CN106590936B - Preparation method and application of tobacco flavor - Google Patents
Preparation method and application of tobacco flavor Download PDFInfo
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- CN106590936B CN106590936B CN201710005270.5A CN201710005270A CN106590936B CN 106590936 B CN106590936 B CN 106590936B CN 201710005270 A CN201710005270 A CN 201710005270A CN 106590936 B CN106590936 B CN 106590936B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a preparation method and application of a tobacco flavor. Mixing aged tobacco leaves with other substances which can generate fermentation fragrance, adding biological enzyme into the mixture for synchronous fermentation, and extracting the synchronous fermentation product by using a certain solvent, wherein the extracted fermentation product can be used as a tobacco shred additive which is added in the tobacco shred flavoring and feeding process or a filter additive which is added in the filter processing process. The method is characterized in that the method adopts a synchronous fermentation method to carry out the co-fermentation of the tobacco leaves and other natural plants, and utilizes the interaction in the fermentation process to lead the fermentation product to integrate the original flavor and the exogenous flavor characteristics of the tobacco leaves, generate new fermentation characteristic flavor and expand the application range of the tobacco leaf fermentation technology. The method is simple and feasible in treatment, and related equipment is the existing equipment in the market and is low in price. The obtained additive can effectively improve the sensory quality of cigarettes after being added into the cigarettes.
Description
Technical Field
The invention relates to the technical field of cigarettes, in particular to a preparation method and application of a tobacco flavor.
Background
The tobacco leaves are modulated and naturally fermented, and although the smoking quality is greatly improved, the fragrance has some defects. In order to keep the relative stability of the quality of cigarette products, the flavor defect is overcome by adding essence and spice substances for smoking while reasonably designing a leaf group formula, namely, the flavoring is also an important measure for improving the quality of the products. The cigarette flavoring can supplement elegant fragrance, endow the cigarette with unique characteristic fragrance, and coordinate fragrance, so that different types and grades of tobacco fragrance are combined and coordinated with each other organically. Covering up or diluting miscellaneous qi. The cigarette can also increase the sweetness, improve the smoking taste, lighten the irritation of smoke and weaken some miscellaneous gas by adding the fragrance, thereby improving the quality.
With the rapid development of the tobacco industry in China, the formation of large brands, the requirement of reducing tar and harm of cigarettes and the further improvement of tobacco products, the demand of essence and spice for high-quality cigarettes is increasing day by day. Generally, the perfume is classified into two categories, i.e., natural perfume and synthetic perfume, according to the source of the perfume, 3000 kinds of natural perfume are known, 7000 kinds of synthetic perfume are more known, and new varieties are still emerging. Among them, the flavors developed from the original sources of tobacco leaves have been considered as a class of products having the best harmony with smoke.
The method has the advantages that related research and exploration are carried out on the tobacco leaves aged by the biological enzyme in the early period, and the enzyme can rapidly ferment and age some components in the tobacco leaves, so that the Maillard reaction is accelerated, and the smoking quality of the tobacco leaves is greatly improved in a short time. In addition, methods for deeply fermenting aged tobacco leaves and extracting effective components of the aged tobacco leaves are also provided, so that substances which are generated in the fermentation process and have adverse effects on smoke are further reduced; however, most of the process is still limited to the fermentation of the tobacco leaves, no exogenous flavor components are introduced, and the flavor types of the tobacco leaf fermentation flavors are limited to a great extent.
Disclosure of Invention
The invention aims to provide a preparation method and application of a tobacco flavor, wherein aged tobacco leaves are mixed with other substances which can generate fermentation fragrance, biological enzyme is added into the tobacco leaves for synchronous fermentation, a certain solvent is adopted to extract a synchronous fermentation product, and the extracted fermentation product can be used as a tobacco shred additive which is added in the tobacco shred flavoring and feeding process or a filter tip additive which is added in the filter tip processing process.
The invention is realized by the following technical scheme: a preparation method of a tobacco flavor comprises the following steps:
(1) putting the aged tobacco leaves and other substances capable of generating fermentation fragrance into a closed reactor together, wherein the mass ratio of the tobacco leaves to the other substances capable of generating fermentation fragrance is 10:1-1:1, adding biological enzyme accounting for 0.01-0.05% of the mass of the tobacco leaves, fermenting for 10-60 days under the conditions that the temperature is 40-65 ℃ and the humidity is 60-95%, synchronously performing chemical component fermentation on the tobacco leaves and the co-fermentation substances, synchronously generating fermentation substances with characteristic fragrance through the interaction of the components, and taking out the fermentation substances, wherein the fermentation substances comprise residues and generated other substances;
(2) extracting the fermented substance obtained in step (1) with a solvent, wherein the volume of the solvent is 1-1.2 times of the volume of the tobacco leaves, and removing insoluble components in the residue to obtain a solution extract;
(3) evaporating the solution extract obtained in the step (2) to dryness to obtain an extract, adding glycerol triacetate with the same volume as the solvent in the step (2) to dissolve again, filtering after the soluble substance of the glycerol triacetate in the extract is fully dissolved, and separating filter residue from the solution to obtain the tobacco flavor solution and the tobacco flavor filter residue.
Diluting or concentrating the tobacco flavor part to a suitable concentration, and adding into the filter tip in the filter tip processing process, wherein the addition amount is 0.2-1 μ g of tobacco flavor solid in each filter tip; the part of the filter residue tobacco flavor is used as a tobacco shred additive and is added in the tobacco shred flavoring and feeding process, and the filter residue tobacco flavor is added into the tobacco shred feed liquid in an amount which is 0.1 to 5 percent of the mass of the tobacco shred feed liquid.
The tobacco shred feed liquid refers to a mixed formula solution of spices, sugar materials and other components added in the cigarette production process, and the feed liquid formulas of cigarettes of different brands are different, and the cigarette shred feed liquid is the prior art.
The substance capable of generating the fermentation fragrance in the step (1) is one or more of natural plant materials such as petals, lotus leaves, bamboo fragments, wood, aniseed, fruits and the like.
The added biological enzyme in the step (1) is one or more of saccharifying enzyme, pectinase, amylase, cellulase, aspergillus, protease, yeast powder and other biological enzymes.
The extraction solvent adopted in the step (2) is one of water, ethanol, ethyl acetate, n-hexane, butane and petroleum ether.
The invention has the advantages and effects that: the method is characterized in that the method adopts a synchronous fermentation method to carry out the co-fermentation of the tobacco leaves and other natural plants, and utilizes the interaction in the fermentation process to lead the fermentation product to integrate the original flavor and the exogenous flavor characteristics of the tobacco leaves, generate new fermentation characteristic flavor and expand the application range of the tobacco leaf fermentation technology. The method is simple and feasible in treatment, and related equipment is the existing equipment in the market and is low in price. The obtained additive can effectively improve the sensory quality of the cigarettes after being added into the cigarettes, and the sensory evaluation score can be improved by 1-1.5 points.
Detailed Description
It will be appreciated by those skilled in the art that the following examples are illustrative of the invention only and should not be taken as limiting the scope of the invention. The examples do not specify particular techniques or conditions, and are performed according to the techniques or conditions described in the literature in the art or according to the product specifications. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available by purchase.
The invention is further illustrated by the following examples, but not limited to the materials and conditions illustrated.
Example 1
(1) Placing tobacco leaves and rose petals in a closed reactor according to the mass ratio of 1:1, adding saccharifying enzyme with the total mass fraction of 0.01%, fermenting for 60 days at the temperature of 60 ℃ and the relative humidity of 80%, synchronously performing chemical component fermentation on the tobacco leaves and the rose petals, generating a fermented substance with characteristic flower fragrance through the interaction of the components, and taking out the fermented substance, wherein the fermented substance comprises residues and other generated substances;
(2) putting the fermented substance obtained in the step (1) into water for extraction, wherein the volume of the water is the same as that of the tobacco leaves, and fully dissolving the soluble substances into the water under vigorous stirring or shaking to obtain an aqueous solution extract;
(3) and (3) evaporating the aqueous solution extract obtained in the step (2) to dryness to obtain an extract, adding glycerol triacetate with the same volume as that of the water in the step (2) to dissolve again, filtering after the soluble matter of the glycerol triacetate in the extract is fully dissolved, and separating filter residue from the solution to obtain solution tobacco flavor and filter residue tobacco flavor.
(4) After the tobacco flavor solution is concentrated to the dry matter mass content of 0.1 percent, the tobacco flavor solution is sprayed on filter tow in the filter processing process, and the adding amount is 0.2 mu g of tobacco flavor solid in each filter rod. And rolling the prepared filter stick into a cigarette. Compared with the cigarette without the additive, the cigarette product has better smoke harmony, outstanding flower fragrance and obviously improved cigarette quality.
(5) Adding tobacco flavor with filter residue into tobacco shred feed liquid with the mass fraction of 0.1%, and adding into tobacco shred in production process to obtain cigarette. Compared with the cigarette without the additive, the cigarette product has better smoke harmony, outstanding flower fragrance and obviously improved cigarette quality.
Example 2
(1) Placing tobacco leaves and lotus leaves in a closed reactor according to the mass ratio of 2:1, adding aspergillus and amylase (mass ratio of 1: 1) with the total mass fraction of 0.05%, fermenting for 10 days at the temperature of 55 ℃ and the relative humidity of 90%, synchronously performing chemical component fermentation on the tobacco leaves and the lotus leaves, generating a fermented substance with the characteristic faint scent of the lotus leaves through the interaction of the components, taking out the fermented substance, wherein the fermented substance comprises residues and generated other substances;
(2) putting the fermented substance obtained in the step (1) into ethanol for extraction, wherein the volume of the ethanol is 1.2 times of that of the tobacco leaves, and fully dissolving the soluble substances into the ethanol under vigorous stirring or shaking to obtain an ethanol extract solution;
(3) evaporating the ethanol extract solution obtained in the step (2) to dryness to obtain an extract, adding glycerol triacetate with the same volume as the ethanol in the step (2) to dissolve again, filtering after fully dissolving the soluble substance of the glycerol triacetate in the extract, and separating the filter residue from the solution to obtain a tobacco flavor solution and a tobacco flavor filter residue.
(4) After the tobacco flavor solution is concentrated to the dry matter mass content of 2 percent, the tobacco flavor solution is sprayed on filter tow in the filter processing process, and the adding amount is 1 mu g of tobacco flavor solid in each filter rod. And rolling the prepared filter stick into a cigarette. Compared with the cigarette without the additive, the cigarette product has better smoke harmony, the fresh scent of the lotus leaves is prominent, and the cigarette quality is obviously improved. (5) Adding the filter residue tobacco flavor into the tobacco shred feed liquid according to the mass fraction of 5% of the tobacco shred feed liquid, and adding the tobacco shred flavor into tobacco shreds in the production process to prepare the cigarette. Compared with the cigarette without the additive, the cigarette product has better smoke harmony, the fresh scent of the lotus leaves is prominent, and the cigarette quality is obviously improved.
Example 3
(1) Placing tobacco leaves and bamboo fragments in a closed reactor according to the mass ratio of 1:1, adding cellulase and yeast powder (the mass ratio of 3: 1) with the mass fraction of the tobacco leaves being 0.03%, fermenting for 30 days at 65 ℃ and the relative humidity of 70%, synchronously performing chemical component fermentation on the tobacco leaves and the bamboo fragments, generating a fermented substance with the characteristic bamboo fresh scent through the interaction of the components, taking out the fermented substance, wherein the fermented substance comprises residues and other generated substances;
(2) putting the fermented substance obtained in the step (1) into ethyl acetate for extraction, wherein the volume of the ethyl acetate is 1.1 times of that of the tobacco leaves, and fully dissolving soluble substances into the ethyl acetate under the condition of violent stirring or shaking; obtaining ethyl acetate extract solution;
(3) evaporating the ethyl acetate extract solution obtained in the step (2) to dryness to obtain an extract, adding glycerol triacetate with the volume same as that of the ethyl acetate solvent in the step (2) to dissolve again, filtering after fully dissolving the soluble substances of the glycerol triacetate in the extract, and separating filter residue from the solution to obtain solution tobacco flavor and filter residue tobacco flavor.
(4) After the tobacco flavor solution is concentrated to the dry matter mass content of 1 percent, the tobacco flavor solution is sprayed on filter tow in the filter processing process, and the adding amount is 0.5 mu g of tobacco flavor solid in each filter rod. And rolling the prepared filter stick into a cigarette. Compared with the cigarette without the additive, the cigarette product has better smoke harmony, prominent bamboo fresh flavor and obviously improved cigarette quality.
(5) Adding the tobacco flavor with filter residue into the tobacco shred feed liquid according to the mass fraction of 1%, and adding into tobacco shred in the production process to prepare cigarette. Compared with the cigarette without the additive, the cigarette product has better smoke harmony, prominent bamboo fresh flavor and obviously improved cigarette quality.
Example 4
(1) Placing tobacco leaves and agarwood fragments in a closed reactor according to the mass ratio of 5:1, adding cellulase and protease (the mass ratio is 3: 1) with the mass fraction of 0.04% of the tobacco leaves, fermenting for 50 days under the conditions of 60 ℃ and 95% of relative humidity, synchronously performing chemical component fermentation on the tobacco leaves and the agarwood fragments, generating a fermented substance with characteristic agilawood fragrance through the interaction of the components, taking out the fermented substance, wherein the fermented substance comprises residues and other generated substances;
(2) putting the fermented substance obtained in the step (1) into n-hexane for extraction, wherein the volume of the n-hexane is the same as that of the tobacco leaves, and fully dissolving the soluble substances into the n-hexane under vigorous stirring or shaking to obtain an n-hexane extract solution;
(3) evaporating the n-hexane solution extract obtained in the step (2) to dryness to obtain an extract, adding glycerol triacetate with the same volume as the n-hexane solvent in the step (2) to dissolve again, filtering after fully dissolving the soluble substance of the glycerol triacetate in the extract, and separating filter residue from the solution to obtain a solution tobacco flavor and a filter residue tobacco flavor.
(4) After the tobacco flavor solution is concentrated to the dry matter mass content of 0.8 percent, the tobacco flavor solution is sprayed on filter tow in the filter processing process, and the adding amount is 0.3 mu g of tobacco flavor solid in each filter rod. And rolling the prepared filter stick into a cigarette. Compared with the cigarette without the additive, the cigarette product has better smoke harmony, outstanding agilawood fragrance and obviously improved cigarette quality.
(5) Adding the tobacco flavor with filter residue into the tobacco shred feed liquid according to the mass fraction of 2%, and adding into tobacco shred in the production process to obtain cigarette. Compared with the cigarette without the additive, the cigarette product has better smoke harmony, outstanding agilawood fragrance and obviously improved cigarette quality.
Example 5
(1) Placing tobacco leaves and star anises into a closed reactor according to the mass ratio of 10:1, adding cellulase and aspergillus (the mass ratio is 2: 1) with the mass fraction of 0.04% of the tobacco leaves, fermenting for 20 days under the conditions of 40 ℃ and 80% of relative humidity, fully fermenting chemical components in the tobacco leaves, synchronously fermenting the chemical components in the tobacco leaves and the star anises, generating a fermented substance with characteristic spicy fragrance through the interaction of the components, taking out the fermented substance, wherein the fermented substance comprises residues and other generated substances;
(2) putting the fermented substance obtained in the step (1) into butane for extraction, wherein the volume of the butane is 1.2 times of that of the tobacco leaves, and fully dissolving soluble substances into the butane under the condition of violent stirring or shaking to obtain a butane extract solution;
(3) evaporating the butane extract solution obtained in the step (2) to dryness to obtain an extract, adding glycerol triacetate with the same volume as the butane solvent in the step (2) to dissolve again, filtering after fully dissolving the soluble substance of the glycerol triacetate in the extract, and separating filter residue from the solution to obtain a solution cigarette flavor and a filter residue cigarette flavor.
(4) After the tobacco flavor solution is concentrated to the dry matter mass content of 1.5 percent, the tobacco flavor solution is sprayed on filter tow in the filter processing process, and the adding amount is 0.8 mu g of tobacco flavor solid in each filter rod. And rolling the prepared filter stick into a cigarette. Compared with cigarettes without the additive, the cigarette product has the advantages of better smoke harmony, prominent spicy flavor and obviously improved cigarette quality.
(5) Adding the filter residue tobacco flavor into the tobacco shred feed liquid according to the mass fraction of 3 percent of the tobacco shred feed liquid, and adding the tobacco shred flavor into tobacco shreds in the production process to prepare the cigarette. Compared with cigarettes without the additive, the cigarette product has the advantages of better smoke harmony, prominent spicy flavor and obviously improved cigarette quality.
Example 6
(1) Placing tobacco leaves and oranges into a closed reactor according to the mass ratio of 7:1, adding pectinase and aspergillus (the mass ratio is 2: 1) with the mass fraction of 0.03 percent of the tobacco leaves, fermenting for 50 days at 65 ℃ and the relative humidity of 60 percent to fully ferment chemical components in the tobacco leaves, synchronously fermenting the chemical components in the tobacco leaves and the oranges, generating fermented substances with characteristic fruit fragrance through the interaction of the components, and taking out the fermented substances, wherein the fermented substances comprise residues and other generated substances;
(2) putting the fermented substance obtained in the step (1) into petroleum ether for extraction, wherein the volume of the petroleum ether is 1.2 times of that of the tobacco leaves, and fully dissolving the soluble substances into the petroleum ether under vigorous stirring or shaking to obtain a petroleum ether extract solution;
(3) evaporating the petroleum ether extract solution obtained in the step (2) to dryness to obtain an extract, adding glycerol triacetate with the same volume as the petroleum ether solvent in the step (2) to dissolve again, filtering after fully dissolving the soluble substances of the glycerol triacetate in the extract, and separating filter residue from the solution to obtain solution tobacco flavor and filter residue tobacco flavor.
(4) After the tobacco flavor solution is concentrated to the dry matter mass content of 1.2 percent, the tobacco flavor solution is sprayed on filter tow in the filter processing process, and the adding amount is 0.2 mu g of tobacco flavor solid in each filter rod. And rolling the prepared filter stick into a cigarette. Compared with cigarettes without the additive, the cigarette product has the advantages of better smoke harmony, prominent fruit fragrance and obviously improved cigarette quality.
(5) Adding tobacco flavor with filter residue into tobacco shred feed liquid with the mass fraction of 0.5%, and adding into tobacco shred in production process to obtain cigarette. Compared with cigarettes without the additive, the cigarette product has the advantages of better smoke harmony, prominent fruit fragrance and obviously improved cigarette quality.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (4)
1. A preparation method of a tobacco flavor is characterized by comprising the following steps: comprises the following steps:
(1) putting the aged tobacco leaves and other substances capable of generating fermentation fragrance into a closed reactor together, wherein the mass ratio of the tobacco leaves to the other substances capable of generating fermentation fragrance is 10:1-1:1, adding biological enzyme accounting for 0.01-0.05% of the mass of the tobacco leaves, fermenting for 10-60 days under the conditions that the temperature is 40-65 ℃ and the humidity is 60-95%, synchronously performing chemical component fermentation on the tobacco leaves and the co-fermentation substances, synchronously generating fermentation substances with characteristic fragrance through the interaction of the components, and taking out the fermentation substances, wherein the fermentation substances comprise residues and generated other substances; the fermentation is interacted, so that the fermentation product integrates the intrinsic fragrance and the exogenous fragrance of the tobacco leaves, and new fermentation characteristic fragrance is generated; the substance capable of generating fermentation fragrance is one or more of petal, lotus leaf, bamboo fragment, wood, aniseed and fruit; the biological enzyme is one or more of saccharifying enzyme, pectinase, amylase, cellulase and protease;
(2) extracting the fermented substance obtained in step (1) with a solvent, wherein the volume of the solvent is 1-1.2 times of the volume of the tobacco leaves, and removing insoluble components in the residue to obtain a solution extract;
(3) evaporating the solution extract obtained in the step (2) to dryness to obtain an extract, adding glycerol triacetate with the same volume as the solvent in the step (2) to dissolve again, filtering after the soluble substance of the glycerol triacetate in the extract is fully dissolved, and separating filter residue from the solution to obtain the tobacco flavor solution and the tobacco flavor filter residue.
2. The preparation method of the tobacco flavor according to claim 1, characterized by comprising the following steps: the extraction solvent in the step (2) is one of water, ethanol, ethyl acetate, n-hexane, butane and petroleum ether.
3. A tobacco flavor obtained by the method for preparing a tobacco flavor according to claim 1, which comprises a solution tobacco flavor and a residue tobacco flavor.
4. The use of the tobacco flavor of claim 3, wherein: diluting or concentrating the tobacco flavor part to a suitable concentration, and adding into the filter tip in the filter tip processing process, wherein the addition amount is 0.2-1 μ g of tobacco flavor solid in each filter tip; the part of the filter residue tobacco flavor is used as a tobacco shred additive and is added in the tobacco shred flavoring and feeding process, and the filter residue tobacco flavor is added into the tobacco shred feed liquid in an amount which is 0.1 to 5 percent of the mass of the tobacco shred feed liquid.
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| CN107586614A (en) * | 2017-10-24 | 2018-01-16 | 昆明坤九香精香料有限公司 | A kind of preparation method and applications of cigarette cognac flavour |
| CN108048215A (en) * | 2017-12-12 | 2018-05-18 | 湖北中烟工业有限责任公司 | A kind of preparation method of tobacco fig maillard reaction thing |
| CN108451003B (en) * | 2018-01-30 | 2020-08-07 | 湖北中烟工业有限责任公司 | Method for preparing burley tobacco reactant by using hydrolase and application |
| CN108451004B (en) * | 2018-01-30 | 2020-09-08 | 湖北中烟工业有限责任公司 | Method for preparing burley tobacco reactant by using fruit extract and application |
| CN109619642B (en) * | 2018-11-14 | 2022-04-19 | 河南中烟工业有限责任公司 | Tobacco extract for enhancing flavor of tobacco and preparation method thereof |
| CN110403236B (en) * | 2019-07-04 | 2021-07-27 | 江西中烟工业有限责任公司 | Cigarette dry bead filter rod with function of improving smoke permeation |
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| CN105942575A (en) * | 2016-07-01 | 2016-09-21 | 云南中烟工业有限责任公司 | Buccal tobacco product containing tobacco secondary fermentation product and preparation method thereof |
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| CN1903089B (en) * | 2006-08-08 | 2011-05-25 | 云南瑞升烟草技术（集团）有限公司 | Fermented tobacco extractive and its preparation method |
| CN101497844B (en) * | 2008-01-30 | 2011-11-23 | 湖北中烟工业有限责任公司 | Method for preparing cigarette flavor by microbial fermentation of coffee |
| CN102273724A (en) * | 2010-06-11 | 2011-12-14 | 谢勤 | Manufacturing method for leafy flavoring essence for tobacco |
| CN102551192B (en) * | 2012-01-20 | 2014-04-30 | 湖北中烟工业有限责任公司 | Method for preparing camphor tree leaf tobacco flavor |
| CN203251955U (en) * | 2013-05-02 | 2013-10-30 | 福建中烟工业有限责任公司 | Fruity filter tip bar |
| CN105768194B (en) * | 2016-05-13 | 2018-05-01 | 广东中烟工业有限责任公司 | Fermentation buccal cigarette |
| CN106136304B (en) * | 2016-07-21 | 2017-11-28 | 云南中烟工业有限责任公司 | A kind of cigarette flavors additive and preparation method and application |
| CN106235394B (en) * | 2016-07-30 | 2017-10-27 | 江西中烟工业有限责任公司 | A kind of Composite fermentation type turn to red because of sun burn tobacco extract and its application in electronic cigarette |
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| CN105942575A (en) * | 2016-07-01 | 2016-09-21 | 云南中烟工业有限责任公司 | Buccal tobacco product containing tobacco secondary fermentation product and preparation method thereof |
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