CN110810796A - Toona sinensis essence and application thereof - Google Patents

Toona sinensis essence and application thereof Download PDF

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Publication number
CN110810796A
CN110810796A CN201911189682.4A CN201911189682A CN110810796A CN 110810796 A CN110810796 A CN 110810796A CN 201911189682 A CN201911189682 A CN 201911189682A CN 110810796 A CN110810796 A CN 110810796A
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China
Prior art keywords
agent
extract
essence
fragrance
chinese toon
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CN201911189682.4A
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Chinese (zh)
Inventor
陈金明
林常腾
雷冬明
林立涌
石灿焕
陈恺嘉
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GUANGZHOU LEVON FLAVOUR AND FRAGRANCE TECHNOLOGY Co
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GUANGZHOU LEVON FLAVOUR AND FRAGRANCE TECHNOLOGY Co
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Priority to CN201911189682.4A priority Critical patent/CN110810796A/en
Publication of CN110810796A publication Critical patent/CN110810796A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/10Natural spices, flavouring agents or condiments; Extracts thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/10Natural spices, flavouring agents or condiments; Extracts thereof
    • A23L27/12Natural spices, flavouring agents or condiments; Extracts thereof from fruit, e.g. essential oils
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/10Natural spices, flavouring agents or condiments; Extracts thereof
    • A23L27/12Natural spices, flavouring agents or condiments; Extracts thereof from fruit, e.g. essential oils
    • A23L27/13Natural spices, flavouring agents or condiments; Extracts thereof from fruit, e.g. essential oils from citrus fruits
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/205Heterocyclic compounds
    • A23L27/2052Heterocyclic compounds having oxygen or sulfur as the only hetero atoms
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/205Heterocyclic compounds
    • A23L27/2054Heterocyclic compounds having nitrogen as the only hetero atom
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/26Meat flavours
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/29Fruit flavours
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20Method-related aspects
    • A61L2209/21Use of chemical compounds for treating air or the like

Abstract

The invention discloses a toona sinensis essence and application thereof, wherein the essence is composed of a toona sinensis bud extract, a main agent, a toona sinensis characteristic fragrance raw material, a vegetable fragrant agent, a fragrance hair-penetrating agent, a bean fragrant agent, a fruit fragrant agent, a green fragrant agent, a pungent agent, a meat fragrant agent, a fragrance fresh agent and a solvent. The main fragrance agent is composed of herba Taraxaci extract, fructus Tamarindi Indicae extract, herba Cassotiae extract, karaya gum, 2-amyl pyridine, neomethyl hesperidin dihydrochalcone, ethyl fenchyl alcohol, furfuryl mercaptan and 3, 4-dimethyl thiophene. At present, no report of preparation of the Chinese toon sprout essence exists, the Chinese toon sprout essence has harmonious fragrance and has the characteristic fragrance of natural Chinese toon sprouts, and the essence can be applied to food, daily cosmetics, air fresheners and the like and has important application value.

Description

Toona sinensis essence and application thereof
Technical Field
The invention belongs to the field of foods and fine chemicals, relates to essence, and particularly relates to essence with natural cedrela sinensis fragrance and application thereof.
Background
The Chinese toon is also called mountain Chinese toon, Chinese toon flower, Chinese toon bud, Chinese toon head, etc., and is called as "vegetable on tree". The unique aroma of the Chinese toon is well received by people all the time, the Chinese toon sprouts have high medicinal value, and reportedly have cool nature and bitter taste, enter lung, stomach and large intestine channels, have the effects of strengthening stomach, regulating qi, clearing heat, stopping bleeding, diminishing inflammation, detoxifying, moistening skin, improving eyesight and the like, and also have the functions of dispelling wind, sterilizing, detoxifying and the like.
The Chinese toon sprouts have the advantages of medicinal effect, rich nutrient components and high nutritive value, particularly the unique flavor and fragrance of the Chinese toon, so that the Chinese toon sprouts become the favorite vegetables in spring, and the tender leaves and the tender sprouts of the Chinese toon sprouts have strong fragrance and are deeply favored by people. The unique aroma of the Chinese toon sprouts is utilized, and various famous vegetables can be cooked by the Chinese toon sprouts, such as Chinese toon fried sliced meat, Chinese toon fried eggs, Chinese toon bean curd, Chinese toon mixed flour, fried Chinese toon, pickled Chinese toon and the like.
The Chinese toon sprouts are widely applied to daily life of people, the fragrance of the Chinese toon sprouts is quite popular with people, however, the simulation and blending of the fragrance of the Chinese toon sprouts are only reported, if the Chinese toon sprout essence is developed, the natural characteristic fragrance of the Chinese toon sprouts is simulated, the Chinese toon sprout essence can be applied to food cooking, the flavor requirement of people on the fragrance of the Chinese toon is met, the Chinese toon sprout essence can also be applied to the perfuming of daily cosmetics, the Chinese toon sprout essence has important application value, and certain social benefits are certainly generated. Therefore, the development of the essence of the Chinese toon sprouts has important significance.
Disclosure of Invention
The invention aims to provide a cedrela sinensis essence.
The invention also aims to provide application of the cedrela sinensis essence.
The purpose of the invention is realized by the following technical scheme:
the cedrela sinensis essence comprises the following raw materials in percentage by mass:
Figure BDA0002293250620000011
the main fragrance agent is composed of herba Taraxaci extract, fructus Tamarindi Indicae extract, herba Cassotiae extract, karaya gum, 2-amyl pyridine, neomethyl hesperidin dihydrochalcone, ethyl fenchyl alcohol, furfuryl mercaptan and 3, 4-dimethyl thiophene.
The raw materials of the characteristic aroma of the cedrela sinensis are more than one of phloretin, 2-methyl thiofuroate or benzyl isothiohydrogen;
according to the aroma characteristics of the Chinese toon sprouts, the aroma of the Chinese toon sprouts is decomposed into main body aroma, bean aroma, fruit aroma, green aroma, spicy aroma and the like, then corresponding aroma raw materials are selected according to the aroma characteristics of the aroma raw materials to carry out blending simulation, and the Chinese toon sprout essence with vivid aroma is finally obtained through numerous modifications and formula adjustments. The formula of the cedrela sinensis essence is disclosed for the first time. At present, no report about blending of the cedrela sinensis essence is found.
The Chinese toon sprout extract, the dandelion extract, the tamarind seed extract and the hyssop extract are respectively extracted by adopting a supercritical carbon dioxide extraction process; specifically, the raw materials (such as Chinese toon sprouts, dandelion, tamarind seeds or hyssop) are put into an extraction kettle, carbon dioxide is introduced, the extraction flow rate is 15g/min, the extraction pressure is 250bar, the extraction temperature is 52 ℃, and the extraction time is 2 hours;
the vegetable fragrance agent is diallyl disulfide and/or dimethyl sulfide.
The fragrance hair penetrating agent is 1-p-menthene-4-alcohol and/or myrtenol, and the components can enhance the fragrance hair penetrating performance of the cedrela sinensis bud essence.
The bean essence is preferably semen Sojae Preparatum tincture.
The fruit flavor agent is preferably fructus Siraitiae Grosvenorii tincture and/or bergamot oil.
The green scent is preferably 2-hexenal.
The spice is preferably caryophyllene and/or basil oil.
The meat flavor is preferably 2-aminoxypropionic acid.
The aroma freshener is preferably 1-octen-3-ol, and can enhance the freshness of the aroma of the Chinese toon sprout essence.
Preferably, the cedrela sinensis essence comprises the following raw materials in percentage by mass:
Figure BDA0002293250620000031
Figure BDA0002293250620000041
the solvent is any one of ethanol, propylene glycol or salad oil.
The preparation method of the cedrela sinensis essence provided by the invention comprises the steps of mixing the raw materials, and uniformly stirring to obtain the cedrela sinensis essence.
The cedrela sinensis essence can be applied to food and daily chemicals (including cosmetics, air fresheners and the like).
Compared with the prior art, the invention has the following advantages and effects:
at present, no report of preparation of the Chinese toon sprout essence exists, the Chinese toon sprout essence has harmonious fragrance and has the characteristic fragrance of natural Chinese toon sprouts, and the essence can be applied to food, daily cosmetics, air fresheners and the like and has important application value.
Detailed Description
The present invention will be described in further detail with reference to examples, but the embodiments of the present invention are not limited thereto.
Each of the raw materials used in the following examples is a commercially available product unless otherwise specified herein.
Example 1
The essence with the characteristic aroma of natural Chinese toon sprouts comprises the following raw materials in percentage by mass:
1% of semen Sojae Preparatum tincture; 1% of diallyl disulfide; fructus momordicae tincture 0.1%; 8% of dandelion extract; 0.1% of tamarind seed extract; 0.12% of hyssop extract; 0.5% of karaya gum; 0.02% of 2-amyl pyridine; phloretin 0.01%; 2% of 1-octen-3-ol; 0.7 percent of 1-p-menthene-4-alcohol; 0.5% of neohesperidin dihydrochalcone; 0.01 percent of 2-sulfo furoic acid methyl ester; 1.5% of myrtenol; 0.001% of benzyl isothiocyanate; 2% of ethyl fenchyl alcohol; 0.01 percent of 2-aminoxypropionic acid; 1% of furfuryl mercaptan; 1% of 2-hexenal; dimethyl sulfide 0.5%; 3% of caryophyllene; 3% of bergamot oil; 0.5% of basil oil; 1.5 percent of 3, 4-dimethylthiophene; 20% of Chinese toon sprout extract; the balance being dipropylene glycol.
The obtained toona sinensis essence has the characteristic fragrance of toona sinensis buds, fresh fragrance, more prominent vegetable fragrance and harmonious whole fragrance through smell identification analysis.
Example 2
The essence with the characteristic aroma of natural Chinese toon sprouts comprises the following raw materials in percentage by mass:
3% of semen Sojae Preparatum tincture; diallyl disulfide 0.1%; fructus momordicae tincture 0.8%; 1% of dandelion extract; 1% of tamarind seed extract; 0.05% of hyssop extract; karaya gum 1.2%; 0.001% of 2-pentyl pyridine; phloretin 0.2%; 0.5 percent of 1-octen-3-ol; 2.1% of 1-p-menthene-4-ol; 0.01% of neohesperidin dihydrochalcone; 0.1% of 2-thiofuroic acid methyl ester; 0.2% of myrtenol; 0.05% of benzyl isothiocyanate; 0.5% of ethyl fenchyl alcohol; 0.1 percent of 2-aminoxypropionic acid; 0.1% of furfuryl mercaptan; 3% of 2-hexenal; dimethyl sulfide 0.01%; 10% of caryophyllene; 0.5 percent of bergamot oil; 3% of basil oil; 0.1% of 3, 4-dimethylthiophene; 50% of Chinese toon sprout extract; the balance of ethanol.
The mutual blending cedrela sinensis essence has strong natural aroma and strong aroma, has the characteristic aroma of cedrela sinensis buds, and has the overall aroma of being sweet and pungent and slightly cool after being subjected to smell identification analysis.
Example 3
The essence with the characteristic aroma of natural Chinese toon sprouts comprises the following raw materials in percentage by mass:
2% of semen Sojae Preparatum tincture; diallyl disulfide 0.5%; fructus momordicae tincture 0.5%; 5% of dandelion extract; tamarind seed extract 0.6%; 0.1% of hyssop extract; 0.9% of karaya gum; 0.01% of 2-amyl pyridine; phloretin 0.1%; 1% of 1-octen-3-ol; 1.5% of 1-p-menthene-4-ol; 0.2% of neohesperidin dihydrochalcone; 0.05 percent of 2-sulfo furoic acid methyl ester; 1% of myrtenol; 0.02% of benzyl isothiocyanate; 1% of ethyl fenchyl alcohol; 0.05 percent of 2-aminoxypropionic acid; 0.3 percent of furfuryl mercaptan; 2% of 2-hexenal; dimethyl sulfide 0.1%; 7% of caryophyllene; 2% of bergamot oil; 2% of basil oil; 1% of 3, 4-dimethylthiophene; chinese toon sprout extract 40%; the balance of salad oil.
The mutual matching Chinese toon essence has the advantages that through the analysis of smell discrimination, the characteristic aroma of natural Chinese toon buds is prominent, the integral aroma is coordinated, the natural feeling is strong, and the aroma is soft, fine and vivid.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.

Claims (10)

1. The cedrela sinensis essence is characterized by comprising the following raw materials in percentage by mass:
the main fragrance agent is composed of herba Taraxaci extract, fructus Tamarindi Indicae extract, hyssop extract, karaya gum, 2-amyl pyridine, neomethyl hesperidin dihydrochalcone, ethyl fenchyl alcohol, furfuryl mercaptan and 3, 4-dimethyl thiophene;
the raw materials of the characteristic aroma of the cedrela sinensis are more than one of phloretin, 2-methyl thiofuroate or benzyl isothiohydrogen.
2. The cedrela sinensis essence according to claim 1, characterized in that: the Chinese toon sprout extract, the dandelion extract, the tamarind seed extract and the hyssop extract are respectively extracted by adopting a supercritical carbon dioxide extraction process.
3. The cedrela sinensis essence according to claim 1, characterized in that: the Chinese toon sprout extract, the dandelion extract, the tamarind seed extract and the hyssop extract are prepared by putting raw materials into an extraction kettle, introducing carbon dioxide, and extracting at the flow rate of 15g/min, the extraction pressure of 250bar, the extraction temperature of 52 ℃ and the extraction time of 2 hours.
4. The cedrela sinensis essence according to claim 1, characterized in that:
the vegetable fragrance agent is diallyl disulfide and/or dimethyl sulfide;
the fragrance hair-penetrating agent is 1-p-menthene-4-alcohol and/or myrtenol.
5. The cedrela sinensis essence according to claim 1, characterized in that:
the bean aromatic is a tincture of semen Sojae Preparatum;
the fruit flavor agent is fructus Siraitiae Grosvenorii tincture and/or bergamot oil.
6. The cedrela sinensis essence according to claim 1, characterized in that:
the green aromatic agent is 2-hexenal;
the spice is caryophyllene and/or basil oil.
7. The cedrela sinensis essence according to claim 1, characterized in that:
the meat flavor agent is 2-aminoxypropionic acid;
the fresh aroma agent is 1-octene-3-ol.
8. The toona sinensis essence according to claim 1, wherein the raw materials comprise the following components in percentage by mass:
Figure FDA0002293250610000021
Figure FDA0002293250610000031
9. the essence of Toona sinensis according to claim 1 or 8, wherein: the solvent is any one of ethanol, propylene glycol or salad oil.
10. Use of cedrela sinensis essence according to any one of claims 1-9 in food and daily chemicals.
CN201911189682.4A 2019-11-28 2019-11-28 Toona sinensis essence and application thereof Withdrawn CN110810796A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113388452A (en) * 2021-06-08 2021-09-14 云南中烟工业有限责任公司 Tobacco essence with Chinese toon aroma and cigarette containing essence

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113388452A (en) * 2021-06-08 2021-09-14 云南中烟工业有限责任公司 Tobacco essence with Chinese toon aroma and cigarette containing essence

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