CN116463171B - Essence for enhancing cigarette aroma and preparation method and application thereof - Google Patents
Essence for enhancing cigarette aroma and preparation method and application thereof Download PDFInfo
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- CN116463171B CN116463171B CN202310469274.4A CN202310469274A CN116463171B CN 116463171 B CN116463171 B CN 116463171B CN 202310469274 A CN202310469274 A CN 202310469274A CN 116463171 B CN116463171 B CN 116463171B
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 89
- 230000002708 enhancing effect Effects 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title abstract description 21
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 63
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 51
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 51
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical group CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 49
- 239000002904 solvent Substances 0.000 claims abstract description 49
- PPXUHEORWJQRHJ-UHFFFAOYSA-N ethyl isovalerate Chemical compound CCOC(=O)CC(C)C PPXUHEORWJQRHJ-UHFFFAOYSA-N 0.000 claims abstract description 42
- KQNPFQTWMSNSAP-UHFFFAOYSA-N isobutyric acid Chemical compound CC(C)C(O)=O KQNPFQTWMSNSAP-UHFFFAOYSA-N 0.000 claims abstract description 37
- DHKHKXVYLBGOIT-UHFFFAOYSA-N 1,1-Diethoxyethane Chemical compound CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 claims abstract description 36
- PHTQWCKDNZKARW-UHFFFAOYSA-N isoamylol Chemical compound CC(C)CCO PHTQWCKDNZKARW-UHFFFAOYSA-N 0.000 claims abstract description 34
- IAEGWXHKWJGQAZ-UHFFFAOYSA-N trimethylpyrazine Chemical compound CC1=CN=C(C)C(C)=N1 IAEGWXHKWJGQAZ-UHFFFAOYSA-N 0.000 claims abstract description 31
- KVFIJIWMDBAGDP-UHFFFAOYSA-N ethylpyrazine Chemical compound CCC1=CN=CC=N1 KVFIJIWMDBAGDP-UHFFFAOYSA-N 0.000 claims abstract description 30
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims abstract description 28
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims abstract description 28
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000003205 fragrance Substances 0.000 claims abstract description 20
- SPEUIVXLLWOEMJ-UHFFFAOYSA-N acetaldehyde dimethyl acetal Natural products COC(C)OC SPEUIVXLLWOEMJ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000001803 2-(ethoxymethyl)pyrazine Substances 0.000 claims abstract description 17
- MMKWCKGYULOKET-UHFFFAOYSA-N 2-Ethoxy-3-methylpyrazine Chemical compound CCOC1=NC=CN=C1C MMKWCKGYULOKET-UHFFFAOYSA-N 0.000 claims abstract description 17
- PPPFFGVGWFKTHX-UHFFFAOYSA-N 2-Methyl-(3 or 5 or 6)-(methylthio)pyrazine (mixture of isomers) Chemical compound CSC1=NC=CN=C1C PPPFFGVGWFKTHX-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000001795 2-methyl-3-methylsulfanylpyrazine Substances 0.000 claims abstract description 17
- UJNOLBSYLSYIBM-WISYIIOYSA-N [(1r,2s,5r)-5-methyl-2-propan-2-ylcyclohexyl] (2r)-2-hydroxypropanoate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(=O)[C@@H](C)O UJNOLBSYLSYIBM-WISYIIOYSA-N 0.000 claims abstract description 17
- 239000000796 flavoring agent Substances 0.000 claims abstract description 17
- 235000019634 flavors Nutrition 0.000 claims abstract description 17
- RTNPCOBSXBGDMO-ARJAWSKDSA-N (Z)-non-6-enal Chemical compound CC\C=C/CCCCC=O RTNPCOBSXBGDMO-ARJAWSKDSA-N 0.000 claims abstract description 16
- GXANMBISFKBPEX-ARJAWSKDSA-N cis-3-hexenal Chemical compound CC\C=C/CC=O GXANMBISFKBPEX-ARJAWSKDSA-N 0.000 claims abstract description 16
- GXANMBISFKBPEX-UHFFFAOYSA-N hex-3c-enal Natural products CCC=CCC=O GXANMBISFKBPEX-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 14
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 14
- 239000010634 clove oil Substances 0.000 claims abstract description 14
- 229930007744 linalool Natural products 0.000 claims abstract description 14
- FKUPPRZPSYCDRS-UHFFFAOYSA-N Cyclopentadecanolide Chemical compound O=C1CCCCCCCCCCCCCCO1 FKUPPRZPSYCDRS-UHFFFAOYSA-N 0.000 claims abstract description 12
- 150000001299 aldehydes Chemical class 0.000 claims abstract description 4
- 238000002156 mixing Methods 0.000 claims description 45
- 241000208125 Nicotiana Species 0.000 claims description 34
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 34
- 239000000203 mixture Substances 0.000 claims description 33
- 238000003756 stirring Methods 0.000 claims description 24
- 238000000034 method Methods 0.000 claims description 20
- FFVHXGZXDRXFLQ-UHFFFAOYSA-N cyclopentadecanol Chemical compound OC1CCCCCCCCCCCCCC1 FFVHXGZXDRXFLQ-UHFFFAOYSA-N 0.000 claims description 18
- 239000002304 perfume Substances 0.000 claims description 14
- ZRSNZINYAWTAHE-UHFFFAOYSA-N p-methoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C=C1 ZRSNZINYAWTAHE-UHFFFAOYSA-N 0.000 claims description 11
- 238000005303 weighing Methods 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 4
- 239000003085 diluting agent Substances 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 239000000243 solution Substances 0.000 claims 6
- 239000012895 dilution Substances 0.000 claims 1
- 238000010790 dilution Methods 0.000 claims 1
- 239000000686 essence Substances 0.000 description 75
- 230000000052 comparative effect Effects 0.000 description 17
- 230000001953 sensory effect Effects 0.000 description 16
- 238000011156 evaluation Methods 0.000 description 13
- 239000000779 smoke Substances 0.000 description 13
- 230000000694 effects Effects 0.000 description 12
- 238000012360 testing method Methods 0.000 description 8
- 239000007789 gas Substances 0.000 description 7
- 230000007794 irritation Effects 0.000 description 7
- 206010013911 Dysgeusia Diseases 0.000 description 5
- KYQCOXFCLRTKLS-UHFFFAOYSA-N Pyrazine Chemical compound C1=CN=CC=N1 KYQCOXFCLRTKLS-UHFFFAOYSA-N 0.000 description 4
- 239000008368 mint flavor Substances 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- 230000002195 synergetic effect Effects 0.000 description 4
- PCNDJXKNXGMECE-UHFFFAOYSA-N Phenazine Natural products C1=CC=CC2=NC3=CC=CC=C3N=C21 PCNDJXKNXGMECE-UHFFFAOYSA-N 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- -1 pyrazine compound Chemical class 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 230000001603 reducing effect Effects 0.000 description 3
- 210000000697 sensory organ Anatomy 0.000 description 3
- 235000019640 taste Nutrition 0.000 description 3
- YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical group O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 description 2
- 235000019606 astringent taste Nutrition 0.000 description 2
- 235000019658 bitter taste Nutrition 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 230000000873 masking effect Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 150000003216 pyrazines Chemical class 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 description 1
- OXQOBQJCDNLAPO-UHFFFAOYSA-N 2,3-Dimethylpyrazine Chemical class CC1=NC=CN=C1C OXQOBQJCDNLAPO-UHFFFAOYSA-N 0.000 description 1
- FINHMKGKINIASC-UHFFFAOYSA-N Tetramethylpyrazine Chemical class CC1=NC(C)=C(C)N=C1C FINHMKGKINIASC-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- CAWHJQAVHZEVTJ-UHFFFAOYSA-N methylpyrazine Chemical class CC1=CN=CC=N1 CAWHJQAVHZEVTJ-UHFFFAOYSA-N 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 210000003928 nasal cavity Anatomy 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings
- C11B9/0046—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings
- C11B9/0049—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms
- C11B9/0053—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms both rings being six-membered
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0092—Heterocyclic compounds containing only N as heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention relates to an essence for enhancing cigarette aroma and a preparation method and application thereof, wherein the essence for cigarettes comprises 2-ethyl pyrazine, 2,3, 5-trimethyl pyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methyl pyrazine, cis-3-hexenal, cis-6-nonenal, acetaldehyde diethyl acetal, cyclopentadecanolide, menthyl lactate, anisyl aldehyde, clove oil, isobutyric acid, dodecanoic acid, phenethyl alcohol, isoamyl alcohol, linalool, ethyl isovalerate, ethyl acetate and a solvent, and the solvent is ethanol, propylene glycol and glycerol with a mass ratio of 6-12:2-6:1-3. The essence of the invention has rich fragrance, the compatibility of the formula is high, the fragrance of each component is fully reserved through a specific solvent, and the essence is especially suitable for enhancing the fragrance of cigarettes, and can mask bad miscellaneous flavor and enhance eating.
Description
Technical Field
The invention belongs to the technical field of essence and spice, and particularly relates to an essence for enhancing cigarette aroma, a preparation method and application thereof.
Background
The traditional tobacco products are applied to a large number of cases of low purity, insufficient fragrance and insufficient alcohol and are easy to leave dry and astringent taste feeling for consumers and have unpleasant residual taste, so that the flavoring of cigarettes is one of important links in the production of cigarettes, and the cigarettes are endowed with certain fragrance style through essence, meanwhile, the adverse effects of reducing irritation, residue and the like are achieved, and the quality of the cigarettes is improved. The essence for cigarettes is prepared from a plurality of monomers or synthetic perfume raw materials, has a certain perfume type, can be directly or indirectly used for perfuming mixture of cigarettes, and can endow different styles to cigarette smoke, for example, the concentration of the smoke can be increased, the smoke effect can be improved, the smoke quality can be improved, and the richness of the smoke can be effectively improved. At present, in the application of cigarette flavoring, the natural extract with the aroma style is widely applied to the cigarette flavoring. However, the quality of the essence prepared from the natural extract is greatly fluctuated due to the interference of a plurality of factors, such as the restrictions and influences of raw material varieties, planting conditions, environmental factors and the like, and the fluctuation of the quality can greatly influence the end product. The tobacco essence prepared by the synthetic perfume has the advantages of low cost, safety, large yield and the like, along with the rapid increase of market demands, the natural perfume source is limited, the synthetic perfume is continuously enlarged under the condition that the market demands cannot be fully met, more importantly, the synthetic perfume product is multiple in structure and various in variety, the requirement of differentiated blending of the perfume product is better met, for example, chinese patent CN115505458A discloses a tobacco nut perfume, the perfume comprises methyl pyrazine compounds, dimethyl pyrazine compounds, trimethyl pyrazine compounds and tetramethyl pyrazine compounds, the pyrazine compounds are taken as main perfume sources, raw materials are simple and easy to obtain, the cost is low, the perfume feeling of tobacco smoke can be obviously improved, but the tobacco perfume has poorer irritation reducing effect on the smoke, the perfume is single, the synergistic effect of other additive components is difficult to determine, and the application has great limitation. Chinese patent CN115322832A discloses a cool flavor, tobacco sheets and non-combustible cigarettes, the patent technology adopts a synergistic effect which accords with a sweetener and has a certain effect on mint flavor, the edible cool flavor is well coordinated with smoke, the miscellaneous gas of tobacco shreds can be well covered, the bitter taste and taste of the mint flavor are greatly reduced by the flavor formula, the smoking experience is improved, the flavor of the flavor formula is single, the cool flavor is mainly generated, the richness of the flavor of the smoke is insufficient, and the mint flavor easily covers other flavors, so that the compatibility of the flavor formula and other flavor components is difficult to coordinate, the rich cigarette flavor cannot be achieved, and the irritation of the smoke can be reduced.
Therefore, aiming at the defects of the prior art, the tobacco essence with rich layers is developed, and simultaneously, the tobacco essence can have good coordination effect with smoke, obviously improve the irritation of the smoke, keep the fragrance lasting, and has a certain significance to the field of cigarettes.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides the essence for enhancing the fragrance of cigarettes, and the preparation method and application thereof.
In a first aspect, the present invention provides a flavour enhancement for cigarettes, the flavour composition for cigarettes comprising 2-ethylpyrazine, 2,3, 5-trimethylpyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methylpyrazine, cis-3-hexenal, cis-6-nonenal, acetaldehyde diethyl acetal, cyclopentadecanolide, menthyl lactate, anisyl aldehyde, clove oil, isobutyric acid, dodecanoic acid, phenethyl alcohol, isoamyl alcohol, linalool, ethyl isovalerate, ethyl acetate and a solvent;
the solvent is a mixture of ethanol, propylene glycol and glycerol.
Further, the essence for cigarettes comprises, by mass, 0.1-0.6 part of 2-ethylpyrazine, 0.4-1 part of 2,3, 5-trimethylpyrazine, 0.1-2 parts of 2-methyl-3- (methylthio) pyrazine, 0.1-1 part of 2-ethoxy-3-methylpyrazine, 0.1-2 parts of cis-3-hexenal, 0.1-3 parts of cis-6-nonenal, 0.1-1 part of acetaldehyde diethyl acetal, 0.2-2 parts of cyclopentadecanolide, 0.5-5 parts of menthyl lactate, 0.1-2 parts of anisic aldehyde, 0.5-2 parts of clove oil, 0.2-2 parts of isobutyric acid, 0.1-1 part of dodecanoic acid, 0.1-0.8 part of phenethyl alcohol, 0.5-2 parts of isoamyl alcohol, 0.5-5 parts of linalool, 0.1-2 parts of ethyl isovalerate, 0.1-1 part of ethyl acetate and 15-85 parts of solvent.
Further, the mass ratio of the ethanol to the propylene glycol to the glycerol is (6-12): 2-6): 1-3.
Further, the mass addition amount of the essence for the cigarettes is 0.01-2% of the mass of the tobacco shreds.
Further, the flavour comprises a solid, liquid or semi-solid form.
In a second aspect, the invention also provides a preparation method of the essence for enhancing the aroma of cigarettes, which comprises the following steps:
s1, premix A
Weighing 2-ethylpyrazine, 2,3, 5-trimethylpyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methylpyrazine, acetaldehyde diethyl acetal and isoamyl alcohol, and mixing with 1/3 parts by mass of solvent, and stirring until a uniform solution is formed;
s2, premix B
Mixing menthyl lactate, isobutyric acid and 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s3, premix C
Mixing cis-3-hexenal, cis-6-nonenal, cyclopentadecanol, anisic aldehyde, clove oil, dodecanoic acid, phenethyl alcohol and linalool with 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s4, final mixing
And mixing the premix A with the premix C, adding ethyl isovalerate and ethyl acetate, and finally adding the premix B to obtain the essence for enhancing the fragrance of cigarettes.
Further, the essence for cigarettes comprises, by mass, 0.1-0.6 part of 2-ethylpyrazine, 0.4-1 part of 2,3, 5-trimethylpyrazine, 0.1-2 parts of 2-methyl-3- (methylthio) pyrazine, 0.1-1 part of 2-ethoxy-3-methylpyrazine, 0.1-2 parts of cis-3-hexenal, 0.1-3 parts of cis-6-nonenal, 0.1-1 part of acetaldehyde diethyl acetal, 0.2-2 parts of cyclopentadecanolide, 0.5-5 parts of menthyl lactate, 0.1-2 parts of anisic aldehyde, 0.5-2 parts of clove oil, 0.2-2 parts of isobutyric acid, 0.1-1 part of dodecanoic acid, 0.1-0.8 part of phenethyl alcohol, 0.5-2 parts of isoamyl alcohol, 0.5-5 parts of linalool, 0.1-2 parts of ethyl isovalerate, 0.1-1 part of ethyl acetate and 15-85 parts of solvent.
Further, the solvent is a mixture of ethanol, propylene glycol and glycerol in the mass ratio of (6-12) (2-6) (1-3).
In a third aspect, the invention also provides a use method of the essence for enhancing the aroma of cigarettes, and the use method comprises the step of applying the prepared essence to tobacco shreds.
The invention also provides a preferred use method of the essence for enhancing the fragrance of cigarettes, which comprises the following steps:
s1, premix A
Weighing 2-ethylpyrazine, 2,3, 5-trimethylpyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methylpyrazine, acetaldehyde diethyl acetal and isoamyl alcohol, and mixing with 1/3 parts by mass of solvent, and stirring until a uniform solution is formed;
s2, premix B
Mixing menthyl lactate, isobutyric acid and 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s3, premix C
Mixing cis-3-hexenal, cis-6-nonenal, cyclopentadecanol, anisic aldehyde, clove oil, dodecanoic acid, phenethyl alcohol and linalool with 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s4, final mixing
And mixing the premix A with the premix C, adding ethyl isovalerate and ethyl acetate, then applying the mixture to tobacco shreds, and finally applying the premix B to the tobacco shreds.
According to the form of the essence, the use method including but not limited to spraying, soaking and the like can be adopted in the use process.
Further, the essence can be selectively diluted or not diluted in the using method, the diluent adopted by the essence in the using method is a mixture of ethanol, propylene glycol and glycerol, and the mass ratio of the ethanol to the propylene glycol to the glycerol is (6-12): 2-6): 1-3.
Compared with the prior art, the invention has the following beneficial effects:
(1) The essence for enhancing the aroma of the cigarettes provided by the invention contains rich ingredients and contains pyrazine, aldehydes, esters, alcohols and other compounds, and the prepared essence has rich, plump and fine aroma, including nut, flower aroma and fruit aroma, and is used in the cigarettes, so that good experience is obtained in the smoking process of the cigarettes.
(2) The essence for enhancing the aroma of the cigarettes provided by the invention can mask miscellaneous gases in the cigarettes but retain the aroma of the essence, and the appropriate solvent is adopted to fully exert the aroma components in the essence, so that the irritation of the cigarettes is obviously reduced, and the bad aftertaste is reduced.
(3) The essence for enhancing the aroma of the cigarettes is suitable for being added into the cigarettes at one time, and meanwhile, the effect of the essence can be fully exerted through stepwise addition.
Detailed Description
The experimental methods of the present invention, in which specific conditions are not specified in the following examples, are generally conducted under conventional conditions or under conditions recommended by the manufacturer. The various chemicals commonly used in the examples are commercially available.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention.
The terms "comprising" and "having" and any variations thereof, are intended to cover a non-exclusive inclusion. For example, a process, method, apparatus, article, or device that comprises a list of steps is not limited to the elements or modules listed but may alternatively include additional steps not listed or inherent to such process, method, article, or device.
The present invention will be further described in detail with reference to the following embodiments, in order to make the objects, technical solutions and advantages of the present invention more apparent. It should be understood that the description is only illustrative and is not intended to limit the scope of the invention. In addition, in the following description, descriptions of well-known structures and techniques are omitted so as not to unnecessarily obscure the present invention.
The invention is further illustrated by the following examples, which are not intended to limit the scope of the invention.
Example 1 preparation of essence for enhancing aroma of cigarette
The specific composition formula of the essence for enhancing the aroma of cigarettes prepared in the embodiment is shown in table 1;
table 1:
the solvents in table 1 are ethanol, propylene glycol and glycerol mixtures in a mass ratio of 6:2:1;
the preparation method adopts the composition formula of the essence, and comprises the following specific steps:
s1, premix A
Weighing 2-ethylpyrazine, 2,3, 5-trimethylpyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methylpyrazine, acetaldehyde diethyl acetal and isoamyl alcohol, and mixing with 1/3 parts by mass of solvent, and stirring until a uniform solution is formed;
s2, premix B
Mixing menthyl lactate, isobutyric acid and 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s3, premix C
Mixing cis-3-hexenal, cis-6-nonenal, cyclopentadecanol, anisic aldehyde, clove oil, dodecanoic acid, phenethyl alcohol and linalool with 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s4, final mixing
And mixing the premix A with the premix C, adding ethyl isovalerate and ethyl acetate, and finally adding the premix B to obtain the essence for enhancing the fragrance of cigarettes.
Example 2 preparation of essence for enhancing aroma of cigarette
The specific composition formula of the essence for enhancing the aroma of cigarettes prepared in the embodiment is shown in table 2;
table 2:
the solvents in table 2 are ethanol, propylene glycol and glycerol mixtures in a mass ratio of 10:6:1;
the preparation method adopts the composition formula of the essence, and comprises the following specific steps:
s1, premix A
Weighing 2-ethylpyrazine, 2,3, 5-trimethylpyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methylpyrazine, acetaldehyde diethyl acetal and isoamyl alcohol, and mixing with 1/3 parts by mass of solvent, and stirring until a uniform solution is formed;
s2, premix B
Mixing menthyl lactate, isobutyric acid and 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s3, premix C
Mixing cis-3-hexenal, cis-6-nonenal, cyclopentadecanol, anisic aldehyde, clove oil, dodecanoic acid, phenethyl alcohol and linalool with 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s4, final mixing
And mixing the premix A with the premix C, adding ethyl isovalerate and ethyl acetate, and finally adding the premix B to obtain the essence for enhancing the fragrance of cigarettes.
Example 3 preparation of essence for enhancing aroma of cigarette
The specific composition formula of the essence for enhancing the aroma of cigarettes prepared in the embodiment is shown in table 3;
table 3:
the solvents in table 3 are ethanol, propylene glycol and glycerol mixtures in a mass ratio of 6:6:1;
the preparation method adopts the composition formula of the essence, and comprises the following specific steps:
s1, premix A
Weighing 2-ethylpyrazine, 2,3, 5-trimethylpyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methylpyrazine, acetaldehyde diethyl acetal and isoamyl alcohol, and mixing with 1/3 parts by mass of solvent, and stirring until a uniform solution is formed;
s2, premix B
Mixing menthyl lactate, isobutyric acid and 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s3, premix C
Mixing cis-3-hexenal, cis-6-nonenal, cyclopentadecanol, anisic aldehyde, clove oil, dodecanoic acid, phenethyl alcohol and linalool with 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s4, final mixing
And mixing the premix A with the premix C, adding ethyl isovalerate and ethyl acetate, and finally adding the premix B to obtain the essence for enhancing the fragrance of cigarettes.
Example 4 preparation of essence for enhancing aroma of cigarette
The specific composition formula of the essence for enhancing the aroma of cigarettes prepared in the embodiment is shown in table 4;
table 4:
the solvents in table 4 are ethanol, propylene glycol, and glycerol mixtures in a mass ratio of 12:1:3;
the preparation method adopts the composition formula of the essence, and comprises the following specific steps:
s1, premix A
Weighing 2-ethylpyrazine, 2,3, 5-trimethylpyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methylpyrazine, acetaldehyde diethyl acetal and isoamyl alcohol, and mixing with 1/3 parts by mass of solvent, and stirring until a uniform solution is formed;
s2, premix B
Mixing menthyl lactate, isobutyric acid and 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s3, premix C
Mixing cis-3-hexenal, cis-6-nonenal, cyclopentadecanol, anisic aldehyde, clove oil, dodecanoic acid, phenethyl alcohol and linalool with 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s4, final mixing
And mixing the premix A with the premix C, adding ethyl isovalerate and ethyl acetate, and finally adding the premix B to obtain the essence for enhancing the fragrance of cigarettes.
Test example one, effect of the essence of the invention on the sensory quality of cigarettes
The essence for enhancing the aroma of the cigarettes prepared in examples 1-4 is directly sprayed on tobacco shreds, the adding amount of the essence is 1% of the mass of the tobacco shreds, cigarettes without the essence are taken as blank groups, 10 volunteers with normal senses are collected to form an evaluation group, the sensory quality of the cigarettes is evaluated according to GB 5606.4-2005, evaluation indexes comprise aroma, harmony, miscellaneous gases, irritation and aftertaste, the total evaluation is 100 points, and specific evaluation results are shown in Table 5;
TABLE 5
The essence for enhancing the aroma of the cigarettes prepared in the embodiments 1-4 is used in the cigarettes, has plump and rich aroma, mainly contains nut, flower aroma and fruit aroma, can mask bad miscellaneous gases of the cigarettes, and meanwhile, the emitted mint flavor does not mask other aroma, has no bitter and astringent taste, good taste, fine obtained aroma and high harmony, has no irritation, and the result in Table 5 shows that the cigarette feel mass fraction of the embodiments 1-4 is 89.80-97.80, belongs to monovalent classes, and the cigarettes of the embodiments 1-2 have pure and comfortable aftertaste, wherein the embodiment 2 has the best effect.
The essence formulation for enhancing the aroma of the cigarettes in examples 1 to 4 is prepared by mixing premix A with premix C, adding ethyl isovalerate and ethyl acetate, applying the mixture to tobacco shreds, applying premix B to the tobacco shreds, collecting 10 volunteers with normal sense organs to form an evaluation group, evaluating the sense organ quality of the cigarettes according to GB 5606.4-2005, and evaluating the sense organ quality of the obtained cigarettes, wherein the total addition amount of the essence is 1% of the mass of the tobacco shreds, and the result is shown in Table 6;
TABLE 6
As can be seen from the combination of tables 5 and 6, the essence for enhancing the fragrance of the cigarettes prepared by the method has a great influence on the sensory effect of the cigarettes by adopting different spraying steps, wherein the sensory effect of the cigarettes obtained by adopting a mode of adding premix step by step is better.
Test example II, effect of the essence of the invention on the sensory comfort of cigarettes
The essence formulation for enhancing the aroma of cigarettes in examples 1-4 is prepared by mixing premix A with premix C, adding ethyl isovalerate and ethyl acetate, spraying the mixture on tobacco shreds, and finally applying premix B to the tobacco shreds, wherein the total adding amount of the essence is 1% of the mass of the tobacco shreds, evaluating the sensory comfort of the cigarettes according to YC/T496-2014 industry standard, and collecting 10 volunteers with normal senses to form an evaluation group, wherein the evaluation indexes comprise:
(1) The feeling of the mouth, throat, nasal cavity and smoke is realized;
(2) Judging the index grade of the sour, sweet and bitter;
the specific evaluation results are shown in Table 7;
TABLE 7
As can be seen from the results in table 7, the sensory comfort of the tobacco essence for enhancing the aroma of cigarettes prepared by the invention is remarkably improved compared with that of a blank group, wherein the tobacco essence is prepared by taking example 2 as the optimal essence formula.
Comparative example 1
The difference from example 2 is that 2-ethoxy-3-methylpyrazine and acetaldehyde diethyl acetal are not added, and 2-methyl-3- (methylthio) pyrazine is used to make up to 1.9 parts, and the remaining components and preparation steps are identical.
Comparative example 2
The difference from example 2 was that 2-methyl-3- (methylthio) pyrazine was not added, 2-ethoxy-3-methylpyrazine was used to make up to 0.9 part, acetaldehyde diethyl acetal was added in an amount of 1.4 parts, isoamyl alcohol was added in an amount of 0.1 part, and the remaining components and preparation steps were identical.
Comparative example 3
The difference from example 2 is that menthyl lactate is added in an amount of 0.1 part, isobutyric acid is added in an amount of 1.2 parts, and the remaining components and the preparation steps are identical.
Comparative example 4
The difference from example 2 is that the substitution of isobutyric acid with leaf alcohol isobutyrate was added in an amount of 0.3 parts, the remaining components and the preparation steps were identical.
Comparative example 5
The difference from example 2 is that cis-3-hexenal was not added, and cis-6-nonenal was used in an amount of 2.8 parts, and the remaining components and the preparation steps were identical.
Comparative example 6
The difference from example 2 is that cyclopentadecanolide is replaced with gamma-butyrolactone, the remaining components and preparation steps being identical.
Comparative example 7
The difference from example 2 is that ethyl isovalerate and ethyl acetate are not added, the solvent is used for supplementing, and the rest components and the preparation steps are identical.
Influence of the essence prepared in test example III and comparative examples 1 to 7 on the sensory quality of cigarettes
According to the first judging mode of the test example, the essence formulas prepared in the comparative examples 1-7 are respectively prepared by mixing premix A with premix C, adding ethyl isovalerate and ethyl acetate (the step of the comparative example 7 is added with a solvent, namely, a mixture of ethanol, propylene glycol and glycerol with the mass ratio of 12:1:3), then applying the mixture to tobacco shreds, finally applying premix B to the tobacco shreds, wherein the total adding amount of the essence is 1% of the mass of the tobacco shreds, and carrying out sensory quality judgment on the obtained cigarettes, wherein the result is shown in Table 8;
TABLE 8
The comparison results show that the essences prepared in comparative examples 1 to 7 are used for reducing the sensory quality obtained in cigarettes compared with examples 1 and 2, wherein the reduction is more remarkable in comparative examples 3 to 6, and the synergistic effect of menthyl lactate and isobutyric acid can be used for covering the effect of most of miscellaneous gases in cigarettes in combination with the essence formulas in comparative examples 1 to 7, and the fragrance of cigarettes is fine, smooth and rich, and the aftertaste is pure and comfortable in the specific proportion range of the menthyl lactate and isobutyric acid; the cis-3-hexenal and cis-6-nonenal also have better effect on masking and stimulating miscellaneous gases in cigarettes, and the aftertaste is pure and comfortable; the 2-ethyl pyrazine, 2,3, 5-trimethyl pyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methyl pyrazine, acetaldehyde diethyl acetal and isoamyl alcohol in the pyrazine compound have better synergistic effect, the fragrance of the pyrazine compound can be fully exerted, and the nut fragrance is further enhanced through the acetaldehyde diethyl acetal and the isoamyl alcohol; in addition, the ethyl isovalerate and the ethyl acetate have certain action and effect on the emission of fragrance and the masking of miscellaneous gases.
Influence of essence prepared in test example IV and comparative examples 1 to 7 on sensory and organoleptic comfort of cigarettes
(3) According to the evaluation mode consistent with the second evaluation mode of the test example, the essence formulas of the comparative examples 1-7 are prepared by firstly mixing premix A with premix C, adding ethyl isovalerate and ethyl acetate, spraying the mixture on tobacco shreds, finally applying premix B on the tobacco shreds, wherein the total addition amount of the essence is 1% of the mass of the tobacco shreds, evaluating the sensory comfort of cigarettes according to YC/T496-2014 industry standard, collecting 10 volunteers with normal senses to form an evaluation group, and the specific evaluation results are shown in Table 9;
TABLE 9
Comparative examples 8 to 11
The difference from example 2 is that the solvent composition in the flavour formulation is different, as shown in table 10;
table 10
Test example five, influence of solvent in essence on sensory quality of cigarette
According to the first evaluation mode of the test example, the essence formulas prepared in the comparative examples 8-11 are respectively prepared by mixing premix A with premix C, adding ethyl isovalerate and ethyl acetate, then applying the mixture to tobacco shreds, finally applying premix B to the tobacco shreds, wherein the total adding amount of the essence is 1% of the mass of the tobacco shreds, and performing sensory quality evaluation on the obtained cigarettes, wherein the result is shown in Table 11;
TABLE 11
As can be seen from the comparison of the results in Table 6 and Table 11, the solvent component in the essence has a larger influence on the sensory quality of cigarettes, wherein the solvent obtained by adopting the mode of compounding ethanol, propylene glycol and glycerol has a better promotion effect on the volatility of the aroma component in the essence formula, and the composition and proportion of the solvent have a larger influence on the volatility component in the essence because the solvent occupies a larger specific gravity in the essence component, including the stability of pyrazine compounds, aldehyde compounds and the like, and further have a larger difference on the sensory quality of the essence when the essence acts on cigarettes, and the mixed solvent of ethanol, propylene glycol and glycerol has the mass ratio of (6-12): (2-6): (1-3) ensures that the prepared essence plays the best role in cigarettes.
It should be noted that, in the present specification, specific features, structures, materials, or characteristics may be arbitrarily combined, and in order to simplify the description, all possible combinations of the features in the foregoing embodiments are not described, and those skilled in the art may combine and combine the features of the different embodiments and the different embodiments described in the present specification without contradiction.
The above examples illustrate only a few embodiments of the invention, which are described in detail and are not to be construed as limiting the scope of the invention. It should be noted that it will be apparent to those skilled in the art that several variations and modifications can be made without departing from the spirit of the invention, which are all within the scope of the invention. Accordingly, the scope of protection of the present invention is to be determined by the appended claims.
Claims (9)
1. The essence for enhancing the fragrance of the cigarettes is characterized by comprising, by mass, 0.1-0.6 part of 2-ethylpyrazine, 0.4-1 part of 2,3, 5-trimethylpyrazine, 0.1-2 parts of 2-methyl-3- (methylthio) pyrazine, 0.1-1 part of 2-ethoxy-3-methylpyrazine, 0.1-2 parts of cis-3-hexenal, 0.1-3 parts of cis-6-nonenal, 0.1-1 part of acetaldehyde diethyl acetal, 0.2-2 parts of cyclopentadecanolide, 0.5-5 parts of menthyl lactate, 0.1-2 parts of anisic aldehyde, 0.5-2 parts of clove oil, 0.2-2 parts of isobutyric acid, 0.1-1 part of dodecanoic acid, 0.1-0.8 part of phenethyl alcohol, 0.5-2 parts of isoamyl alcohol, 0.5-5 parts of linalool, 0.1-2 parts of ethyl isovalerate, 0.1-2 parts of ethyl acetate and 0.1-85 parts of a solvent;
the solvent is a mixture of ethanol, propylene glycol and glycerol in a mass ratio of (6-12) (2-6) (1-3).
2. The essence for enhancing aroma of cigarettes according to claim 1, wherein the essence for cigarettes comprises, by mass, 0.5 part of 2-ethylpyrazine, 0.8 part of 2,3, 5-trimethylpyrazine, 0.5 part of 2-methyl-3- (methylthio) pyrazine, 0.4 part of 2-ethoxy-3-methylpyrazine, 0.8 part of cis-3-hexenal, 2 parts of cis-6-nonenal, 1 part of acetaldehyde diethyl acetal, 1.5 part of cyclopentadecanol, 1 part of menthyl lactate, 0.6 part of anisyl aldehyde, 0.8 part of clove oil, 0.3 part of isobutyric acid, 0.6 part of dodecanoic acid, 0.8 part of phenethyl alcohol, 0.5 part of isoamyl alcohol, 1.8 part of linalool, 0.6 part of ethyl isovalerate, 0.5 part of ethyl acetate and 85 parts of solvent;
the solvent is a mixture of ethanol, propylene glycol and glycerol with the mass ratio of 10:1.
3. The essence for enhancing cigarette aroma according to claim 1, wherein the added amount of the essence for cigarette is 0.01-2% of the mass of tobacco shreds.
4. The aroma-enhancing essence of cigarettes according to claim 1, wherein the essence comprises a solid, liquid or semi-solid form.
5. A method for preparing the essence for enhancing the aroma of cigarettes according to any one of claims 1 to 4, comprising the following steps:
s1, premix A
Weighing 2-ethylpyrazine, 2,3, 5-trimethylpyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methylpyrazine, acetaldehyde diethyl acetal and isoamyl alcohol, and mixing with 1/3 parts by mass of solvent, and stirring until a uniform solution is formed;
s2, premix B
Mixing menthyl lactate, isobutyric acid and 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s3, premix C
Mixing cis-3-hexenal, cis-6-nonenal, cyclopentadecanol, anisic aldehyde, clove oil, dodecanoic acid, phenethyl alcohol and linalool with 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
s4, final mixing
And mixing the premix A with the premix C, adding ethyl isovalerate and ethyl acetate, and finally adding the premix B to obtain the essence for enhancing the fragrance of cigarettes.
6. A method of using the essence for enhancing the aroma of cigarettes according to any one of claims 1 to 4, wherein the method comprises the following steps:
(1) Premix A
Weighing 2-ethylpyrazine, 2,3, 5-trimethylpyrazine, 2-methyl-3- (methylthio) pyrazine, 2-ethoxy-3-methylpyrazine, acetaldehyde diethyl acetal and isoamyl alcohol, and mixing with 1/3 parts by mass of solvent, and stirring until a uniform solution is formed;
(2) Premix B
Mixing menthyl lactate, isobutyric acid and 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
(3) Premix C
Mixing cis-3-hexenal, cis-6-nonenal, cyclopentadecanol, anisic aldehyde, clove oil, dodecanoic acid, phenethyl alcohol and linalool with 1/3 of the solvent by mass, and stirring until a uniform solution is formed;
(4) And mixing the premix A with the premix C, adding ethyl isovalerate and ethyl acetate, then applying the mixture to tobacco shreds, and finally applying the premix B to the tobacco shreds.
7. The method of claim 6, wherein the flavor is optionally diluted or undiluted.
8. The method of claim 7, wherein the diluent used for the selective dilution of the perfume is a mixture of ethanol, propylene glycol and glycerol.
9. The use method according to claim 8, wherein the mass ratio of the ethanol, the propylene glycol and the glycerol is (6-12): 2-6): 1-3.
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