CN115595209B - Essence formula with rose characteristics, preparation method and application thereof - Google Patents
Essence formula with rose characteristics, preparation method and application thereof Download PDFInfo
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- CN115595209B CN115595209B CN202211361001.XA CN202211361001A CN115595209B CN 115595209 B CN115595209 B CN 115595209B CN 202211361001 A CN202211361001 A CN 202211361001A CN 115595209 B CN115595209 B CN 115595209B
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- 241000220317 Rosa Species 0.000 title claims abstract description 86
- 238000002360 preparation method Methods 0.000 title abstract description 7
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims abstract description 20
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 claims abstract description 20
- ZYEMGPIYFIJGTP-UHFFFAOYSA-N O-methyleugenol Chemical compound COC1=CC=C(CC=C)C=C1OC ZYEMGPIYFIJGTP-UHFFFAOYSA-N 0.000 claims abstract description 20
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 claims abstract description 20
- JOZKFWLRHCDGJA-UHFFFAOYSA-N citronellol acetate Chemical compound CC(=O)OCCC(C)CCC=C(C)C JOZKFWLRHCDGJA-UHFFFAOYSA-N 0.000 claims abstract description 20
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 claims abstract description 20
- FNAZRRHPUDJQCJ-UHFFFAOYSA-N henicosane Chemical compound CCCCCCCCCCCCCCCCCCCCC FNAZRRHPUDJQCJ-UHFFFAOYSA-N 0.000 claims abstract description 20
- NDJKXXJCMXVBJW-UHFFFAOYSA-N heptadecane Chemical compound CCCCCCCCCCCCCCCCC NDJKXXJCMXVBJW-UHFFFAOYSA-N 0.000 claims abstract description 20
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 20
- LQERIDTXQFOHKA-UHFFFAOYSA-N nonadecane Chemical compound CCCCCCCCCCCCCCCCCCC LQERIDTXQFOHKA-UHFFFAOYSA-N 0.000 claims abstract description 20
- FIGVVZUWCLSUEI-UHFFFAOYSA-N tricosane Chemical compound CCCCCCCCCCCCCCCCCCCCCCC FIGVVZUWCLSUEI-UHFFFAOYSA-N 0.000 claims abstract description 20
- CRDAMVZIKSXKFV-FBXUGWQNSA-N (2-cis,6-cis)-farnesol Chemical compound CC(C)=CCC\C(C)=C/CC\C(C)=C/CO CRDAMVZIKSXKFV-FBXUGWQNSA-N 0.000 claims abstract description 10
- 239000000260 (2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-ol Substances 0.000 claims abstract description 10
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 10
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 claims abstract description 10
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 10
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 claims abstract description 10
- JOZKFWLRHCDGJA-LLVKDONJSA-N Citronellyl acetate Natural products CC(=O)OCC[C@H](C)CCC=C(C)C JOZKFWLRHCDGJA-LLVKDONJSA-N 0.000 claims abstract description 10
- 239000005770 Eugenol Substances 0.000 claims abstract description 10
- 239000005792 Geraniol Substances 0.000 claims abstract description 10
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 claims abstract description 10
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 claims abstract description 10
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 claims abstract description 10
- 235000000484 citronellol Nutrition 0.000 claims abstract description 10
- 229960002217 eugenol Drugs 0.000 claims abstract description 10
- 229940043259 farnesol Drugs 0.000 claims abstract description 10
- 229930002886 farnesol Natural products 0.000 claims abstract description 10
- HIGQPQRQIQDZMP-UHFFFAOYSA-N geranil acetate Natural products CC(C)=CCCC(C)=CCOC(C)=O HIGQPQRQIQDZMP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229940113087 geraniol Drugs 0.000 claims abstract description 10
- HIGQPQRQIQDZMP-DHZHZOJOSA-N geranyl acetate Chemical compound CC(C)=CCC\C(C)=C\COC(C)=O HIGQPQRQIQDZMP-DHZHZOJOSA-N 0.000 claims abstract description 10
- 229930007744 linalool Natural products 0.000 claims abstract description 10
- 229940116837 methyleugenol Drugs 0.000 claims abstract description 10
- PRHTXAOWJQTLBO-UHFFFAOYSA-N methyleugenol Natural products COC1=CC=C(C(C)=C)C=C1OC PRHTXAOWJQTLBO-UHFFFAOYSA-N 0.000 claims abstract description 10
- CRDAMVZIKSXKFV-UHFFFAOYSA-N trans-Farnesol Natural products CC(C)=CCCC(C)=CCCC(C)=CCO CRDAMVZIKSXKFV-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims description 11
- 239000000796 flavoring agent Substances 0.000 claims description 10
- 235000019634 flavors Nutrition 0.000 claims description 10
- 241000208125 Nicotiana Species 0.000 claims description 7
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 7
- SKSLQVWNRUWRAQ-UHFFFAOYSA-N icosa-1,3,5,7,9-pentaene Chemical compound CCCCCCCCCCC=CC=CC=CC=CC=C SKSLQVWNRUWRAQ-UHFFFAOYSA-N 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 5
- YKNWIILGEFFOPE-UHFFFAOYSA-N pentacosane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCC YKNWIILGEFFOPE-UHFFFAOYSA-N 0.000 claims description 4
- 239000000341 volatile oil Substances 0.000 abstract description 25
- 235000019504 cigarettes Nutrition 0.000 abstract description 24
- 230000000694 effects Effects 0.000 abstract description 9
- 235000004789 Rosa xanthina Nutrition 0.000 abstract description 8
- 241000109329 Rosa xanthina Species 0.000 abstract description 8
- CBFCDTFDPHXCNY-UHFFFAOYSA-N icosane Chemical compound CCCCCCCCCCCCCCCCCCCC CBFCDTFDPHXCNY-UHFFFAOYSA-N 0.000 abstract description 4
- VAMFXQBUQXONLZ-UHFFFAOYSA-N n-alpha-eicosene Natural products CCCCCCCCCCCCCCCCCCC=C VAMFXQBUQXONLZ-UHFFFAOYSA-N 0.000 abstract description 2
- 239000003205 fragrance Substances 0.000 description 40
- 239000000779 smoke Substances 0.000 description 15
- 238000011156 evaluation Methods 0.000 description 6
- 239000002304 perfume Substances 0.000 description 6
- 235000009508 confectionery Nutrition 0.000 description 5
- 230000007794 irritation Effects 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- 230000001953 sensory effect Effects 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 206010013911 Dysgeusia Diseases 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 238000003908 quality control method Methods 0.000 description 3
- 235000013305 food Nutrition 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 235000011449 Rosa Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000010617 anise oil Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a formula of essence with rose characteristics, which comprises the following components in parts by mass: 1-5 parts of linalool; 1-3 parts of phenethyl alcohol; 40-65 parts of citronellol; 12-25 parts of geraniol; 0.5-3 parts of citronellyl acetate; 1-2 parts of eugenol; 0.5-2 parts of geranyl acetate; 2-4 parts of methyl eugenol; 1-7 parts of farnesol; 0.2-2 parts of n-heptadecane; 10-15 parts of n-nonadecane; 1-5 parts of n-heneicosane; 1-3 parts of n-tricosane; 0.5-2 parts of n-eicosane. The invention also discloses a preparation method and application of the essence formula with the characteristic of roses. The usage amount of the essence formula with the characteristic of the roses is only 0.5-3ppm when the essence formula is used for perfuming cigarettes, the aroma-enhancing effect is equivalent to that of the rose essential oil, and the use cost is greatly reduced.
Description
Technical Field
The invention belongs to the field of essence and spice and food flavoring, and particularly relates to a formula of essence with rose characteristics, a preparation method thereof and application of the essence with rose characteristics in tobacco.
Background
The rose fragrance has the characteristics of elegant and soft fragrance, fine fragrance, sweet taste and the like, and the essence with the rose characteristic fragrance is always favored by the market and is concerned by industrial enterprises. The rose essential oil is light yellow liquid obtained by extracting fresh rose flowers, has intense and durable rose fragrance, and is an important natural spice for highlighting the characteristic of the rose fragrance. The rose essential oil has very wide application in cigarette flavoring, can effectively improve the quality of smoke, endow the cigarettes with characteristic aroma such as flower aroma, sweet aroma and the like, improve the aftertaste and reduce miscellaneous gas and irritation.
However, the rose essential oil greatly limits the application of the rose essential oil in the market due to low yield, quality control, excessive price and the like. At present, researchers based on analysis data of chemical instruments, the prepared rose essence obviously lacks natural smell of natural roses, and the problems of heavy miscellaneous gas, increased irritation, uncoordinated aroma and the like can occur when the rose essence is applied to flavoring cigarettes. The rose essence for cigarettes with good use effect is added with natural perfume raw materials such as rose essential oil, for example, the rose essence for cigarettes described in Chinese patent No. CN102925289B, and natural perfume such as rose essential oil and anise oil are added, so that the quality control of the essence is affected by the quality difference of the natural perfume, and meanwhile, the preparation cost is increased.
The present invention has been made to solve the above problems.
Disclosure of Invention
The invention aims to provide a formula and application of a tobacco essence with rose fragrance, and the tobacco rose essence is prepared by using a modern analysis technology and sensory combination analysis method only by using a single fragrance raw material, so that the characteristics of improving smoke fragrance, improving aftertaste, reducing irritation and the like of rose essential oil are maintained, the preparation cost is greatly reduced, and the application limitation of the rose characteristic fragrance in cigarette flavoring is overcome.
The invention adopts the following technical scheme:
the invention discloses a formula of essence with rose characteristics, which comprises the following components in parts by mass: 1-5 parts of linalool; 1-3 parts of phenethyl alcohol; 40-65 parts of citronellol; 12-25 parts of geraniol; 0.5-3 parts of citronellyl acetate; 1-2 parts of eugenol; 0.5-2 parts of geranyl acetate; 2-4 parts of methyl eugenol; 1-7 parts of farnesol; 0.2-2 parts of n-heptadecane; 10-15 parts of n-nonadecane; 1-5 parts of n-heneicosane; 1-3 parts of n-tricosane; 0.5-2 parts of n-eicosane.
Preferably, the composition comprises the following components in parts by weight: 1.6 parts of linalool; 1.3 parts of phenethyl alcohol; 43.1 parts of citronellol; 20.2 parts of geraniol; 0.9 parts of citronellyl acetate; eugenol 1.2 parts; 1.7 parts of geranyl acetate; 3.2 parts of methyl eugenol; 1.7 parts of farnesol and 1.9 parts of n-heptadecane; 15.7 parts of n-nonadecane; 5.7 parts of n-heneicosane; 1.2 parts of n-tricosane; 0.5 part of n-eicosapentaene.
Preferably, the composition comprises the following components in parts by weight: 4 parts of linalool; 0.6 part of phenethyl alcohol; 63 parts of citronellol; 12.4 parts of geraniol; 2.9 parts of citronellyl acetate; eugenol 1.7 parts; 0.7 parts of geranyl acetate; 3 parts of methyl eugenol; 7 parts of farnesol and 0.1 part of n-heptadecane; 0.1 part of n-nonadecane; 1.4 parts of n-heneicosane; 2.3 parts of n-tricosane; 0.6 part of n-eicosapentaene.
The invention discloses a preparation method of the essence formula with the characteristic of roses, which is characterized in that linalool, phenethyl alcohol, citronellol, geraniol, citronellyl acetate, eugenol, geranyl acetate, methyl eugenol, farnesol, n-heptadecane, n-nonadecane, n-heneicosane, n-tricosane and n-pentacosane are weighed according to proportion, and are uniformly mixed and then placed in a shade place for more than one week, so that the essence formula with the characteristic of roses is obtained. The essence formula is prepared by mixing the ingredients according to the components, and then standing in a container at a shady and cool place for more than one week.
In a third aspect, the invention discloses the use of the rose-featured flavor formulation for tobacco with a rose-featured scent.
Preferably, the essence of the rose feature is added to tobacco in an amount of 0.5-3ppm.
Compared with the prior art, the invention has the remarkable advantages that:
1. the essence formula with the characteristic of the rose is characterized in that each component is an additive raw material allowed to be used in food, and essence products prepared by the components are safe and effective, so that the style characteristics of the rose essence and the stability of the product quality can be effectively ensured. Meanwhile, each component in the rose essence is the component reported to exist in the high-quality rose essential oil, so that the essence prepared based on the components effectively avoids the sense negative effect caused by non-rose natural perfume and chemical solvents on the basis of guaranteeing the fragrance and style of the rose.
2. The essence formula with the characteristic of the rose does not contain natural perfume raw materials such as the rose essential oil, avoids quality control difference caused by quality fluctuation of the natural perfume, and effectively reduces the cost (the cost of the essence formula with the characteristic of the rose is at least reduced by fifty times of the cost of the rose essential oil).
3. The essence formula with the characteristic of the roses is used in the cigarette flavoring at the ppm level, the dosage is small, the flavoring effect is obvious, and the adverse effect on cigarette smoke is avoided. The invention only utilizes the rose essence for cigarettes prepared from monomer fragrance raw materials, and realizes the flavoring effect of cigarettes similar to that of rose essential oil.
Drawings
Fig. 1 is a fragrance radar chart of the rose-featured flavor formulation of example 1 (rose No. 1 flavor) and the rose-featured flavor formulation of example 2 (rose No. two flavor).
Fig. 2 and 3 are schematic diagrams of smoke characteristics, comfort characteristics and smoke flavor changes of the blank cigarettes added with the rose essential oil, the essence formula of example 1 (rose first essence) and the essence formula of example 2 (rose second essence).
Detailed Description
The technical scheme of the present invention will be further described with reference to the specific embodiments, but the scope of the present invention is not limited thereto.
Example 1
The essence formula (rose first essence) with the rose characteristics in the embodiment comprises the following components in parts by weight:
1.6 parts of linalool; 1.3 parts of phenethyl alcohol; 43.1 parts of citronellol; 20.2 parts of geraniol; 0.9 parts of citronellyl acetate; eugenol 1.2 parts; 1.7 parts of geranyl acetate; 3.2 parts of methyl eugenol; 1.7 parts of farnesol and 1.9 parts of n-heptadecane; 15.7 parts of n-nonadecane; 5.7 parts of n-heneicosane; 1.2 parts of n-tricosane; 0.5 part of n-eicosapentaene.
The formula of the essence with the rose characteristics has elegant and soft rose characteristic fragrance, strong and pleasant fragrance, unobvious chemical smell and good natural feel. The fragrance radar chart of the essence formula with the rose characteristics is shown in fig. 1, and the essence formula radar chart shows obvious fragrance notes such as flower fragrance, sweet fragrance, faint scent and the like, has typical rose fragrance characteristics in sense, and has natural pleasant fragrance and pleasant feel.
Example 2
The essence formula (rose No. two essence) with the rose characteristics in the embodiment comprises the following components in parts by weight:
4 parts of linalool; 0.6 part of phenethyl alcohol; 63 parts of citronellol; 12.4 parts of geraniol; 2.9 parts of citronellyl acetate; eugenol 1.7 parts; 0.7 parts of geranyl acetate; 3 parts of methyl eugenol; 7 parts of farnesol and 0.1 part of n-heptadecane; 0.1 part of n-nonadecane; 1.4 parts of n-heneicosane; 2.3 parts of n-tricosane; 0.6 part of n-eicosapentaene.
The essence formula with the rose characteristics also has elegant and soft rose characteristic fragrance, strong and pleasant fragrance, unobvious chemical smell and good natural feel. The fragrance radar chart of the compound essence is shown in fig. 1, and compared with the essence described in the embodiment 1, the essence formula also has obvious main body fragrance of floral fragrance, sweet fragrance, faint scent and the like, has typical rose fragrance characteristics in sense, slightly differs in fragrance style, and has natural pleasant fragrance, so that people feel pleasant.
Example 3
The embodiment is the application and evaluation of the flavoring of the cigarette essence with the characteristic of rose fragrance.
The rose essential oil used as a comparative reference in this example was the damascene rose essential oil in bulgarica, purchased from Laboratory Bulgarska Rosa ltd (Sofia, bulgaria).
The cigarette flavoring method comprises the following steps: the absolute ethyl alcohol is used as a solvent to dilute the rose essential oil sample and the essence formula with the rose characteristics, and then a perfuming injector is used for perfuming the reference cigarettes. The sample of rose essential oil and the flavoring injection of the essence formula with the characteristic of the rose of the invention are all 1ppm.
Sensory evaluation method of cigarettes: the cigarette sensory evaluation group consists of 10 panelists with provincial panelists or more. Sensory evaluation is carried out on cigarettes from three aspects of comfort characteristics, smoke characteristics and aroma styles, and the final evaluation result of each index is the average value of scores given by 10 judges. Specific evaluation indexes and scores are as follows:
(1) The score ranges of the indexes of the smoke characteristics are-5 to 5 minutes, 0.5 minutes is a scoring unit, and the reference score is carried out by taking the reference blank cigarette as 0.
(2) The score range of each index of the comfort characteristic is-5 to 5 minutes, 0.5 is a scoring unit, and the control scoring is carried out by taking the reference blank cigarette as 0.
(3) The score range of the smoke flavor is 0-3 minutes, the score unit is 0.5 minutes, and the reference score is carried out by taking the reference blank cigarette as 0.
The smoke characteristics, comfort characteristics and smoke aroma changes of the rose essential oil, the first rose essence and the second rose essence are shown in fig. 2 and 3. As can be seen from fig. 2 and 3, in the aspect of smoke characteristics, the rose essential oil and the essence formula with the rose characteristics of the invention can improve the aroma quantity and aroma quality of cigarette smoke, reduce miscellaneous gas to a certain extent, improve the original smoke concentration of the cigarette, and the first rose essence and the second rose essence have more obvious improvement effects than the rose essential oil. In the aspect of comfort characteristics, after the rose essential oil or the formula of the rose characteristic essence disclosed by the invention is added, the hair penetration can be improved, the fine and soft sense is increased, the negative senses such as extra irritation and residues are not brought, and the improvement effect of the first rose essence and the second rose essence is more obvious than that of the rose essential oil. In the aspect of the change of the fragrance, the rose essence can obviously improve the fragrance, the sweet fragrance and the flower fragrance in the smoke, and compared with the rose essential oil, the fragrance of the rose-characteristic essence formula is similar, the fragrance of the flower fragrance and the sweet fragrance are similar as a whole, and the expression is better. The rose special essence not only maintains the characteristics of improving the smoke flavor of the rose essential oil, improving the aftertaste, reducing the irritation and the like, but also has more obvious effect; the cost of the essence formula with the characteristic of the roses is greatly lower than that of the rose essential oil, and the application limitation of the characteristic fragrance of the roses in flavoring cigarettes is overcome.
The foregoing is only used to describe the detailed embodiments of the present invention, but the technical solution of the present invention is not limited to the above-mentioned method. Equivalent modifications and variations of the proposed technique, which are known to those skilled in the art, are intended to be included within the scope of the claims of the present invention, without departing from the basic principles of the present technique.
Claims (5)
1. The essence composition with the rose characteristics is characterized by comprising the following components in parts by mass: 1.6 parts of linalool; 1.3 parts of phenethyl alcohol; 43.1 parts of citronellol; 20.2 parts of geraniol; 0.9 parts of citronellyl acetate; eugenol 1.2 parts; 1.7 parts of geranyl acetate; 3.2 parts of methyl eugenol; 1.7 parts of farnesol and 1.9 parts of n-heptadecane; 15.7 parts of n-nonadecane; 5.7 parts of n-heneicosane; 1.2 parts of n-tricosane; 0.5 part of n-eicosapentaene.
2. The essence composition with the rose characteristics is characterized by comprising the following components in parts by mass: 4 parts of linalool; 0.6 part of phenethyl alcohol; 63 parts of citronellol; 12.4 parts of geraniol; 2.9 parts of citronellyl acetate; eugenol 1.7 parts; 0.7 parts of geranyl acetate; 3 parts of methyl eugenol; 7 parts of farnesol and 0.1 part of n-heptadecane; 0.1 part of n-nonadecane; 1.4 parts of n-heneicosane; 2.3 parts of n-tricosane; 0.6 part of n-eicosapentaene.
3. The method for preparing the essence composition with the rose characteristics according to claim 1 or 2, wherein linalool, phenethyl alcohol, citronellol, geraniol, citronellyl acetate, eugenol, geranyl acetate, methyl eugenol, farnesol, n-heptadecane, n-nonadecane, n-heneicosane, n-tricosane and n-pentacosane are weighed according to proportion, and are placed in a shade place for more than one week after being uniformly mixed, so that the essence composition with the rose characteristics is obtained.
4. Use of a flavour composition with rose characteristics according to claim 1 or 2 for use in tobacco with rose characteristics.
5. The use according to claim 4, wherein the rose-distinctive flavour composition is added to tobacco in an amount of 0.5-3ppm.
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