CN113388452A - Tobacco essence with Chinese toon aroma and cigarette containing essence - Google Patents
Tobacco essence with Chinese toon aroma and cigarette containing essence Download PDFInfo
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- CN113388452A CN113388452A CN202110636344.1A CN202110636344A CN113388452A CN 113388452 A CN113388452 A CN 113388452A CN 202110636344 A CN202110636344 A CN 202110636344A CN 113388452 A CN113388452 A CN 113388452A
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- Prior art keywords
- cigarette
- aroma
- chinese toon
- essence
- tobacco
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0011—Aliphatic compounds containing S
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
- A24C5/00—Making cigarettes; Making tipping materials for, or attaching filters or mouthpieces to, cigars or cigarettes
- A24C5/005—Treatment of cigarette paper
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/002—Cigars; Cigarettes with additives, e.g. for flavouring
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
- A24D3/048—Tobacco smoke filters characterised by their shape or structure containing additives
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0023—Aliphatic compounds containing nitrogen as the only heteroatom
Abstract
The invention relates to a tobacco essence with Chinese toon aroma, which comprises the following components in percentage by mass: 0.01% -0.04% of 3-methylnonane-2, 4-dione; 0.03% -1.5% of 2-methyl thioether; 0.005-0.03% of 2-ethyl-3, 5-dimethyl pyrazine. The essence also comprises a solvent, 10-30% of beta-cyclodextrin, 10-30% of pregelatinized starch or 10-30% of octenyl succinic acid starch ester. The invention also relates to a cigarette containing the tobacco essence with the Chinese toon aroma note, which is added to a cigarette filter tip, the surface of cigarette paper or the surface of cigarette cut tobacco, so that smoke generated by the cigarette has the Chinese toon aroma note, and the cigarette essence further has the effects of increasing the richness of cigarette aroma, reducing stimulation, increasing the Chinese toon aroma, and improving the smoking comfort and satisfaction of the cigarette.
Description
Technical Field
The invention belongs to the technical field of tobacco, and particularly relates to tobacco essence with a Chinese toon aroma note and a cigarette containing the essence.
Background
With the international cigarette inhibition call and the increasing concern of cigarette consumers on the self health, the low-harm cigarette becomes the mainstream of the cigarette in the future world, but the harm reduction is accompanied with the loss of the cigarette aroma and the deterioration of the comfort level, while the cigarette flavoring and charging can set off and supplement the cigarette aroma, increase the smoke concentration, improve the taste, remove and cover miscellaneous gas, reduce the irritation, also can endow the product with the characteristic aroma with beautiful appearance, highlight the personalized style of the cigarette product, and the research, development and application of the cigarette flavoring and charging are becoming one of the most key technologies for keeping the cigarette aroma in the harm and tar reduction work. The smoking satisfaction and pleasure of the cigarettes are improved, and the technical problem to be solved urgently in the existing cigarette aroma-increasing and moisture-keeping technology is solved.
The natural Chinese toon aroma essence in the market is mainly an extract of Chinese toon plants, and has the difference of raw material varieties caused by different factors such as soil, climate, growth environment and the like, so that the quality stability of the product cannot be guaranteed; meanwhile, in the preparation process, the obtained product is more or less mixed with ineffective components such as pigments and vegetable wax which influence the quality of aroma by mainly adopting separation and enrichment means such as organic solvent extraction, steam distillation and the like; in addition, the extract also contains some unknown chemical components, which brings potential safety hazards for the product quality safety of food and daily chemical industries.
At present, the essence with Chinese toon style characteristics is also prepared by a method of compounding a plurality of components in the prior art. CN110810796A discloses an essence of toona sinensis containing 1 extract of toona sinensis, 8 extracts of plants, 16 standard products, which has the aroma of toona sinensis, however, the toona sinensis extract has obvious aroma, i.e. the essence of toona sinensis is provided or toona sinensis extract, and other extracts and standard products are only auxiliary effects and belong to components which do not contribute to aroma.
Therefore, it is desirable to prepare essence with toona sinensis style characteristics by a multi-component compounding method without using toona sinensis extract.
Disclosure of Invention
The present invention has been made to solve the above problems.
The invention provides a tobacco essence with Chinese toon aroma, which comprises the following components in percentage by weight:
0.01% -0.04% of 3-methylnonane-2, 4-dione;
0.03% -1.5% of 2-methyl thioether;
0.005-0.03% of 2-ethyl-3, 5-dimethyl pyrazine.
Preferably, the perfume further comprises a solvent selected from glyceryl triacetate, an aqueous ethanol solution, an aqueous propylene glycol solution or an aqueous glycerol solution.
Preferably, the volume concentration of ethanol in the ethanol water solution is 50-80%; the volume ratio of the propylene glycol in the propylene glycol aqueous solution is 5:5-9: 1; the volume ratio of the glycerol in the glycerol aqueous solution is 6:4-9: 1.
Preferably, the essence further comprises 10% -30% of beta-cyclodextrin, 10% -30% of pregelatinized starch or 10% -30% of starch octenyl succinate.
Preferably, the preparation method of the tobacco essence with Chinese toon note comprises the following steps: according to the composition content of the essence, the 3-methyl nonane-2, 4-dione, 2-methyl thioether and 2-ethyl-3, 5-dimethyl pyrazine are taken, added with the solvent, oscillated under the airtight condition of 20-50 ℃ for 20-50min to fully dissolve the raw materials, prepared into uniform solution, barreled, placed in a dark and cool place, and stored for 12-72h to obtain the tobacco essence with the Chinese toon aroma. If solid flavor is to be prepared, a substance such as beta-cyclodextrin, pregelatinized starch or octenyl succinate starch may be added to adsorb the liquid flavor to obtain solid flavor.
According to the second aspect of the invention, the cigarette containing the essence for cigarettes with Chinese toon aroma is added to the surfaces of cigarette filters, cigarette coil paper or cigarette cut tobacco, so that smoke generated by the cigarette has the Chinese toon aroma. Wherein, the cigarette is not limited to a traditional cigarette or a heating cigarette.
The specific addition method is as follows:
preferably, the cigarette filter tip is added into a cigarette filter tip according to the dosage of 0.6-5 mu L per filter tip, a cigarette sample is rolled by a Yunyan (purple) tobacco leaf group, and other auxiliary materials and essence are kept unchanged to prepare the cigarette sample.
Preferably, the cigarette sample is prepared by spraying the additive to the surface of cigarette paper according to the dosage of 0.8-3.0 mL/hectogram paper, rolling the cigarette sample by Hongtashan (1956) leaf group, and keeping the rest auxiliary materials and essence unchanged.
Preferably, the cigarette sample is prepared by spraying the additive to the surface of the cut tobacco of the cigarette according to the dosage of 0.06-5.00 mL/hectogram cut tobacco, rolling the cigarette sample by adopting Hongta (classical 100) leaf group, and keeping the rest auxiliary materials and essence unchanged.
Preferably, the cigarette sample is prepared by spraying the amount of 0.03-3.00 mL/hectogram of the heated cigarette tobacco shred to the surface of the heated cigarette tobacco shred, rolling the cigarette sample by adopting Yunan Zhongyan cigarette in the heated cigarette X tobacco shred, and keeping the rest auxiliary materials and essence unchanged.
Compared with the prior art, the invention has the following beneficial effects:
1. according to the invention, 3-methylnonane-2, 4-dione with fennel flavor, 2-methyl thioether with asparagus flavor, 2-ethyl-3, 5-dimethylpyrazine with nut flavor and a solvent are combined to prepare the essence with the characteristic of Chinese toon aroma style, and the essence has obvious Chinese toon aroma and rich aroma. The invention combines three substances of 3-methyl nonane-2, 4-diketone, 2-methyl thioether and 2-ethyl-3, 5-dimethyl pyrazine which do not have the toona type odor in the presence of a solvent, but unexpectedly obtains the toona type tobacco essence, which is completely unexpected by the inventor, and the formula is simple, only 3-methyl nonane-2, 4-diketone, 2-methyl thioether, 2-ethyl-3, 5-dimethyl pyrazine and the solvent are needed, compared with the toona type essence used in the prior art, the formula of the invention is simpler, does not contain a plurality of components which do not contribute to the odor, and is more beneficial to implementation.
2. The tobacco essence with Chinese toon aroma disclosed by the invention is added into cigarettes, so that the cigarette aroma amount can be increased, the cigarettes are endowed with obvious Chinese toon aroma, and the tobacco essence with Chinese toon aroma has the effects of increasing the richness of the cigarette aroma, reducing the stimulation, increasing the Chinese toon aroma, and improving the smoking comfort and satisfaction of the cigarettes.
3. The invention relates to a tobacco essence with Chinese toon aroma, which is prepared from 3 standard substances and 1 solvent, has simple components, does not have components which do not contribute to aroma effectively, has simple and easy preparation method, is suitable for large-scale production and has good application prospect.
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Detailed Description
The present invention is further illustrated by the following examples, which are not intended to be limiting, and any variations or modifications based on the teachings of the present invention are within the scope of the present invention. The examples do not specify particular techniques or conditions, and are performed according to the techniques or conditions described in the literature in the art or according to the product specifications. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available by purchase.
In addition, because no standard test instrument exists for evaluating the cigarette aroma at present, the cigarette aroma evaluation method adopts the most conventional sensory evaluation method in the cigarette field to test, 10 professional sensory evaluation personnel can suck the cigarette samples of the following comparative examples and examples, the irritation, the stink bug rhyme, the aroma richness and the smoke comfort of the sample are scored and the average value is taken, the cigarette sample added with the essence is calculated according to the average value, and the improvement degree of each index is compared with the original cigarette sample without the essence.
Comparative example 1
Mixing 0.01% of 3-methyl nonane-2, 4-dione and 99.99% of glyceryl triacetate according to the mass percentage, oscillating for 20min at 40 ℃ to fully dissolve the raw materials, preparing into uniform solution, barreling, placing in a dark and cool place, and storing for 24 hours to obtain the essence A.
Adding the essence A into a cigarette filter according to the using amount of 0.6 mu L per filter, rolling a cigarette sample by using a Yunyan (purple) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing to obtain a cigarette sample 1, carrying out comparison smoking evaluation on the cigarette sample 1 and a Yunyan (purple) product according to GB5606.4-2005 (Table 1), and simultaneously scoring the two fennel, asparagus, nut and Chinese toon (Table 2), wherein the comparison finds that: compared with the Yunyan (purple) product, the fennel of the cigarette sample 1 is increased by 7.5%, and the Chinese toon aroma is increased by 0%.
TABLE 1 sensory evaluation of different samples according to GB5606.4-2005
TABLE 2 Bean, spicy, floral, toona sinensis tables for different samples
Comparative example 2
Mixing 0.03% of 2-methyl sulfide and 99.97% of glyceryl triacetate according to mass percent, oscillating for 20min at 40 ℃ to fully dissolve the raw materials, preparing into uniform solution, barreling, placing in a dark and cool place, and storing for 24 hours to obtain the essence B.
Adding the essence B into a cigarette filter according to the using amount of 0.6 mu L per filter, rolling a cigarette sample by using a Yunyan tobacco (purple) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing a cigarette sample 2, carrying out comparison smoking evaluation on the cigarette sample 2 and a Yunyan tobacco (purple) product according to GB5606.4-2005 (Table 3), and simultaneously grading fennel, asparagus incense, nut incense and Chinese toon incense (Table 4), wherein the comparison finds that: in the cigarette sample 2, the asparagus aroma is increased by 9% and the toona sinensis aroma is increased by 0% compared with the yunyan (purple) product.
TABLE 3 sensory evaluation of different samples according to GB5606.4-2005
TABLE 4 tables for bean, spicy, floral, cedrela sinensis scores for different samples
Comparative example 3
Mixing 0.005% of 2-ethyl-3, 5-dimethyl pyrazine and 99.995% of glyceryl triacetate according to the mass percentage, oscillating for 20min at 40 ℃ to fully dissolve the raw materials, preparing into a uniform solution, barreling, placing in a dark and cool place, and storing for 24 hours to obtain the essence B.
Adding the essence C into a cigarette filter according to the dosage of 0.6 mu L per filter, rolling a cigarette sample by using a Yunyan (purple) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing a cigarette sample 3, carrying out comparison smoking evaluation on the cigarette sample 3 and a Yunyan (purple) product according to GB5606.4-2005 (Table 5), and simultaneously grading fennel, asparagus incense, nut incense and Chinese toon incense (Table 6), wherein the comparison finds that: in cigarette sample 3, the nut aroma is increased by 13.5% and the toona aroma is increased by 0% relative to the yunyan (purple) product.
TABLE 5 sensory evaluation of different samples according to GB5606.4-2005
TABLE 6 Bean, spicy, floral, toona sinensis tables for different samples
Example 1
Mixing 0.01% of 3-methyl nonane-2, 4-dione, 0.03% of 2-methyl thioether, 0.005% of 2-ethyl-3, 5-dimethyl pyrazine and 99.955% of glyceryl triacetate according to mass percent, oscillating for 20min at 30 ℃ to fully dissolve the raw materials, preparing into uniform solution, barreling, and storing in a dark and cool place for 24 hours to obtain the essence D.
Adding the essence D into a cigarette filter according to the using amount of 0.6 mu L per filter, rolling a cigarette sample by using a Yunyan (purple) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing a cigarette sample 4, carrying out comparison smoking evaluation on the cigarette sample 4 and a Yunyan (purple) product according to GB5606.4-2005 (Table 7), and simultaneously grading fennel, asparagus incense, nut incense and Chinese toon incense (Table 8), wherein the comparison finds that: compared with a Yunyan (purple) product, the cigarette sample 4 has the advantages that the aroma richness is increased by 3.46%, the irritation is reduced by 1.23%, the Chinese toon charm is increased from 0 point to 1.5 points, and the smoke harmony is improved by 1.56%.
TABLE 7 sensory evaluation of different samples according to GB5606.4-2005
TABLE 8 Bean, spice, flower, and cedrela sinensis tables for different samples
Example 2
Mixing 0.04% of 3-methylnonane-2, 4-dione, 1.5% of 2-methyl thioether, 0.03% of 2-ethyl-3, 5-dimethyl pyrazine and 98.43% of 70% alcohol by volume percentage, oscillating for 20min at 40 ℃ to fully dissolve the raw materials, preparing into uniform solution, barreling, and storing in dark and cool places for 48 hours to obtain the essence E.
Spraying the essence E onto the surface of cigarette paper according to the amount of 0.8 mL/hectogram paper, rolling a cigarette sample by using a Hongtashan (1956) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing a cigarette sample 5, carrying out comparison smoking evaluation on the cigarette sample 5 and a Hongtashan (1956) product according to GB5606.4-2005 (Table 9), and grading fennel, asparagus, nut and Chinese toon fragrance (Table 10), wherein the comparison shows that: compared with a Yunyan (purple) product, the cigarette sample 5 has the advantages that the aroma richness is increased by 6.55%, the irritation is reduced by 5.56%, the Chinese toon charm is increased from 0 point to 5.5 points, and the smoke harmony is improved by 2.39%.
TABLE 9 sensory evaluation of different samples according to GB5606.4-2005
TABLE 10 bean, spice, floral, cedrela sinensis score tables for different samples
Example 3
Mixing 0.02% of 3-methyl nonane-2, 4-dione, 1% of 2-methyl thioether, 0.02% of 2-ethyl-3, 5-dimethyl pyrazine and 98.96% of propylene glycol aqueous solution in a volume ratio of 8:2 according to mass percent, oscillating at 50 ℃ for 30min to fully dissolve the raw materials, preparing into uniform solution, barreling, placing in a dark and cool place, and storing for 72 hours to obtain the essence F.
Spraying the essence F onto the surface of the cut tobacco of the cigarette according to the using amount of 3.00 mL/hectogram cut tobacco, rolling the cigarette sample by adopting a Hongtai mountain (classic 100) leaf group, keeping the rest auxiliary materials and the essence unchanged, preparing to obtain a cigarette sample 6, comparing and smoking the cigarette sample 6 with a Hongtai mountain (classic 100) product according to GB5606.4-2005 (Table 11), and grading fennel, asparagus, nut and Chinese toon fragrance of the two (Table 12), wherein the comparison finds that: compared with a Yunyan (purple) product, the cigarette sample 6 has the advantages that the aroma richness is increased by 6.59%, the irritation is reduced by 4.94%, and the Chinese toon charm is increased from 0 point to 5 points.
TABLE 11 sensory evaluation of different samples according to GB5606.4-2005
TABLE 12 tables for bean, spicy, floral, cedrela sinensis scores for different samples
Example 4
Mixing 0.03% of 3-methyl nonane-2, 4-dione, 1.2% of 2-methyl thioether, 0.02% of 2-ethyl-3, 5-dimethyl pyrazine, 88.75% of glycerol aqueous solution with the volume ratio of 7:3 and 10% of beta-cyclodextrin according to mass percent, stirring for 40min at 45 ℃ to fully mix the raw materials, preparing uniform spice, filling into a barrel, placing in a dark and cool place, and storing for 48 hours to obtain the essence G.
Spraying the essence G on the surface of the heated cigarette tobacco shreds according to the using amount of 2.00 mL/hectogram heated cigarette tobacco shreds, making the cigarette tobacco shreds into cigarette samples, keeping the other auxiliary materials and the essence unchanged, preparing to obtain cigarette samples 7, comparing and smoking the cigarette samples 7 with the samples before the spice is applied according to GB5606.4-2005 (Table 13), and meanwhile, grading fennel, asparagus incense, nut incense and Chinese toon incense (Table 14), wherein the comparison shows that: compared with a Yunyan (purple) product, the cigarette sample 7 has the advantages that the aroma richness is increased by 2.48%, the irritation is reduced by 4.53%, and the Chinese toon charm is increased from 0 point to 3.5 points.
TABLE 13 sensory evaluation of different samples according to GB5606.4-2005
TABLE 14 Bean, spice, floral, and cedrela sinensis score tables for different samples
Claims (6)
1. The tobacco essence with Chinese toon aroma is characterized by comprising the following components in percentage by mass:
0.01% -0.04% of 3-methylnonane-2, 4-dione;
0.03% -1.5% of 2-methyl thioether;
0.005-0.03% of 2-ethyl-3, 5-dimethyl pyrazine.
2. The tobacco flavor with Chinese toon note according to claim 1, further comprising a solvent selected from triacetin, an aqueous ethanol solution, an aqueous propylene glycol solution, or an aqueous glycerol solution.
3. The tobacco flavor with Chinese toon note according to claim 2, wherein the volume concentration of ethanol in the ethanol aqueous solution is 50-80%; the volume ratio of the propylene glycol in the propylene glycol aqueous solution is 5:5-9: 1; the volume ratio of the glycerol in the glycerol aqueous solution is 6:4-9: 1.
4. The tobacco flavor with Chinese toon note according to claim 1 or 2, characterized in that it further comprises 10% -30% of beta-cyclodextrin, 10% -30% of pregelatinized starch or 10% -30% of octenyl succinate starch.
5. A cigarette comprising the tobacco flavor with Chinese toon aroma according to claim 2 or 4, characterized in that the tobacco flavor with Chinese toon aroma is added to a cigarette filter, a surface of a cigarette paper or a surface of cut tobacco of the cigarette so that smoke generated by the cigarette has Chinese toon aroma.
6. The cigarette of claim 5, wherein the amount is from 0.6 to 5 μ L per filter; spraying the mixture to the surface of cigarette bobbin paper according to the dosage of 0.8-3.0 mL/hectogram bobbin paper; spraying the mixture to the surface of the cut tobacco of the cigarette according to the using amount of 0.06-5.00 mL/hectogram cut tobacco; spraying the heated tobacco shreds to the surface of the heated tobacco shreds according to the amount of 0.03-3.00 mL/hectogram.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110636344.1A CN113388452A (en) | 2021-06-08 | 2021-06-08 | Tobacco essence with Chinese toon aroma and cigarette containing essence |
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| CN202110636344.1A CN113388452A (en) | 2021-06-08 | 2021-06-08 | Tobacco essence with Chinese toon aroma and cigarette containing essence |
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| CN113388452A true CN113388452A (en) | 2021-09-14 |
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