CN113355160A - Ailanthus-flavored essence for cigarettes and cigarettes containing essence - Google Patents
Ailanthus-flavored essence for cigarettes and cigarettes containing essence Download PDFInfo
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- CN113355160A CN113355160A CN202110636279.2A CN202110636279A CN113355160A CN 113355160 A CN113355160 A CN 113355160A CN 202110636279 A CN202110636279 A CN 202110636279A CN 113355160 A CN113355160 A CN 113355160A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0023—Aliphatic compounds containing nitrogen as the only heteroatom
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention relates to a Chinese toon flavor essence for cigarettes, which comprises the following components in percentage by mass: 0.01 to 6.73 percent of 2-isopropyl-3-methoxyl pyrazine; 0.60% -12.11% of eugenol; 0.01 to 0.04 percent of beta-ionone. The essence also comprises a solvent, 3-30% of beta-cyclodextrin, 3-30% of pregelatinized starch or 3-30% of octenyl succinic acid starch ester. The invention also relates to a cigarette containing the toona sinensis flavor, wherein the toona sinensis flavor is added to the surface of a cigarette filter tip, a cigarette coil paper or the surface of cigarette cut tobacco, so that smoke generated by the cigarette has a toona sinensis note. According to the invention, three substances, namely 2-isopropyl-3-methoxypyrazine, eugenol and beta-ionone, which do not have the toona sinensis flavor are combined in the presence of a solvent, and the toona sinensis flavor for cigarettes is obtained unexpectedly.
Description
Technical Field
The invention belongs to the technical field of tobacco, and particularly relates to a stink-bug type essence for cigarettes and a cigarette containing the essence.
Background
With the international cigarette inhibition call and the increasing concern of cigarette consumers on the self health, the low-harm cigarette becomes the mainstream of the cigarette in the future world, but the harm reduction is accompanied with the loss of the cigarette aroma and the deterioration of the comfort level, while the cigarette flavoring and charging can set off and supplement the cigarette aroma, increase the smoke concentration, improve the taste, remove and cover miscellaneous gas, reduce the irritation, also can endow the product with the characteristic aroma with beautiful appearance, highlight the personalized style of the cigarette product, and the research, development and application of the cigarette flavoring and charging are becoming one of the most key technologies for keeping the cigarette aroma in the harm and tar reduction work. The smoking satisfaction and pleasure of the cigarettes are improved, and the technical problem to be solved urgently in the existing cigarette aroma-increasing and moisture-keeping technology is solved.
The natural Chinese toon aroma essence in the market is mainly an extract of Chinese toon plants, and has the difference of raw material varieties caused by different factors such as soil, climate, growth environment and the like, so that the quality stability of the product cannot be guaranteed; meanwhile, in the preparation process, the obtained product is more or less mixed with ineffective components such as pigments and vegetable wax which influence the quality of aroma by mainly adopting separation and enrichment means such as organic solvent extraction, steam distillation and the like; in addition, the extract also contains some unknown chemical components, which brings potential safety hazards for the product quality safety of food and daily chemical industries.
At present, the essence with Chinese toon style characteristics is also prepared by a method of compounding a plurality of components in the prior art. CN110810796A discloses an essence of toona sinensis containing 1 extract of toona sinensis, 8 extracts of plants, 16 standard products, which has the aroma of toona sinensis, however, the toona sinensis extract has obvious aroma, i.e. the essence of toona sinensis is provided or toona sinensis extract, and other extracts and standard products are only auxiliary effects and belong to components which do not contribute to aroma.
Therefore, it is desirable to prepare essence with toona sinensis style characteristics by a multi-component compounding method without using toona sinensis extract.
Disclosure of Invention
The present invention has been made to solve the above problems.
The invention provides a Chinese toon flavor essence for cigarettes, which comprises the following components in percentage by weight:
0.01 to 6.73 percent of 2-isopropyl-3-methoxyl pyrazine;
0.60% -12.11% of eugenol;
0.01 to 0.04 percent of beta-ionone.
Preferably, the perfume further comprises a solvent selected from glyceryl triacetate, an aqueous ethanol solution, an aqueous propylene glycol solution or an aqueous glycerol solution.
Preferably, the volume concentration of ethanol in the ethanol water solution is 60-90%; the volume ratio of the propylene glycol in the propylene glycol aqueous solution is 5:5-8: 2; the volume ratio of the glycerol in the glycerol aqueous solution is 6:4-9: 1.
Preferably, the essence further comprises 3% -30% of beta-cyclodextrin, 3% -30% of pregelatinized starch or 3% -30% of octenyl succinic acid starch ester.
Preferably, the preparation method of the essence with Chinese toon flavor comprises the following steps: according to the composition content of the essence, the 2-isopropyl-3-methoxyl pyrazine, the eugenol and the beta-ionone are taken, the solvent is added, the raw materials are fully dissolved by oscillation for 10-40min under the closed condition of 20-60 ℃, the uniform solution is prepared and then is barreled, and the barreled solution is placed in a dark and cool place and is preserved for 12-48h, so that the toona sinensis flavor essence is obtained. If solid flavor is to be prepared, a substance such as beta-cyclodextrin, pregelatinized starch or octenyl succinate starch may be added to adsorb the liquid flavor to obtain solid flavor.
The invention provides a cigarette containing the toona sinensis flavor, wherein the toona sinensis flavor is added to the surface of a cigarette filter, a cigarette paper or the surface of cut tobacco of the cigarette so as to enable smoke generated by the cigarette to have a toona sinensis note. Wherein, the cigarette is not limited to a traditional cigarette or a heating cigarette.
The specific addition method is as follows:
preferably, the cigarette filter tip is added into a cigarette filter tip according to the dosage of 0.2-2 mu L per filter tip, a cigarette sample is rolled by a Yunyan (purple) tobacco leaf group, and other auxiliary materials and essence are kept unchanged to prepare the cigarette sample.
Preferably, the cigarette sample is prepared by spraying the additive to the surface of cigarette paper according to the dosage of 0.5-2.0 mL/hectogram paper, rolling the cigarette sample by Hongtashan (1956) leaf group, and keeping the rest auxiliary materials and essence unchanged.
Preferably, the cigarette sample is prepared by spraying the additive to the surface of the cut tobacco of the cigarette according to the dosage of 0.03-4.00 mL/hectogram cut tobacco, rolling the cigarette sample by adopting Hongta (classical 100) leaf group, and keeping the rest auxiliary materials and essence unchanged.
Preferably, the cigarette sample is prepared by spraying the amount of 0.01-2.00 mL/hectogram of the heated cigarette tobacco shred to the surface of the heated cigarette tobacco shred, rolling the cigarette sample by adopting Yunan Zhongyan cigarette in the heated cigarette X tobacco shred, and keeping the rest auxiliary materials and essence unchanged.
Compared with the prior art, the invention has the following beneficial effects:
1. the essence with the characteristic of Chinese toon aroma style is prepared by combining 2-isopropyl-3-methoxypyrazine with pea aroma, eugenol with spicy aroma, beta-ionone with violet aroma and a solvent, and has an obvious Chinese toon aroma and rich aroma. The preparation method is characterized in that three substances, namely 2-isopropyl-3-methoxypyrazine, eugenol and beta-ionone, which do not have the toona type fragrance are combined in the presence of a solvent, and the toona type tobacco essence is unexpectedly obtained, which is completely unexpected by the inventor, and the formula is simple, namely only the 2-isopropyl-3-methoxypyrazine, the eugenol, the beta-ionone and the solvent are needed.
2. The essence with Chinese toon flavor is added into cigarettes, can increase the cigarette aroma amount, endows the cigarettes with obvious Chinese toon flavor, and has the effects of increasing the richness of the cigarette flavor, reducing stimulation, increasing the Chinese toon flavor, and improving the smoking comfort and satisfaction of the cigarettes.
3. The Chinese toon flavor essence disclosed by the invention is simple in composition, simple in preparation method, suitable for large-scale production and good in application prospect, and has no components which contribute ineffectively to aroma, and the simplest formula of the Chinese toon flavor essence only consists of 3 standard substances and 1 solvent.
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Detailed Description
The present invention is further illustrated by the following examples, which are not intended to be limiting, and any variations or modifications based on the teachings of the present invention are within the scope of the present invention. The examples do not specify particular techniques or conditions, and are performed according to the techniques or conditions described in the literature in the art or according to the product specifications. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available by purchase.
In addition, because no standard test instrument exists for evaluating the cigarette aroma at present, the cigarette aroma evaluation method adopts the most conventional sensory evaluation method in the cigarette field to test, 10 professional sensory evaluation personnel can suck the cigarette samples of the following comparative examples and examples, the irritation, the stink bug rhyme, the aroma richness and the smoke comfort of the sample are scored and the average value is taken, the cigarette sample added with the essence is calculated according to the average value, and the improvement degree of each index is compared with the original cigarette sample without the essence.
Comparative example 1
Mixing 0.01% of 2-isopropyl-3-methoxypyrazine and 99.99% of glyceryl triacetate according to mass percent, oscillating for 20min at 40 ℃ to fully dissolve the raw materials, preparing into uniform solution, barreling, placing in a dark and cool place, and storing for 24 hours to obtain the essence A.
Adding the essence A into a cigarette filter according to the dosage of 0.2 mu L per filter, rolling a cigarette sample by using a Yunyan tobacco (purple) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing to obtain a cigarette sample 1, carrying out comparison smoking evaluation on the cigarette sample 1 and a Yunyan tobacco (purple) product according to GB5606.4-2005 (Table 1), and simultaneously grading bean fragrance, spicy fragrance, flower fragrance and heaven tree fragrance of the two cigarettes (Table 2), wherein the comparison finds that: compared with the Yunyan (purple) product, the bean fragrance of the cigarette sample 1 is increased by 5%, the irritation is reduced by 0%, and the Chinese toon aroma is increased by 0%.
TABLE 1 sensory evaluation of different samples according to GB5606.4-2005
TABLE 2 Bean, spicy, floral, toona sinensis tables for different samples
Comparative example 2
Mixing 0.60% of eugenol and 99.40% of glyceryl triacetate according to the mass percentage, oscillating for 20min at 40 ℃ to fully dissolve the raw materials, preparing into uniform solution, barreling, placing in a dark and cool place, and storing for 24 hours to obtain the essence B.
Adding the essence B into a cigarette filter according to the dosage of 0.2 mu L per filter, rolling a cigarette sample by using a Yunyan tobacco (purple) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing to obtain a cigarette sample 2, carrying out comparison smoking evaluation on the cigarette sample 2 and a Yunyan tobacco (purple) product according to GB5606.4-2005 (Table 3), and grading bean fragrance, spicy fragrance, flower fragrance and heaven tree fragrance of the two products (Table 4), wherein the comparison finds that: compared with the Yunyan (purple) product, the spicy flavor of the cigarette sample 2 is increased by 7.5%, and the Chinese toon aroma is increased by 0%.
TABLE 3 sensory evaluation of different samples according to GB5606.4-2005
TABLE 4 tables for bean, spicy, floral, cedrela sinensis scores for different samples
Comparative example 3
Mixing 0.01% of beta-ionone and 99.99% of glyceryl triacetate according to the mass percentage, oscillating for 20min at 40 ℃ to fully dissolve the raw materials, preparing into uniform solution, barreling, placing in a dark and cool place, and storing for 24 hours to obtain the essence B.
Adding the essence C into a cigarette filter according to the dosage of 0.2 mu L per filter, rolling a cigarette sample by using a Yunyan (purple) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing a cigarette sample 3, carrying out comparison smoking evaluation on the cigarette sample 3 and a Yunyan (purple) product according to GB5606.4-2005 (Table 5), and grading bean fragrance, spicy fragrance, flower fragrance and heaven tree fragrance of the two products (Table 6), wherein the comparison shows that: in cigarette sample 3, compared with the Yunyan tobacco (purple) product, the flower fragrance is increased by 15%, and the Chinese toon aroma is increased by 0%.
TABLE 5 sensory evaluation of different samples according to GB5606.4-2005
TABLE 6 Bean, spicy, floral, toona sinensis tables for different samples
Example 1
Mixing 0.01% of 2-isopropyl-3-methoxypyrazine, 0.60% of eugenol, 0.01% of beta-ionone and 99.38% of glyceryl triacetate according to mass percent, oscillating for 20min at 40 ℃ to fully dissolve the raw materials, preparing into uniform solution, barreling, placing in a dark and cool place, and storing for 24 hours to obtain the essence D.
Adding the essence D into a cigarette filter according to the dosage of 0.2 mu L per filter, rolling a cigarette sample by using a Yunyan (purple) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing to obtain a cigarette sample 4, carrying out comparison smoking evaluation on the cigarette sample 4 and a Yunyan (purple) product according to GB5606.4-2005 (Table 7), and simultaneously grading bean fragrance, spicy fragrance, flower fragrance and heaven tree fragrance of the two cigarettes (Table 8), wherein the comparison finds that: compared with a Yunyan (purple) product, the cigarette sample 4 has the advantages that the aroma richness is increased by 3.11%, the irritation is reduced by 1.85%, the Chinese toon charm is increased from 0 point to 2 points, and the smoke harmony is improved by 1.11%.
TABLE 7 sensory evaluation of different samples according to GB5606.4-2005
TABLE 8 Bean, spice, flower, and cedrela sinensis tables for different samples
Example 2
Mixing 6.73% of 2-isopropyl-3-methoxypyrazine, 12.11% of eugenol, 0.04% of beta-ionone and 81.12% of 70% alcohol by volume percentage, oscillating for 20min at 40 ℃ to fully dissolve the raw materials, preparing into uniform solution, barreling, placing in dark and cool places, and storing for 48 hours to obtain the essence E.
Spraying the essence E on the surface of cigarette paper according to the amount of 0.5 mL/hectogram paper, rolling a cigarette sample by using a Hongtashan (1956) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing to obtain a cigarette sample 5, carrying out comparison smoking evaluation on the cigarette sample 5 and a Hongtashan (1956) product according to GB5606.4-2005 (Table 9), and grading bean fragrance, spicy fragrance, flower fragrance and toona sinensis fragrance of the cigarette sample 5 and the Hongtashan (1956) product (Table 10), wherein the comparison finds that: compared with a Yunyan (purple) product, the cigarette sample 5 has the advantages that the aroma richness is increased by 6.21%, the irritation is reduced by 4.94%, the Chinese toon charm is increased from 0 point to 5 points, and the smoke harmony is improved by 2.17%.
TABLE 9 sensory evaluation of different samples according to GB5606.4-2005
TABLE 10 bean, spice, floral, cedrela sinensis score tables for different samples
Example 3
Mixing 5% of 2-isopropyl-3-methoxypyrazine, 5% of eugenol, 0.02% of beta-ionone and 89.98% of propylene glycol aqueous solution with the volume ratio of 8:2 according to the mass percentage, oscillating for 30min at 50 ℃ to fully dissolve the raw materials, preparing uniform solution, barreling, placing in a dark place and a cool place, and storing for 72 hours to obtain the essence F.
Spraying the essence F on the surface of the cut tobacco of the cigarette according to the using amount of 3.00 mL/hectogram cut tobacco, rolling the cigarette sample by adopting a Hongtai mountain (classic 100) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing to obtain a cigarette sample 6, comparing and smoking the cigarette sample 6 with a Hongtai mountain (classic 100) product according to GB5606.4-2005 (Table 11), and grading the bean fragrance, the spicy fragrance, the flower fragrance and the Chinese toon fragrance of the two (Table 12), wherein the comparison shows that: compared with a Yunyan (purple) product, the cigarette sample 6 has the advantages that the aroma richness is increased by 6.59%, the irritation is reduced by 5.56%, and the Chinese toon charm is increased from 0 point to 5.3 points.
TABLE 11 sensory evaluation of different samples according to GB5606.4-2005
TABLE 12 tables for bean, spicy, floral, cedrela sinensis scores for different samples
Example 4
Mixing 3% of 2-isopropyl-3-methoxypyrazine, 3% of eugenol, 0.04% of beta-ionone, 83.96% of glycerol aqueous solution with the volume ratio of 7:3 and 10% of beta-cyclodextrin according to the mass percentage, stirring for 40min at 45 ℃ to fully mix the raw materials, preparing uniform spice, barreling, placing in a dark and cool place, and storing for 36 hours to obtain the essence G.
Spraying the essence G on the surface of the heated cigarette tobacco shreds according to the using amount of 1.00 mL/hectogram heated cigarette tobacco shreds, making the cigarette tobacco shreds into cigarette samples, keeping the other auxiliary materials and the essence unchanged, preparing to obtain cigarette samples 7, comparing and evaluating the cigarette samples 7 and the samples before applying the essence according to GB5606.4-2005 (Table 13), and grading bean fragrance, spicy fragrance, flower fragrance and Chinese toon fragrance of the two cigarettes (Table 14), wherein the comparison shows that: compared with a Yunyan (purple) product, the cigarette sample 7 has the advantages that the aroma richness is increased by 3.19%, the irritation is reduced by 4.35%, and the Chinese toon charm is increased from 0 point to 3 points.
TABLE 13 sensory evaluation of different samples according to GB5606.4-2005
TABLE 14 Bean, spice, floral, and cedrela sinensis score tables for different samples
Claims (6)
1. The toona sinensis flavor for cigarettes is characterized by comprising the following components in percentage by mass:
0.01 to 6.73 percent of 2-isopropyl-3-methoxyl pyrazine;
0.60% -12.11% of eugenol;
0.01 to 0.04 percent of beta-ionone.
2. The essence of Ailanthi of claim 1, further comprising a solvent selected from triacetin, aqueous ethanol, aqueous propylene glycol or aqueous glycerol.
3. The essence of Chinese toon odor type according to claim 2, wherein the volume concentration of ethanol in the ethanol aqueous solution is 60-90%; the volume ratio of the propylene glycol in the propylene glycol aqueous solution is 5:5-8: 2; the volume ratio of the glycerol in the glycerol aqueous solution is 6:4-9: 1.
4. The essence of any of claims 1 to 2, further comprising 3% to 30% of beta-cyclodextrin, 3% to 30% of pregelatinized starch, or 3% to 30% of octenyl succinate starch.
5. A cigarette comprising the essence of Ailanthi type according to claim 2 or 4, wherein the essence of Ailanthi type is added to a cigarette filter, a surface of a cigarette paper or a surface of cut tobacco of the cigarette so that smoke generated by the cigarette has an Ailanthi note.
6. The cigarette of claim 5, wherein the amount is from 0.2 to 2 μ L per filter; spraying the mixture to the surface of cigarette bobbin paper according to the dosage of 0.5-2.0 mL/hectogram bobbin paper; spraying the mixture to the surface of the cut tobacco of the cigarette according to the dosage of 0.03-4.00 mL/hectogram cut tobacco; spraying the heated tobacco shreds to the surface of the heated tobacco shreds according to the amount of 0.01-2.00 mL/hectogram.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113755245A (en) * | 2021-09-08 | 2021-12-07 | 云南中烟工业有限责任公司 | Avocado-flavor essence, preparation method thereof and cigarette containing avocado-flavor essence |
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| US20180187123A1 (en) * | 2015-09-24 | 2018-07-05 | Givaudan Sa | Perfume Compositions |
| CN110699183A (en) * | 2019-11-04 | 2020-01-17 | 四川中烟工业有限责任公司 | Tobacco essence with spicy fragrance |
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| US20180187123A1 (en) * | 2015-09-24 | 2018-07-05 | Givaudan Sa | Perfume Compositions |
| CN110699183A (en) * | 2019-11-04 | 2020-01-17 | 四川中烟工业有限责任公司 | Tobacco essence with spicy fragrance |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113755245A (en) * | 2021-09-08 | 2021-12-07 | 云南中烟工业有限责任公司 | Avocado-flavor essence, preparation method thereof and cigarette containing avocado-flavor essence |
| CN113755245B (en) * | 2021-09-08 | 2023-11-24 | 云南中烟工业有限责任公司 | Avocado-flavored essence, preparation method thereof and cigarette containing avocado-flavored essence |
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