CN103478889B - The pipe tobacco of tea flower fragrance and tobacco product - Google Patents
The pipe tobacco of tea flower fragrance and tobacco product Download PDFInfo
- Publication number
- CN103478889B CN103478889B CN201310446699.XA CN201310446699A CN103478889B CN 103478889 B CN103478889 B CN 103478889B CN 201310446699 A CN201310446699 A CN 201310446699A CN 103478889 B CN103478889 B CN 103478889B
- Authority
- CN
- China
- Prior art keywords
- tea flower
- tobacco
- pipe
- tea
- flower
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Abstract
The invention belongs to spices and Field of Tobacco, relate to a kind of pipe tobacco and tobacco product of tea flower fragrance.Particularly, the present invention relates to a kind of pipe tobacco, it contains tea flower extract.The invention still further relates to described pipe tobacco for the preparation of the purposes of tobacco product such as cigarette, tobacco product such as cigarette containing described pipe tobacco.Cigarette of the present invention has Tea Flower feature note, and with this fragrant harmony of cigarette tobacco, the flavor and taste of cigarette obviously improves, and pleasant impression is comfortable, and flue gas is fine and smooth, soft, effectively reduces pungent stimulation and the xerostomia sense of flue gas.And this flavouring essence for tobacco preparation technology is simple, and the adding technology in cigarette does not change the original processing technology of cigarette and equipment.
Description
Technical field
The invention belongs to spices and Field of Tobacco, relate to a kind of pipe tobacco and tobacco product of tea flower fragrance.
Background technology
" Chinese-style cigarette " core competitiveness forms selling point style, embodies personalized and differentiation, sucks custom with what adapt to consumer.Essence spice for cigarette is Chinese-style cigarette " soul " place, and scientifically flavoring and casing in cigarette is the important means of outstanding product style characteristic.Effective component extracting from natural herbal plant, is added in cigarette, can give cigarette special aromatic style, and some active components in natural plants to a certain degree can reduce some harmful components in cigarette smoke, improves the security of smoking.
Huang Tianhui (CN101317692A) discloses a kind of extracting method of Jasmine medicinal extract, and the preparation method of additive agent for jasmine fragrance type cigarette and the application in cigarette thereof, reaches and makes the effects such as cigarette smoke is fine and smooth, soft.Disclosing a kind of Chinese prickly ash, lemon and apple in Huanglong etc. (CN102687901A) is tobacco aromatics prepared by raw material, and applies in perfuming cigarette, and cigarette can be made to have delicate fragrance type characteristic.
Tea Flower is the flower of Theaceae Camellia Plants tea tree, is a kind of without the need to planting cultivation, enriching and reproducible natural resources.In recent years the comprehensive utilization of Tea Flower is more and more paid attention to.Tea Flower is containing various active compositions such as abundant aroma substance and protein, Tea Polyphenols, tea polysaccharide, Tea Saponin, flavonoids, amino acid, vitamin, trace element and superoxide dismutase (SOD), theobromines.The features such as it is fresh and clean that Tea flower essence prepared by tea flower extract has fragrance, and sweet spiciness is strongly fragrant, have higher using value.
Still need at present and want suitable additive and correlation technique, with the cigarette of production tea flower fragrance.
Summary of the invention
The present inventor through in depth research and performing creative labour, obtain the preparation technology of tea flower extract and correspondingly obtain tea flower extract (essential oil of the flower of Camellia sinensis, Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil).The present inventor is surprised to find, obtained tea flower extract (one or more mixture) is put in cigarette, cigarette can be made to have the note of the tea tree fragrance of a flower, the flavor and taste of cigarette improves obviously, with this fragrant harmony of cigarette tobacco, pleasant impression is comfortable, and flue gas is fine and smooth, soft, effectively reduce pungent stimulation and the xerostomia sense of flue gas.Thus provide following invention:
One aspect of the present invention relates to a kind of pipe tobacco, and it contains tea flower extract.
Described tea flower extract can use and be selected from following method preparation: normal temperature lixiviate, heating and refluxing extraction, surname extraction, ultrasound on extracting, microwave auxiliary extraction, enzyme process auxiliary extraction, accelerated solvent extraction, supercritical fluid extraction, Simultaneous distillation-extraction etc.But preferably, be tea flower extract that this paper records below.
Described tea flower extract can be the mixture that the extract that obtains from single variety Tea Flower or different varieties of tea plant flower obtain extract.
In the ethanol that tea flower extract is dissolved in 60%-80% or propane diols, be mixed with the Tea flower essence that concentration range is 1%-10%.In perfuming cigarette operation, equably Tea flower essence is sprayed onto on finished product tobacco leaf formulation pipe tobacco, after storing 0-24h, rolls into cigarette.The consumption of Tea flower essence is the 0.01-3% of finished product tobacco leaf formulation pipe tobacco weight.
Pipe tobacco according to any one of the present invention, wherein, the content of described tea flower extract or consumption are the 0.01-3 ‰ of pipe tobacco weight; Preferably, be 0.05 ‰-1.5 ‰; More preferably, be 0.1 ‰-1 ‰, be particularly preferably 0.2 ‰-0.8 ‰, 0.2 ‰-0.5 ‰, 0.5 ‰-0.8 ‰; Particularly, be 0.2 ‰, 0.3 ‰, 0.4 ‰, 0.5 ‰, 0.6 ‰, 0.7 ‰ or 0.8 ‰.
Pipe tobacco according to any one of the present invention, wherein, described pipe tobacco is finished product tobacco leaf formulation pipe tobacco; Particularly, be made up of tobacco leaf silk, stem, expanded cut tobacco and optional reconstituted tobacco silk; Particularly, described reconstituted tobacco silk is tobacco thin filament; Preferably, according to percentage by weight, tobacco leaf silk 75%-80%, stem 10%-16%, expanded cut tobacco are 4%-6%, tobacco thin filament 6%-8%.
Pipe tobacco according to any one of the present invention, wherein, described tea flower extract be selected from essential oil of the flower of Camellia sinensis, Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil any one, two kinds, three kinds or four kinds.
Pipe tobacco according to any one of the present invention, wherein, described tea flower extract is the mixture of Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil; Preferably, according to percentage by weight, Tea Flower tincture 25%-70%, Tea Flower medicinal extract 15%-55%, Tea Flower absolute oil 15%-20%.In one embodiment of the invention, Tea Flower tincture 25%, Tea Flower medicinal extract 55%, Tea Flower absolute oil 20%; In another embodiment of the invention, Tea Flower tincture 70%, Tea Flower medicinal extract 15%, Tea Flower absolute oil 15%.
The present inventor is also surprised to find, when using above-mentioned three kinds of extracts (mixture of Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil) and consumption thereof, the cigarette obtained has the note of Tea Flower feature, harmony fragrant with cigarette, aroma quality obviously improves, and fragrance exquisiteness is soft, and mouthfeel is fresh and sweet, assorted gas and dry sensation obviously improve, and pleasant impression is clean.Wherein allowing inventor impressive is especially the fresh and sweet feature of mouthfeel.
Tincture, medicinal extract, absolute oil and essential oil that the Tea Flower of different cultivars extracts have certain difference.Tincture, medicinal extract, absolute oil and essential oil can be used in combination, it can be same seeds, also can different tree species.Pipe tobacco according to any one of the present invention, wherein, tincture used, medicinal extract, absolute oil and essential oil are independently for being selected from Fujian Anxi Tieguanyin Tea tea tree, District, Xinyang Area, Henan Province high-quality green tea tea tree, the tincture of Tea Flower of Wuyi Mountain, fujian Wuyi cliff tea tea tree and yunnan puer tea tea tree, medicinal extract, absolute oil and essential oil.
In a specific embodiment of the present invention, the extract that pipe tobacco is used, Xinyang Maojian Tea tea tree tincture 25%, Wuyi cliff tea Tea Flower medicinal extract 55%, Wuyi cliff tea Tea Flower absolute oil 20%; In another specific embodiments of the present invention, Anxi Tieguanyin Tea Tea Flower tincture 70%, Xinyang Maojian Tea tea tree flower concrete 15%, Wuyi cliff tea Tea Flower absolute oil 15%.
The invention still further relates to the extractive composition (mixture of Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil) of above-mentioned use.
Pipe tobacco according to any one of the present invention, wherein, described essential oil of the flower of Camellia sinensis obtains as follows:
(1) taking a certain amount of Tea Flower loads in the decompression extraction element being furnished with trapping cold-trap;
(2) add the water of Tea Flower weight at least 5 times, and the temperature of the water added is more than 80 DEG C, at least 5min is soaked in sealing, is cooled to 30-70 DEG C;
(3-1) carry out reduced steam distillation, temperature used is identical with cooled temperature in step (2), and vacuum is 1-17kpa, collects distillate;
Preferably, also comprise step (3-2): repeat operation 1 time in step (2) and (3-1) or repeatedly, and merge distillate;
(4) in using, low polar organic solvent carries out 1 time the distillate obtained in step (3-1) or step (3-2) or repeatedly back extraction (such as 2,3,4 or 5 times, preferably 3 times), obtains stripping workshop; Stripping workshop is concentrated, obtains concentrate;
(5) use concentrate weight 2-4 absolute ethyl alcohol doubly to carry out backwash to the concentrate obtained in step (4), during reduced pressure concentration removing wherein remains, after low polar organic solvent, obtain essential oil of the flower of Camellia sinensis.
Pipe tobacco according to any one of the present invention, wherein, step (2) meet following 1.-any one 4. in item or multinomial:
The amount of the water 1. added is 5-50 times of Tea Flower weight, is preferably 5-40 times or 8-40 times, is more preferably 10-30 doubly;
The temperature of the water 2. added is preferably more than 85 DEG C, is more preferably more than 90 DEG C, more preferably more than 95 DEG C, is particularly preferably boiling water;
3. the time sealing immersion is 5min-4h, is preferably 5min-4h, 5min-3h or 5min-2h, is more preferably 5-60min, 5-50min or 5-40min, is particularly preferably 5-30min;
4. 30-70 DEG C is cooled to; Such as 30-40 DEG C, 45-55 DEG C or 60-70 DEG C.
Pipe tobacco according to any one of the present invention, wherein, step is cooled to 30-70 DEG C in (2), such as 30-40 DEG C, 30-50 DEG C, 30-60 DEG C, 40-50 DEG C, 45-55 DEG C, 40-60 DEG C, 40-70 DEG C, 50-60 DEG C, 50-70 DEG C or 60-70 DEG C.
Those skilled in the art know, and vacuum and vapo(u)rizing temperature are corresponding to a certain extent, need to guarantee to allow under to fixed temperature and vacuum the distilled water in cucurbit and aroma component steam.
Be not limited to theoretical restriction, temperature is lower, and required vacuum is less, and temperature is higher, and required vacuum is larger.The present inventor finds, when temperature is 30 DEG C, and vacuum 2.5kpa; The speed that distills less of 2.5kpa can be faster; When temperature is 70 DEG C, vacuum 17kpa; The speed that distills less of 17kpa can be faster.
Be not limited to theoretical restriction, on the other hand, under the prerequisite of temperature setting, if vacuum is too low, meeting bumping may be caused, pot liquid is gone out; If vacuum is too high, pot liquid may be made to distill not out, do not have the effect of decompression distillation.Therefore, the vacuum ranges that each temperature value correspondence one is proper.
Therefore, about the vacuum of the distillation of reduced steam described in step (3-1) or (3-2), those skilled in the art can set according to the theory above selected temperature reference or this area knowledge, also with reference to vacuum ranges below, or can adjust on this basis:
Such as 1-12kPa, 1-10kPa, 1-9.5kPa, 1-9kPa, 1-8.5kPa, 1-8kPa, 1-7.5kPa or 1-7kPa; Such as 2.5-7kPa, 1-2kPa, 1-3kPa, 1-4kPa, 1-5kPa, 1-6kPa, 2-3kPa, 2-4kPa, 2-5kPa, 2-6kPa, 2-7kPa, 3-4kPa, 3-5kPa, 3-6kPa, 3-7kPa, 4-5kPa, 4-6kPa, 4-7kPa, 5-6kPa, 5-7kPa, 6-7kPa, 6-12kPa, 8-12kPa, 10-12kPa, 1kPa, 2kPa, 3kPa, 4kPa, 5kPa, 6kPa, 7kPa, 8kPa, 9kPa, 10kPa, 11kPa or 12kPa.
Pipe tobacco according to any one of the present invention, wherein, in step (4), in described low polar organic solvent be selected from absolute ether and ethyl acetate any one, or two kinds with the mixture of arbitrary proportion.Ethyl acetate.In described, the consumption of low polar organic solvent can be the 1/4-1/3 of distillate volume.
The decompression extraction element used can be commercially available, and those skilled in the art also can carry out combination by the routine instrument device be purchased and realize.
Pipe tobacco according to any one of the present invention, wherein, described Tea Flower tincture, Tea Flower medicinal extract or Tea Flower absolute oil, respectively by following steps 1), step 1)-2) or step 1)-3) obtained:
1) ultra high pressure extraction: take a certain amount of Tea Flower and put into ultra high pressure extraction tank, add the edible alcohol of at least 2 times of (w/w) Tea Flower weight, carry out ultra high pressure extraction, obtain Tea Flower tincture 1, the concentration of wherein said edible alcohol is 20-70%(mass concentration); Preferably, 1/5-1/10 Tea Flower tincture 1 being concentrated into original volume obtains Tea Flower tincture 2;
2) Tea Flower medicinal extract is prepared: the Tea Flower tincture 1 obtained in step 1) or Tea Flower tincture 2 are concentrated further, obtain Tea Flower medicinal extract;
3) Tea Flower absolute oil is prepared: with a certain amount of 95% ethanol resuspension step 2) the Tea Flower medicinal extract that obtains, then carry out freezing processing (such as-10 DEG C to-20 DEG C), cooling time is that 16-48h(is preferably 20-36h), then filter, concentrated, obtain Tea Flower absolute oil.
Pipe tobacco according to any one of the present invention, wherein, step 1) meet following 1.-any one 6. in item or multinomial:
1. for adopted Tea Flower is Tea Flower fresh flower, dried flower, spray Ethanol Treatment Tea Flower, alcohol immersion Tea Flower described in;
2. release immediately after ultra high pressure extraction;
3. add the edible alcohol of at least 2-15 doubly (w/w) Tea Flower weight, be preferably 2-10 doubly, 2-8 doubly, 3-8 doubly (w/w), be more preferably 4-7 doubly (w/w);
④150-500Mpa；
5. the dwell time is 5-120min, is preferably 5-60min, is more preferably 10-30min.
6. the concentration of edible alcohol used is 40-70%(mass concentration).
Pipe tobacco according to any one of the present invention, wherein, in step 1), particularly, the concentration of described edible alcohol is 20-70%(mass concentration), 20-40%, 20-50%, 40-50%, 50-70%, 20%, 30%, 40%, 50%, 60%, 70%.
Pipe tobacco according to any one of the present invention, wherein, in step 1), release immediately after ultra high pressure extraction.
Pipe tobacco according to any one of the present invention, wherein, in step 1), the pressure of described super-pressure is 150-500Mpa; Particularly, be 150-250Mpa, 150-300Mpa, 250-300Mpa, 250-350Mpa, 250-500Mpa, 300-350Mpa, 300-500Mpa, 350-500Mpa, 150Mpa, 200Mpa, 250Mpa, 300Mpa, 350Mpa, 400Mpa, 450Mpa, 500Mpa etc.
The ultra high pressure extraction device used can be commercially available.
The purposes in tobacco product such as cigarette prepared by pipe tobacco according to any one of another aspect of the present invention relates to.
Another aspect of the invention relates to a tobacco articles, and it contains the pipe tobacco according to any one of the present invention; Particularly, described tobacco product is cigarette.
In the present invention,
" tea tree " in described " Tea Flower ", if not otherwise specified, refers to the plant of Theales (Theales), Theaceae (Theaceae) or Camellia (Camellis).
In the embodiment that the present invention is concrete, described tea tree is Fujian Anxi Tieguanyin Tea tea tree, District, Xinyang Area, Henan Province high-quality green tea tea tree, Wuyi Mountain, fujian Wuyi cliff tea tea tree or yunnan puer tea tea tree.
In one aspect of the invention, " flower " in described " Tea Flower " comprising: perianth, oecium, gynoecium.Perianth comprises: calyx (being made up of sepal), corolla (being made up of petal).The color of flower and fragrance are from corolla.Stamen comprises: filigree and flower pesticide.Gynoecium comprises: column cap, style and ovary.
In one aspect of the invention, term " Tea Flower " can be fresh flower, also can be dry flower; If do not have specified otherwise, it refers to complete Tea Flower or a part for Tea Flower; It at least comprises petal; Alternatively, one or more being selected from sepal, stamen and gynoecium are also comprised.
In the embodiment that the present invention is concrete, described Tea Flower is the Tea Flower picking up from Fujian Anxi Tieguanyin Tea tea tree, District, Xinyang Area, Henan Province high-quality green tea tea tree, Wuyi Mountain, fujian Wuyi cliff tea tea tree or yunnan puer tea tea tree.
Tea Flower of the present invention can be Tea Flower fresh flower, dried flower, spray Ethanol Treatment Tea Flower, saline sook Tea Flower or alcohol immersion Tea Flower.
Term " essential oil ", in broad terms, essential oil refer to from spice berry and secrete fragrant animal organ to extract the general name of the volatility fragrant containing substance goods obtained through processing, in the narrow sense, essential oil only refers to the goods with steam distillation, milling process, cold grinding method or cracking process fragrant containing substance obtained from spice berry organ (as flower, leaf, branch, skin, scapus, root, fruit, seed etc.).In actual applications, normal its narrow sense of employing.
Term " tincture " or " tincture " refer to uses certain density ethanol, lixiviate spice berry organ or exudate and secrete fragrant animal containing fragrant organ or its aroma material preparation containing some ethanol obtained containing fragrant secretion.Under normal temperature, obtained tincture is called " cold process tincture "; Tincture obtained under heated reflux condition is called " hot method tincture ".
Term " medicinal extract ", in a broad sense, medicinal extract refers to organic solvent extraction spice berry organ or its exudate (as resin, natural gum, balm), removing solvent for use and the general designation of aroma material preparation that obtains.From in the narrow sense, medicinal extract only refer to organic solvent extraction spice berry organ obtain not containing the aroma material preparation of solvent for use and moisture.
Term " absolute oil ", in a broad sense, refers to the solution extracting the fragrant composition in medicinal extract, botany bar gum, balm or face cream with high concentration ethanol, through freezing processing, elimination insoluble matter, then after pressure reducing and steaming ethanol the general designation of the aroma material preparation of gained.
In the present invention, Tea flower essence also refers to tea flower extract, includes but not limited to: Tea Flower tincture, medicinal extract and/or absolute oil; Alternatively, it also comprises auxiliary material (carrier, solvent, pigment, antioxidant, anticorrisive agent, humectant, fumet etc.).
In the present invention, particularly, described tobacco product is the tobacco product that can suck, and is preferably cigarette.
In the present invention, described pipe tobacco can be tobacco leaf silk; Also can be finished product tobacco leaf formulation pipe tobacco; Particularly, described finished product tobacco leaf formulation pipe tobacco is made up of tobacco leaf silk, stem, expanded cut tobacco and optional reconstituted tobacco silk; Particularly, described reconstituted tobacco silk is tobacco thin filament.Preferably, according to percentage by weight, described finished product tobacco leaf formulation pipe tobacco consists of tobacco leaf silk 75%-80%, stem 10%-16%, expanded cut tobacco is 4%-6%, tobacco thin filament 6%-8%.
The beneficial effect of the invention
Add in cigarette by obtained Tea flower essence, cigarette can be made to have Tea Flower feature note, the flavor and taste of cigarette improves, and with this fragrant harmony of cigarette tobacco, pleasant impression is comfortable, and flue gas is fine and smooth, soft, effectively reduces pungent stimulation and the xerostomia sense of flue gas.And this cigarette additive preparation technology is simple, and the adding technology in cigarette does not change the original processing technology of cigarette and equipment.
Detailed description of the invention
Below in conjunction with embodiment, embodiment of the present invention are described in detail, but it will be understood to those of skill in the art that the following example only for illustration of the present invention, and should not be considered as limiting scope of the present invention.Unreceipted actual conditions person in embodiment, the condition of conveniently conditioned disjunction manufacturer suggestion is carried out.Agents useful for same or the unreceipted production firm person of instrument, being can by the conventional products of commercial acquisition.
preparation example 1: the preparation of essential oil of the flower of Camellia sinensis
1. experiment material
Tea Flower picks up from the Tie Guanyin tea plant in Anxi, Fujian.
2. the preparation of essential oil of the flower of Camellia sinensis
Step is as follows:
(1) take certain quantity of fresh Tea Flower to load in decompression extraction element, add the boiling water of Tea Flower weight 10 times, sealing is cooled to 30 DEG C after soaking 5min;
(2) on the decompressor being furnished with trapping cold-trap, carry out reduced steam distillation, temperature is: 30 DEG C, and vacuum is: 1kpa, collects distillate;
(3) decompression distillation complete after add Tea Flower weight 5 times boiling water in extraction element, repeat decompression distillation twice according to step (3) after merge and collect liquid;
(4) add 0.3 times and collect the long-pending absolute ether back extraction of liquid three times, merge stripping workshop and be concentrated into 1/10 of fresh Tea Flower weight;
(5) essential oil of the flower of Camellia sinensis is refined: the absolute ethyl alcohol adding concentrate 3 times in step (4) carries out backwash, reduced pressure concentration remove wherein after residual anhydrous ether essential oil of the flower of Camellia sinensis.
preparation example 2: the preparation of Tea Flower tincture
1. experiment material
Tea Flower picks up from the Tie Guanyin tea plant in Anxi, Fujian.
2. the preparation of Tea Flower tincture
Step is as follows:
(1) described Tea Flower includes but not limited to fresh Tea Flower, dried flower, alcohol immersion process Tea Flower, spray Ethanol Treatment Tea Flower etc.;
(2) ultra high pressure extraction: take certain quantity of fresh Tea Flower and put into ultra high pressure extraction tank, adds the edible alcohol that 7 times of concentration to Tea Flower weight are 20%, carries out release immediately after ultra high pressure extraction; The pressure of described super-pressure is: 150MPa, the dwell time: 30min;
(3) namely the 1/5-1/10 being concentrated into original volume after the extract in step (2) being carried out suction filtration obtains Tea Flower tincture.
preparation example 3: the preparation of Tea Flower tincture and Tea Flower medicinal extract
1. experiment material
Tea Flower picks up from the high-quality green tea tea tree of District, Xinyang Area, Henan Province.
2. the preparation of Tea Flower medicinal extract
Step is as follows:
(1) described Tea Flower includes but not limited to fresh Tea Flower, dried flower, alcohol immersion process Tea Flower, spray Ethanol Treatment Tea Flower etc.;
(2) ultra high pressure extraction: take certain quantity of fresh Tea Flower and put into ultra high pressure extraction tank, 4 times of concentration to Tea Flower weight are 40% edible alcohol, carry out release immediately after ultra high pressure extraction; The pressure of described super-pressure is: 500MPa, the dwell time: 10min;
(3) namely the 1/5-1/10 being concentrated into original volume after the extract in step (2) being carried out suction filtration obtains Tea Flower tincture;
(4) Tea Flower medicinal extract is prepared: Tea Flower medicinal extract can be obtained by concentrated for the Tea Flower tincture obtained in step (3) continuation.
preparation example 4: the preparation of Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil
1. experiment material
Tea Flower picks up from the Wuyi cliff tea tea tree of Wuyi Mountain, fujian.
2. the preparation of Tea Flower absolute oil
Step is as follows:
(1) described Tea Flower includes but not limited to fresh Tea Flower, dried flower, alcohol immersion process Tea Flower, spray Ethanol Treatment Tea Flower etc.;
(2) ultra high pressure extraction: take certain quantity of fresh Tea Flower and put into ultra high pressure extraction tank, 5 times of concentration to Tea Flower weight are 70% edible alcohol, carry out release immediately after ultra high pressure extraction; The pressure of described super-pressure is: 300MPa, the dwell time: 20min;
(3) namely the 1/5-1/10 being concentrated into original volume after the extract in step (2) being carried out suction filtration obtains Tea Flower tincture;
(4) Tea Flower medicinal extract is prepared: Tea Flower medicinal extract can be obtained by concentrated for the Tea Flower tincture obtained in step (3) continuation;
(5) Tea Flower absolute oil is prepared: with a certain amount of 95% ethanol back dissolving Tea Flower medicinal extract, filter after freezing (such as-10 DEG C to-20 DEG C) 24-48h, concentrated, obtain Tea Flower absolute oil.
The tea flower extract that preparation example 1-4 obtains is used for the following examples.
embodiment 1: the preparation of tea flower fragrance 1# pipe tobacco and 1# cigarette
1. get the essential oil of the flower of Camellia sinensis (prepared by preparation example 1) of 25 parts by weight, the Tea Flower tincture of 75 parts by weight mixes (prepared by preparation example 3), be dissolved in the ethanol of 70% and be configured to the solution that mass concentration is 4%, obtain Tea flower essence.
2. get appropriate Tea flower essence, conventionally the process of perfuming to be sprayed onto equably on finished product tobacco leaf formulation pipe tobacco (wherein tobacco leaf silk 75%, stem 12%, expanded cut tobacco be 6% and tobacco thin filament 7%), obtain tea flower fragrance 1# pipe tobacco.The consumption of Tea flower essence is 0.5% of finished product tobacco leaf formulation pipe tobacco weight, and the consumption of its tea flower extract is 0.2 ‰ of finished product tobacco leaf formulation pipe tobacco weight.
3. obtained 1# pipe tobacco is preserved 24h, conventionally roll into cigarette.Obtain the 1# cigarette of tea flower fragrance.
Compared with the contrast cigarette that the ethanol of only add identical weight number 70% is obtained, the present embodiment obtains the note that 1# cigarette has Tea Flower feature, harmony fragrant with cigarette, and aroma quality obviously improves, and assorted gas and excitant are obviously improved, and pleasant impression is clean.
embodiment 2: the preparation of tea flower fragrance 2# pipe tobacco and 2# cigarette
1. the Tea Flower absolute oil (prepared by preparation example 4) getting the Tea Flower tincture (prepared by preparation example 3) of 25 parts by weight, the Tea Flower medicinal extract (prepared by preparation example 4) of 55 parts by weight and 20 parts by weight mixes, be dissolved in the ethanol of 60% and be configured to the solution that mass concentration is 10%, obtain Tea flower essence.
2. get appropriate Tea flower essence, conventionally the process of perfuming is sprayed onto (wherein tobacco leaf silk 78%, stem 10%, expanded cut tobacco 4% or tobacco thin filament 8%) on finished product tobacco leaf formulation pipe tobacco equably, obtains tea flower fragrance 2# pipe tobacco.The consumption of Tea flower essence is 0.4% of finished product tobacco leaf formulation pipe tobacco weight, and the consumption of its tea flower extract is 0.4 ‰ of finished product tobacco leaf formulation pipe tobacco weight.
3. obtained 2# pipe tobacco is preserved 24h, conventionally roll into cigarette.Obtain the 2# cigarette of tea flower fragrance.
Compared with the contrast cigarette that 60% ethanol only adding identical weight number is obtained, the present embodiment obtains the note that 2# cigarette has Tea Flower feature, harmony fragrant with cigarette, aroma quality obviously improves, and fragrance is fine and smooth, and mouthfeel is fresh and sweet, assorted gas and dry sensation obviously improve, and pleasant impression is clean.
embodiment 3: the preparation of tea flower fragrance 3# pipe tobacco and 3# cigarette
1. the Tea Flower absolute oil (prepared by preparation example 4) getting the Tea Flower tincture (prepared by preparation example 2) of 70 parts by weight, the Tea Flower medicinal extract (prepared by preparation example 3) of 15 parts by weight and 15 parts by weight mixes, be dissolved in the ethanol of appropriate 80% solution being configured to 10%, obtain Tea flower essence.
2. get appropriate Tea flower essence, conventionally the process of perfuming is sprayed onto (wherein tobacco leaf silk 80%, stem 10%, expanded cut tobacco 4% or tobacco thin filament 6%) on finished product tobacco leaf formulation pipe tobacco equably, obtains tea flower fragrance 3# pipe tobacco.The consumption of Tea flower essence is 0.8% of finished product tobacco leaf formulation pipe tobacco weight, and the consumption of its tea flower extract is 0.8 ‰ of finished product tobacco leaf formulation tobacco quality.
3. obtained 3# pipe tobacco is preserved 24h, conventionally roll into cigarette.Obtain the 3# cigarette of tea flower fragrance.
Compared with the contrast cigarette that 80% ethanol only adding identical weight number is obtained, the present embodiment obtains the note that 3# cigarette has Tea Flower feature, harmony fragrant with cigarette, fragrance enriches, and fragrance exquisiteness is soft, and mouthfeel is fresh and sweet, assorted gas and dry sensation obviously improve, and pleasant impression is clean.
Although the specific embodiment of the present invention has obtained detailed description, it will be understood to those of skill in the art that.According to disclosed all instructions, can carry out various amendment and replacement to those details, these change all within protection scope of the present invention.Four corner of the present invention is provided by claims and any equivalent thereof.
Claims (41)
1. a pipe tobacco, it contains tea flower extract;
Described tea flower extract is essential oil of the flower of Camellia sinensis, and optional be selected from Tea Flower tincture, Tea Flower medicinal extract and Tea Flower absolute oil any one, two or three;
Described essential oil of the flower of Camellia sinensis obtains as follows:
(1) taking a certain amount of Tea Flower loads in the decompression extraction element being furnished with trapping cold-trap;
(2) add the water of Tea Flower weight at least 5 times, and the temperature of the water added is more than 80 DEG C, at least 5min is soaked in sealing, is cooled to 30-70 DEG C;
(3-1) carry out reduced steam distillation, temperature used is identical with cooled temperature in step (2), and vacuum is 1-17kpa, collects distillate;
(4) in using, low polar organic solvent carries out 1 time or repeatedly back extraction the distillate obtained, and obtains stripping workshop; Stripping workshop is concentrated, obtains concentrate;
(5) use concentrate weight 2-4 absolute ethyl alcohol doubly to carry out backwash to the concentrate obtained in step (4), during reduced pressure concentration removing wherein remains, after low polar organic solvent, obtain essential oil of the flower of Camellia sinensis.
2. pipe tobacco according to claim 1, wherein, the content of described tea flower extract or consumption are 0.01 ‰-3 ‰ of pipe tobacco weight.
3. pipe tobacco according to claim 1, wherein, the content of described tea flower extract or consumption are 0.1 ‰-1 ‰ of pipe tobacco weight.
4. pipe tobacco according to claim 1, wherein, the content of described tea flower extract or consumption are 0.2 ‰-0.8 ‰ of pipe tobacco weight.
5. pipe tobacco according to claim 2, wherein, described pipe tobacco is finished product tobacco leaf formulation pipe tobacco.
6. pipe tobacco according to claim 5, wherein, described finished product tobacco leaf formulation pipe tobacco is made up of tobacco leaf silk, stem, expanded cut tobacco and optional reconstituted tobacco silk.
7. pipe tobacco according to claim 6, wherein, described reconstituted tobacco silk is tobacco thin filament.
8. pipe tobacco according to claim 7, wherein, tobacco leaf silk 75%-80%, stem 10%-16%, expanded cut tobacco are 4%-6%, tobacco thin filament 6%-8%.
9. pipe tobacco according to claim 1, wherein, also comprises step (3-2): repeat operation 1 time in step (2) and (3-1) or repeatedly, and merge distillate; Continue step (4) again.
10. pipe tobacco according to claim 1, wherein, step (2) meet following 1.-any one 4. in item or multinomial:
The amount of the water 1. added is 5-50 times of Tea Flower weight;
The temperature of the water 2. added is more than 85 DEG C;
3. the time sealing immersion is 5min-4h;
4. 30-70 DEG C is cooled to.
11. pipe tobaccos according to claim 10, wherein, the amount of the water added is 5-40 times of Tea Flower weight.
12. pipe tobaccos according to claim 10, wherein, the amount of the water added is 8-40 times of Tea Flower weight.
13. pipe tobaccos according to claim 10, wherein, the amount of the water added is 10-30 times of Tea Flower weight.
14. pipe tobaccos according to claim 10, wherein, the temperature of the water added is more than 90 DEG C.
15. pipe tobaccos according to claim 10, wherein, the temperature of the water added is more than 95 DEG C.
16. pipe tobaccos according to claim 10, wherein, the water added is boiling water.
17. pipe tobaccos according to claim 10, wherein, the time that sealing is soaked is 5min-3h.
18. pipe tobaccos according to claim 10, wherein, the time that sealing is soaked is 5min-2h.
19. pipe tobaccos according to claim 10, wherein, the time that sealing is soaked is 5-60min.
20. pipe tobaccos according to claim 10, wherein, the time that sealing is soaked is 5-50min.
21. pipe tobaccos according to claim 10, wherein, the time that sealing is soaked is 5-40min.
22. pipe tobaccos according to claim 10, wherein, the time that sealing is soaked is 5-30min.
23. pipe tobaccos according to claim 10, wherein, are cooled to 30-40 DEG C.
24. pipe tobaccos according to claim 10, wherein, are cooled to 45-55 DEG C.
25. pipe tobaccos according to claim 10, wherein, are cooled to 60-70 DEG C.
26. pipe tobaccos according to claim 1, wherein, in step (4), in described low polar organic solvent be selected from absolute ether and ethyl acetate any one.
27. pipe tobaccos according to claim 1, wherein, described Tea Flower tincture, Tea Flower medicinal extract or Tea Flower absolute oil, respectively by following steps 1), step 1)-2) or step 1)-3) obtained:
1) ultra high pressure extraction: take a certain amount of Tea Flower and put into ultra high pressure extraction tank, add the edible alcohol of at least 2 times of Tea Flower weight, carry out ultra high pressure extraction, obtain Tea Flower tincture 1, the mass concentration of wherein said edible alcohol is 20-70%;
2) prepare Tea Flower medicinal extract: by step 1) in the Tea Flower tincture 1 that obtains concentrate further, obtain Tea Flower medicinal extract;
3) Tea Flower absolute oil is prepared: with a certain amount of 95% ethanol resuspension step 2) the Tea Flower medicinal extract that obtains, then carry out freezing processing, cooling time is 16-48h, then filters, concentrated, obtains Tea Flower absolute oil.
28. pipe tobaccos according to claim 27, wherein, step 1) also comprise 1/5-1/10 Tea Flower tincture 1 being concentrated into original volume and obtain Tea Flower tincture 2; Continue step 2 again) Tea Flower tincture 2 is concentrated further.
29. pipe tobaccos according to claim 27 or 28, wherein, step 3) in, cooling time is 20-36h.
30. pipe tobaccos according to claim 27 or 28, wherein, step 1) meet following 1.-any one 6. in item or multinomial:
1. adopted Tea Flower is Tea Flower fresh flower, dried flower, spray Ethanol Treatment Tea Flower, saline sook Tea Flower or alcohol immersion Tea Flower;
2. release immediately after ultra high pressure extraction;
3. the edible alcohol of at least 1-15 times of Tea Flower weight is added;
④150－500Mpa；
5. the dwell time is 5-120min;
6. the mass concentration of edible alcohol used is 40-70%.
31. pipe tobaccos according to claim 30, wherein, add the edible alcohol of 1-10 times of Tea Flower weight.
32. pipe tobaccos according to claim 30, wherein, add the edible alcohol of 2-10 times of Tea Flower weight.
33. pipe tobaccos according to claim 30, wherein, add the edible alcohol of 2-8 times of Tea Flower weight.
34. pipe tobaccos according to claim 30, wherein, add the edible alcohol of 3-8 times of Tea Flower weight.
35. pipe tobaccos according to claim 30, wherein, add the edible alcohol of 4-7 times of Tea Flower weight.
36. pipe tobaccos according to claim 30, wherein, the dwell time is 5-60min.
37. pipe tobaccos according to claim 30, wherein, the dwell time is 10-30min.
The purposes in tobacco product prepared by pipe tobacco according to any one of 38. claims 1 to 37.
39. according to purposes according to claim 38, and wherein, described tobacco product is cigarette.
40. 1 tobacco articles, it contains the pipe tobacco according to any one of claims 1 to 37.
41. tobacco products according to claim 40, wherein, described tobacco product is cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310446699.XA CN103478889B (en) | 2013-09-27 | 2013-09-27 | The pipe tobacco of tea flower fragrance and tobacco product |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310446699.XA CN103478889B (en) | 2013-09-27 | 2013-09-27 | The pipe tobacco of tea flower fragrance and tobacco product |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103478889A CN103478889A (en) | 2014-01-01 |
| CN103478889B true CN103478889B (en) | 2016-02-03 |
Family
ID=49819748
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310446699.XA Active CN103478889B (en) | 2013-09-27 | 2013-09-27 | The pipe tobacco of tea flower fragrance and tobacco product |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103478889B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110487924B (en) * | 2019-07-31 | 2022-04-01 | 上海烟草集团有限责任公司 | Method for detecting cigarette perfuming uniformity based on additional marker |
| CN111449274B (en) * | 2020-04-09 | 2022-02-15 | 福建中烟工业有限责任公司 | Ginseng extract and preparation method and application thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5031646A (en) * | 1990-01-16 | 1991-07-16 | R. J. Reynolds Tobacco Company | Cigarette |
| CN1321735A (en) * | 2001-05-24 | 2001-11-14 | 南京农业大学 | Method for extracting onion oil |
| CN101108842A (en) * | 2006-07-18 | 2008-01-23 | 扬州大学 | Process technique for extracting tea polyphenol from tree plant flower |
| CN103215138A (en) * | 2013-05-10 | 2013-07-24 | 红塔烟草(集团)有限责任公司 | Additive for improving quality of cut stem, as well as preparation method, device and application thereof |
| CN103251532A (en) * | 2013-05-09 | 2013-08-21 | 浙江大学 | Tea flower skin cream containing tea flower |
-
2013
- 2013-09-27 CN CN201310446699.XA patent/CN103478889B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5031646A (en) * | 1990-01-16 | 1991-07-16 | R. J. Reynolds Tobacco Company | Cigarette |
| CN1321735A (en) * | 2001-05-24 | 2001-11-14 | 南京农业大学 | Method for extracting onion oil |
| CN101108842A (en) * | 2006-07-18 | 2008-01-23 | 扬州大学 | Process technique for extracting tea polyphenol from tree plant flower |
| CN103251532A (en) * | 2013-05-09 | 2013-08-21 | 浙江大学 | Tea flower skin cream containing tea flower |
| CN103215138A (en) * | 2013-05-10 | 2013-07-24 | 红塔烟草(集团)有限责任公司 | Additive for improving quality of cut stem, as well as preparation method, device and application thereof |
Non-Patent Citations (3)
| Title |
|---|
| 响应面法优化生姜精油超高压提取工艺的研究;纵伟等;《中国调味品》;20080831;第56-57页的第1.2.1、3节，第55页的右栏 * |
| 茶树花精油的亚临界水提工艺及在卷烟中的应用研究;白晓莉等;《食品工业》;20130630;第120、121页的第1.1-1.3节，第2.6节 * |
| 茶树花香气成分研究及其香精的制备;顾亚萍等;《食品研究与开发》;20080131;第187页右栏1.2.1和1.2.2 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103478889A (en) | 2014-01-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103478894B (en) | There is the camellia extract composition of pungent note and the application in cigarette thereof | |
| CN103468410B (en) | Tea flower extract composition and its use in cigarette | |
| CN103484248B (en) | Tea flower essence with fresh and sweet characteristics, and application of essence in cigarettes | |
| CN103497837B (en) | A kind of essential oil of the flower of Camellia sinensis, its preparation method and the application in cigarette thereof | |
| CN103525558B (en) | Tea flower essence with fruity flavor characteristic and application thereof to cigarettes | |
| CN101485490B (en) | Preparation method of additive agent capable of causing flue-cured tobacco to have fragrance of oolong tea, flavoring as well as application in flue-cured tobacco | |
| CN103478885B (en) | A kind of reconstituted tobacoo containing tea flower extract and preparation method thereof | |
| CN106221915B (en) | Preparation method of perfume, perfume and application thereof | |
| CN106190572A (en) | A kind of prepare the method for spice, spice and application thereof | |
| CN110205200B (en) | Myrtle-flavored essence and myrtle-flavored electronic cigarette liquid and preparation method thereof | |
| CN103497836B (en) | A kind of Tea flower essence, its preparation method and the application in cigarette thereof | |
| CN101444332B (en) | Health care blended type cigarette | |
| CN103510425A (en) | Tea flower fragrance combination and lined paper coated with same | |
| CN111418892A (en) | Cigarette filter stick additive and application thereof | |
| CN112457914A (en) | Spicy base for improving smoking comfort of heated cigarettes and application thereof | |
| CN103478889B (en) | The pipe tobacco of tea flower fragrance and tobacco product | |
| CN103478904B (en) | The tobacco auxiliary material of tea flower fragrance and tobacco product | |
| KR20090132127A (en) | Green tea of tangerine, rape or camellia having good taste and the method for preparing thereof | |
| CN110358630B (en) | Spice with fresh and spicy flavor for cigarettes, preparation method of spice and application of spice in cigarettes | |
| KR20170022426A (en) | Mixed tea using platycodon and manufacturing method of the leached tea | |
| CN107853420A (en) | A kind of white tea preparation method containing white orchid | |
| CN107227205A (en) | A kind of preparation method of okra essential oil | |
| CN112056613A (en) | Preparation method of cigarette filter stick with gardenia fragrance | |
| CN110804497A (en) | Preparation method of saffron extract for tobacco bead blasting | |
| CN110720658B (en) | Preparation method of acacia flower extract for tobacco bead blasting |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |