CN109022151A - A kind of cigarette of Siraitia grosvenorii flavor quick-fried pearl liquid and preparation method thereof - Google Patents
A kind of cigarette of Siraitia grosvenorii flavor quick-fried pearl liquid and preparation method thereof Download PDFInfo
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- CN109022151A CN109022151A CN201810768074.8A CN201810768074A CN109022151A CN 109022151 A CN109022151 A CN 109022151A CN 201810768074 A CN201810768074 A CN 201810768074A CN 109022151 A CN109022151 A CN 109022151A
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- siraitia grosvenorii
- quick
- fried pearl
- cigarette
- zimbabwe
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/003—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing less than six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/0076—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing less than six atoms
Abstract
The invention discloses a kind of cigarette of Siraitia grosvenorii flavor quick-fried pearl liquid and preparation method thereof.The cigarette of the Siraitia grosvenorii flavor is by obtaining after Glycerin, mixed triester with caprylic acid capric acid, Siraitia grosvenorii concentrate, overcritical Zimbabwe's pure tobacco oil, Siraitia grosvenorii flavor deployment with quick-fried pearl liquid.The Siraitia grosvenorii concentrate is to be obtained by Siraitia grosvenorii by Soxhlet extraction technique, overcritical Zimbabwe's pure tobacco oil is to be obtained by Zimbabwe's smoke-dipping paste by supercritical extracting equipment, the Siraitia grosvenorii essence is by third butyrolactone, 5 methyl furfural, methyl cyclopentenyl ketone, 3-hydroxy-2-butanone, phenethyl isobutyrate,phenylethyl isobutyrate, vanillic aldehyde, ethyl cinnamate, it is obtained after ethyl propionate, second position damascone and Glycerin, mixed triester with caprylic acid capric acid allotment.The quick-fried pearl liquid has arhat fruit flavor during smoking property of cigarette, and mouthfeel is sweet, and pleasant impression is completely comfortable, and has moderate strength sense.And the preparation method of the quick-fried pearl liquid is easy, and stable product quality can be widely applied in quick-fried pearl cigarette product.
Description
Technical field
The present invention relates to essence spice for cigarette field more particularly to a kind of cigarette of Siraitia grosvenorii flavor quick-fried pearl liquid and its preparations
Method.
Background technique
Quick-fried pearl liquid is positioned at the oily liquids in the quick-fried pearl in tobacco filter, and smoker can be in smoking process
In pinch brokenly quick-fried pearl, go out quick-fried pearl liquid stream, realize artificial controllable characteristic fragrance release during smoking property of cigarette, reduce extraneous ring
Loss of the border to the influence and essence of inhaling taste makes the fragrance of cigarette richer pleasant, comfortable, coordination, humectation, is that cigarette tax is fragrant
Innovative technology.
The fragrance and mouthfeel of quick-fried pearl cigarette derive from quick-fried pearl liquid, and the ingredient of quick-fried pearl liquid is mainly flavors and fragrances, natural to extract
Object and Glycerin, mixed triester with caprylic acid capric acid solvent.In order to guarantee the quality of quick-fried pearl, quick-fried pearl liquid usually require that be it is oil-soluble, invest feature perfume
Gas will be coordinated well with cigarette perfume, and mouthfeel is more comfortable, sweet, is conducive to reducing tar and reducing harm.
Although quick-fried pearl cigarette is general lack of fragrance and cigarette perfume currently, in the market there are a certain number of quick-fried pearl cigarette
Organic coordination is not able to satisfy the pumping requirements of different consumers.Accordingly, it is desirable to provide a kind of new technology solves above-mentioned ask
Topic.
Summary of the invention
The object of the present invention is to provide a kind of cigarette of Siraitia grosvenorii flavor quick-fried pearl liquid and preparation method thereof.By tobacco filter
After implosion pearl pinches brokenly, Siraitia grosvenorii fragrance is obvious, and mouthfeel is sweet, and pleasant impression is completely comfortable, and strength sense is moderate, can achieve and cloud and mist essence
The identical smoking result of oil.The preparation method of the quick-fried pearl liquid is easy, and stable product quality can be widely applied to quick-fried pearl cigarette
In product.
To achieve the goals above, the present invention provides a kind of quick-fried pearl liquid of cigarette of Siraitia grosvenorii flavor.
With this corresponding, the present invention also provides the cigarette of the Siraitia grosvenorii flavor preparation methods of quick-fried pearl liquid.
The technical solution adopted by the present invention is specific as follows.
The quick-fried pearl liquid of a kind of cigarette of Siraitia grosvenorii flavor, it is characterised in that be by following raw material tune count by weight percentage
With forming: Glycerin, mixed triester with caprylic acid capric acid 75%-90%, Siraitia grosvenorii concentrate 1%-5%, overcritical Zimbabwe's pure tobacco oil 2%-10%, sieve
Chinese fruity essence 5%-10%.
A kind of preparation method of the quick-fried pearl liquid of the cigarette of Siraitia grosvenorii flavor, comprising the following steps:
(1) it takes new fresh fructus momordicae to be exposed to the sun drying, makes Siraitia grosvenorii moisture content lower than 10%；Dry Siraitia grosvenorii is weighed, is crushed through pulverizer
At shape fine crushing；Ethyl alcohol is added, cold soaking 10-24h, cold to mention three times in extraction kettle, and wherein concentration of alcohol is 60wt%-95wt%, material
Liquor ratio is 1:5-1:10；Combined extract, by Soxhlet extraction technique, the temperature of evaporation and concentration is 80 DEG C, vacuum degree 0.095
Mpa is Siraitia grosvenorii concentrate after concentration.
(2) Zimbabwe's smoke-dipping paste is taken, is extracted using supercritical extracting equipment, 45-60 DEG C of extraction temperature, extraction pressure
Power is 50-80Mpa, extraction time 150min, and the extract obtained after the completion of extraction is filtered with filter press, and filtrate is
Overcritical Zimbabwe's pure tobacco oil.
(3) third butyrolactone 0.2%-0.6%, 5 methyl furfural 0.3%-1.0%, methyl cyclopentene alcohol are taken by weight percentage
Ketone 0.5%-2.0%, 3-hydroxy-2-butanone 0.3%-0.8%, phenethyl isobutyrate,phenylethyl isobutyrate 0.1%-0.5%, vanillic aldehyde 0.05%-0.3%, ethyl cinnamate
0.1%-0.8%, ethyl propionate 0.1%-0.4%, second position damascone 0.1%-0.5% and Glycerin, mixed triester with caprylic acid capric acid 40%-80%, by formula ratio
Mixing is Siraitia grosvenorii essence.
(4) glycerol decanoate, Siraitia grosvenorii concentrate, overcritical Zimbabwe's pure tobacco oil, arhat fruity are measured by formula
Essence is the quick-fried pearl liquid of cigarette of Siraitia grosvenorii flavor after dissolution mixing.
The utility model has the advantages that the quick-fried pearl liquid of Siraitia grosvenorii that preparation method through the invention is prepared overcomes in sundown
The quick-fried pearl liquid of fruity and cigarette perfume cannot be coordinated very well, not be able to satisfy the shortcomings that consumer sensory's demand, and quick-fried pearl liquid of the invention exists
Flue gas is full when suction, and strength is moderate, and the sweet fine and smooth and pleasant impression of mouthfeel is completely comfortable, and the preparation method letter of the quick-fried pearl liquid
Just, stable product quality can be widely applied in quick-fried pearl cigarette product.
Specific embodiment
Invention is further explained combined with specific embodiments below.
Embodiment 1
(1) it takes new fresh fructus momordicae to be exposed to the sun drying, makes Siraitia grosvenorii moisture content lower than 10%；Dry Siraitia grosvenorii is weighed, pulverizer crushes
At shape fine crushing；It is the ethyl alcohol that 90wt% concentration is added in 1:8 ratio in solid-liquid ratio, cold soaking is for 24 hours, cold to mention three times in extraction kettle, filtering
Combined extract afterwards, by Soxhlet extraction technique, the temperature of evaporation and concentration is 80 DEG C, and vacuum degree is 0.095 Mpa, and standby is concentrated
With.
(2) Zimbabwe's smoke-dipping paste is taken, is extracted using supercritical extracting equipment, 55 DEG C of extraction temperature, extracting pressure
For 60Mpa, extraction time 150min, the extract obtained after the completion of extraction is filtered with filter press, obtains overcritical saliva bar
Cloth Wei pure tobacco oil.
(3) third butyrolactone 0.5%, 5 methyl furfural 1.0%, methyl cyclopentenyl ketone 1.0%, second are taken by weight percentage
Acyloin 0.5%, phenethyl isobutyrate,phenylethyl isobutyrate 0.3%, vanillic aldehyde 0.2%, ethyl cinnamate 0.5%, ethyl propionate 0.25%, second position damascone
0.4% and Glycerin, mixed triester with caprylic acid capric acid 70%, edible Siraitia grosvenorii essence is obtained after mentioned component is mixed.
(4) weight percent takes Glycerin, mixed triester with caprylic acid capric acid 80%, Siraitia grosvenorii concentrate 5%, overcritical Zimbabwe's pure tobacco oil
8%, Siraitia grosvenorii essence 7%, mentioned component is uniformly mixed, and obtains the quick-fried pearl liquid of Siraitia grosvenorii flavor.
Embodiment 2
(1) it takes new fresh fructus momordicae to be exposed to the sun drying, makes Siraitia grosvenorii moisture content lower than 10%；Dry Siraitia grosvenorii is weighed, pulverizer crushes
At shape fine crushing；In solid-liquid ratio be 1:10 ratio be added 95wt% concentration ethyl alcohol, extraction kettle in cold soaking for 24 hours, cold to mention three times, mistake
Combined extract after filter, by Soxhlet extraction technique, the temperature of evaporation and concentration is 80 DEG C, and vacuum degree is 0.095 Mpa, after concentration
It is spare.
(2) Zimbabwe's smoke-dipping paste is taken, is extracted using supercritical extracting equipment, 45 DEG C of extraction temperature, extracting pressure
For 50Mpa, extraction time 150min, the extract obtained after the completion of extraction is filtered with filter press, obtains overcritical saliva bar
Cloth Wei pure tobacco oil.
(3) third butyrolactone 0.5%, 5 methyl furfural 0.8%, methyl cyclopentenyl ketone 1.5%, second are taken by weight percentage
Acyloin 0.5%, phenethyl isobutyrate,phenylethyl isobutyrate 0.5%, vanillic aldehyde 0.2%, ethyl cinnamate 0.5%, ethyl propionate 0.25%, second position damascone
0.5% and Glycerin, mixed triester with caprylic acid capric acid 80%, edible Siraitia grosvenorii essence is obtained after mentioned component is mixed.
(4) take Glycerin, mixed triester with caprylic acid capric acid 83%, Siraitia grosvenorii concentrate 2%, overcritical Zimbabwe tobacco net by weight percentage
Oily 5%, Siraitia grosvenorii essence 10%, mentioned component is uniformly mixed, the quick-fried pearl liquid of Siraitia grosvenorii flavor is obtained.
Embodiment 3
(1) it takes new fresh fructus momordicae to be exposed to the sun drying, makes Siraitia grosvenorii moisture content lower than 10%；Dry Siraitia grosvenorii is weighed, pulverizer crushes
At shape fine crushing；It is the ethyl alcohol that 95wt% concentration is added in 1:8 ratio in solid-liquid ratio, cold soaking is for 24 hours, cold to mention three times in extraction kettle, filtering
Combined extract afterwards, by Soxhlet extraction technique, the temperature of evaporation and concentration is 80 DEG C, and vacuum degree is 0.095 Mpa, and standby is concentrated
With.
(2) Zimbabwe's smoke-dipping paste is taken, is extracted using supercritical extracting equipment, 45 DEG C of extraction temperature, extracting pressure
For 50Mpa, extraction time 150min, the extract obtained after the completion of extraction is filtered with filter press, obtains overcritical saliva bar
Cloth Wei pure tobacco oil.
(3) third butyrolactone 0.5%, 5 methyl furfural 1.0%, methyl cyclopentenyl ketone 1.5%, second are taken by weight percentage
Acyloin 0.5%, phenethyl isobutyrate,phenylethyl isobutyrate 0.3%, vanillic aldehyde 0.2%, ethyl cinnamate 0.5%, ethyl propionate 0.25%, second position damascone
0.4% and Glycerin, mixed triester with caprylic acid capric acid 80%, edible Siraitia grosvenorii essence is obtained after mentioned component is mixed.
(4) take Glycerin, mixed triester with caprylic acid capric acid 85%, Siraitia grosvenorii concentrate 3%, overcritical Zimbabwe tobacco net by weight percentage
Oily 7%, Siraitia grosvenorii essence 5%, mentioned component is uniformly mixed, the quick-fried pearl liquid of Siraitia grosvenorii flavor is obtained.
10mL is taken to inject the quick-fried pearl liquid of the Siraitia grosvenorii flavor being prepared in embodiment 1, embodiment 2, embodiment 3
Into ramuscule cigarette nozzle stick.And after taking commercially available edible Siraitia grosvenorii essence to be diluted to 0.3wt% with Glycerin, mixed triester with caprylic acid capric acid, 10mL is taken
Dilution be injected in ramuscule cigarette nozzle stick, as a comparison case 1.The essential oil extracted in cloud and mist ethyl alcohol is taken to be diluted to 1wt%
Afterwards, cloud and mist essential oil dilution is taken to be injected in ramuscule cigarette nozzle stick, as a comparison case 2.Carry out integrated sensory's quality evaluation.As a result
It is as follows:
Embodiment 1: flue gas is full, Siraitia grosvenorii gives off a strong fragrance, mouthfeel is sweet, strength is big, pleasant impression is comfortable.
Embodiment 2: exquisiteness that flue gas is strong, Siraitia grosvenorii gives off a strong fragrance, mouthfeel is fresh and sweet, strength is moderate, pleasant impression is clean.
Embodiment 3: flue gas is full, Siraitia grosvenorii soft aroma and delicate mouthfeel are sweet, strength is moderate, pleasant impression is clean.
Comparative example 1: flue gas is strong, Siraitia grosvenorii fragrance is coordinated, sweet sense is not good enough, strength is insufficient, pleasant impression is not good enough.
Comparative example 2: flue gas is strong, fragrance is coordinated, strength is moderate.
It can be seen that from result, the quick-fried pearl liquid of the Siraitia grosvenorii flavor that preparation method through the invention is prepared has arhat
Fruit flavor, mouthfeel is sweet, and pleasant impression is completely comfortable, and has moderate strength sense, can achieve smoke panel test identical with cloud and mist essential oil
As a result, and the quick-fried pearl liquid preparation method it is easy, stable product quality can be widely applied in quick-fried pearl cigarette product.
Claims (4)
1. a kind of quick-fried pearl liquid of cigarette of Siraitia grosvenorii flavor, it is characterised in that be by following material allocation count by weight percentage
It forms: Glycerin, mixed triester with caprylic acid capric acid 75%-90%, Siraitia grosvenorii concentrate 1%-5%, overcritical Zimbabwe's pure tobacco oil 2%-10%, arhat
Fruity essence 5%-10%.
2. a kind of preparation method of the quick-fried pearl liquid of the cigarette for realizing Siraitia grosvenorii flavor described in claim 1, it is characterized in that
In following steps:
S1: new fresh fructus momordicae is taken to be exposed to the sun drying, by the moisture control of the Siraitia grosvenorii below 10%；The Siraitia grosvenorii is weighed,
It is put into pulverizer and is ground into shape fine crushing；Ethyl alcohol is added, the cold soaking 10-24h in extraction kettle, cold to mention three times, combined extract is led to
Soxhlet extraction technique is crossed, temperature is 80 DEG C, and vacuum degree is 0.095 Mpa, and Siraitia grosvenorii concentrate is obtained after concentration；
S2: being taken Zimbabwe's smoke-dipping paste, extracted using supercritical extracting equipment, the extract filter press obtained after extraction
It is filtered, obtains overcritical Zimbabwe's pure tobacco oil；
S3: taking third butyrolactone 0.2%-0.6%, 5 methyl furfural 0.3%-1.0%, methyl cyclopentenyl ketone 0.5%-2.0%, and second is even
Relation by marriage 0.3%-0.8%, phenethyl isobutyrate,phenylethyl isobutyrate 0.1%-0.5%, vanillic aldehyde 0.05%-0.3%, ethyl cinnamate 0.1%-0.8%, ethyl propionate
0.1%-0.4%, second position damascone 0.1%-0.5% and Glycerin, mixed triester with caprylic acid capric acid 40%-80%, obtains oil-soluble after mentioned component is mixed
Siraitia grosvenorii essence；
S4: Glycerin, mixed triester with caprylic acid capric acid 75%-92%, the Siraitia grosvenorii concentrate 1%-5%, overcritical Zimbabwe's pure tobacco oil are taken
The cigarette of the Siraitia grosvenorii flavor is prepared with quick-fried pearl in 2%-10%, the Siraitia grosvenorii essence 5%-10% after mixing mentioned component
Liquid.
3. preparation method according to claim 2, it is characterised in that concentration of alcohol described in step S1 is 60wt%-
95wt%, solid-liquid ratio 1:5-1:10.
4. preparation method according to claim 2, it is characterised in that extraction conditions described in step S2 is extraction temperature
45-60 DEG C, extracting pressure 50-80Mpa, extraction time 150min.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810768074.8A CN109022151A (en) | 2018-07-13 | 2018-07-13 | A kind of cigarette of Siraitia grosvenorii flavor quick-fried pearl liquid and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810768074.8A CN109022151A (en) | 2018-07-13 | 2018-07-13 | A kind of cigarette of Siraitia grosvenorii flavor quick-fried pearl liquid and preparation method thereof |
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Family
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110079393A (en) * | 2019-04-29 | 2019-08-02 | 亿利耐雀生物科技有限公司 | A kind of quick-fried pearl essential oil and its preparation method and application |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101427847A (en) * | 2008-11-28 | 2009-05-13 | 华芳烟用香料有限公司 | Process for producing Zimbabwe tobacco clean oil and uses thereof |
| CN101633866A (en) * | 2009-06-02 | 2010-01-27 | 华宝食用香精香料（上海）有限公司 | Cigarette siraitia grosvenorii additive and preparation method and application thereof |
| CN102304430A (en) * | 2011-03-17 | 2012-01-04 | 广州市澳键丰泽生物科技有限公司 | Formula of tobacco flavoring essence with sweet fragrance |
| CN102304428A (en) * | 2011-03-17 | 2012-01-04 | 广州市澳键丰泽生物科技有限公司 | Formula of tobacco flavoring essence with sweet fragrance |
| CN102994228A (en) * | 2012-10-25 | 2013-03-27 | 罗瑞雪 | Preparation method of tobacco absolute |
| CN105861152A (en) * | 2016-05-27 | 2016-08-17 | 山东中烟工业有限责任公司 | Tobacco flavor with sweet smoke and application |
| CN106036998A (en) * | 2016-07-18 | 2016-10-26 | 江苏浩丰生物科技有限公司 | Blast bead capable of making up for deficiencies in cigarette fragrance and moist sense and preparation method of blast bead |
| CN106433990A (en) * | 2016-11-23 | 2017-02-22 | 河南中烟工业有限责任公司 | Siraitia grosvenorii essence, preparation method and application of siraitia grosvenorii essence in cigarettes |
| CN106867675A (en) * | 2017-02-21 | 2017-06-20 | 江西中烟工业有限责任公司 | A kind of cigarette preparation method of Momordica grosvenori essence |
| CN107177419A (en) * | 2017-07-20 | 2017-09-19 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl Momordica grosvenori essence and its application in cigarette |
-
2018
- 2018-07-13 CN CN201810768074.8A patent/CN109022151A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101427847A (en) * | 2008-11-28 | 2009-05-13 | 华芳烟用香料有限公司 | Process for producing Zimbabwe tobacco clean oil and uses thereof |
| CN101633866A (en) * | 2009-06-02 | 2010-01-27 | 华宝食用香精香料（上海）有限公司 | Cigarette siraitia grosvenorii additive and preparation method and application thereof |
| CN102304430A (en) * | 2011-03-17 | 2012-01-04 | 广州市澳键丰泽生物科技有限公司 | Formula of tobacco flavoring essence with sweet fragrance |
| CN102304428A (en) * | 2011-03-17 | 2012-01-04 | 广州市澳键丰泽生物科技有限公司 | Formula of tobacco flavoring essence with sweet fragrance |
| CN102994228A (en) * | 2012-10-25 | 2013-03-27 | 罗瑞雪 | Preparation method of tobacco absolute |
| CN105861152A (en) * | 2016-05-27 | 2016-08-17 | 山东中烟工业有限责任公司 | Tobacco flavor with sweet smoke and application |
| CN106036998A (en) * | 2016-07-18 | 2016-10-26 | 江苏浩丰生物科技有限公司 | Blast bead capable of making up for deficiencies in cigarette fragrance and moist sense and preparation method of blast bead |
| CN106433990A (en) * | 2016-11-23 | 2017-02-22 | 河南中烟工业有限责任公司 | Siraitia grosvenorii essence, preparation method and application of siraitia grosvenorii essence in cigarettes |
| CN106867675A (en) * | 2017-02-21 | 2017-06-20 | 江西中烟工业有限责任公司 | A kind of cigarette preparation method of Momordica grosvenori essence |
| CN107177419A (en) * | 2017-07-20 | 2017-09-19 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl Momordica grosvenori essence and its application in cigarette |
Non-Patent Citations (2)
| Title |
|---|
| 李雪梅等: "利用超临界流体萃取技术制备烟草净油的研究", 《中国烟草学报》 * |
| 郑小嘎等: "罗汉果浸膏挥发性成分分析及在卷烟中的应用", 《烟草科技》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110079393A (en) * | 2019-04-29 | 2019-08-02 | 亿利耐雀生物科技有限公司 | A kind of quick-fried pearl essential oil and its preparation method and application |
| CN110079393B (en) * | 2019-04-29 | 2021-12-28 | 亿利耐雀生物科技有限公司 | Pearl blasting essential oil and preparation method and application thereof |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
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