field of cigarette production, in particular to a liquorice-flavored dried bead for a cigarette filter and a preparation method thereof.
Background
With the rapid development of the economy of China, the requirement of consumers on the internal quality of cigarettes is higher and higher. Compared with the foreign famous brands, the domestic cigarette products have certain gaps in the aspects of smoking quality, sensory comfort and the like, such as weak fragrance, strong dryness, insufficient sweetness, poorer comfort and the like. Therefore, increasing cigarette aroma, reducing dryness and improving comfort are inevitable trends in the development of domestic cigarettes.
The liquorice is widely applied to the aspects of medicine, food, cosmetics, tobacco, animal husbandry and the like. In the face of its wide application and potential value, people in various fields such as scientific research personnel, scholars, doctors, farmers and the like have increasingly deep knowledge and research on it. The liquorice has good functions of moistening lung, relieving cough and eliminating phlegm, and the liquorice extract has fresh and sweet herb fragrance, strong fragrance, lasting fragrance and soft aftertaste. The flavoring agent has good effects of enriching the cigarette fragrance, improving the taste of smoking, increasing the sweet and moist feeling and covering up the miscellaneous gas when being used in the cigarette, and has good application prospect.
In the cigarette production process, the tobacco shred flavoring process has important significance for forming cigarette style. The traditional tobacco shred flavoring process is to spray surface aroma on the surface of tobacco shreds in a flavoring roller in a spraying mode. The surface aroma of the flavoring mode is only attached to the surface of the cut tobacco and is difficult to permeate into the cut tobacco, so the surface aroma loss is easily caused. Moreover, the surface aroma changes on the surface of the cut tobacco due to combustion, and is not easy to be caught by consumers. In addition, when there are many volatile substances in the top note, the ability to fix the note is difficult to ensure. If the fragrance fixing capacity of the top note needs to be improved, a fragrance fixing agent which is difficult to volatilize needs to be added in the top note, so that the perfuming roller is polluted, the cleaning cost of perfuming equipment is increased, and the problem of perfume pollution among different batches also exists. Therefore, how to provide a technology which can reduce the cost of flavoring the cigarette and avoid the pollution of the spice is a technical problem which needs to be solved urgently in the field.
Patent application No. CN201611113935 discloses a method for preparing tobacco radix Glycyrrhizae extract, comprising puffing radix Glycyrrhizae slice under high pressure, extracting with supercritical CO2, and molecular distilling to obtain tobacco radix Glycyrrhizae extract. The method improves the extraction yield of effective components in the liquorice, the glycyrrhizic acid content in the obtained liquorice extract is higher, and the liquorice extract can play a role in enriching the tobacco fragrance, moistening the smoke and correcting the smoking taste when being applied to cigarettes.
The patent with the application number of CN201810416392.8 discloses a liquorice aroma component for cigarettes and an extraction method and application thereof, belonging to the field of cigarette flavors. The extraction method comprises the following steps: crushing liquorice, adding a mixed solvent consisting of ethanol and water for flash extraction, and filtering to obtain an extracting solution A; concentrating the extracting solution A, adding ethanol for precipitation and impurity removal to obtain an extracting solution B; and concentrating the extracting solution B, adding propylene glycol for aging, and obtaining the lower clear liquid which is the liquorice aroma component for the cigarettes. According to the method for extracting the tobacco liquorice aroma components, liquorice is crushed and then subjected to flash extraction, concentration, precipitation impurity removal, concentration and aging to prepare the tobacco flavor, the method greatly extracts the liquorice aroma components, and miscellaneous substances influencing the cigarette smoking aroma are removed.
The patent with the application number of CN201910266961.X discloses a cigarette filter stick flavor enhancing particle and a cigarette filter stick, wherein the cigarette filter stick flavor enhancing particle comprises a flower fragrance particle and a cool fragrance particle, and the ratio of the flower fragrance particle to the cool fragrance particle is 1:2-1:10 in parts by weight; the flower fragrance granules comprise a flower fragrance agent and flower fragrance master batches, and the mass of the flower fragrance agent is 3 per mill-1% of that of the flower fragrance master batches; the cooling granules comprise a cooling agent and a cooling master batch, and the mass of the cooling agent is 3 per mill-1% of that of the cooling master batch.
In the above patents, the preparation process of the licorice flavor components of the first two inventions is complicated, and the production cost is high; the third patent uses plant flower extract as floral scent agent, menthol as cooling agent to change scent, glycerin or high boiling point alcohol as scent fixing solvent, and kudzu root powder as carrier; the granulation method is not described in detail, and the granulation operation is supposed to be needed, the process is slightly complex, and the improvement of the smoke mainly increases the flower fragrance and the cool feeling. In another patent, the popping beads are used as a carrier, and the puffed food can be taken only after being pinched broken, the preparation process is slightly complex, the quality requirement is high, the yield is low, the fragrance is released quickly after being pinched and broken, the concentration is high, and the feeling of smoking is not uniform.
Disclosure of Invention
The purpose of the invention is as follows: in order to make up for the defects of the prior art, the invention provides the liquorice-flavored dry bead for the cigarette filter and the preparation method thereof.
The technical scheme is as follows: the liquorice-flavored dry beads for the cigarette filter comprise carrier microspheres, wherein liquorice flavoring agents and liquorice sweetening agents are adsorbed on the carrier microspheres, the mass of the liquorice flavoring agents is 0.5-8% of that of the carrier microspheres, and the mass of the liquorice sweetening agents is 0.02-0.5% of that of the carrier microspheres.
Preferably, the licorice flavoring agent accounts for 3-6% of the mass of the carrier microsphere, and the licorice sweetening agent accounts for 0.1-0.3% of the mass of the carrier microsphere; more preferably, the licorice flavor agent accounts for 4-5% of the mass of the carrier microsphere, and the licorice sweetener accounts for 0.1-0.2% of the mass of the carrier microsphere.
The liquorice-flavored dried beads for the cigarette filter tip, which are prepared by the invention, have the characteristic style of enriching the baking sweetness and fragrance of cigarettes, highlighting the sweetness and moistness of the liquorice, covering up miscellaneous gases, increasing the smoothness of smoke and ensuring comfortable aftertaste.
Wherein, the liquorice flavoring agent is mainly used for increasing the unique fragrance of the liquorice, and the liquorice sweetening agent is mainly used for increasing the sweet feeling.
The Glycyrrhrizae radix sweetener is glycyrrhetate (including glycyrrhetinic acid monoglucuronide), is the main sweet component in Glycyrrhrizae radix, and has high sweetness.
The licorice flavoring agent is one of licorice essences, and the preparation method comprises the following steps: adding an ethanol aqueous solution of which the weight ratio is 6-15 times that of liquorice into the liquorice, wherein the mass fraction of the ethanol aqueous solution is 40-95%, performing reflux extraction at the temperature of 70-90 ℃ for 1-3 hours each time for 2-4 times, filtering, combining filtrates, concentrating and drying to obtain an extract; dissolving the extract with ethyl acetate 4-10 times the weight of the extract and water 4-10 times the weight of the extract, extracting for 1-3 times, separating ethyl acetate layer, mixing, concentrating, and drying to obtain Glycyrrhrizae radix flavoring agent. Preferably, in the preparation process of the liquorice flavoring agent, the dosage of the ethanol water solution is 10 times, the mass fraction is 80%, and the liquorice flavoring agent is extracted for 2 times at 85 ℃ and each time lasts for 2 hours; dissolving the extractum with 5 times of ethyl acetate and 5 times of water, and extracting for 1 time. The water layer after extraction contains more glycyrrhizic acid components, and can be used for preparing Glycyrrhrizae radix sweetener.
The carrier microsphere is selected from one or more of various types of macroporous adsorption resins, the mesh number of the carrier microsphere is selected from 4-80 meshes, and D101 macroporous adsorption resin of 40-70 meshes is preferably used. Compared with adsorbing materials such as microcrystalline cellulose and starch, the macroporous adsorption resin has the best adsorption effect, and in the macroporous adsorption resins of various types, the adsorption effect and the cost are comprehensively compared, so that the material cost is reduced under the condition of ensuring a good adsorption effect by the D101 type; the microspheres of 4-80 meshes are all suitable for cigarette filters, but the surface area of the microspheres of 40-70 meshes is large compared with the microspheres of less than 40 meshes, the adsorption speed and the drying speed are higher, while the microspheres of more than 70 meshes are easy to generate static electricity and dust flying, so that the microspheres of 40-70 meshes are optimal.
The invention also provides a preparation method of the liquorice-flavored dried beads for the cigarette filter, which comprises the following steps: and (3) placing the carrier microspheres into a solution containing a liquorice flavoring agent and a liquorice sweetening agent for adsorption, and drying after adsorption. Wherein the drying temperature is 40-60 deg.C, and the drying time is 2-5 h.
Specifically, the preparation method of the liquorice-flavored dried beads for the cigarette filter comprises the following steps:
taking 0.5-8% of liquorice flavoring agent by weight ratio of carrier microspheres, adding 40% of ethanol with volume fraction of 95% for dissolution, taking 0.02-0.5% of liquorice sweetening agent for dissolution by 5% of deionized water, mixing the two solutions, adding the carrier microspheres with required meshes, just immersing the microspheres in the liquid surface, fully adsorbing for 8-24 hours, directly taking out the microspheres, drying for 2-5 hours at 40-60 ℃ until no obvious alcohol taste exists, thus obtaining dry bead particles, and measuring the loss on drying of the dry bead particles to be 5-7%; and (4) excessive drying is not performed so as to avoid odor loss, and finally, a screen with a corresponding mesh number is selected for size stabilization to screen out the target product.
Preferably, the preparation method of the liquorice-flavored dried beads for the cigarette filter comprises the following steps:
taking 3-6% of liquorice flavoring agent by weight of carrier microspheres, adding 40% of ethanol with volume fraction of 95% for dissolving, taking 0.1-0.3% of liquorice sweetening agent for dissolving by using 5% of deionized water, mixing the two solutions, adding the carrier microspheres with required meshes, just immersing the microspheres on the liquid surface, fully adsorbing for 12-16 hours, directly taking out the microspheres, drying for 2.5-3.5 hours at 50-55 ℃ until no obvious alcohol smell exists, thus obtaining dry bead particles, and measuring the drying weight loss of the dry bead particles to be 5.5-6.5%; and (4) excessive drying is not performed so as to avoid odor loss, and finally, a screen with a corresponding mesh number is selected for size stabilization to screen out the target product.
Has the advantages that:
the liquorice-flavored dry beads for the cigarette filter tip disclosed by the invention are added with the fragrance component and the sweet component extracted from the liquorice, are healthy and harmless, have the characteristic styles of enriching the baking sweet fragrance of cigarettes and highlighting the sweet feeling of the liquorice, cover up miscellaneous gas, increase the smooth feeling of smoke and have comfortable aftertaste. The preparation process is simple, the flavoring agent is easy to add into cigarette filters, mass production is easy to realize, the surface aroma loss of the tobacco shred flavoring link can be avoided, and the cost is reduced.
Detailed Description
The invention will be further elucidated with reference to the following specific examples.
In a particular embodiment of the present invention, the substrate is,
the preparation method of the liquorice flavoring agent comprises the following steps:
adding an ethanol water solution with the weight ratio of 10 times that of the liquorice into the liquorice, wherein the mass fraction of the ethanol water solution is 80%, performing reflux extraction for 2 times at the temperature of 85 ℃, each time for 2 hours, filtering, combining filtrates, concentrating and drying to obtain an extract; and dissolving the extract by using ethyl acetate and water in an amount which is 5 times of the weight of the extract, extracting for 1 time, separating an ethyl acetate layer, combining, concentrating and drying to obtain the liquorice flavoring agent.
The licorice sweeteners used in the following examples are all glycyrrhetinic acid monoglucuronide, sourced from yillier canary biotechnology limited.
The carrier microsphere is D101 macroporous adsorption resin of 40-70 meshes.
Example 1A Licorice root flavored dried bead for cigarette Filter
The following amounts (mass fractions) are based on the mass of the D101 macroporous adsorbent resin.
Dissolving 5% of liquorice flavoring agent in 40% of 95% ethanol by volume, dissolving 0.2% of liquorice sweetening agent in 5% of deionized water, mixing the two solutions, adding 40-70 mesh D101 resin, soaking the microspheres for 16 hours to fully adsorb, directly taking out, drying at 50-55 ℃ for 2.5-3.5 hours until no obvious alcohol taste exists, and obtaining dry bead particles, wherein the weight loss of the dry bead particles is about 6.1% by measurement; must not be over-dried to avoid odor loss; finally, sieving with a sieve of 40-70 meshes to obtain the final product.
Example 2A Licorice root flavored dried bead for cigarette Filter
The following amounts (mass fractions) are based on the mass of the D101 macroporous adsorbent resin.
Dissolving 8% of liquorice flavoring agent in 95% ethanol with the volume fraction of 40%, dissolving 0.5% of liquorice sweetening agent in 5% deionized water, mixing the two solutions, adding 40-70 mesh D101 resin, soaking the microspheres for 16 hours to fully adsorb, directly taking out the microspheres, drying at 50-55 ℃ for 2.5-3.5 hours until no obvious alcohol taste exists, thus obtaining dry bead particles, and measuring the weight loss of the dry bead particles to be about 6.5%; must not be over-dried to avoid odor loss; finally, sieving with a sieve of 40-70 meshes to obtain the final product.
Example 3A Licorice root flavored dried bead for cigarette Filter
The following amounts (mass fractions) are based on the mass of the D101 macroporous adsorbent resin.
Dissolving 6% of liquorice flavoring agent in 95% ethanol with the volume fraction of 40%, dissolving 0.3% of liquorice sweetening agent in 5% deionized water, mixing the two solutions, adding 40-70 mesh D101 resin, soaking the microspheres for 16 hours to fully adsorb, directly taking out the microspheres, drying at 50-55 ℃ for 2.5-3.5 hours until no obvious alcohol taste exists, thus obtaining dry bead particles, and measuring the weight loss of the dry bead particles to be about 6.3%; must not be over-dried to avoid odor loss; finally, sieving with a sieve of 40-70 meshes to obtain the final product.
Example 4A Licorice root flavored dried bead for cigarette Filter
The following amounts (mass fractions) are based on the mass of the D101 macroporous adsorbent resin.
Dissolving 3% of liquorice flavoring agent in 40% of 95% ethanol by volume, dissolving 0.1% of liquorice sweetening agent in 5% of deionized water, mixing the two solutions, adding 40-70 mesh D101 resin, soaking the microspheres for 16 hours for full adsorption, taking out the microspheres after the liquid surface is dried, drying the microspheres at 50-55 ℃ for 2.5-3.5 hours until no obvious alcohol taste exists, and obtaining dry bead particles, wherein the weight loss of the dry bead particles is measured to be about 5.8%; must not be over-dried to avoid odor loss; finally, sieving with a sieve of 40-70 meshes to obtain the final product.
EXAMPLE 5 Licorice-flavored dried beads for cigarette Filter
The following amounts (mass fractions) are based on the mass of the D101 macroporous adsorbent resin.
Dissolving 0.5% of liquorice flavoring agent in 40% of 95% ethanol by volume, dissolving 0.05% of liquorice sweetening agent in 5% of deionized water, mixing the two solutions, adding 40-70 mesh D101 resin, soaking the microspheres in the solution for 16 hours for full adsorption, taking out the microspheres after the solution is dried, drying the microspheres at 50-55 ℃ for 2.5-3.5 hours until no obvious alcohol taste exists, and obtaining dry bead particles, wherein the weight loss of the dry bead particles is measured to be about 5.3%; must not be over-dried to avoid odor loss; finally, sieving with a sieve of 40-70 meshes to obtain the final product.
Example 6 sensory evaluation test
The liquorice-flavored dry beads are placed in the center of a filter stick through a filter stick forming machine and added into a cigarette filter stick, the dry beads are placed in the middle of the filter stick, 150mg of dry beads are added into each cigarette, and then a cigarette sample is rolled and connected to obtain the liquorice-flavored dry bead cigarette.
Sensory comparative smoking was performed on the applied samples, with 10 members of the sensory smoking panel, and the standard for smoking was as described in GB5606.4-2005 "part 4 of cigarettes: sensory technical requirements, the average of the results of the smoke panel test. The 'gloss' item in the standard is the appearance shape of the cut tobacco and does not participate in evaluation.
TABLE 1 Licorice root flavor dried bead cigarette smoking result table
| Sample (I) | Fragrance | Coordination of | Miscellaneous qi | Stimulation of | Aftertaste | Total up to |
| Blank sample | 24.3 | 4.0 | 8.1 | 15.2 | 20.4 | 72 |
| Example 1 | 26.5 | 4.8 | 8.6 | 16.3 | 21.2 | 77.4 |
| Example 2 | 26.8 | 3.9 | 7.8 | 14.1 | 20.7 | 73.3 |
| Example 3 | 26.6 | 4.6 | 8.5 | 15.8 | 20.9 | 76.4 |
| Example 4 | 25.3 | 4.5 | 8.4 | 15.5 | 20.7 | 74.4 |
| Example 5 | 24.6 | 4.3 | 8.2 | 15.4 | 20.6 | 73.1 |
From the above results, it can be seen that the addition of the dry licorice-flavored beads of the present invention enriches the characteristic style of the sweet and fragrant baked cigarette, highlights the sweet and moist feeling of licorice, masks offensive odor, increases the smooth feeling of smoke, and provides a pleasant aftertaste, with preferred embodiments 1 and 3.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. The licorice-flavored dry beads for the cigarette filter are characterized by comprising carrier microspheres, wherein licorice flavoring agents and licorice sweetening agents are adsorbed on the carrier microspheres, the mass of the licorice flavoring agents is 0.5-8% of that of the carrier microspheres, and the mass of the licorice sweetening agents is 0.02-0.5% of that of the carrier microspheres.
2. The licorice-flavored dry beads for cigarette filters according to claim 1, wherein the licorice flavor is 3 to 6% by mass of the carrier microspheres, and the licorice sweetener is 0.1 to 0.3% by mass of the carrier microspheres.
3. The licorice-flavored dry bead for cigarette filters according to claim 1, wherein the licorice sweetener is glycyrrhetate.
4. The licorice-flavored dry beads for cigarette filters according to claim 3, wherein the glycyrrhetate is glycyrrhetinic acid monoglucuronide.
5. The licorice-flavored dried beads for cigarette filters according to claim 1, wherein the licorice flavor is prepared by the following method: adding an ethanol aqueous solution of which the weight ratio is 6-15 times that of liquorice into the liquorice, wherein the mass fraction of the ethanol aqueous solution is 40-95%, performing reflux extraction at the temperature of 70-90 ℃ for 1-3 hours each time for 2-4 times, filtering, combining filtrates, concentrating and drying to obtain an extract; dissolving the extract with ethyl acetate 4-10 times the weight of the extract and water 4-10 times the weight of the extract, extracting for 1-3 times, separating ethyl acetate layer, mixing, concentrating, and drying to obtain Glycyrrhrizae radix flavoring agent.
6. The licorice-flavored dried beads for cigarette filters according to claim 1, wherein the carrier microspheres are macroporous adsorbent resins.
7. The licorice-flavored dried beads for cigarette filters according to claim 6, wherein the macroporous adsorbent resin is D101 macroporous adsorbent resin.
8. The licorice-flavored dried beads for cigarette filters according to claim 1, wherein the carrier microspheres have a mesh size of 4 to 80 mesh.
9. The method for preparing licorice-flavored dried beads for cigarette filters according to any one of claims 1 to 8, comprising: and (3) placing the carrier microspheres into a solution containing a liquorice flavoring agent and a liquorice sweetening agent for adsorption, and drying after adsorption.
10. The method for preparing licorice-flavored dried beads for cigarette filters according to claim 9, wherein the drying temperature is 40-60 ℃ and the drying time is 2-5 hours.
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