CN104388192A - Rose-type essence for cigarettes for women and application of flavor - Google Patents
Rose-type essence for cigarettes for women and application of flavor Download PDFInfo
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- CN104388192A CN104388192A CN201410729584.6A CN201410729584A CN104388192A CN 104388192 A CN104388192 A CN 104388192A CN 201410729584 A CN201410729584 A CN 201410729584A CN 104388192 A CN104388192 A CN 104388192A
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- extract
- rose
- cigarette
- type essence
- oil
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 60
- 239000000796 flavoring agent Substances 0.000 title description 3
- 235000019634 flavors Nutrition 0.000 title description 2
- 239000000284 extract Substances 0.000 claims abstract description 107
- 241000220317 Rosa Species 0.000 claims abstract description 66
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 claims abstract description 46
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 39
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 36
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 34
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 claims abstract description 24
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims abstract description 24
- WDAXFOBOLVPGLV-UHFFFAOYSA-N ethyl isobutyrate Chemical compound CCOC(=O)C(C)C WDAXFOBOLVPGLV-UHFFFAOYSA-N 0.000 claims abstract description 24
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000005792 Geraniol Substances 0.000 claims abstract description 23
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 claims abstract description 23
- 229940113087 geraniol Drugs 0.000 claims abstract description 23
- 244000061176 Nicotiana tabacum Species 0.000 claims abstract description 18
- 235000004936 Bromus mango Nutrition 0.000 claims abstract description 15
- 235000014826 Mangifera indica Nutrition 0.000 claims abstract description 15
- 235000009184 Spondias indica Nutrition 0.000 claims abstract description 15
- 239000000341 volatile oil Substances 0.000 claims abstract description 15
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims abstract description 13
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000001605 (5-methyl-2-propan-2-ylcyclohexyl) acetate Substances 0.000 claims abstract description 12
- AYJXHIDNNLJQDT-UHFFFAOYSA-N 2,6,6-Trimethyl-2-cyclohexene-1,4-dione Chemical compound CC1=CC(=O)CC(C)(C)C1=O AYJXHIDNNLJQDT-UHFFFAOYSA-N 0.000 claims abstract description 12
- XHXUANMFYXWVNG-UHFFFAOYSA-N D-menthyl acetate Natural products CC(C)C1CCC(C)CC1OC(C)=O XHXUANMFYXWVNG-UHFFFAOYSA-N 0.000 claims abstract description 12
- YKVWPZJHENXDAJ-VOTSOKGWSA-N Megastigmatrienone Chemical compound CC1=CC(=O)CC(C)(C)C1\C=C\C=C YKVWPZJHENXDAJ-VOTSOKGWSA-N 0.000 claims abstract description 12
- ZOZIRNMDEZKZHM-UHFFFAOYSA-N Phenethyl phenylacetate Chemical compound C=1C=CC=CC=1CCOC(=O)CC1=CC=CC=C1 ZOZIRNMDEZKZHM-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000012907 honey Nutrition 0.000 claims abstract description 12
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 12
- 239000004310 lactic acid Substances 0.000 claims abstract description 12
- 240000007228 Mangifera indica Species 0.000 claims abstract 3
- 241000208125 Nicotiana Species 0.000 claims description 22
- 239000003921 oil Substances 0.000 claims description 22
- 235000011201 Ginkgo Nutrition 0.000 claims description 14
- 235000008100 Ginkgo biloba Nutrition 0.000 claims description 14
- 244000250129 Trigonella foenum graecum Species 0.000 claims description 14
- 235000001484 Trigonella foenum graecum Nutrition 0.000 claims description 14
- 235000001019 trigonella foenum-graecum Nutrition 0.000 claims description 14
- 239000009609 fructus phyllanthi Substances 0.000 claims description 13
- 239000003205 fragrance Substances 0.000 claims description 12
- 241000628997 Flos Species 0.000 claims description 11
- 240000004760 Pimpinella anisum Species 0.000 claims description 11
- 235000012550 Pimpinella anisum Nutrition 0.000 claims description 11
- 229940067107 phenylethyl alcohol Drugs 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 7
- 244000194101 Ginkgo biloba Species 0.000 claims 2
- 235000019640 taste Nutrition 0.000 abstract description 11
- 230000008901 benefit Effects 0.000 abstract description 6
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 abstract 2
- 239000000779 smoke Substances 0.000 abstract 2
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 abstract 1
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 abstract 1
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 abstract 1
- 239000005711 Benzoic acid Substances 0.000 abstract 1
- 235000003385 Diospyros ebenum Nutrition 0.000 abstract 1
- 206010013911 Dysgeusia Diseases 0.000 abstract 1
- 241000792913 Ebenaceae Species 0.000 abstract 1
- 239000009429 Ginkgo biloba extract Substances 0.000 abstract 1
- 239000010617 anise oil Substances 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 235000010233 benzoic acid Nutrition 0.000 abstract 1
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 abstract 1
- 235000000484 citronellol Nutrition 0.000 abstract 1
- 239000001902 eugenia caryophyllata l. bud oil Substances 0.000 abstract 1
- 235000020765 fenugreek extract Nutrition 0.000 abstract 1
- 229940068052 ginkgo biloba extract Drugs 0.000 abstract 1
- 235000020686 ginkgo biloba extract Nutrition 0.000 abstract 1
- 229930007744 linalool Natural products 0.000 abstract 1
- 235000019659 mouth feeling Nutrition 0.000 abstract 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 17
- 239000003546 flue gas Substances 0.000 description 17
- 239000002994 raw material Substances 0.000 description 17
- 241000218628 Ginkgo Species 0.000 description 12
- 241001093152 Mangifera Species 0.000 description 12
- 239000002304 perfume Substances 0.000 description 12
- 239000000243 solution Substances 0.000 description 10
- 238000003756 stirring Methods 0.000 description 7
- 238000000605 extraction Methods 0.000 description 6
- 238000001914 filtration Methods 0.000 description 6
- 238000010992 reflux Methods 0.000 description 6
- 230000000391 smoking effect Effects 0.000 description 5
- 235000013599 spices Nutrition 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 235000019633 pungent taste Nutrition 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 238000007873 sieving Methods 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 244000119298 Emblica officinalis Species 0.000 description 1
- 235000015489 Emblica officinalis Nutrition 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 241001312519 Trigonella Species 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 239000008369 fruit flavor Substances 0.000 description 1
- 238000012792 lyophilization process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000874 microwave-assisted extraction Methods 0.000 description 1
- 238000000199 molecular distillation Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000002390 rotary evaporation Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
Abstract
The invention discloses a rose-type essence for cigarettes for women. The rose-type essence is prepared by mixing the following components: 1.0-2.5% of rose flower essential oil, 0.1-0.5% of clove bud oil, 0.01-0.1% of anise oil, 1.5%-3.0% of citronellol, 0.1-0.5% of geraniol, 0.2-0.5% of linalool, 0.5-1.5% of phenethyl alcohol, 0.1%-1.0% of ethyl isobutyrate, 0.2-1.5% of phenylethyl phenylacetate, 0.1-0.3% of menthyl acetate, 0.5-1.0% of ginkgo biloba extract, 0.1-1.0% of mango extract, 0.05-0.5% of coffee extract, 0.1-1.0% of emblica extract, 1.0-2.0% of ebony extract, 0.5-1.0% of red date extract, 0.01-0.05% of fenugreek extract, 0.5-1.5% of aromatic tobacco extract, 0.01-0.1% of lactic acid, 0.02-0.08% of benzoic acid, 0.02-0.05% of oxoisophorone, 0.5%-1.0% of megastigmatrienone, 0.5-1.0% of honey, 40.0-60.0% of 70% ethanol and the balance of propylene glycol. By adding rose-type essence into tobacco shreds, the tobacco shreds are rolled into cigarettes having the advantages of delicate and soft smoke, pleasant mouth feeling, clean aftertaste, pure and mild taste, harmonious smoke incense and the like.
Description
Technical field
The invention belongs to technical field of cigarette flavors, specifically refer to a kind of Rose type essence for Ms's cigarette and application thereof.
Technical background
Because " smoking with healthy " problem more and more receives the concern of society, produce the direction having become tobacco industry survival and development with " high fragrance, low tar, the less harmful " cigarette product that is principal feature.But while reducing tar and reducing harm, often cause cigarette odor-absorbing composition to lose in a large number, fragrance obviously weakens, and is difficult to satisfy the demands of consumers.Therefore, carry out the exploitation of compensating aroma technical study and essence and flavoring agent, become an urgent demand of cigarette industry.Such as, domestic many tobacco companies, while allotment cigarette composition, adopt again the way of additional various spices or essence, mostly to make up the deficiency of cigarette fragrance.Meanwhile, in order to the style and features of outstanding brand, exploitation has the flavouring essence for tobacco of feature odor type, such as various floral type, fruit flavour type, saline taste type essence, has become the target that each large tobacco enterprise is endeavoured to study.
Ms's cigarette is also called " female's cigarette ", and refer to needs for female smoker and the cigarette that designs, its outward appearance is general more very thin, exquisite, packs based on fashion bright colors lines, and its suction taste is mostly with fruit aroma or flowery odour, more fresh and clean.In recent years, along with the development of China's economic, the continuous enhancing of the independent consciousness of women, show that the age of women's individual character arrives, smoking is no longer the patent of man, and the women of a part of high salary white collar and individual character of following the fashion also joins these ranks.Due to physiology and psychological difference, the male sex and women embody distinct feature in cigarette consumption demand.Flue gas is fine and smooth, elegant in smell, inhale taste alcohol and, pleasant impression cigarette that is pure, comfortable taste often enjoys female smoker to welcome, this is that the adjustment of Ms's cigarette perfume formulation and exploitation specify direction.Universal along with " Smoking is harmful to your health " this idea, modern female smoker is following the fashion, while individual character, and more focus on the health and safety problem of cigarette, low-harm type cigarette product becomes the object that female smoker more and more pays close attention to.
Summary of the invention
The object of the invention is to according to rose deeply by the feature that Ms likes, a kind of Rose type essence for Ms's cigarette and application thereof are provided, it can give Ms's cigarette graceful naturally rose characteristic perfume, have that flue gas exquisiteness is soft, comfortable taste, pleasant impression be clean, inhale taste alcohol and, the advantage such as the fragrant coordination of cigarette, the pungency that when effectively can alleviate suction, flue gas causes throat simultaneously, has potential harm reduction effect.
For achieving the above object, a kind of Rose type essence for Ms's cigarette designed by the present invention, it is mixed by following compositions in weight percentage: the rose ethereal oil of 1.0 ~ 2.5%, the Flos Caryophylli oil of 0.1 ~ 0.5%, the star aniseed oil of 0.01 ~ 0.1%, the geraniol of 1.5 ~ 3.0%, the Geraniol of 0.1 ~ 0.5%, the phantol of 0.2 ~ 0.5%, the phenylethyl alcohol of 0.5 ~ 1.5%, the ethyl isobutyrate of 0.1 ~ 1.0%, the phenylethyl phenylacetate of 0.2 ~ 1.5%, the menthyl acetate of 0.1 ~ 0.3%, the Folium Ginkgo extract of 0.5 ~ 1.0%, the mango extract of 0.1 ~ 1.0%, the coffee extract of 0.05 ~ 0.5%, the Fructus Phyllanthi extract of 0.1 ~ 1.0%, the Fructus Mume extract of 1.0 ~ 2.0%, the red date medicinal extract of 0.5 ~ 1.0%, the fenugreek concrete of 0.01 ~ 0.05%, 0.5 ~ 1.5% Turkish tobaccos extract, the lactic acid of 0.01 ~ 0.1%, the phenylformic acid of 0.02 ~ 0.08%, the ketoisophorone of 0.02 ~ 0.05%, the Megastigmatrienone of 0.5 ~ 1.0%, the honey of 0.5 ~ 1.0%, 70% ethanol of 40.0 ~ 60.0%, all the other are propylene glycol.
Preferably, it is mixed by following compositions in weight percentage: the rose ethereal oil of 1.5 ~ 2.0%, the Flos Caryophylli oil of 0.2 ~ 0.3%, the star aniseed oil of 0.01 ~ 0.05%, the geraniol of 1.5 ~ 2.5%, the Geraniol of 0.1 ~ 0.3%, the phantol of 0.2 ~ 0.5%, the phenylethyl alcohol of 0.5 ~ 1.0%, the ethyl isobutyrate of 0.1 ~ 0.5%, the phenylethyl phenylacetate of 0.5 ~ 1.0%, the menthyl acetate of 0.1 ~ 0.2%, the Folium Ginkgo extract of 0.7 ~ 1.0%, the mango extract of 0.5 ~ 1.0%, the coffee extract of 0.2 ~ 0.4%, the Fructus Phyllanthi extract of 0.2 ~ 0.8%, the Fructus Mume extract of 1.0 ~ 1.5%, the red date medicinal extract of 0.5 ~ 0.8%, the fenugreek concrete of 0.03 ~ 0.05%, the Turkish tobaccos extract of 0.6 ~ 1.2%, the lactic acid of 0.05 ~ 0.1%, the phenylformic acid of 0.03 ~ 0.06%, the ketoisophorone of 0.02 ~ 0.05%, the Megastigmatrienone of 0.5 ~ 0.7%, the honey of 0.6 ~ 0.8%, 70% ethanol of 45.0 ~ 55.0%, all the other are propylene glycol.
Again further, described volume fraction of ethanol is 70%.
Said components raw material carries out being uniformly mixed according to after weight percent batching by preparation method of the present invention in container.
The present invention also provides a kind of application of Rose type essence in Ms's cigarette for Ms's cigarette: comprise the following steps:
Taking Rose type essence, to be dissolved in volume fraction be in 70% ethanolic soln, obtain the Rose type fragrance solution that massfraction is 10 ~ 70%, then it is evenly sprayed on the blank pipe tobacco of Ms's cigarette, and rolls into cigarette, wherein, the addition of Rose type essence is 0.01 ~ 0.05% of pipe tobacco weight.
Advantage of the present invention is as follows:
1, the present invention is based on the alcohols monomer perfume being rich in rose suggestion, and independent development also employs various plants natural extract, while enriching tobacco aromatics using range of choice, makes the allotment of the Rose type essence for Ms's cigarette obtain comparatively quantum jump.
2, the present invention plant containing natural extract and traditional monomer cigarette perfume material through scientific and rational compatibility, allotment obtains a kind of Rose type essence for Ms's cigarette, can give Ms's cigarette graceful naturally rose characteristic perfume, have that flue gas exquisiteness is soft, comfortable taste, pleasant impression be clean, inhale taste alcohol and, the advantage such as the fragrant coordination of cigarette, the pungency that when effectively can alleviate suction, flue gas causes throat simultaneously, has potential harm reduction effect.
3, the present invention has that preparation method is simple, economical and practical, raw material is easy to the advantages such as acquisition.
Embodiment
Below in conjunction with specific embodiment, method of the present invention is described in further detail.
Embodiment 1
Take following raw material components (by 100g formula): the rose ethereal oil of 2g, the Flos Caryophylli oil of 0.2g, the star aniseed oil of 0.02g, the geraniol of 2g, the Geraniol of 0.4g, the phantol of 0.2g, the phenylethyl alcohol of 1.0g, the ethyl isobutyrate of 0.6g, the phenylethyl phenylacetate of 0.7g, the menthyl acetate of 0.1g, the Folium Ginkgo extract of 1g, the mango extract of 0.5g, the coffee extract of 0.2g, the Fructus Phyllanthi extract of 0.5g, the Fructus Mume extract of 1.0g, the red date medicinal extract of 0.5g, the fenugreek concrete of 0.02g, the Turkish tobaccos extract of 1.0g, the lactic acid of 0.02g, the phenylformic acid of 0.06g, the ketoisophorone of 0.03g, the Megastigmatrienone of 0.8g, the honey of 0.5g, the volume fraction of 50g is 70% ethanol, all the other are propylene glycol.Namely above-mentioned raw materials is evenly obtained Rose type essence 1 in container for stirring.Getting appropriate Rose type essence 1, to be dissolved in volume fraction be in 70% ethanolic soln, obtains the Rose type fragrance solution that massfraction is 10%, then it is evenly sprayed on the blank pipe tobacco of Yellow Crane Tower " heart is blue " Ms's cigarette, and rolls into cigarette.The addition of Rose type essence is 0.01% of pipe tobacco weight.
Embodiment 2
Take following raw material components (by 100g formula): the rose ethereal oil of 1.5g, the Flos Caryophylli oil of 0.3g, the star aniseed oil of 0.05g, the geraniol of 1.5g, the Geraniol of 0.5g, the phantol of 0.4g, the phenylethyl alcohol of 0.8g, the ethyl isobutyrate of 0.4g, the phenylethyl phenylacetate of 1.0g, the menthyl acetate of 0.3g, the Folium Ginkgo extract of 0.8g, the mango extract of 1.0g, the coffee extract of 0.3g, the Fructus Phyllanthi extract of 0.3g, the Fructus Mume extract of 1.5g, the red date medicinal extract of 0.8g, the fenugreek concrete of 0.05g, the Turkish tobaccos extract of 0.8g, the lactic acid of 0.1g, the phenylformic acid of 0.02g, the ketoisophorone of 0.04g, the Megastigmatrienone of 0.5g, the honey of 0.7g, the volume fraction of 40g is 70% ethanol, all the other are propylene glycol.Namely above-mentioned raw materials is evenly obtained Rose type essence 2 in container for stirring.Getting appropriate Rose type essence 2, to be dissolved in volume fraction be in 70% ethanolic soln, obtains the Rose type fragrance solution that massfraction is 70%, then it is evenly sprayed on the blank pipe tobacco of Yellow Crane Tower " heart is blue " Ms's cigarette, and rolls into cigarette.The addition of Rose type essence is 0.05% of pipe tobacco weight.
Embodiment 3
Take following raw material components (by 100g formula): the rose ethereal oil of 1.8g, the Flos Caryophylli oil of 0.5g, the star aniseed oil of 0.1g, the geraniol of 2.5g, the Geraniol of 0.2g, the phantol of 0.3g, the phenylethyl alcohol of 1.2g, the ethyl isobutyrate of 0.6g, the phenylethyl phenylacetate of 1.2g, the menthyl acetate of 0.25g, the Folium Ginkgo extract of 0.5g, the mango extract of 0.7g, the coffee extract of 0.2g, the Fructus Phyllanthi extract of 0.5g, the Fructus Mume extract of 1.2g, the red date medicinal extract of 0.6g, the fenugreek concrete of 0.04g, the Turkish tobaccos extract of 1.0g, the lactic acid of 0.05g, the phenylformic acid of 0.04g, the ketoisophorone of 0.05g, the Megastigmatrienone of 0.6g, the honey of 0.6g, the volume fraction of 60g is 70% ethanol, all the other are propylene glycol.Namely above-mentioned raw materials is evenly obtained Rose type essence 3 in container for stirring.Getting appropriate Rose type essence 3, to be dissolved in volume fraction be in 70% ethanolic soln, obtains the Rose type fragrance solution that massfraction is 50%, then it is evenly sprayed on the blank pipe tobacco of Yellow Crane Tower " heart is blue " Ms's cigarette, and rolls into cigarette.The addition of Rose type essence is 0.03% of pipe tobacco weight.
Embodiment 4
Take following raw material components (by 100g formula): the rose ethereal oil of 1.8g, the Flos Caryophylli oil of 0.3g, the star aniseed oil of 0.08g, the geraniol of 2.5g, the Geraniol of 0.4g, the phantol of 0.5g, the phenylethyl alcohol of 0.8g, the ethyl isobutyrate of 0.4g, the phenylethyl phenylacetate of 0.8g, the menthyl acetate of 0.15g, the Folium Ginkgo extract of 0.6g, the mango extract of 0.8g, the coffee extract of 0.15g, the Fructus Phyllanthi extract of 0.8g, the Fructus Mume extract of 1.5g, the red date medicinal extract of 0.8g, the fenugreek concrete of 0.02g, the Turkish tobaccos extract of 0.8g, the lactic acid of 0.08g, the phenylformic acid of 0.02g, the ketoisophorone of 0.03g, the Megastigmatrienone of 0.7g, the honey of 0.5g, the volume fraction of 55g is 70% ethanol, all the other are propylene glycol.Namely above-mentioned raw materials is evenly obtained Rose type essence 4 in container for stirring.Getting appropriate Rose type essence 4, to be dissolved in volume fraction be in 70% ethanolic soln, obtains the Rose type fragrance solution that massfraction is 50%, then it is evenly sprayed on the blank pipe tobacco of Yellow Crane Tower " heart is blue " Ms's cigarette, and rolls into cigarette.The addition of Rose type essence is 0.02% of pipe tobacco weight.
Embodiment 5
Take following raw material components (by 100g formula): the rose ethereal oil of 2.5g, the Flos Caryophylli oil of 0.1g, the star aniseed oil of 0.01g, the geraniol of 1.8g, the Geraniol of 0.1g, the phantol of 0.3g, the phenylethyl alcohol of 0.5g, the ethyl isobutyrate of 0.1g, the phenylethyl phenylacetate of 0.2g, the menthyl acetate of 0.2g, the Folium Ginkgo extract of 0.7g, the mango extract of 0.1g, the coffee extract of 0.05g, the Fructus Phyllanthi extract of 0.1g, the Fructus Mume extract of 2g, the red date medicinal extract of 1g, the fenugreek concrete of 0.01g, the Turkish tobaccos extract of 0.5g, the lactic acid of 0.01g, the phenylformic acid of 0.03g, the ketoisophorone of 0.02g, the Megastigmatrienone of 1g, the honey of 1g, the volume fraction of 45g is 70% ethanol, all the other are propylene glycol.Namely above-mentioned raw materials is evenly obtained Rose type essence 5 in container for stirring.Getting appropriate Rose type essence 5, to be dissolved in volume fraction be in 70% ethanolic soln, obtains the Rose type fragrance solution that massfraction is 20%, then it is evenly sprayed on the blank pipe tobacco of Yellow Crane Tower " heart is blue " Ms's cigarette, and rolls into cigarette.The addition of Rose type essence is 0.01% of pipe tobacco weight.
Embodiment 6
Take following raw material components (by 100g formula): the rose ethereal oil of 1g, the Flos Caryophylli oil of 0.25g, the star aniseed oil of 0.03g, the geraniol of 1.7g, the Geraniol of 0.3g, the phantol of 0.3g, the phenylethyl alcohol of 1.5g, the ethyl isobutyrate of 1g, the phenylethyl phenylacetate of 1.5g, the menthyl acetate of 0.3g, the Folium Ginkgo extract of 1g, the mango extract of 0.6g, the coffee extract of 0.4g, the Fructus Phyllanthi extract of 1g, the Fructus Mume extract of 1.4g, the red date medicinal extract of 0.7g, the fenugreek concrete of 0.03g, the Turkish tobaccos extract of 1.5g, the lactic acid of 0.05g, the phenylformic acid of 0.08g, the ketoisophorone of 0.04g, the Megastigmatrienone of 0.5g, the honey of 0.8g, the volume fraction of 52g is 70% ethanol, all the other are propylene glycol.Namely above-mentioned raw materials is evenly obtained Rose type essence 6 in container for stirring.Getting appropriate Rose type essence 6, to be dissolved in volume fraction be in 70% ethanolic soln, obtains the Rose type fragrance solution that massfraction is 60%, then it is evenly sprayed on the blank pipe tobacco of Yellow Crane Tower " heart is blue " Ms's cigarette, and rolls into cigarette.The addition of Rose type essence is 0.05% of pipe tobacco weight.
Embodiment 7
Take following raw material components (by 100g formula): the rose ethereal oil of 1.8g, the Flos Caryophylli oil of 0.28g, the star aniseed oil of 0.04g, the geraniol of 3g, the Geraniol of 0.2g, the phantol of 0.4g, the phenylethyl alcohol of 1.3g, the ethyl isobutyrate of 0.5g, the phenylethyl phenylacetate of 0.5g, the menthyl acetate of 0.2g, the Folium Ginkgo extract of 0.8g, the mango extract of 0.8g, the coffee extract of 0.5g, the Fructus Phyllanthi extract of 0.2g, the Fructus Mume extract of 1.2g, the red date medicinal extract of 0.5g, the fenugreek concrete of 0.05g, the Turkish tobaccos extract of 1.2g, the lactic acid of 0.08g, the phenylformic acid of 0.02g, the ketoisophorone of 0.03g, the Megastigmatrienone of 0.7g, the honey of 0.7g, the volume fraction of 48g is 70% ethanol, all the other are propylene glycol.Namely above-mentioned raw materials is evenly obtained Rose type essence 7 in container for stirring.Getting appropriate Rose type essence 7, to be dissolved in volume fraction be in 70% ethanolic soln, obtains the Rose type fragrance solution that massfraction is 40%, then it is evenly sprayed on the blank pipe tobacco of Yellow Crane Tower " heart is blue " Ms's cigarette, and rolls into cigarette.The addition of Rose type essence is 0.02% of pipe tobacco weight.
In embodiment 1 ~ 7, rose ethereal oil is by Rose through vacuum lyophilization process, after pulverizing and sieving, uses supercritical CO
2the essential oil product that abstraction technique prepares.
Folium Ginkgo extract, after being pulverized the Ginkgo Leaf that dries, uses the ethanolic soln of 50 ~ 80% to carry out refluxing extraction, more after filtration, the concentrated extract obtained.
Mango extract is by the pulp of mango after squeezing fragmentation, uses the ethanolic soln of 30 ~ 70% to carry out refluxing extraction, more after filtration, the concentrated extract obtained.
Coffee extract, after being pulverized by coffee, sieving, carries out refluxing extraction with the aqueous solution, more after filtration, the concentrated extract obtained.
Fructus Phyllanthi extract, after being pulverized by phyllanthus emblica, sieving, uses microwave extraction after spending the night by aqueous solution soaking, more after filtration, the concentrated extract obtained.
Fructus Mume extract carries out refluxing extraction after using the alcohol solution dipping of 40 ~ 75% to spend the night dry dark plum, more after filtration, the concentrated extract obtained.
Red date medicinal extract obtains red date powder particle by after dry red date pre-treatment, carries out ultrasonic extraction with after 50 ~ 70% alcohol solution dippings, then obtain red date medicinal extract through rotary evaporation is concentrated.
Fenugreek concrete be by trigonella seed through parch, pulverize after, carry out refluxing extraction with 60 ~ 80% ethanolic solns, more after filtration, concentrated obtain fenugreek concrete.
Turkish tobaccos extract is by Turkish tobaccos after chopping process, carries out refluxing extraction with 50 ~ 70% ethanolic solns, adopts the extract that molecular distillation technique prepares.
All the other raw materials used are commercially available.
Sensory evaluating smoking's effect of several plant natural extract:
Rose ethereal oil: feature rose suggestion, soft, fine and smooth flue gas, cigarette perfume is coordinated, and pleasant impression is comfortable.
Folium Ginkgo extract: enrich cigarette perfume (or spice), gas of being thoroughly fuming, increases sweet sense.
Mango extract: enrich cigarette perfume (or spice), reduce and stimulate, pleasant impression is comfortable, and flue gas is fine and smooth, soft.
Coffee extract: reducing throat stimulates, soft flue gas increases the sweet sense of flue gas.
Fructus Phyllanthi extract: improve the property sent out thoroughly, soft flue gas, slightly improves pleasant impression, slightly reduces stimulation.
Fructus Mume extract: soft flue gas, reducing throat stimulates, and increases flue gas concentration.
Red date medicinal extract: enrich cigarette perfume (or spice), improves the property sent out thoroughly, enrichment flue gas.
Fenugreek concrete: enrich cigarette perfume (or spice), slightly increase flue gas concentration, reduces and stimulates, cover assorted gas.
Turkish tobaccos extract: increase perfume quantity, improves flue gas concentration.
Sensory evaluating smoking's result shows: Rose type essence 1 ~ 7 can give Ms's cigarette graceful naturally rose characteristic perfume, have that flue gas exquisiteness is soft, comfortable taste, pleasant impression be clean, inhale taste alcohol and, the advantage such as the fragrant coordination of cigarette, the pungency that when effectively can alleviate suction, flue gas causes throat simultaneously, has potential harm reduction effect.
Claims (4)
1., for a Rose type essence for Ms's cigarette, it is mixed by following compositions in weight percentage: the rose ethereal oil of 1.0 ~ 2.5%, the Flos Caryophylli oil of 0.1 ~ 0.5%, the star aniseed oil of 0.01 ~ 0.1%, the geraniol of 1.5 ~ 3.0%, the Geraniol of 0.1 ~ 0.5%, the phantol of 0.2 ~ 0.5%, the phenylethyl alcohol of 0.5 ~ 1.5%, the ethyl isobutyrate of 0.1 ~ 1.0%, the phenylethyl phenylacetate of 0.2 ~ 1.5%, the menthyl acetate of 0.1 ~ 0.3%, the Folium Ginkgo extract of 0.5 ~ 1.0%, the mango extract of 0.1 ~ 1.0%, the coffee extract of 0.05 ~ 0.5%, the Fructus Phyllanthi extract of 0.1 ~ 1.0%, the Fructus Mume extract of 1.0 ~ 2.0%, the red date medicinal extract of 0.5 ~ 1.0%, the fenugreek concrete of 0.01 ~ 0.05%, 0.5 ~ 1.5% Turkish tobaccos extract, the lactic acid of 0.01 ~ 0.1%, the phenylformic acid of 0.02 ~ 0.08%, the ketoisophorone of 0.02 ~ 0.05%, the Megastigmatrienone of 0.5 ~ 1.0%, the honey of 0.5 ~ 1.0%, the ethanol of 40.0 ~ 60.0%, all the other are propylene glycol.
2., according to claim 1 for the Rose type essence of Ms's cigarette, it is characterized in that: it is mixed by following compositions in weight percentage: the rose ethereal oil of 1.5 ~ 2.0%, the Flos Caryophylli oil of 0.2 ~ 0.3%, the star aniseed oil of 0.01 ~ 0.05%, the geraniol of 1.5 ~ 2.5%, the Geraniol of 0.1 ~ 0.3%, the phantol of 0.2 ~ 0.5%, the phenylethyl alcohol of 0.5 ~ 1.0%, the ethyl isobutyrate of 0.1 ~ 0.5%, the phenylethyl phenylacetate of 0.5 ~ 1.0%, the menthyl acetate of 0.1 ~ 0.2%, the Folium Ginkgo extract of 0.7 ~ 1.0%, the mango extract of 0.5 ~ 1.0%, the coffee extract of 0.2 ~ 0.4%, the Fructus Phyllanthi extract of 0.2 ~ 0.8%, the Fructus Mume extract of 1.0 ~ 1.5%, the red date medicinal extract of 0.5 ~ 0.8%, the fenugreek concrete of 0.03 ~ 0.05%, the Turkish tobaccos extract of 0.6 ~ 1.2%, the lactic acid of 0.05 ~ 0.1%, the phenylformic acid of 0.03 ~ 0.06%, the ketoisophorone of 0.02 ~ 0.05%, the Megastigmatrienone of 0.5 ~ 0.7%, the honey of 0.6 ~ 0.8%, the ethanol of 45.0 ~ 55.0%, all the other are propylene glycol.
3. according to claim 1 or 2 for the Rose type essence of Ms's cigarette, it is characterized in that: described volume fraction of ethanol is 70%.
4. described in a claim 1 for the application of Rose type essence in Ms's cigarette of Ms's cigarette: it is characterized in that: comprise the following steps:
Taking Rose type essence is dissolved in volume fraction 70% ethanolic soln, obtain the Rose type fragrance solution that massfraction is 10 ~ 70%, then it is evenly sprayed on the blank pipe tobacco of Ms's cigarette, and rolls into cigarette, wherein, the addition of Rose type essence is 0.01 ~ 0.05% of pipe tobacco weight.
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