CN113974204B - Sweet and spicy electronic cigarette tobacco tar and preparation method thereof - Google Patents
Sweet and spicy electronic cigarette tobacco tar and preparation method thereof Download PDFInfo
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- CN113974204B CN113974204B CN202111404805.9A CN202111404805A CN113974204B CN 113974204 B CN113974204 B CN 113974204B CN 202111404805 A CN202111404805 A CN 202111404805A CN 113974204 B CN113974204 B CN 113974204B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Fats And Perfumes (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses an electronic cigarette tobacco tar with a sweet and pungent flavor and a preparation method thereof, wherein the electronic cigarette tobacco tar is prepared from the following raw materials in parts by weight: 2 to 15 portions of red date extract, 0.5 to 8 portions of maple extract, 0.03 to 0.3 portion of vinasse subcritical extract, 0.05 to 0.1 portion of ethyl maltol, 0.5 to 1 portion of vanillin, 0.003 to 0.03 portion of anise oil, 0.002 to 0.02 portion of clove oil, 0.01 to 0.1 portion of heliotropin, 0.01 to 0.1 portion of p-methoxyacetophenone, 0.02 to 0.2 portion of damascone and 50 to 120 portions of solvent. The electronic cigarette tobacco tar can endow the electronic cigarette with a sweet and spicy smoking flavor, has elegant and strong fragrance, and meets the sensory requirements of the consumer groups.
Description
Technical Field
The invention relates to the technical field of electronic cigarette tobacco tar, in particular to sweet-pungent electronic cigarette tobacco tar and a preparation method thereof.
Background
With the continuous deepening of environmental protection consciousness and health consciousness of people and the rapid development of electronic information technology, novel tobacco products are produced. Electronic cigarettes are a new type of tobacco products, and generally refer to products that use electronic atomization equipment to heat tobacco tar to obtain a feeling of simulating real cigarette smoking. Compared with the traditional cigarette, the electronic cigarette does not contain tar and 460 chemical substances which are contained in the traditional cigarette and easily cause respiratory system and cardiovascular system diseases, so that the teeth of a person are prevented from yellowing, and the diseases are reduced; because the electronic cigarette does not need to be burnt, carbon monoxide gas harmful to human bodies is not contained, and aerosol generated by the electronic cigarette is easily and quickly diluted in air, the harm of second-hand smoke to the environment is reduced, and the hidden danger of fire disasters is eliminated. In recent years, electronic cigarettes are popular among more and more consumers as a substitute for traditional cigarettes, and the global market is rapidly increasing.
The tobacco tar is a key factor for endowing the electronic cigarette with taste style characteristics and determining smoking quality. The flavor of the electronic cigarette tobacco tar in the current market mainly takes mint and fruit flavors, and the electronic cigarette tobacco tar lacks the strength and taste similar to those of tobacco, so that the requirements of consumers on aroma and taste cannot be met.
Disclosure of Invention
In order to overcome the technical defects, the invention provides the electronic cigarette tobacco tar with the pungent and sweet flavor and the preparation method thereof.
In order to achieve the technical effect, the invention provides the electronic cigarette tobacco tar with the sweet and pungent flavor, which is prepared from the following raw materials in parts by weight: 2 to 15 parts of red date extract, 0.5 to 8 parts of maple extract, 0.03 to 0.3 part of vinasse subcritical extract, 0.05 to 0.1 part of ethyl maltol, 0.5 to 1 part of vanillin, 0.003 to 0.03 part of star anise oil, 0.002 to 0.02 part of clove oil, 0.01 to 0.1 part of heliotropin, 0.01 to 0.1 part of p-methoxyacetophenone, 0.02 to 0.2 part of damascenone and 50 to 120 parts of solvent.
Wherein the solvent is one or more of 75% ethanol, water, propylene glycol and glycerol. By 75% ethanol is meant an aqueous ethanol solution having a concentration of 75% by volume ethanol.
The vinasse subcritical extract is prepared by the following steps: loading the vinasse into a subcritical extraction tank, sealing and vacuumizing, then injecting an extracting agent into the extraction tank, wherein the material-liquid ratio (weight ratio of the vinasse to the extracting agent) is 1:3-6, extracting for 50min at the temperature of 40 ℃ and under the pressure of 0.8MPa, then transferring the extract into an evaporation tank, gasifying and separating the extracting agent, and extracting the subcritical vinasse extract.
The extraction agent is one of dimethyl ether, n-butane, methanol, ethyl acetate and acetone.
The invention also provides a preparation method of the electronic cigarette tobacco tar with the pungent and sweet flavor, which comprises the following steps:
step one, mixing the following raw materials in parts by weight, and uniformly stirring to obtain a sweet fragrant base: 2-15 parts of red date extract, 0.5-8 parts of maple extract and 0.03-0.3 part of vinasse subcritical extract;
step two, mixing 50-120 parts (by weight) of solvent with the sweet fragrance base obtained in the step one, and treating for 5-15min at the ultrasonic frequency of 20kHz and the temperature of 25 ℃ to obtain a sweet fragrance base diluent;
step three, mixing the following raw materials in parts by weight with the sweet fragrance base diluent, and uniformly stirring to obtain the pungent and sweet electronic cigarette tobacco tar: 0.05 to 0.1 portion of ethyl maltol, 0.5 to 1 portion of vanillin, 0.003 to 0.03 portion of star anise oil, 0.002 to 0.02 portion of clove oil, 0.01 to 0.1 portion of heliotropin, 0.01 to 0.1 portion of p-methoxyacetophenone and 0.02 to 0.2 portion of damascenone.
In the invention, the main raw materials for providing the sweet and spicy main body are as follows: anise oil, clove oil, red date extract and vinasse subcritical extract. The star anise oil is light yellow liquid, and mainly comprises anethole, benzyl alcohol and cinnamomum camphora, has clear and spicy fennel fragrance and sweet taste; the clove oil is yellow liquid, mainly contains eugenol and alpha-caryophyllene, and has the characteristic fragrance of medicinal fragrance, radix aucklandiae, spice and clove; the red date extract is reddish brown pasty liquid, mainly contains 5-hydroxymethyl furfural, furfural and palmitic acid, is rich in protein, fat, saccharides, carotene, vitamins and trace elements such as calcium, phosphorus, iron and the like, has higher nutritional value, has the characteristic sweet taste of red dates, and can generate natural, rich and pleasant sweet and pungent taste when matched with anise oil and clove oil; the subcritical extract of the vinasse is light yellow liquid, the main components of the subcritical extract are ethyl acetate, phenethyl alcohol, 2,3-butanediol and the like, the subcritical extract has vinous aroma, spicy aroma and baking aroma, the subcritical extraction mode is more environment-friendly and pollution-free than the traditional solvent extraction mode, the active ingredients of the extract are kept and are not damaged and oxidized, the subcritical extract can be rich and harmonious in aroma, and the aroma is natural. The maple extract and vanillin in the formula are used as a fragrance-fixing base and are coordinated with the fragrance of a main body, so that the sweet feeling can be increased, the fragrance components in tobacco tar can be uniformly volatilized, and the fragrance is lasting and stable. The ethyl maltol is used as a modifier, so that baking aroma is generated in the tobacco tar, the main aroma and sweet feeling can be set off, and the aroma is more beautiful. The heliotropin, the p-methoxyacetophenone and the damascone are used as a blending agent, and the sweet, fresh and sweet and spicy flavors in the anise oil, the clove oil and the red date extract are well blended together, so that the fragrance is strong and mellow.
Compared with the prior art, the invention has the following beneficial effects: the electronic cigarette tobacco tar prepared by the invention has lasting and strong sweet and pungent flavor, is similar to the characteristic aroma of the traditional cigarette, enriches the smoking taste of the electronic cigarette, and can meet different consumption requirements. When a consumer sucks the electronic cigarette tobacco tar, the electronic cigarette has natural aroma, comfortable throat and mouth parts, fine smoke and better throat strength, and can obviously increase the satisfaction of the smoker.
Detailed Description
Examples 1 to 10
The preparation process of the electronic cigarette tobacco tar with the pungent and sweet flavor of the embodiments 1 to 10 is as follows:
loading distiller's grains into subcritical extraction tank, sealing, vacuumizing, injecting n-butane into the extraction tank at a material-liquid ratio (weight ratio of distiller's grains to n-butane) of 1:3, extracting at 40 deg.C under 0.8MPa for 50min, transferring the extractive solution into evaporation tank, gasifying and separating n-butane as extractant, and extracting to obtain subcritical distiller's grains extract.
(1) The raw materials were mixed and stirred uniformly in the parts by weight shown in table 1 to obtain the sweet bases of examples 1 to 10.
Table 1 composition and ratio of sweet essence base in examples 1 to 10
(2) Weighing a certain amount of solvent according to the parts by weight in the table 2, mixing the solvent with the sweet fragrance base obtained in the step one, and treating for 10min at an ultrasonic frequency of 20kHz and a temperature of 25 ℃ to obtain the sweet fragrance base diluent of the embodiment 1-the embodiment 10;
table 2 composition and ratio of sweet base in examples 1 to 10
(3) Weighing the following raw materials in parts by weight in table 3, mixing the raw materials with the sweet fragrance base diluent obtained in the step (2), and uniformly stirring to obtain the pungent and sweet electronic cigarette tobacco tar of the examples 1 to 10.
Table 3 compositions and proportions of a sweet and pungent flavored e-cigarette tobacco tar in examples 1-10
Comparative examples 1 to 10
The preparation process of the electronic cigarette tobacco tar with the pungent and sweet flavor of the comparative examples 1 to 10 is as follows:
loading distiller's grains into subcritical extraction tank, sealing, vacuumizing, injecting n-butane into the extraction tank at a material-liquid ratio (weight ratio of distiller's grains to n-butane) of 1:3, extracting at 40 deg.C under 0.8MPa for 50min, transferring the extractive solution into evaporation tank, gasifying and separating extractant, and extracting to obtain subcritical distiller's grain extract.
(1) The raw materials were mixed and stirred uniformly in the weight parts shown in table 4 to obtain the sweet essence bases of comparative examples 1 to 10.
TABLE 4 composition and compounding ratio of sweet essence in comparative examples 1 to 10
(2) Weighing a certain amount of solvent according to the parts by weight in the table 5, mixing the solvent with the sweet fragrance base obtained in the step one, and treating for 10min at an ultrasonic frequency of 20kHz and a temperature of 25 ℃ to obtain sweet fragrance base diluent of the comparison examples 1-10;
TABLE 5 composition and compounding ratio of sweet essence in comparative examples 1 to 10
(3) Weighing the following raw materials in parts by weight in table 6, mixing the raw materials with the sweet fragrance base diluent obtained in the step (2), and uniformly stirring to obtain the pungent and sweet electronic cigarette tobacco tar of the comparative examples 1 to 10.
Table 6 shows the composition and the ratio of a sweet and pungent flavor electronic cigarette liquid in comparative examples 1 to 10
The evaluation method comprises the following steps:
adding 1mL of electronic cigarette tobacco tar into an atomizer, performing smoking evaluation by professional smoking evaluation personnel, selecting indexes of style characteristics (spicy and sweet), aroma characteristics (harmony and richness) and taste characteristics (irritation) of the electronic cigarette according to sensory characteristics of the electronic cigarette, performing sensory evaluation on the electronic cigarette tobacco tar with the spicy and sweet flavors of the embodiment 1-embodiment 10 and the comparative example 1-comparative example 10, obtaining an arithmetic mean value according to evaluation results of various experts, keeping a valid number in the result, and obtaining statistical results shown in Table 7.
Table 7 evaluation results of electronic cigarette tobacco tar having a pungent and sweet flavor in examples 1 to 10 and comparative examples 1 to 10
As can be seen from table 7, the electronic cigarette tobacco tar with the spicy and sweet flavor in examples 1 to 10 has the advantages of prominent spicy and sweet flavor, harmonious and elegant fragrance, comfortable, soft and non-irritating taste. Compared with the prior art 1 and the prior art 2, the red date extract or the maple extract which has the function of sweetening is not added, the mouth is stabier when the red date extract or the maple extract is obviously sucked, and the aroma duration of the comparative example 2 is not long; in the comparative example 3, the subcritical extract of the vinasse is not added, so that the fragrance is unnatural after being sucked and the strength is insufficient; comparative example 4 no ethyl maltol was added, and there was no baking note similar to that of heat burning; in the comparative example 5, vanillin is not added, the aroma lasting time is short, and the aroma is not fine and smooth enough; the clove oil or star anise oil which generates spicy fragrance is not added in the comparison examples 6 and 7, so that the characteristic fragrance is not prominent, the fragrance is unnatural, and the smoke is sweet and greasy; in the comparison examples 8-10, heliotropin or p-methoxyacetophenone or damascone which have a neutralizing effect are not added, so that the fragrance is monotonous and is not harmonious, and the agglomeration of smoke is not good.
Although the invention has been described herein with reference to the illustrated embodiments thereof, which are intended to be illustrative only, the invention is not to be limited thereto, and it is to be understood that numerous other modifications and arrangements can be devised by those skilled in the art that will fall within the spirit and scope of the principles of this disclosure.
Claims (3)
1. The electronic cigarette tobacco tar with the pungent and sweet flavor is characterized by being prepared from the following raw materials in parts by weight: 2 to 15 parts of red date extract, 0.5 to 8 parts of maple extract, 0.03 to 0.3 part of vinasse subcritical extract, 0.05 to 0.1 part of ethyl maltol, 0.5 to 1 part of vanillin, 0.003 to 0.03 part of star anise oil, 0.002 to 0.02 part of clove oil, 0.01 to 0.1 part of heliotropin, 0.01 to 0.1 part of p-methoxyacetophenone, 0.02 to 0.2 part of damascenone and 50 to 120 parts of solvent; the vinasse subcritical extract is prepared by the following steps: filling the vinasse into a subcritical extraction tank, sealing and vacuumizing, then injecting an extracting agent into the extraction tank, wherein the extracting agent is one of dimethyl ether, n-butane, methanol, ethyl acetate and acetone, the material-liquid ratio is 1 to 3-6, extracting for 50min at the temperature of 40 ℃ and under the pressure of 0.8MPa, then transferring the extract into an evaporation tank, gasifying and separating the extracting agent, and extracting the vinasse subcritical extract.
2. The pungent-sweet flavored e-cigarette tobacco tar of claim 1, wherein the solvent is: one or more of 75% ethanol, water, propylene glycol, and glycerol.
3. A preparation method of electronic cigarette tobacco tar with a sweet and pungent flavor is characterized by comprising the following steps:
step one, mixing the following raw materials in parts by weight, and uniformly stirring to obtain a sweet fragrant base: 2 to 15 parts of red date extract, 0.5 to 8 parts of maple extract and 0.03 to 0.3 part of vinasse subcritical extract; the vinasse subcritical extract is prepared by the following steps: filling the vinasse into a subcritical extraction tank, sealing and vacuumizing, then injecting an extracting agent into the extraction tank, wherein the extracting agent is one of dimethyl ether, n-butane, methanol, ethyl acetate and acetone, the material-liquid ratio is 1 to 3-6, extracting for 50min at the temperature of 40 ℃ and under the pressure of 0.8MPa, then transferring the extract into an evaporation tank, gasifying and separating the extracting agent, and extracting the vinasse subcritical extract;
step two, mixing 50 to 120 parts of solvent with the sweet base obtained in the step one, and treating for 5-15min at the ultrasonic frequency of 20kHz and the temperature of 25 ℃ to obtain a sweet base diluent;
step three, mixing the following raw materials in parts by weight with the sweet fragrance base diluent, and uniformly stirring to obtain the pungent and sweet electronic cigarette tobacco tar: 0.05 to 0.1 portion of ethyl maltol, 0.5 to 1 portion of vanillin, 0.003 to 0.03 portion of anise oil, 0.002 to 0.02 portion of clove oil, 0.01 to 0.1 portion of heliotropin, 0.01 to 0.1 portion of methoxy acetophenone and 0.02 to 0.2 portion of damascone.
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| CN113974204B true CN113974204B (en) | 2023-02-28 |
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| CN111671131A (en) * | 2020-06-22 | 2020-09-18 | 福建中烟工业有限责任公司 | Electronic cigarette atomized liquid with flue-cured tobacco and tobacco taste and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11479745B2 (en) * | 2017-04-07 | 2022-10-25 | John I. Haas, Inc. | Hop extraction products and processes for improved beverage fermentation and flavor |
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- 2021-11-24 CN CN202111404805.9A patent/CN113974204B/en active Active
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| CN103756780A (en) * | 2014-01-08 | 2014-04-30 | 王志远 | Method for preparing corn bran oil through combination of tera-hertz radiation and sub-critical extraction |
| CN107586614A (en) * | 2017-10-24 | 2018-01-16 | 昆明坤九香精香料有限公司 | A kind of preparation method and applications of cigarette cognac flavour |
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