CN106867675A - A kind of cigarette preparation method of Momordica grosvenori essence - Google Patents
A kind of cigarette preparation method of Momordica grosvenori essence Download PDFInfo
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- CN106867675A CN106867675A CN201710093929.7A CN201710093929A CN106867675A CN 106867675 A CN106867675 A CN 106867675A CN 201710093929 A CN201710093929 A CN 201710093929A CN 106867675 A CN106867675 A CN 106867675A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
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- Agronomy & Crop Science (AREA)
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- General Health & Medical Sciences (AREA)
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
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Abstract
The invention belongs to tobacco aromaticss technical field, a kind of preparation method of cigarette Momordica grosvenori essence is disclosed, including：Alcohol extracting, Maillard reaction, the step such as ester is carried, refined filtration is purified, be concentrated under reduced pressure.The present invention is reached cigarette flavouring using Maillard reaction, subtracts miscellaneous gas, reduce irritating purpose, and way of purification is separated using extraction, macroporous resin adsorption etc., eliminate the unfavorable product in part, after gained essence is added into cigarette, significantly improve the sweet sense of cigarette smoking, increase sensory comfort, while on the exterior quality of cigarette without influence.
Description
Technical field
Used as extract prepares Momordica grosvenori cigarette with Momordica grosvenori the invention belongs to tobacco aromaticss technical field, more particularly to one kind
The method of essence.
Background technology
Momordica grosvenori is the distinctive cucurbitaceous plant of China, is of high nutritive value, find a good sale in the country such as Japan, Southeast Asia and Hongkong and Macro and
Area.Containing carbohydrate easily absorbed by the body, rich in vitamin, wherein oleic acid and linoleic acid accounts for the 73.2% of TFA, is
Pharmaceutically treat coronary heart disease and the ideal grease of prevention vascular sclerosis.Its is sweet, cool in nature, have removing heat from the lung to relieve cough, moistening lung defaecation,
Disappear pyrolysis heat, eliminating the phlegm, and beneficial liver is promoted the production of body fluid and quenches one's thirst, and promotes stomach and intestine function, suppresses the effects such as asthma and step-down.To chronic bronchitis,
Tonsillitis, sphagitis, pertussis and phlegm-fire cough etc. have good therapeutic effect.In addition to dry fruit product, kind can be also processed into
The various product of class, has application in industries such as medicine, food.
Tobacco can not only produce the fragrance of pleasant pleasure in combustion, can also produce some miscellaneous gas and bitterness, pungent
Taste.Add《Tobacco international framework pact》Implementation, low tar Less harmful cigarette will turn into future world cigarette master
Stream, this inevitably leads to cigarette odor-absorbing reduction, and fragrance is thin out.Therefore, State Tobacco Monopoly Bureau exists《It is long in tobacco business
Phase science and technology development planning outline》In propose flavouring humectation key special subjects work.Exploitation it is new with improve cigarette taste, carry
The natural tobacco aromaticss of cigarette comfort level high, are the active demands of current tobacco industry.
In recent years, spices is prepared by Maillard reaction to have been studied for cigarette flavouring, but due to Chinese medicine such as Momordica grosvenori
Composition is more and complicated, and its reaction with amino acid and its derivative, i.e. Maillard reaction are in itself that need to experience three stages of reaction
Complex process, the maillard reaction product for obtaining usually contains the tens of kinds of materials, these things such as aldehyde, ketone, alcohol, pyrroles, acid, ester
Matter is added into cigarette, and the local flavor of generation and the influence to cigarette are often multi-level, entirely not desired, example
Some new miscellaneous gas and excitant are such as produced, even more so that cigarette is in modulation, ageing and in long-term placement, and yellowing changes colour, because
This, still needing will develop new preparation method, preferably reduce excitant and miscellaneous gas in sucking process, flavouring upgrading, while keeping away
Exempt from the color and luster change in Cigarette processing.
The content of the invention
The invention provides a kind of method that flavouring essence for tobacco is prepared with Fructus Monordicae extract, by arhat obtained in the present invention
Fruity essence and cigarette odor-absorbing phase harmony, significantly increase the sweet sense of cigarette smoking, reduce oral cavity and throat's appearance in aspiration procedure
Burning heat sensation and the peppery sense of thorn, the effects such as with miscellaneous gas, lifting cigarette perfume is reduced.
A kind of cigarette preparation method of Momordica grosvenori essence, it is characterised in that comprise the following steps：
Step one：Momordica grosvenori fresh fruit is crushed, the 75%-95% ethanol solutions of its 3-5 times of quality are added, stirred,
Temperature leaching 3-5h, obtains extract solution at 50-70 DEG C；
Step 2：After extract solution is filtered, Fructus Monordicae extract is concentrated under reduced pressure to give；
Step 3：To amino acid and its derivative is added in Fructus Monordicae extract, 1-6h is reacted at 70-130 DEG C；
Step 4：After adding ethyl acetate ultrasonic extraction, extract is concentrated under reduced pressure to give；
Step 5：To 200-600 weight portion macroporous absorbent resin HPD-100 are added in the extract that step 4 is obtained, first
Washed with deionized water, be washed till colourless, then with the 4-7 times of 50%-80% ethanol elution of resin volume, collect eluent, wash-out
Liquid obtains ultrafiltrate through hollow fiber membrane ultrafiltration device ultrafiltration；
Step 6：After to ultrafiltrate be concentrated under reduced pressure, cigarette Momordica grosvenori essence is obtained final product.
Preferably, concentrated under reduced pressure in the step 2, four, six is entered at vacuum 0.08-0.5MPa and 50-70 DEG C
OK.
Preferably, the amino acid and its derivative are one or more selected from aspartic acid, glutamine, L- paddy ammonia
Acid, L-PROLINE, L-Aspartic acid, serine, glutamic acid, histidine, glycine, threonine, arginine, alanine or bad ammonia
The amino acid and its derivative of acid.
It is particularly preferred that the amino acid is the mixture of glutamine and serine.
Preferably, the step 3 reacts 1-5h at 80-120 DEG C of temperature.
Preferably, the step 4, Momordica grosvenori and ethyl acetate ratio are 1:1-1:2,50-60 DEG C of ultrasonic temperature, time
5-15min。
The Momordica grosvenori essence that method produced according to the present invention is obtained, it is in reconstituted tobacoo, pipe tobacco and mouth rod as addition
Agent is used.
The Momordica grosvenori essence that preparation method of the present invention is obtained as additive use when, can be through propane diols, ethanol, glycerine
In a kind of dissolving after make an addition to pipe tobacco, also can be preferably added in mouth rod after glyceryl triacetate dilution through esters.
General, the product after Maillard reaction may be directly applied in cigarette, reaches flavouring, subtracts miscellaneous gas, and reducing stimulates
Property purpose, and present invention applicant it was unexpectedly observed that Fructus Monordicae extract and amino acid are carried out into Maillard reaction after prepare
Product when being applied in cigarette, not only miscellaneous gas and excitant reduce substantially, it is clear without play that Momordica grosvenori should have completely
The effect of Shu Run is swallowed, meanwhile, unexpectedly, after product is added into cigarette, in later stage modulation, ageing and longer-term storage
In, can cause that cigarette gradually turns yellow and lose color and luster, influence attractive in appearance.The present invention is by specific extraction, absorption and combined filtering
Etc. isolation technics, it is unhelpful to flue gas aesthetic quality to eliminate part, and to the maillard reaction product that cigarette outward appearance is damaged, so that
Reach the purpose for improving natural tobacco quality of flavoring, the more general tobacco aromaticss perfume produced as raw material with Momordica grosvenori of gained essence
Makings is fine and smooth, alcohol and, and cigarette quality is also more stable.
The preferably mixture of glutamine and serine of the invention carries out Maillard reaction with Fructus Monordicae extract, especially excellent
The ratio for selecting glutamine and serine is 2.5:1, the fragrance matter threshold value that the essence that it is obtained is produced is relatively lower, can be at it
30% is reduced on the basis of essence addition prepared by his amino acid, good flavouring effect just can be reached with few addition.
The part comparative example being set forth below in research process of the present invention is better illustrated with to the present invention.
Comparative example
Comparative example 1
Momordica grosvenori fresh fruit is crushed, to 3L95% ethanol is added in the Momordica grosvenori of 1kg, is stirred, control centre's temperature
It is 60 DEG C of temperature leaching 4h.Be concentrated under reduced pressure to obtain Fructus Monordicae extract after extract solution is filtered.To addition 20g L-PROLINEs in extract,
30g glycine, 4h is reacted at 110 DEG C, and natural cooling obtains Momordica grosvenori maillard reaction thing, is filtered using ceramic membrane element, is subtracted
After pressure concentration, cigarette Momordica grosvenori essence is obtained final product.
Comparative example 2
Momordica grosvenori fresh fruit is crushed, to 3L95% ethanol is added in the Momordica grosvenori of 1kg, is stirred, control centre's temperature
It is 60 DEG C of temperature leaching 4h.Be concentrated under reduced pressure to obtain Fructus Monordicae extract after extract solution is filtered.To addition 20g L-PROLINEs in extract,
30g glycine, 4h is reacted at 110 DEG C, and natural cooling obtains Momordica grosvenori maillard reaction thing, plus 200g macroporous absorbent resins
D101, is first eluted with acid solution, and colourless, collection eluent is then washed to deionized water, and eluent is through hollow fiber membrane ultrafiltration device
Ultrafiltration obtains ultrafiltration.After to filtrate be concentrated under reduced pressure, cigarette Momordica grosvenori essence is obtained final product.
Comparative example 3
Momordica grosvenori fresh fruit is crushed, to 3L95% ethanol is added in the Momordica grosvenori of 1kg, is stirred, control centre's temperature
It is 60 DEG C of temperature leaching 4h.Be concentrated under reduced pressure to obtain Fructus Monordicae extract after extract solution is filtered.To addition 20g L-PROLINEs in extract,
30g glycine, 4h is reacted at 110 DEG C, and natural cooling obtains Momordica grosvenori maillard reaction thing, and supernatant is removed in centrifugation, upper poly-
Amide resin post is adsorbed, and first with 15 DEG C of washing post, then is eluted with 65% ethanol solution, collects eluent, and eluent is through hollow
Fibrous ultrafilter ultrafiltration obtains ultrafiltration.After to filtrate be concentrated under reduced pressure, cigarette Momordica grosvenori essence is obtained final product.
Comparative example 5
Momordica grosvenori fresh fruit is crushed, to 3L95% ethanol is added in the Momordica grosvenori of 1kg, is stirred, control centre's temperature
It is 50 DEG C of temperature leaching 5h.Be concentrated under reduced pressure to obtain Fructus Monordicae extract after extract solution is filtered.To addition 20g L-PROLINEs in extract,
30g glycine, 4h is reacted at 110 DEG C, and natural cooling obtains Momordica grosvenori maillard reaction thing, adds 500mL ethyl acetate 50
At DEG C after ultrasonic extraction 10min, it is concentrated under reduced pressure.200g macroporous absorbent resin HPD-100 are added in concentrate, first with deionization
Water is washed, and is washed till colourless, then with 4 times of 50% ethanol elutions of resin volume, collects eluent, and eluent is through Hollow Fiber Ultrafiltration
Device ultrafiltration obtains ultrafiltrate.After to filtrate be concentrated under reduced pressure, cigarette Momordica grosvenori essence is obtained final product.
Comparative example 6
Momordica grosvenori fresh fruit is crushed, to 3L95% ethanol is added in the Momordica grosvenori of 1kg, is stirred, control centre's temperature
It is 50 DEG C of temperature leaching 5h, be concentrated under reduced pressure to obtain Momordica grosvenori concentrate after extract solution is filtered.200g macroporous absorptions are added in concentrate
Resin HPD-100, is first washed with deionized water, is washed till colourless, then with 4 times of 50% ethanol elutions of resin volume, collects wash-out
Liquid, eluent obtains ultrafiltrate through hollow fiber membrane ultrafiltration device ultrafiltration, filtrate is carried out it is concentrated under reduced pressure after, to adding 20g in concentrate
L-PROLINE, 30g glycine reacts 4h at 110 DEG C, and natural cooling obtains Momordica grosvenori maillard reaction thing, concentrated under reduced pressure to obtain final product
Cigarette Momordica grosvenori essence.
Sample prepared by comparative example 1-6 is sprayed onto above low-grade pipe tobacco respectively, spray amount is 2.0 ‰ left sides of tobacco quality
The right side, adds the dilution of 2mL ethanol solutions, is uniformly sprayed on pipe tobacco and is rolled according to the standard of every cigarette gross weight (0.80 ± 0.01) g
Sample, according to Standard, balances 24h evaluation marks in the climatic chamber of temperature (22 ± 2) DEG C relative humidity (60 ± 5) %
Standard asks that the 10 people groups of smokeing panel test carry out sensory evaluating smoking with reference to YC/T138-1998 tobaccos and tobacco product sensory evaluation method, from light
6 indexs such as the damp miscellaneous gas excitant of fragrance harmony and pleasant impression are scored respectively, draw matter of the total score as flue-cured tobacco bud spices
Amount evaluation criterion, while observing color and luster change of the cigarette during technique and storage, concrete outcome table 1.
The comparative example 1-6 sensory evaluation scores of table 1 and color and luster change
Specific embodiment
The technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, this area is common
The every other embodiment that technical staff is obtained under the premise of creative work is not made, belongs to the model of present invention protection
Enclose.
In order to the present invention is described in more detail, it is with Momordica grosvenori to one kind that the present invention is provided with reference to specific embodiment
The method that extract prepares flavouring essence for tobacco is specifically described.
Embodiment 1
Momordica grosvenori fresh fruit is crushed, to 3L95% ethanol is added in the Momordica grosvenori of 1kg, is stirred, control centre's temperature
It is 50 DEG C of temperature leaching 5h.0.5MPa, 70 DEG C of Fructus Monordicae extracts that are concentrated under reduced pressure to obtain after extract solution is filtered.Added in extract
20g lysines, 30g alanine reacts 4h at 110 DEG C, and natural cooling obtains Momordica grosvenori maillard reaction thing.Add 500mL second
Acetoacetic ester after ultrasonic extraction 10min at 50 DEG C, 0.4MPa, 60 DEG C be concentrated under reduced pressure.200g macroporous absorptions are added in concentrate
Resin HPD-100, is first washed with deionized water, is washed till colourless, then with 4 times of 50% ethanol elutions of resin volume, collects wash-out
Liquid, eluent obtains ultrafiltrate through hollow fiber membrane ultrafiltration device ultrafiltration.After to filtrate 0.5MPa, 70 DEG C be concentrated under reduced pressure, cigarette is obtained final product
Use Momordica grosvenori essence.
Embodiment 2
Momordica grosvenori fresh fruit is crushed, to 4L75% ethanol is added in the Momordica grosvenori of 1kg, is stirred, control centre's temperature
It is 60 DEG C of temperature leaching 4h.0.4MPa, 50 DEG C of Fructus Monordicae extracts that are concentrated under reduced pressure to obtain after extract solution is filtered.Added in extract
35g L-Aspartic acids, 6h is reacted at 70 DEG C, and natural cooling obtains Momordica grosvenori maillard reaction thing.Add 500mL ethyl acetate
After ultrasonic extraction 15min at 60 DEG C, 0.4MPa, 50 DEG C be concentrated under reduced pressure.300g macroporous absorbent resins are added in concentrate
HPD-100, is first washed with deionized water, is washed till colourless, then with 5 times of 70% ethanol elutions of resin volume, collects eluent, is washed
De- liquid obtains ultrafiltration through hollow fiber membrane ultrafiltration device ultrafiltration.After to filtrate 0.4MPa, 50 DEG C be concentrated under reduced pressure, cigarette Momordica grosvenori is obtained final product
Essence.
Embodiment 3
Momordica grosvenori fresh fruit is crushed, to 5L80% ethanol is added in the Momordica grosvenori of 1kg, is stirred, control centre's temperature
It is 70 DEG C of temperature leaching 3h.0.5MPa, 70 DEG C of Fructus Monordicae extracts that are concentrated under reduced pressure to obtain after extract solution is filtered.Added in extract
50g glutamine, 20g serines react 6h at 90 DEG C, and natural cooling obtains Momordica grosvenori maillard reaction thing.Add 350mL second
Acetoacetic ester after ultrasonic extraction 10min at 60 DEG C, 0.5MPa, 70 DEG C be concentrated under reduced pressure.400g macroporous absorptions are added in concentrate
Resin HPD-100, is first washed with deionized water, is washed till colourless, then with 6 times of 80% ethanol elutions of resin volume, collects wash-out
Liquid, eluent obtains ultrafiltration through hollow fiber membrane ultrafiltration device ultrafiltration.After to filtrate 0.5MPa, 70 DEG C be concentrated under reduced pressure, cigarette use is obtained final product
Momordica grosvenori essence.
Embodiment 4
Momordica grosvenori fresh fruit is crushed, to 4L95% ethanol is added in the Momordica grosvenori of 1kg, is stirred, control centre's temperature
It is 60 DEG C of temperature leaching 4h.0.5MPa, 70 DEG C of Fructus Monordicae extracts that are concentrated under reduced pressure to obtain after extract solution is filtered.Added in extract
35g glutamic acid, 5h is reacted at 120 DEG C, and natural cooling obtains Momordica grosvenori maillard reaction thing.350mL ethyl acetate is added 50
At DEG C after ultrasonic extraction 10min, 0.5MPa, 70 DEG C be concentrated under reduced pressure.600g macroporous absorbent resins HPD- is added in concentrate
100, first washed with deionized water, it is washed till colourless, then with 7 times of 80% ethanol elutions of resin volume, collect eluent, eluent
Ultrafiltration is obtained through hollow fiber membrane ultrafiltration device ultrafiltration.After to filtrate 0.5MPa, 70 DEG C be concentrated under reduced pressure, cigarette arhat fruity is obtained final product
Essence.
Embodiment 5
Momordica grosvenori fresh fruit is crushed, to 4L95% ethanol is added in the Momordica grosvenori of 1kg, is stirred, control centre's temperature
It is 55 DEG C of temperature leaching 4h.0.5MPa, 70 DEG C of Fructus Monordicae extracts that are concentrated under reduced pressure to obtain after extract solution is filtered.Added in extract
10g arginine, 40g threonines react 5h at 120 DEG C, and natural cooling obtains Momordica grosvenori maillard reaction thing.Add 500mL second
Acetoacetic ester after ultrasonic extraction 10min at 55 DEG C, 0.5MPa, 70 DEG C be concentrated under reduced pressure.500g macroporous absorptions are added in concentrate
Resin HPD-100, is first washed with deionized water, is washed till colourless, then with 7 times of 60% ethanol elutions of resin volume, collects wash-out
Liquid, eluent obtains ultrafiltration through hollow fiber membrane ultrafiltration device ultrafiltration.After to filtrate 0.5MPa, 70 DEG C be concentrated under reduced pressure, cigarette use is obtained final product
Momordica grosvenori essence.
When using, this tobacco aromatics is dissolved through propane diols, ethanol, glycerine equal solvent, can be used for tobacco perfuming, through three second
Acid glyceride dissolving can be used for mouth rod perfuming.Cigarette trial-production sample is made according to production of cigarettes operation.
Each embodiment essence addition, sensory evaluating smoking and color and luster result of variations are shown in Table 2.
The embodiment 1-5 sensory evaluation scores of table 2, color and luster change and essence addition
| Embodiment | Sensory evaluation scores/100 point | Color and luster changes | Essence addition |
| Embodiment 1 | 90.6 | It is unchanged | The 2.3 ‰ of tobacco quality |
| Embodiment 2 | 86.3 | It is unchanged | The 2.1 ‰ of tobacco quality |
| Embodiment 3 | 93.1 | It is unchanged | The 1.4 ‰ of tobacco quality |
| Embodiment 4 | 85.7 | It is unchanged | The 1.8 ‰ of tobacco quality |
| Embodiment 5 | 92.5 | It is unchanged | The 2.0 ‰ of tobacco quality |
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of cigarette preparation method of Momordica grosvenori essence, it is characterised in that comprise the following steps：
Step one：Momordica grosvenori fresh fruit is crushed, the 75%-95% ethanol solutions of its 3-5 times of quality are added, stirred, in 50-
Temperature leaching 3-5h, obtains extract solution at 70 DEG C；
Step 2：After extract solution is filtered, Fructus Monordicae extract is concentrated under reduced pressure to give；
Step 3：To amino acid and its derivative is added in Fructus Monordicae extract, 1-6h is reacted at 70-130 DEG C；
Step 4：After adding ethyl acetate ultrasonic extraction, extract is concentrated under reduced pressure to give；
Step 5：To 200-600 weight portion macroporous absorbent resin HPD-100 are added in the extract that step 4 is obtained, first going
Ionized water is washed, and is washed till colourless, then with the 4-7 times of 50%-80% ethanol elution of resin volume, collects eluent, eluent warp
Hollow fiber membrane ultrafiltration device ultrafiltration obtains ultrafiltrate；
Step 6：After to ultrafiltrate be concentrated under reduced pressure, cigarette Momordica grosvenori essence is obtained final product.
2. preparation method according to claim 1, it is characterised in that concentrated under reduced pressure in the step 2, four, six be
Vacuum 0.08-0.5MPa with 50-70 DEG C at carry out.
3. preparation method according to claim 1, it is characterised in that the amino acid and its derivative are one or more
Selected from aspartic acid, glutamine, Pidolidone, L-PROLINE, L-Aspartic acid, serine, glutamic acid, histidine, sweet ammonia
The amino acid and its derivative of acid, threonine, arginine, alanine or lysine.
4. preparation method according to claim 1, it is characterised in that the amino acid is the mixed of glutamine and serine
Compound.
5. preparation method according to claim 1, it is characterised in that the step 3 reacts 1- at 80-120 DEG C of temperature
5h。
6. preparation method according to claim 1, it is characterised in that the step 4, Momordica grosvenori and ethyl acetate ratio are
1:1-1:2,50-60 DEG C of ultrasonic temperature, time 5-15min.
7. the Momordica grosvenori essence that the preparation method according to claim 1-6 is obtained, it makees in reconstituted tobacoo, pipe tobacco and mouth rod
For additive is used.
8. the Momordica grosvenori essence that the preparation method according to claim 1-6 is obtained, its when being used as additive, through the third two
One kind in alcohol, ethanol, glycerine makes an addition in pipe tobacco after dissolving.
9. the Momordica grosvenori essence that the preparation method according to claim 1-6 is obtained, its when being used as additive, through esters
It is added to after dilution in mouth rod.
10. the Momordica grosvenori essence that the preparation method according to claim 1-6 is obtained, its when being used as additive, through three
It is added in mouth rod after acetin dilution.
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| CN109022151A (en) * | 2018-07-13 | 2018-12-18 | 江苏浩丰生物科技有限公司 | A kind of cigarette of Siraitia grosvenorii flavor quick-fried pearl liquid and preparation method thereof |
| CN109090702A (en) * | 2018-06-29 | 2018-12-28 | 郑州轻工业学院 | The preparation method and applications of Luo Han Guo Paste In Foods maillard reaction product |
| CN109527643A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
| CN109537365A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper |
| CN109924535A (en) * | 2019-03-04 | 2019-06-25 | 海口日岛香料有限公司 | Flower of Fructus Momordicae burns and sucks the preparation method and application spilt in category shredded tobacco for water pipes in flowers and fruits |
| CN111378528A (en) * | 2018-12-29 | 2020-07-07 | 贵州中烟工业有限责任公司 | Method for preparing spice by using fructus momordicae extract as raw material and adopting microchannel reactor and application of method |
| CN114836261A (en) * | 2022-05-06 | 2022-08-02 | 云南中烟新材料科技有限公司 | Method for extracting old medicine orange spice and application of old medicine orange spice in cigarette filter tip |
| WO2022206689A1 (en) * | 2021-04-01 | 2022-10-06 | Epc Natural Products Co., Ltd. | Sweetener and flavoring compositions prepared by glycosylated mogrosides or monk fruit extracts, method of making and method of use thereof |
| CN115161117A (en) * | 2022-07-11 | 2022-10-11 | 湖北中烟工业有限责任公司 | Preparation method and application of Maillard reactant of momordica grosvenori extract |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1854149A (en) * | 2005-04-30 | 2006-11-01 | 永州市希尔天然物料有限公司 | Extraction of Momordica grosvenori beet aglucone V |
| CN101029071A (en) * | 2007-04-05 | 2007-09-05 | 上海交通大学 | Method for preparing high-purity Momordia grosvenori aglycone from Momordia grosvenori |
| CN101496638A (en) * | 2009-03-11 | 2009-08-05 | 云南天宏香精香料有限公司 | Additive agent for Chinese herbal medicine tobacco as well as preparation method and application |
| CN101633866A (en) * | 2009-06-02 | 2010-01-27 | 华宝食用香精香料（上海）有限公司 | Cigarette siraitia grosvenorii additive and preparation method and application thereof |
| CN102408463A (en) * | 2011-11-15 | 2012-04-11 | 威海天泓农业科技有限公司 | Extraction method for mogroside |
| CN102960856A (en) * | 2012-12-10 | 2013-03-13 | 红塔烟草(集团)有限责任公司 | Salty-reducing additive for tobaccos, and preparation method and application of salty-reducing additive |
| JP2014201671A (en) * | 2013-04-05 | 2014-10-27 | 長興実業株式会社 | Flavoring aroma improver and food perfume composition including momordicae fruit extract |
-
2017
- 2017-02-21 CN CN201710093929.7A patent/CN106867675B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1854149A (en) * | 2005-04-30 | 2006-11-01 | 永州市希尔天然物料有限公司 | Extraction of Momordica grosvenori beet aglucone V |
| CN101029071A (en) * | 2007-04-05 | 2007-09-05 | 上海交通大学 | Method for preparing high-purity Momordia grosvenori aglycone from Momordia grosvenori |
| CN101496638A (en) * | 2009-03-11 | 2009-08-05 | 云南天宏香精香料有限公司 | Additive agent for Chinese herbal medicine tobacco as well as preparation method and application |
| CN101633866A (en) * | 2009-06-02 | 2010-01-27 | 华宝食用香精香料（上海）有限公司 | Cigarette siraitia grosvenorii additive and preparation method and application thereof |
| CN102408463A (en) * | 2011-11-15 | 2012-04-11 | 威海天泓农业科技有限公司 | Extraction method for mogroside |
| CN102960856A (en) * | 2012-12-10 | 2013-03-13 | 红塔烟草(集团)有限责任公司 | Salty-reducing additive for tobaccos, and preparation method and application of salty-reducing additive |
| JP2014201671A (en) * | 2013-04-05 | 2014-10-27 | 長興実業株式会社 | Flavoring aroma improver and food perfume composition including momordicae fruit extract |
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|---|---|---|---|---|
| CN108048221A (en) * | 2018-01-05 | 2018-05-18 | 贵州省香瑞莱香料有限公司 | A kind of preparation method of natural oil ben Siraitia grosvenorii flavouring essence for tobacco |
| CN109090702A (en) * | 2018-06-29 | 2018-12-28 | 郑州轻工业学院 | The preparation method and applications of Luo Han Guo Paste In Foods maillard reaction product |
| CN109090702B (en) * | 2018-06-29 | 2021-08-24 | 郑州轻工业学院 | Preparation method and application of Maillard reaction product of fructus momordicae extract |
| CN109022151A (en) * | 2018-07-13 | 2018-12-18 | 江苏浩丰生物科技有限公司 | A kind of cigarette of Siraitia grosvenorii flavor quick-fried pearl liquid and preparation method thereof |
| CN109527643A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method of the filter stick for cigarettes with Siraitia grosvenorii characteristic chicken flavor |
| CN109537365A (en) * | 2018-11-05 | 2019-03-29 | 广西中烟工业有限责任公司 | A kind of preparation method with Siraitia grosvenorii characteristic chicken flavor tipping paper |
| CN111378528A (en) * | 2018-12-29 | 2020-07-07 | 贵州中烟工业有限责任公司 | Method for preparing spice by using fructus momordicae extract as raw material and adopting microchannel reactor and application of method |
| CN109924535A (en) * | 2019-03-04 | 2019-06-25 | 海口日岛香料有限公司 | Flower of Fructus Momordicae burns and sucks the preparation method and application spilt in category shredded tobacco for water pipes in flowers and fruits |
| CN109924535B (en) * | 2019-03-04 | 2022-02-01 | 海口日岛香料有限公司 | Preparation method and application of momordica grosvenori flowers in fruit burning and spraying type hookah |
| WO2022206689A1 (en) * | 2021-04-01 | 2022-10-06 | Epc Natural Products Co., Ltd. | Sweetener and flavoring compositions prepared by glycosylated mogrosides or monk fruit extracts, method of making and method of use thereof |
| CN114836261A (en) * | 2022-05-06 | 2022-08-02 | 云南中烟新材料科技有限公司 | Method for extracting old medicine orange spice and application of old medicine orange spice in cigarette filter tip |
| CN114836261B (en) * | 2022-05-06 | 2023-05-12 | 云南中烟新材料科技有限公司 | Extraction method of old medicine orange spice and application of old medicine orange spice in cigarette filter tips |
| CN115161117A (en) * | 2022-07-11 | 2022-10-11 | 湖北中烟工业有限责任公司 | Preparation method and application of Maillard reactant of momordica grosvenori extract |
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