CN109924535B - Preparation method and application of momordica grosvenori flowers in fruit burning and spraying type hookah - Google Patents
Preparation method and application of momordica grosvenori flowers in fruit burning and spraying type hookah Download PDFInfo
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Abstract
The invention discloses a preparation method and application of momordica grosvenori flowers in fruit burning and spraying type hookah, which comprises the following steps: (a) the method comprises the following steps of (a) crushing dried fruits of momordica grosvenori medicinal materials → loading sample → adding tap water → standing, soaking for 24-48 h, (b) adopting a water bath heating extraction method (extracting for 1 time) → leaching solution → 400-mesh filter cloth for filtering, sealing and standing to obtain filtrate A, (c) adding 50% ethanol solution → acid precipitation for extraction, and fully stirring → filtrate; (d) concentrating the filtrate A → 55-60 ℃ under reduced pressure for 3h → obtaining a concentrated solution A (relative density rho =1.2918), (e) adding the concentrated solution A → raw material 20% propylene glycol 60g → fully shaking → obtaining the concentrated solution A, wherein the density is determined as follows: rho =1.1286, and (f) obtaining a concentrated solution A which is a natural plant momordica grosvenori extract used for preparing the arabian hookah. The method can effectively improve the aroma quality, aroma quantity, fineness and/or sweet feeling of the hookah, reduce the irritation and/or scorched gas of the flower and fruit burning and sprinkling type Arab hookah, and improve the sensory quality of the hookah.
Description
Technical Field
The invention relates to the field of natural plant resource development and utilization and preparation processes of flower and fruit burning products, in particular to a preparation method and application of momordica grosvenori flowers in flower and fruit burning products.
Background
The natural plant momordica grosvenori contains fragrant substances with volatile fragrant components, and the fragrance of the natural plant momordica grosvenori is pleasant and relaxed. With the gradual change of the consumption concept of people, the consumption of the chemical synthetic spice essence is gradually reduced in consideration of the safety and the environmental problems of the chemical synthetic substance, and the application of the natural plant spice is increasingly wide. The natural plant perfume is increasingly popular with people due to the characteristics of green, safety, environmental protection and the like, and the demand of the natural plant perfume is continuously increased every year. China has abundant natural plant spice resources, but due to the laggard technical aspects such as extraction and preparation processes, only a small amount of natural plant spice resources are researched, developed and utilized. The method not only causes the shortage of natural plant natural spices in the market of China, but also seriously wastes precious resources. The flower and fruit burning and spraying products which are applied to the arabian hookah entertainment consumer products at present are mainly made of tobacco and essence, so that natural spices such as plant momordica grosvenori flowers and the like can replace tobacco leaves and synthetic essence. However, the entertainment consumer products such as flower and fruit burning and spraying products are still blank in China, so that great market economic benefits exist, and the trend of future research, development and utilization of the products is also realized.
Flowers and extracts of natural plant momordica grosvenori and other spices are used as raw materials of a flower and fruit burning and sucking product for entertainment consumption products, and the aim is to add fragrance and flavor to the flower and fruit burning and sucking product to generate a good tobacco fragrance effect.
The natural plant is dried flower and extract of fructus Siraitiae Grosvenorii, and Hainan extract, and is obtained by continuously screening flowers of various plants with special fragrance. The natural plant fructus momordicae dried flower and the extract have the effects of clearing heat and detoxicating, eliminating phlegm and relieving cough, nourishing sound and moistening lung, removing halitosis, treating pharyngitis, tonsillitis, color spots, liver spots and pimples, and can emit aromatic fragrance, thereby being the unique quality. However, most researches on plant momordica grosvenori flowers are focused on clinical medicine and food at present, and the preparation process of raw materials of entertainment consumer products, namely flower and fruit burning and sucking products and products in application of the flower and fruit burning and sucking products are not reported.
In conclusion, the invention designs a preparation method and application of momordica grosvenori flowers in flower and fruit burning and sprinkling type hookah.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide a preparation method and application of momordica grosvenori flowers in flower and fruit burning and sprinkling type hookah, which can effectively improve the aroma quality, aroma quantity, fineness and/or sweet feeling of the hookah, reduce the irritation and/or scorched gas of flower and fruit burning and sprinkling type Arabic hookah, and improve the sensory quality of the hookah.
In order to achieve the purpose, the invention is realized by the following technical scheme: the preparation method of the momordica grosvenori flowers in the tobacco smoking products comprises the following steps:
1. firstly, soaking 35% of dried momordica grosvenori flower and 1.7% of edible essence in tap water at normal temperature for 24-48 hours, filtering with 400-mesh filter cloth according to the solid-liquid mass ratio of 1:10, and sealing and standing to obtain a softened momordica grosvenori flower raw material;
2. then adding propylene glycol into the raw material of the momordica grosvenori flower, stirring for 1 hour fully and continuously, sealing and standing for fermentation;
3. adding 30% of fresh jam (banana and candied date, and different fresh fruits can be added according to different tastes) into the raw material of the momordica grosvenori flowers which are well stood in the step 2;
4. mixing flos Momordicae raw material and fresh fruit jam, and sequentially adding Mel 10%, glycerol 5%, glucose 5%, potassium sorbate 0.3%, fructus Siraitiae Grosvenorii and Hainan extract 8%; finally, preparing the momordica grosvenori flower configured fermented product.
The propylene glycol and the edible essence are both edible grade.
5 times of propylene glycol is added into the momordica grosvenori flower raw material.
The fresh fruit jam is prepared by mixing and stirring banana and candied date according to the ratio of 1:1, and other fresh fruits can also be added.
The application of the fermentation product prepared from the momordica grosvenori flowers in preparing the flower and fruit burning and spraying type Arabic hookah is provided.
The preparation method is used for preparing the flower and fruit burning and sucking product by using the main raw materials of the natural plant fructus momordicae extract, the fructus momordicae flowers and the Hainan south Chinese herb extract, and the obtained product is used as an entertainment consumption product for the flower and fruit burning and sucking, so that the healthy ecology and the fragrance quality can be effectively improved, the plant resources are fully utilized, and the entertainment consumption of the flower and fruit burning and sucking product is met.
The invention has the beneficial effects that:
1. the preparation process method of the grosvenor momordica flower configured fermented product has tobacco aroma components and can replace the traditional tobacco leaves;
2. the fermentation product prepared from the momordica grosvenori flowers has good characteristic aroma, can effectively improve aroma quality, aroma quantity, fineness and/or sweetness of the flower and fruit burning and sprinkling type Arabic hookah, reduces irritation and/or scorched gas brought by replacing tobacco leaves, and improves the sensory quality of the hookah;
3. the momordica grosvenori flower fermentation product has a good improvement effect on discomfort of the throat and synthetic essence brought by water absorption smoke;
4. the fermentation product prepared from the momordica grosvenori flowers is applied to the arabian hookah which is a burning and spraying type flower and fruit, and the obtained hookah has better sensory quality during smoking;
5. the preparation process of the fermentation product prepared from the momordica grosvenori flowers is simple, convenient and practical, easy to operate, low in cost and capable of realizing large-scale production;
6. the momordica grosvenori flower prepared by the method disclosed by the invention is a fermentation product, and can be applied to preparation of natural plant spice in the flower and fruit burning and sprinkling type Arabic hookah in the future, so that the method has a good research and development prospect, and the momordica grosvenori flower can be well developed and utilized, so that better economic benefit is realized.
Drawings
The invention is described in detail below with reference to the drawings and the detailed description;
fig. 1 is a report of the examination of the hookah product made of the momordica grosvenori extract of example 1 of the present invention.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.
Example 1: the extraction and preparation process method of the momordica grosvenori and south-of-the-sea medicine extract comprises the following steps:
1) crushing momordica grosvenori and south-of-the-sea medicinal materials, soaking for 24-48 at normal temperature by using 2500 volume of water as a solvent according to the solid-liquid mass ratio of 1:10, extracting for 1 time by adopting a water bath heating extraction method, filtering by using 400-mesh filter cloth, sealing and standing to obtain filtrate;
(2) concentrating 2000ml of filtrate under reduced pressure (RE-6000A rotary evaporator, Shanghai Yangrong Biochemical apparatus factory), concentrating under reduced pressure until the vacuum degree P is 0.095Mpa, the temperature is 55 ℃, the rotation speed is 48rpm/min, collecting the residue, and measuring the relative density rho which is 1.2918 to obtain concentrated solution A;
(3) adding 65% ethanol solution into the filtrate, stirring for 3 hr, performing acid precipitation, sealing, and standing;
(4) adding 60g of 15% propylene glycol of the raw material into the concentrated solution A, and fully shaking up to obtain a concentrated solution with density rho of 1.2086; sealing to obtain the concentrated extract which is the extract of Momordica grosvenori Swingle and south Hainan herbs in example 1.
Example 2:
the momordica grosvenori and southern Hainan medicinal extract B of example 2 is obtained by soaking momordica grosvenori raw materials into essence and spice for softening, and performing the same steps for preparing the extract as those of example 1 in the rest steps.
Example 3:
when preparing the momordica grosvenori and southern Hainan medicinal extract, 2500g of water is used as a solvent, water bath heating extraction is directly carried out without soaking, acid precipitation and stirring extraction are carried out without adding 50% ethanol solution, and the rest steps for preparing the momordica grosvenori and southern Hainan medicinal extract are the same as the step 1, so that the momordica grosvenori and southern Hainan medicinal extract C in the example 3 is obtained.
Example 4:
preparing fructus Siraitiae Grosvenorii and Hainan medicinal extract with 50% ethanol solution by water bath heating reflux extraction method;
weighing the momordica grosvenori and southern Hainan medicinal material pieces with the same weight as that in the example 1;
adding 2500ml of 50% ethanol solution into the crushed pieces of fructus Siraitiae Grosvenorii and south medicinal materials, heating and reflux-extracting at 80 deg.C for 3 hr for 1 time, filtering with 400 mesh filter cloth, sealing and standing to obtain filtrate;
concentrating 2000ml of filtrate under reduced pressure (RE-6000A rotary evaporator, Shanghai Yangrong Biochemical apparatus factory), wherein the vacuum degree P of the reduced pressure concentration is 0.095Mpa, the temperature is 60 ℃, the rotating speed is 42rpm/min, concentrating until the residue is 500ml, collecting the residue, and measuring the relative density rho which is 1.2950 to obtain a concentrated solution D;
adding 60g of 20% propylene glycol of the raw material into the concentrated solution D, and fully shaking up to obtain a concentrated solution with density rho of 1.1320; sealing to obtain the concentrated extract which is the mixed extract D of the momordica grosvenori and the southern Hainan medicine of the comparative example 1.
Analysis and detection 1: sensory quality evaluation
The momordica grosvenori and the southern Hainan herb extracts of the examples 1 to 3 and 4 are respectively added into the momordica grosvenori flower water tobacco in equal amount, the mixture is fully stirred, and the obtained water tobacco fruit fuel samples are numbered as A to D in sequence. Sensory quality evaluation was performed on the hookah samples a to D according to the sample evaluation rule of the sensory evaluation method of reconstituted tobacco (paper-making process) of standard YC/T498-2014, and the results are shown in table 1.
TABLE 1
TABLE 2
TABLE 3
Table 3 hookah sample sensory quality score table;
as can be seen from Table 3, the sensory score of the hookah D is 70.5 points, and the sensory scores of the cigarettes A to C are 72.0 to 77.8 points;
specifically, the aroma quality and the aroma quantity of the cigarettes A-C are improved, and the irritation is reduced;
the sweet feeling and the fineness of the cigarettes A to C are further improved, and the scorched gas of the cigarettes A to B is further reduced;
wherein, the water tobacco has the highest score, the fragrance quantity, the fragrance quality, the fragrance quantity, the pressure removal of miscellaneous gas, the fineness and the sweet feeling are obviously improved, and the irritation and the scorched gas are obviously reduced.
As described above, the momordica grosvenori and southern hainan herb mixed extract of examples 1 to 3 can be used for the hookah, so that the aroma quality, the aroma quantity, the fineness and/or the sweet feeling of the hookah can be effectively improved, the irritation and/or the scorched smell of the hookah are reduced, and the sensory quality of the hookah is improved. Among them, the sample of the mixed extract a of momordica grosvenori and hainan drug of example 1 had the best sensory quality.
Example 5: analyzing chemical components of the mixed extract of the momordica grosvenori and the southern Hainan medicine;
1 gas chromatography mass spectrometry conditions, as shown in tables 1 and 2;
a chromatographic column: HP-5MS, (30m 0.25mm 0.25 μm); carrier gas: high purity helium gas; sample inlet temperature: 280 ℃; he flow rate: 1.0 mL/min; electron energy: 70 eV; ion source temperature: 230 ℃; quadrupole temperature: 150 ℃; solvent retardation: 1 min; transmission line temperature: 280 ℃; temperature programming: keeping the temperature at 80 ℃ for 1min, increasing the temperature from 80 ℃ to 200 ℃ at the speed of 5 ℃/min, increasing the temperature from 200 ℃ to 280 ℃ at the speed of 10 ℃/min, keeping the temperature for 1min, and adopting a full-scan mode;
2 preparing test solution
Accurately weighing 5.0g of the mixed extract of the momordica grosvenori and the southern Hainan medicine prepared in the example 1 into a 50mL volumetric flask, adding absolute ethyl alcohol to a constant volume, oscillating at a constant speed for 15min, standing, taking supernatant, filtering with a 0.45 mu m microporous membrane to obtain a preparation sample solution;
3 results
3.1 results
The water bath heating extraction method, the alcohol extraction method, the extraction under different conditions of soaking and acid precipitation have influence on the extraction efficiency and aroma components in the mixed extract of the momordica grosvenori and the Hainan medicinal herb.
The content of chemical components of the mixed extract of the momordica grosvenori and the south China medicinal herbs is determined by gas chromatography-mass spectrometry (GC-MS) by adopting water bath heating extraction. The main aroma components of furfuryl alcohol, phenylacetaldehyde, furanone, 3, 5-dihydroxy-6-methyl-2, 3-dihydro-4H-pyran-4-one, benzoic acid and dihydrocarveol in the mixed extract of Momordica grosvenori and Hainan drug prepared in example 1 are 0.151%, 0.268%, 0.121%, 1.095%, 1.247% and 0.270%, respectively, as shown in FIG. 1.
Respectively measuring and analyzing the chemical components of the mixed extract B, C, D of fructus Siraitiae Grosvenorii and Hainan medicinal materials by the same method;
example 2: the contents of aroma components such as furfuryl alcohol, phenylacetaldehyde, furanone, 3, 5-dihydroxy-6-methyl-2, 3-dihydro-4H-pyran-4-one, benzoic acid and dihydrocarveol in the prepared mixed extract B of the momordica grosvenori and the Hainan drug are respectively 0.00%, 0.063%, 0.00%, 0.239%, 0.124% and 0.203%;
example 3: the contents of aroma components such as furfuryl alcohol, phenylacetaldehyde, furanone, 3, 5-dihydroxy-6-methyl-2, 3-dihydro-4H-pyran-4-one, benzoic acid, dihydrocarveol and palmitic acid in the prepared mixed extract C of fructus Siraitiae Grosvenorii and Hainan medicine are respectively 0.00%, 0.149%, 0.00%, 0.459%, 0.745%, 0.327% and 1.678%;
example 4: the prepared mixed extract D of fructus Siraitiae Grosvenorii and Hainan medicine contains fragrant components such as furfuryl alcohol, phenylacetaldehyde, furanone, 3, 5-dihydroxy-6-methyl-2, 3-dihydro-4H-pyran-4-one, benzoic acid, and dihydrocarveol 0.006%, 0.013%, 0.001%, 0.016%, 0.025%, and 0.002%;
3.2 results
Example 1 product inspection report of mixed extract a of luo han guo and hainan southern medicine, as shown in table 4;
table 4 table of mass contents and proportions of main aroma components of example 1 and comparative example 1, as shown in the following table:
table 5 table showing the mass contents and proportions of the main aroma components of example 2 and example 1, as follows:
table 6 table showing the mass contents and proportions of the main aroma components of example 3 and example 1, as follows:
table 7 sensory quality evaluation tables for tobacco samples of examples 1 to 3 and comparative example 1:
(Note: A to C represent examples 1 to 3, respectively, and D represents comparative example 1)
Evaluating the characteristic aroma, aroma quality, aroma quantity, fineness and/or sweetness of the comparative example 1 compared with the examples 1-3 by a water bath heating reflux extraction preparation process technology, reducing the irritation and/or scorched smell of the cigarette, and improving the sensory quality of the water smoke (as shown in Table 7);
the 3 momordica grosvenori flowers, momordica grosvenori extracts and southern Hainan herb mixed extracts prepared in comparative example 1 and examples 2 and 3 under different process conditions are evaluated through water bath heating extraction and acid precipitation extraction preparation process technologies, and analysis results show that the momordica grosvenori and southern Hainan herb mixed extract prepared in example 1 has good characteristic aroma compared with other examples 2 and 3, can further improve the aroma quality, aroma quantity, fineness and/or sweet feeling of tobacco, and has good extraction efficiency of tobacco aroma components. The preparation process method of the momordica grosvenori and southern Hainan medicine mixed extract is simple, convenient and practical, easy to operate, low in cost and more suitable for industrial production, and has good research and development prospects when being applied to preparation of natural plant flavors for cigarettes in the future.
The product, namely the fruit burning and absorbing water spraying cigarette, obtained by the preparation process technology and the composition formula of the invention is known by the inspection report of product quality supervision and inspection institute in Hainan province, and all the inspected project indexes meet the requirements (as shown in figure 1).
The foregoing shows and describes the general principles and broad features of the present invention and advantages thereof. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (5)
1. The preparation method of the momordica grosvenori flowers in the fruit burning and spraying type hookah is characterized by comprising the following steps of:
(1) firstly, soaking 35% of dried momordica grosvenori flower and 1.7% of edible essence in tap water at normal temperature for 24-48 hours, filtering with 400-mesh filter cloth according to the solid-liquid mass ratio of 1:10, and sealing and standing to obtain a softened momordica grosvenori flower raw material;
(2) then adding propylene glycol into the raw material of the momordica grosvenori flower, stirring for 1 hour fully and continuously, sealing and standing for fermentation;
(3) putting 30% of fresh fruit jam into the raw material of the momordica grosvenori flowers which are well stood in the step (2);
(4) after the momordica grosvenori flower raw material and the fresh fruit jam are prepared, respectively adding 10% of honey, 5% of glycerol, 5% of glucose, 0.3% of potassium sorbate and 8% of momordica grosvenori and southern Hainan medicinal extract; finally preparing the momordica grosvenori flower configured fermented product, wherein: the extraction and preparation process method of the momordica grosvenori and south-of-the-sea medicine extract comprises the following steps:
(S1) smashing momordica grosvenori and south-of-the-sea medicinal materials, soaking for 24-48 at normal temperature by using 2500ml of water as a solvent according to the solid-liquid mass ratio of 1:10, extracting for 1 time by adopting a water-bath heating extraction method, filtering by using 400-mesh filter cloth, sealing and standing to obtain a filtrate;
(S2) concentrating 2000ml of filtrate under reduced pressure until the vacuum degree P of the reduced pressure concentration is 0.095Mpa, the temperature is 55 ℃, the rotating speed is 48rpm/min, concentrating until the residue is 500ml, collecting the residue, and measuring the relative density rho to be 1.2918 to obtain a concentrated solution A;
(S3) adding 65% ethanol solution into the filtrate, stirring for 3h, performing acid precipitation extraction, sealing and standing;
(S4) adding 60g of 15% propylene glycol of the raw material into the concentrated solution A, and fully shaking up to obtain a concentrated solution with density rho of 1.2086; sealing to obtain the concentrated extract, which is the extract of fructus Siraitiae Grosvenorii and Hainan medicinal materials.
2. The method for preparing fructus momordicae flower in flower and fruit burning and sprinkling type hookah according to claim 1, wherein said propylene glycol, flavoring essence and flavor are both food grade.
3. The method for preparing fructus momordicae flower in fruit burning smoking products type hookah according to claim 1, wherein 5 times of propylene glycol is added into the fructus momordicae flower raw material.
4. The method for preparing fructus momordicae flower in fruit smoking and sprinkling type hookah according to claim 1, wherein the fresh fruit jam is prepared by mixing and mincing banana and candied date in a ratio of 1: 1.
5. The method for preparing the momordica grosvenori flower in the flower and fruit burning and sprinkling type hookah according to the claim 1, wherein the momordica grosvenori flower is prepared with a fermented product and is applied to preparing the flower and fruit burning and sprinkling type arabic hookah.
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