CN103468410B - Tea flower extract composition and its use in cigarette - Google Patents
Tea flower extract composition and its use in cigarette Download PDFInfo
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- CN103468410B CN103468410B CN201310446959.3A CN201310446959A CN103468410B CN 103468410 B CN103468410 B CN 103468410B CN 201310446959 A CN201310446959 A CN 201310446959A CN 103468410 B CN103468410 B CN 103468410B
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Abstract
The invention relates to a tea flower extract composition and its use in a cigarette. The tea flower extract composition comprises iron mercy goddess tea flower extract, robe tea flower extract, cassia tea flower extract and narcissus tea flower extract. The tea flower extract composition is added into the cigarette so that the cigarette has a harmonious fragrance. The tea flower extract composition can improve fullness of a cigarette fragrance and volatility of a cigarette fragrance without change of original cigarette performances and original cigarette processing processes. The tea flower extract composition has a sweet taste, promotes secretion of saliva of a smoker, improves miscellaneous gas and irritation and improves integral smoking quality.
Description
Technical field
The invention belongs to tobacco spice technical field, relate to a kind of camellia extract composition and the application in cigarette thereof.
Background technology
Essence and flavoring agent is widely used in the fields such as tobacco, food, daily use chemicals, and natural perfume due to its composition complicated, fragrance enriches, fragrance remaining time is the indispensable raw material of preparing essence lastingly.
International tobacco industry pays much attention to the development and application of essence spice for cigarette, and the technology of production application high-quality essence and flavoring agent is used as the core technology of oneself.Along with tobacco industry technical progress and greatly develop the proposition of Chinese-style cigarette target, essence spice for cigarette technology as the important core technology of tobacco industry, as one of formation Chinese-style cigarette quality characteristic, the key making Chinese-style cigarette core technology.Essence and flavoring agent can give the style and features of cigarette product uniqueness, improves the suction quality of cigarette product, is one of important connotation of constructing Chinese-style cigarette core competitiveness.Still there is certain deficiency in current domestic cigarette product, the Application and Development of novel essence spice for cigarette is an important solution route in style and features and suction quality etc.
There is abundant natural perfume material resource in China, about has more than 500 to plant scented plants and is distributed widely in 20 provinces and cities, but only have minority to be exploited, and there is the problems such as level of processing is low, utilisation technology is single.
Tea tree (Camellia sinensis) is Theaceae Camellia Plants, and its cultivation has had history in thousand, and in China, distributed pole is wide.Tea Flower is very abundant as the by product resource in Tea Production process.Tea Flower has the advantages that the florescence is long, the amount of blooming is large and fragrance is fresh and sweet, has high value of exploiting and utilizing.In recent years, the comprehensive utilization of Tea Flower is more and more paid attention to.
Multiple beneficial composition and the active substances such as Tea Flower rich in proteins, tea-polyphenol, tea polysaccharide, tea saponin, flavonoid, amino acid, VITAMIN, trace element and superoxide-dismutase (SOD), Theobromine, have hypoglycemic, reducing blood-fat, anticoagulant, antithrombotic, nourishing, beauty treatment and the effect such as anticancer.Containing number of chemical material and aroma component in Tea Flower.The aroma component of Tea Flower is mainly alcohols, ester class, aldehydes and lower alkyl hydrocarbons, and wherein the relative content of methyl phenyl ketone, 2-enanthol, phthalic acid two (2-ethylhexyl) ester, phantol is higher.The Tea flower essence fragrance prepared by tea flower extract is fresh and clean, and sweet spiciness is strongly fragrant, has higher potential using value.
Have no the flavor compositions prepared by tea flower extract and the application in cigarette thereof at present.
Goal of the invention of the present invention is to provide a kind of camellia extract composition and preparation method thereof, and said composition is as the application of cigaret additive in cigarette.Contriver carries out extraction and isolation by different modes method to Tea Flower effective constituent, and to be combined in different forms by extract for the feature of cigarette product and be applied in cigarette, to improve style and features and the suction quality of cigarette product.
Summary of the invention
A first aspect of the present invention provides a kind of composition of tea flower extract, and it is formulated by Tie Guanyin tea plant flower extract, Radix Campylotropis Hirtella (Herba Myrsines Africanae) tea flower extract, Chinese cassia tree tea flower extract and narcissus tea flower extract.
Composition described according to a first aspect of the present invention, wherein said extract is Tea Flower medicinal extract, essential oil of the flower of Camellia sinensis, Tea Flower absolute oil and/or Tea Flower tincture or its combination.
Composition described according to a first aspect of the present invention, the preparation method of wherein said Tea Flower medicinal extract, Tea Flower absolute oil and/or Tea Flower tincture comprises the step of raw material Tea Flower being carried out to ultra high pressure extraction.
Composition described according to a first aspect of the present invention, in a specific embodiment, the preparation method of described Tea Flower tincture, Tea Flower medicinal extract and/or Tea Flower absolute oil, comprises following step (1), step (1)-(2) or step (1)-(3):
(1) ultra high pressure extraction: take a certain amount of Tea Flower and put into ultra high pressure extraction tank, add the edible ethanol of at least 2 times of (w/w) Tea Flower weight, carry out ultra high pressure extraction, obtain Tea Flower tincture 1, the concentration of wherein said edible ethanol is 20-70%(mass concentration); Preferably, 1/5-1/10 Tea Flower tincture 1 being concentrated into original volume obtains Tea Flower tincture 2;
(2) Tea Flower medicinal extract is prepared: the Tea Flower tincture 1 obtained in step (1) or Tea Flower tincture 2 are concentrated further, obtain Tea Flower medicinal extract;
(3) Tea Flower absolute oil is prepared: the Tea Flower medicinal extract obtained with a certain amount of 95% ethanol resuspension step (2), then freezing treatment (such as-10 DEG C to-20 DEG C) is carried out, freezing time is that 16-48h(is preferably 20-36h) then filter, concentrated, obtain Tea Flower absolute oil.
In the present invention, freezing temperature can be-10 DEG C to-20 DEG C.
In a specific embodiment, in the preparation method of above-mentioned Tea Flower tincture, Tea Flower medicinal extract and/or Tea Flower absolute oil, in step (1), described for adopted Tea Flower be Tea Flower fresh flower, dried flower, spray Ethanol Treatment Tea Flower, saline soak Tea Flower or alcohol immersion Tea Flower.
In a specific embodiment, in the preparation method of above-mentioned Tea Flower tincture, Tea Flower medicinal extract and/or Tea Flower absolute oil, in step (1), add the edible ethanol of at least 2-15 times of (w/w) Tea Flower weight, be preferably 2-10 doubly, 2-8 doubly, 3-8 doubly (w/w), be more preferably 4-7 doubly (w/w), such as 4 times, 5 times, 6 times or 7 times (w/w).
In a specific embodiment, in the preparation method of above-mentioned Tea Flower tincture, Tea Flower medicinal extract and/or Tea Flower absolute oil, in step (1), particularly, the concentration of described edible ethanol is 20-70%(mass concentration), 20-40%, 20-50%, 40-50%, 50-70%, 20%, 30%, 40%, 50%, 60%, 70%.
In a specific embodiment, in the preparation method of above-mentioned Tea Flower tincture, Tea Flower medicinal extract and/or Tea Flower absolute oil, in step (1), release immediately after ultra high pressure extraction.
In a specific embodiment, in the preparation method of above-mentioned Tea Flower tincture, Tea Flower medicinal extract and/or Tea Flower absolute oil, in step (1), the pressure of described ultra-high voltage is 150-500Mpa; Particularly, be 150-250Mpa, 150-300Mpa, 250-300Mpa, 250-350Mpa, 250-500Mpa, 300-350Mpa, 300-500Mpa, 350-500Mpa, 150Mpa, 200Mpa, 250Mpa, 300Mpa, 350Mpa, 400Mpa, 450Mpa, 500Mpa etc.
In a specific embodiment, in the preparation method of above-mentioned Tea Flower tincture, Tea Flower medicinal extract and/or Tea Flower absolute oil, in step (1), dwell time is 5-120min, be preferably 5-60min, be more preferably 10-30min, such as 10-15min, 10-20min, 10-25min, 15-20min, 15-25min, 15-30min, 20-25min, 20-30min, 25-30min, 10min, 15min, 20min, 25min, 30min etc.
In a specific embodiment, in the preparation method of above-mentioned Tea Flower tincture, Tea Flower medicinal extract and/or Tea Flower absolute oil, concentrated in step (1) or (2) can be the method that those skilled in the art know, such as suction filtration concentrates.
Composition described according to a first aspect of the present invention, in a specific embodiment, the preparation method of wherein said essential oil of the flower of Camellia sinensis is reduced steam distillation method.
Composition described according to a first aspect of the present invention, in a specific embodiment, the preparation method of described essential oil of the flower of Camellia sinensis, comprises the steps:
(1) taking a certain amount of Tea Flower loads in the decompression extraction element being furnished with trapping cold-trap;
(2) add the water of Tea Flower weight at least 5 times, and the temperature of the water added is more than 80 DEG C, at least 5min is soaked in sealing, is cooled to 30-70 DEG C;
(3-1) carry out reduced steam distillation, temperature used is identical with cooled temperature in step (2), and vacuum tightness is 1-17kpa, collects distillate;
Preferably, also comprise step (3-2): the operation 1 time in repeating step (2) and (3-1) or repeatedly, and merge distillate;
(4) in using, low polar organic solvent carries out 1 time the distillate obtained in step (3-1) or step (3-2) or repeatedly back extraction (such as 2,3,4 or 5 times, preferably 3 times), obtains stripping workshop; Stripping workshop is concentrated, obtains enriched material;
(5) use enriched material weight 2-4 dehydrated alcohol doubly to carry out backwash to the enriched material obtained in step (4), during concentrating under reduced pressure removing wherein remains, after low polar organic solvent, obtain essential oil of the flower of Camellia sinensis.
In a specific embodiment, in the preparation method of above-mentioned essential oil of the flower of Camellia sinensis, for adopted Tea Flower is Tea Flower fresh flower, dried flower, spray Ethanol Treatment Tea Flower, saline soak Tea Flower or alcohol immersion Tea Flower described in step (1).
In a specific embodiment, in the preparation method of above-mentioned essential oil of the flower of Camellia sinensis, the amount of the water added in step (2) is 5-50 times of Tea Flower weight, be preferably 5-40 times or 8-40 times, be more preferably 10-30 doubly, such as 10-15 doubly, 10-20 doubly, 10-25 doubly, 15-20 doubly, 15-25 doubly, 15-30 doubly, 20-25 doubly, 20-30 doubly, 10 times, 11 times, 12 times, 13 times, 14 times, 15 times, 16 times, 17 times, 18 times, 19 times, 20 times, 21 times, 22 times, 23 times, 24 times, 25 times, 26 times, 27 times, 28 times, 29 times or 30 times.
In a specific embodiment, in the preparation method of above-mentioned essential oil of the flower of Camellia sinensis, the temperature of the water added in step (2) is preferably more than 85 DEG C, is more preferably more than 90 DEG C, more preferably more than 95 DEG C, such as 95 DEG C, 96 DEG C, 97 DEG C, 98 DEG C, 99 DEG C, preferably 100 DEG C; Particularly preferably, the water added is boiling water.Soak and carry out at ambient pressure, the temperature of the boiling water of immersion is generally 100 DEG C, and those skilled in the art know, according to atmospheric difference, boiling point is different.
In a specific embodiment, in the preparation method of above-mentioned essential oil of the flower of Camellia sinensis, the time that in step (2), sealing is soaked is 5min-4h, be preferably 5min-4h, 5min-3h or 5min-2h, be more preferably 5-60min, 5-50min or 5-40min, be particularly preferably 5-30min, such as 5-18min, 5-20min, 5-25min or 18-30min.
In a specific embodiment, in the preparation method of above-mentioned essential oil of the flower of Camellia sinensis, step is cooled to 30-70 DEG C in (2), such as 30-40 DEG C, 30-50 DEG C, 30-60 DEG C, 40-50 DEG C, 45-55 DEG C, 40-60 DEG C, 40-70 DEG C, 50-60 DEG C, 50-70 DEG C or 60-70 DEG C.
Those skilled in the art know, and vacuum tightness and distillation temperature are corresponding to a certain extent, need to guarantee to allow under to fixed temperature and vacuum tightness the distilled water in matrass and aroma component steam.
Be not limited to theoretical restriction, temperature is lower, and required vacuum tightness is less, and temperature is higher, and required vacuum tightness is larger.The present inventor finds, when temperature is 30 DEG C, and vacuum tightness 2.5kpa; The speed that distills less of 2.5kpa can be faster; When temperature is 70 DEG C, vacuum tightness 17kpa; The speed that distills less of 17kpa can be faster.
Be not limited to theoretical restriction, on the other hand, under the prerequisite of temperature setting, if vacuum tightness is too low, may bumping be caused, extraction pot liquid is gone out; If vacuum tightness is too high, extraction pot liquid may be made to distill not out, do not have the effect of underpressure distillation.Therefore, the vacuum ranges that each temperature value correspondence one is proper.
Therefore, about the vacuum tightness of the distillation of reduced steam described in step (3-1) or (3-2), those skilled in the art can set according to the theory above selected temperature reference or this area knowledge, also with reference to vacuum ranges below, or can adjust on this basis:
Such as 1-12kPa, 1-10kPa, 1-9.5kPa, 1-9kPa, 1-8.5kPa, 1-8kPa, 1-7.5kPa or 1-7kPa; Such as 2.5-7kPa, 1-2kPa, 1-3kPa, 1-4kPa, 1-5kPa, 1-6kPa, 2-3kPa, 2-4kPa, 2-5kPa, 2-6kPa, 2-7kPa, 3-4kPa, 3-5kPa, 3-6kPa, 3-7kPa, 4-5kPa, 4-6kPa, 4-7kPa, 5-6kPa, 5-7kPa, 6-7kPa, 6-12kPa, 8-12kPa, 10-12kPa, 1kPa, 2kPa, 3kPa, 4kPa, 5kPa, 6kPa, 7kPa, 8kPa, 9kPa, 10kPa, 11kPa or 12kPa.
In a specific embodiment, in the preparation method of above-mentioned essential oil of the flower of Camellia sinensis, in step (4), in described low polar organic solvent be selected from anhydrous diethyl ether and ethyl acetate any one; Ethyl acetate.In described, the consumption of low polar organic solvent can be the 1/4-1/3 of distillate volume.
In a specific embodiment, in the preparation method of above-mentioned essential oil of the flower of Camellia sinensis, the decompression extraction element used can be commercially available, or the preferred decompression extraction element used in the Chinese patent application (application number is 200910111996.2) that publication number is 101920127A.
Composition described according to a first aspect of the present invention, in one embodiment of the invention, it is made up of the component of following weight part:
Composition according to a first aspect of the present invention described in any one, in a specific embodiment, it is made up of the component of following weight part:
Composition according to a first aspect of the present invention described in any one, in a specific embodiment, it is made up of the component of following weight part:
Composition according to a first aspect of the present invention described in any one, in a specific embodiment, it is made up of the component of following weight part:
Composition according to a first aspect of the present invention described in any one, in a specific embodiment, it is made up of the component of following weight part:
The composition of the tea flower extract described in first aspect present invention can be used as cigaret additive, particularly as cigarette flavors.The addition manner of said composition is: use dissolve with ethanol to be mixed with perfuming solution, be sprayed onto in pipe tobacco by perfuming dissolution homogeneity, concrete usage ratio is 0.001 ~ 0.5% of tobacco quality.Described ethanol can be the aqueous ethanolic solution of 50 ~ 95%, preferably the aqueous ethanolic solution of 60 ~ 80%, more preferably the aqueous ethanolic solution of 65 ~ 75%, is particularly preferably the aqueous ethanolic solution of 70%.The consumption of ethanol is: 50 ~ 63(such as 50,52,52.5,63 by weight).
Therefore, composition described in any one of first aspect present invention can also comprise ethanol, preferably the aqueous ethanolic solution of 50 ~ 95%, further preferably 60 ~ 80% aqueous ethanolic solution, more preferably the aqueous ethanolic solution of 65 ~ 75%, is particularly preferably the aqueous ethanolic solution of 70%.Preferred ethanol content is: 50 ~ 63(such as 50,52,52.5,63 by weight).
A second aspect of the present invention provides the purposes of the composition described in any one of first aspect present invention in cigarette, preferably as the purposes of cigaret additive, particularly preferably as the purposes of cigarette flavors.Preferably, said composition may be used for the internal lining paper, filter stick etc. of pipe tobacco, thin slice, cigarette.
A third aspect of the present invention provides a kind of cigarette, and it comprises the composition described in any one of first aspect present invention.Preferably, the quality of described composition is 0.001 ~ 0.5% of tobacco quality, is preferably the 0.015 ~ 0.045%(such as 0.045,0.035,0.015 of tobacco quality).
Detailed Description Of The Invention
The various term used in the present invention and phrase have and well known to a person skilled in the art general sense, but have special definition in this article, are as the criterion with implication as defined herein.
In the present invention, " tea tree " in described " Tea Flower ", if not otherwise specified, refers to the plant of Theales (Theales), Theaceae (Theaceae) or Camellia (Camellis);
In one aspect of the invention, " flower " in described " Tea Flower " comprising: perianth, androecium, gynoecium.Perianth comprises: calyx (being made up of sepal), corolla (being made up of petal).The color of flower and fragrance are from corolla.Stamen comprises: filigree and flower pesticide.Gynoecium comprises: column cap, style and ovary.
In one aspect of the invention, term " Tea Flower " can be fresh flower, also can be dry flower; If do not have specified otherwise, it refers to complete Tea Flower or a part for Tea Flower; It at least comprises petal; Alternatively, one or more being selected from sepal, stamen and gynoecium are also comprised.
In the present invention, described tea flower extract, includes but not limited to: essential oil of the flower of Camellia sinensis, Tea Flower tincture, Tea Flower medicinal extract and/or Tea Flower absolute oil; Alternatively, it also comprises auxiliary material (carrier, solvent, pigment, antioxidant, sanitas, humectant, sweetener etc.).
Tea Flower described in the present invention extracts can pass through normal temperature lixiviate, heating and refluxing extraction, surname extraction, ultrasound on extracting, microwave auxiliary extraction, enzyme process auxiliary extraction, accelerated solvent extraction, supercritical fluid extraction, Simultaneous distillation-extraction, wet distillation, the combination of any one or a few method of underpressure distillation etc. is prepared from, also can by commercially available (such as: Aohuada Perfume Technology (Guangzhou) Co., Ltd., Huabao Edible Essence & Condiment (Shanghai), Hangzhou Jie Min essence and flavoring agent company limited, Shenzhen Bowden essence and flavoring agent company limited).
The separation method that described Tea Flower extracts can be the combination of any one or a few method of filtering separation, centrifugation, membrane sepn, molecular distillation, column chromatography, chromatographic separation etc.
Term " tincture " or " tincture " refer to uses certain density ethanol, lixiviate spice berry organ or exudate and secrete fragrant animal containing fragrant organ or its aroma material preparation containing some amount ethanol obtained containing fragrant secretory product.Tincture is worth to be called " cold process tincture " under normal temperature; Tincture obtained under heated reflux condition is called " hot method tincture "." Tea Flower tincture " used in the present invention by commercially available, also can prepare by various ordinary method.
In one embodiment of the invention, described " Tea Flower tincture " can prepare by the following method:
(1) described Tea Flower includes but not limited to fresh Tea Flower, dried flower, alcohol immersion process Tea Flower, spray Ethanol Treatment Tea Flower etc.;
(2) ultra high pressure extraction: take certain quantity of fresh Tea Flower and put into ultra high pressure extraction tank, adds the edible ethanol that 7 times of concentration to Tea Flower weight are 20%, carries out release immediately after ultra high pressure extraction; The pressure of described ultra-high voltage is: 150MPa, the dwell time: 30min;
(3) namely the 1/5-1/10 being concentrated into original volume after the extract in step (2) being carried out suction filtration obtains Tea Flower tincture.
Term " essential oil ", in broad terms, essential oil refer to from spice berry and secrete fragrant animal organ to extract the general name of the volatility fragrant containing substance goods obtained through processing, in the narrow sense, essential oil only refers to the goods with steam distillation, milling process, cold grinding method or dry distillation fragrant containing substance obtained from spice berry organ (as flower, leaf, branch, skin, scapus, root, fruit, seed etc.).In actual applications, normal its narrow sense of employing." essential oil of the flower of Camellia sinensis " used in the present invention by commercially available, also can prepare by various ordinary method.
In one embodiment of the invention, described " essential oil of the flower of Camellia sinensis " can prepare by the following method:
(1) take certain quantity of fresh Tea Flower to load in decompression extraction element, add the boiling water of Tea Flower weight 30 times, sealing is cooled to 70 DEG C after soaking 30min;
(2) on the reliever being furnished with trapping cold-trap, carry out reduced steam distillation, temperature is: 70 DEG C, and vacuum tightness is: 12kpa, collects distillate;
(3) underpressure distillation complete after add Tea Flower weight 25 times boiling water in extraction element, repeat underpressure distillation twice according to step (3) after merge and collect liquid;
(4) add 0.3 times and collect the long-pending ethyl acetate back extraction of liquid three times, merge stripping workshop and be concentrated into 1/10 of fresh Tea Flower weight; ;
(5) essential oil of the flower of Camellia sinensis is refined: the dehydrated alcohol adding concentrated solution 3 times in step (4) carries out backwash, concentrating under reduced pressure remove wherein after residual ethyl acetate essential oil of the flower of Camellia sinensis.
Term " medicinal extract ", in a broad sense, medicinal extract refers to organic solvent extraction spice berry organ or its exudate (as resin, natural gum, balm), removing solvent for use and the general designation of aroma material preparation that obtains.From in the narrow sense, medicinal extract only refer to organic solvent extraction spice berry organ obtain not containing the aroma material preparation of solvent for use and moisture." Tea Flower medicinal extract " used in the present invention by commercially available, also can prepare by various ordinary method.
In one embodiment of the invention, described " Tea Flower medicinal extract " can prepare by the following method:
(1) described Tea Flower includes but not limited to fresh Tea Flower, dried flower, alcohol immersion process Tea Flower, spray Ethanol Treatment Tea Flower etc.;
(2) ultra high pressure extraction: take certain quantity of fresh Tea Flower and put into ultra high pressure extraction tank, 4 times of concentration to Tea Flower weight are 40% edible ethanol, carry out release immediately after ultra high pressure extraction; The pressure of described ultra-high voltage is: 500MPa, the dwell time: 10min;
(3) namely the 1/5-1/10 being concentrated into original volume after the extract in step (2) being carried out suction filtration obtains Tea Flower tincture;
(4) Tea Flower medicinal extract is prepared: Tea Flower medicinal extract can be obtained by concentrated for the Tea Flower tincture obtained in step (3) continuation.
Term " absolute oil ", in a broad sense, refers to the solution extracting the fragrant composition in medicinal extract, resinoid, balm or face cream with high concentration ethanol, through freezing treatment, elimination insolubles, then after pressure reducing and steaming ethanol the general designation of the aroma material preparation of gained." Tea Flower absolute oil " used in the present invention by commercially available, also can prepare by various ordinary method.
In one embodiment of the invention, described " Tea Flower absolute oil " can prepare by the following method:
(1) described Tea Flower includes but not limited to fresh Tea Flower, dried flower, alcohol immersion process Tea Flower, spray Ethanol Treatment Tea Flower etc.;
(2) ultra high pressure extraction: take certain quantity of fresh Tea Flower and put into ultra high pressure extraction tank, 5 times of concentration to Tea Flower weight are 70% edible ethanol, carry out release immediately after ultra high pressure extraction; The pressure of described ultra-high voltage is: 300MPa, the dwell time: 20min;
(3) namely the 1/5-1/10 being concentrated into original volume after the extract in step (2) being carried out suction filtration obtains Tea Flower tincture;
(4) Tea Flower medicinal extract is prepared: Tea Flower medicinal extract can be obtained by concentrated for the Tea Flower tincture obtained in step (3) continuation;
(5) Tea Flower absolute oil is prepared: with a certain amount of 95% ethanol back dissolving Tea Flower medicinal extract, filter after freezing (such as-10 DEG C to-20 DEG C) 24-48h, concentrated, obtain Tea Flower absolute oil.
The beneficial effect of the invention
The composition fragrance clear and natural of tea flower extract provided by the invention, highest quality, the sweet breath of graceful band, can be widely used in tobacco, food and household chemicals field etc.
Sensory evaluating smoking's result shows: join in cigarette by described camellia extract composition, cigarette flavor is coordinated, do not change cigarette original performance, do not change on the basis of the original complete processing of cigarette, the fullness ratio of cigarette flavor can be promoted, improve the property sent out thoroughly of cigarette flavor, the impression that the person Hui Tian that brings cigarette smoking promotes the production of body fluid, assorted gas, pungency improve, and overall sucking quality is improved.This camellia extract composition not only improves the flavouring essence quality of cigarette, and improves the sense organ comfort level of cigarette, therefore has more the meaning and value of actual production.
Embodiment
Below in conjunction with embodiment, embodiment of the present invention are described in detail, but it will be understood to those of skill in the art that the following example only for illustration of the present invention, and should not be considered as limiting scope of the present invention.Unreceipted actual conditions person in embodiment, the condition of conveniently conditioned disjunction manufacturers suggestion is carried out.Agents useful for same or the unreceipted production firm person of instrument, being can by the conventional products of commercial acquisition.
The Tea Flower tincture used in embodiment below prepares by the following method:
(1) raw material: fresh Tie Guanyin tea plant flower, Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower, Chinese cassia tree Tea Flower or narcissus Tea Flower;
(2) ultra high pressure extraction: take certain quantity of fresh Tea Flower and put into ultra high pressure extraction tank, adds the edible ethanol that 7 times of concentration to Tea Flower weight are 20%, carries out release immediately after ultra high pressure extraction; The pressure of described ultra-high voltage is: 150MPa, the dwell time: 30min;
(3) namely the 1/5-1/10 being concentrated into original volume after the extract in step (2) being carried out suction filtration obtains kwan-yin Tea Flower tincture, Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower tincture, Chinese cassia tree Tea Flower tincture or narcissus Tea Flower tincture.
The essential oil of the flower of Camellia sinensis used in embodiment below prepares by the following method:
(1) take certain quantity of fresh Tea Flower (fresh Tie Guanyin tea plant flower, Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower, Chinese cassia tree Tea Flower or narcissus Tea Flower) to load in decompression extraction element, add the boiling water of Tea Flower weight 30 times, sealing is cooled to 70 DEG C after soaking 30min;
(2) on the reliever being furnished with trapping cold-trap, carry out reduced steam distillation, temperature is: 70 DEG C, and vacuum tightness is: 12kpa, collects distillate;
(3) underpressure distillation complete after add Tea Flower weight 25 times boiling water in extraction element, repeat underpressure distillation twice according to step (3) after merge and collect liquid;
(4) add 0.3 times and collect the long-pending ethyl acetate back extraction of liquid three times, merge stripping workshop and be concentrated into 1/10 of fresh Tea Flower weight; ;
(5) essential oil of the flower of Camellia sinensis is refined: the dehydrated alcohol adding concentrated solution 3 times in step (4) carries out backwash, concentrating under reduced pressure remove wherein after residual ethyl acetate Tie Guanyin tea plant flower essential oil, Radix Campylotropis Hirtella (Herba Myrsines Africanae) essential oil of the flower of Camellia sinensis, Chinese cassia tree essential oil of the flower of Camellia sinensis or narcissus essential oil of the flower of Camellia sinensis.
The Tea Flower medicinal extract used in embodiment below prepares by the following method:
(1) raw material: fresh Tie Guanyin tea plant flower, Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower, Chinese cassia tree Tea Flower or narcissus Tea Flower;
(2) ultra high pressure extraction: take certain quantity of fresh Tea Flower and put into ultra high pressure extraction tank, 4 times of concentration to Tea Flower weight are 40% edible ethanol, carry out release immediately after ultra high pressure extraction; The pressure of described ultra-high voltage is: 500MPa, the dwell time: 10min;
(3) namely the 1/5-1/10 being concentrated into original volume after the extract in step (2) being carried out suction filtration obtains Tea Flower tincture;
(4) Tea Flower medicinal extract is prepared: Tie Guanyin tea plant flower concrete, Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower medicinal extract, Chinese cassia tree tea tree flower concrete or narcissus tea tree flower concrete can be obtained by concentrated for the Tea Flower tincture obtained in step (3) continuation.
The Tea Flower absolute oil used in embodiment below prepares by the following method:
(1) raw material: fresh Tie Guanyin tea plant flower, Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower, Chinese cassia tree Tea Flower or narcissus Tea Flower;
(2) ultra high pressure extraction: take certain quantity of fresh Tea Flower and put into ultra high pressure extraction tank, 5 times of concentration to Tea Flower weight are 70% edible ethanol, carry out release immediately after ultra high pressure extraction; The pressure of described ultra-high voltage is: 300MPa, the dwell time: 20min;
(3) namely the 1/5-1/10 being concentrated into original volume after the extract in step (2) being carried out suction filtration obtains Tea Flower tincture;
(4) Tea Flower medicinal extract is prepared: Tea Flower medicinal extract can be obtained by concentrated for the Tea Flower tincture obtained in step (3) continuation;
(5) Tea Flower absolute oil is prepared: with a certain amount of 95% ethanol back dissolving Tea Flower medicinal extract, filter after freezing (such as-10 DEG C to-20 DEG C) 24-48h, concentrated, obtain Tie Guanyin tea plant extrait, Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower absolute oil, Chinese cassia tree tea tree extrait or narcissus tea tree extrait.
The ethanol used in embodiment below reaches international fragrance (Guangzhou) company limited purchased from China of Australia, SC3005.
Sensory evaluating smoking's experiment below in embodiment to be smoked panel test comparison to cigarette sample by GB5606.4-2005 by the sensory evaluating smoking council of Fujian China Tobacco Industrial Co., Ltd..Sensory Quality of Cigarette judgment criteria is as shown in Table A.
Table A Sensory Quality of Cigarette judgment criteria
Sensory evaluating smoking's inspection rule:
1, participating in the number of smokeing panel test is 13 people.
2, aesthetic quality scores employing centesimal system, and highest score is 100 points.
3, projects are all divided into 0.5 unit of scoring.
4, when smokeing panel test score to gloss, fragrance, harmony, assorted gas, pungency, pleasant impression six projects, each project quality reaches the requirement of respective item, then correspondingly score.
Embodiment 1:
According to the formula in following table 1, tea flower extract various in table 1 is mixed, prepare camellia extract composition.
Table 1
Embodiment 1 is prepared the camellia extract composition that obtains according to the ratio in upper table 1, add 70% aqueous ethanolic solution, obtain camellia extract composition ethanolic soln.The camellia extract composition ethanolic soln obtained evenly is sprayed onto on pipe tobacco by 0.045% of pipe tobacco weight, after baking, rolls into cigarette.Wherein 0# in contrast, on pipe tobacco, only spray the aqueous ethanolic solution of 70%.Then carry out sensory evaluating smoking's experiment by GB5606.4-2005, comparison scoring event of smokeing panel test is in table 2.
Table 2 Sensory Quality of Cigarette inspection source recording
Smoking result shows, the score of 1# to 4# is all higher than 0#, and wherein 1# composition score is the highest, contrasts with 0#, cigarette flavor harmony, and fragrance is light, the rich raising of fragrance, and the fragrance thoroughly property sent out improves, and assorted gas improves, and suction comfortableness gets a promotion.
Embodiment 2:
According to the formula in following table 3, tea flower extract various in table 3 is mixed, prepare camellia extract composition.
Table 3
Embodiment 2 is prepared the camellia extract composition that obtains according to the ratio in upper table 3, add 70% aqueous ethanolic solution, obtain camellia extract composition ethanolic soln.The camellia extract composition ethanolic soln obtained evenly is sprayed onto on pipe tobacco by 0.035% of pipe tobacco weight, after baking, rolls into cigarette.Wherein 0# in contrast, on pipe tobacco, only spray the aqueous ethanolic solution of 70%.Then carry out sensory evaluating smoking's experiment by GB5606.4-2005, comparison result of smokeing panel test is in table 4.
Table 4 Sensory Quality of Cigarette inspection source recording
Smoking result shows, the score of 1# to 4# is all higher than 0#, and wherein 1# composition score is the highest, contrasts with 0#, cigarette flavor harmony, and fragrance is abundant long, gives off a strong fragrance, and Hui Tian promotes the production of body fluid sense obviously, and pungency obviously alleviates.
Embodiment 3:
According to the formula in following table 5, tea flower extract various in table 5 is mixed, prepare camellia extract composition.
Table 5
Embodiment 3 is prepared the camellia extract composition that obtains according to the ratio in upper table 5, add 70% aqueous ethanolic solution, obtain camellia extract composition ethanolic soln.The camellia extract composition ethanolic soln obtained evenly is sprayed onto on pipe tobacco by 0.015% of pipe tobacco weight, after baking, rolls into cigarette.Wherein 0# in contrast, on pipe tobacco, only spray the aqueous ethanolic solution of 70%.Then carry out sensory evaluating smoking's experiment by GB5606.4-2005, comparison result of smokeing panel test is in table 6.
Table 6 Sensory Quality of Cigarette inspection source recording
Smoking result shows, the score of 1# to 4# is all higher than 0#, and wherein 1# composition score is the highest, contrasts with 0#, and cigarette flavor is coordinated, and fragrance fullness ratio gets a promotion, fragrance clear and natural, assorted gas, pungency be improved significantly.
Embodiment 4:
According to the formula in following table 7, tea flower extract various in table 7 is mixed, prepare camellia extract composition.
Table 7
Embodiment 4 is prepared the camellia extract composition that obtains according to the ratio in upper table 7, add 70% aqueous ethanolic solution, obtain camellia extract composition ethanolic soln.The camellia extract composition ethanolic soln obtained evenly is sprayed onto on pipe tobacco by 0.045% of pipe tobacco weight, after baking, rolls into cigarette.Wherein 0# in contrast, on pipe tobacco, only spray the aqueous ethanolic solution of 70%.Then carry out sensory evaluating smoking's experiment by GB5606.4-2005, comparison result of smokeing panel test is in table 8.
Table 8 Sensory Quality of Cigarette inspection source recording
Smoking result shows, the score of 1# to 4# is all higher than 0#, and wherein 1# composition score is the highest, contrasts with 0#, cigarette flavor coordinate, fragrance is gentle and fragrance remaining time is long, flue gas circle with, improve alcohol and the degree of smoke, increase fragrance fullness ratio, set off nature cigarette fragrant, abirritate.
Claims (101)
1. a composition for tea flower extract, wherein the content of each component is as follows:
2. the composition of claim 1, wherein the content of Tie Guanyin tea plant flower concrete is 19-21 weight part.
3. the composition of claim 1, wherein the content of Tie Guanyin tea plant flower concrete is 20 weight parts.
4. the composition of claim 1, wherein the content of Tie Guanyin tea plant flower essential oil is 1-3 weight part.
5. the composition of claim 1, wherein the content of Tie Guanyin tea plant flower essential oil is 2 weight parts.
6. the composition of claim 1, wherein the content of Tie Guanyin tea plant flower tincture is 18-20 weight part.
7. the composition of claim 1, wherein the content of Tie Guanyin tea plant flower tincture is 19 weight parts.
8. the composition of claim 1, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) essential oil of the flower of Camellia sinensis is 0.4-0.6 weight part.
9. the composition of claim 1, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) essential oil of the flower of Camellia sinensis is 0.5 weight part.
10. the composition of claim 1, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower absolute oil is 2-4 weight part.
The composition of 11. claims 1, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower absolute oil is 3 weight parts.
The composition of 12. claims 1, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower tincture is 0.4-0.6 weight part.
The composition of 13. claims 1, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower tincture is 0.5 weight part.
The composition of 14. claims 1, wherein the content of Chinese cassia tree tea tree extrait is 1.2-1.8 weight part.
The composition of 15. claims 1, wherein the content of Chinese cassia tree tea tree extrait is 1.5 weight parts.
The composition of 16. claims 1, wherein the content of Chinese cassia tree Tea Flower tincture is 0.8-1.2 weight part.
The composition of 17. claims 1, wherein the content of Chinese cassia tree Tea Flower tincture is 1 weight part.
The composition of 18. claims 1, wherein the content of narcissus tea tree flower concrete is 1.2-1.8 weight part.
The composition of 19. claims 1, wherein the content of narcissus tea tree flower concrete is 1.5 weight parts.
The composition of 20. claims 1, wherein the content of narcissus essential oil of the flower of Camellia sinensis is 0.8-1.2 weight part.
The composition of 21. claims 1, wherein the content of narcissus essential oil of the flower of Camellia sinensis is 1 weight part.
The composition of 22. claims 1, wherein the content of each component is as follows:
The composition of 23. claims 1, wherein the content of each component is as follows:
The composition of 24. 1 kinds of tea flower extract, wherein the content of each component is as follows:
The composition of 25. claims 24, wherein the content of Tie Guanyin tea plant flower concrete is 0.4-0.6 weight part.
The composition of 26. claims 24, wherein the content of Tie Guanyin tea plant flower concrete is 0.5 weight part.
The composition of 27. claims 24, wherein the content of Tie Guanyin tea plant extrait is 1.2-1.8 weight part.
The composition of 28. claims 24, wherein the content of Tie Guanyin tea plant extrait is 1.5 weight parts.
The composition of 29. claims 24, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower medicinal extract is 10-12 weight part.
The composition of 30. claims 24, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower medicinal extract is 11 weight parts.
The composition of 31. claims 24, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) essential oil of the flower of Camellia sinensis is 4-5 weight part.
The composition of 32. claims 24, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) essential oil of the flower of Camellia sinensis is 4.5 weight parts.
The composition of 33. claims 24, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower absolute oil is 21-23 weight part.
The composition of 34. claims 24, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower absolute oil is 22 weight parts.
The composition of 35. claims 24, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower tincture is 2-3 weight part.
The composition of 36. claims 24, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower tincture is 2.5 weight parts.
The composition of 37. claims 24, wherein the content of Chinese cassia tree essential oil of the flower of Camellia sinensis is 1.2-1.8 weight part.
The composition of 38. claims 24, wherein the content of Chinese cassia tree essential oil of the flower of Camellia sinensis is 1.5 weight parts.
The composition of 39. claims 24, wherein the content of narcissus tea tree flower concrete is 1.2-1.8 weight part.
The composition of 40. claims 24, wherein the content of narcissus tea tree flower concrete is 1.5 weight parts.
The composition of 41. claims 24, wherein the content of narcissus tea tree extrait is 2-3 weight part.
The composition of 42. claims 24, wherein the content of narcissus tea tree extrait is 2.5 weight parts.
The composition of 43. claims 24, wherein the content of each component is as follows:
The composition of 44. claims 24, wherein the content of each component is as follows:
The composition of 45. 1 kinds of tea flower extract, wherein the content of each component is as follows:
The composition of 46. claims 45, wherein the content of Tie Guanyin tea plant flower essential oil is 1-3 weight part.
The composition of 47. claims 45, wherein the content of Tie Guanyin tea plant flower essential oil is 2 weight parts.
The composition of 48. claims 45, wherein the content of Tie Guanyin tea plant extrait is 1.2-1.8 weight part.
The composition of 49. claims 45, wherein the content of Tie Guanyin tea plant extrait is 1.5 weight parts.
The composition of 50. claims 45, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower medicinal extract is 3-4 weight part.
The composition of 51. claims 45, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower medicinal extract is 3.5 weight parts.
The composition of 52. claims 45, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower absolute oil is 1.2-1.8 weight part.
The composition of 53. claims 45, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower absolute oil is 1.5 weight parts.
The composition of 54. claims 45, wherein the content of Chinese cassia tree essential oil of the flower of Camellia sinensis is 1.2-1.8 weight part.
The composition of 55. claims 45, wherein the content of Chinese cassia tree essential oil of the flower of Camellia sinensis is 1.5 weight parts.
The composition of 56. claims 45, wherein the content of narcissus tea tree flower concrete is 14-16 weight part.
The composition of 57. claims 45, wherein the content of narcissus tea tree flower concrete is 15 weight parts.
The composition of 58. claims 45, wherein the content of narcissus essential oil of the flower of Camellia sinensis is 6-7 weight part.
The composition of 59. claims 45, wherein the content of narcissus essential oil of the flower of Camellia sinensis is 6.5 weight parts.
The composition of 60. claims 45, wherein the content of narcissus Tea Flower tincture is 16-17 weight part.
The composition of 61. claims 45, wherein the content of narcissus Tea Flower tincture is 16.5 weight parts.
The composition of 62. claims 45, wherein the content of each component is as follows:
The composition of 63. claims 45, wherein the content of each component is as follows:
The composition of 64. 1 kinds of tea flower extract, wherein the content of each component is as follows:
The composition of 65. claims 64, wherein the content of Tie Guanyin tea plant flower concrete is 1.2-1.8 weight part.
The composition of 66. claims 64, wherein the content of Tie Guanyin tea plant flower concrete is 1.5 weight parts.
The composition of 67. claims 64, wherein the content of Tie Guanyin tea plant extrait is 0.8-1.2 weight part.
The composition of 68. claims 64, wherein the content of Tie Guanyin tea plant extrait is 1 weight part.
The composition of 69. claims 64, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) essential oil of the flower of Camellia sinensis is 0.8-1.2 weight part.
The composition of 70. claims 64, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) essential oil of the flower of Camellia sinensis is 1 weight part.
The composition of 71. claims 64, wherein the content of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower absolute oil is 1.2-1.8 weight part.
The composition of 72. claims 64, wherein content 1.5 weight part of Radix Campylotropis Hirtella (Herba Myrsines Africanae) Tea Flower absolute oil.
The composition of 73. claims 64, wherein the content of Chinese cassia tree tea tree flower concrete is 17-18 weight part.
The composition of 74. claims 64, wherein the content of Chinese cassia tree tea tree flower concrete is 17.5 weight parts.
The composition of 75. claims 64, wherein the content of Chinese cassia tree essential oil of the flower of Camellia sinensis is 1.2-1.8 weight part.
The composition of 76. claims 64, wherein the content of Chinese cassia tree essential oil of the flower of Camellia sinensis is 1.5 weight parts.
The composition of 77. claims 64, wherein the content of Chinese cassia tree tea tree extrait is 6-7 weight part.
The composition of 78. claims 64, wherein the content of Chinese cassia tree tea tree extrait is 6.5 weight parts.
The composition of 79. claims 64, wherein the content of Chinese cassia tree Tea Flower tincture is 4-5 weight part.
The composition of 80. claims 64, wherein the content of Chinese cassia tree Tea Flower tincture is 4.5 weight parts.
The composition of 81. claims 64, wherein the content of narcissus essential oil of the flower of Camellia sinensis is 0.4-0.6 weight part.
The composition of 82. claims 64, wherein the content of narcissus essential oil of the flower of Camellia sinensis is 0.5 weight part.
The composition of 83. claims 64, wherein the content of narcissus Tea Flower tincture is 1.2-1.8 weight part.
The composition of 84. claims 64, wherein the content of narcissus Tea Flower tincture is 1.5 weight parts.
The composition of 85. claims 64, wherein the content of each component is as follows:
The composition of 86. claims 64, wherein the content of each component is as follows:
The composition of 87. any one of claim 1 to 86, also comprises ethanol in said composition.
The composition of 88. claims 87, wherein said ethanol is the aqueous ethanolic solution of 50 ~ 95%.
The composition of 89. claims 87, wherein said ethanol is the aqueous ethanolic solution of 60 ~ 80%.
The composition of 90. claims 87, wherein said ethanol is the aqueous ethanolic solution of 65 ~ 75%.
The composition of 91. claims 87, wherein said ethanol is the aqueous ethanolic solution of 70%.
The composition of 92. any one of claim 88 to 91, wherein said ethanol content is: by weight 50 ~ 63.
The composition of 93. any one of claim 88 to 91, the content of wherein said ethanol is 50 weight parts, 52 weight parts, 52.5 weight parts or 63 weight parts.
The purposes of composition in cigarette of 94. any one of claim 1 to 93.
The composition of 95. any one of claim 1 to 93 is as the purposes of cigaret additive.
The composition of 96. any one of claim 1 to 93 is as the purposes of cigarette flavors.
The purposes of 97. any one of claim 94 to 96, described composition is used for pipe tobacco, thin slice, the internal lining paper of cigarette or filter stick.
98. 1 kinds of cigarette, it comprises the composition of any one of claim 1 to 93.
Cigarette described in 99. claims 98, the quality of wherein said composition is 0.001 ~ 0.5% of tobacco quality.
Cigarette described in 100. claims 98, the quality of wherein said composition is 0.015 ~ 0.045% of tobacco quality.
Cigarette described in 101. claims 98, the quality of wherein said composition is 0.045%, 0.035% or 0.015% of tobacco quality.
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| CN103484247B (en) * | 2013-09-27 | 2016-03-23 | 福建中烟工业有限责任公司 | A kind of Tea Flower stage extraction thing, its preparation method and the application in cigarette thereof |
| CN104629913A (en) * | 2015-01-05 | 2015-05-20 | 浙江工业大学 | Essence for cigarettes |
| CN104963235A (en) * | 2015-06-29 | 2015-10-07 | 安徽顺彤包装材料有限公司 | Lining paper coated with oolong extracting solution |
| CN105133421A (en) * | 2015-06-29 | 2015-12-09 | 安徽顺彤包装材料有限公司 | Coating liquid of peony fragrant type cigarette lining paper |
| CN105146746B (en) * | 2015-08-25 | 2016-08-17 | 中国烟草总公司郑州烟草研究院 | A kind of tea polyphenols tobacco humectant and the application in Medicated cigarette thereof |
| CN105929099B (en) * | 2016-07-14 | 2018-10-19 | 福建中烟工业有限责任公司 | A method of detection hydrosol volatile ingredient |
| CN105996115B (en) * | 2016-07-18 | 2018-08-17 | 福建中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke with extra-strong tea just object extract preparation processed |
| CN105996116B (en) * | 2016-07-18 | 2018-06-15 | 福建中烟工业有限责任公司 | Contain the extra-strong tea just composition of object extract processed and its application |
| CN106037012B (en) * | 2016-07-18 | 2019-03-15 | 福建中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke |
| CN106174683B (en) * | 2016-07-29 | 2018-05-15 | 福建中烟工业有限责任公司 | A kind of composition and the tobacco juice for electronic smoke containing said composition |
| CN106398873B (en) * | 2016-12-09 | 2019-12-06 | 宜春元博山茶油科技农业开发有限公司 | preparation method of tea tree flower essential oil |
| CN108125277B (en) * | 2018-03-21 | 2021-03-05 | 福建中烟工业有限责任公司 | Electronic cigarette and manufacturing method thereof |
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