CN102776068A - Paste type microcapsule flavoring rose essence and preparation method thereof - Google Patents
Paste type microcapsule flavoring rose essence and preparation method thereof Download PDFInfo
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- CN102776068A CN102776068A CN2012102887434A CN201210288743A CN102776068A CN 102776068 A CN102776068 A CN 102776068A CN 2012102887434 A CN2012102887434 A CN 2012102887434A CN 201210288743 A CN201210288743 A CN 201210288743A CN 102776068 A CN102776068 A CN 102776068A
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Abstract
The invention discloses a paste type microcapsule flavoring rose essence and a preparation method thereof. The paste type microcapsule flavoring rose essence comprises the following components in percentage by weight: 5-25% of flavoring rose essence, 10-50% of beta-cyclodextrin, 0.1-2% of xanthan gum and the balance of deionized water. The preparation method comprises the following steps: uniformly dispersing the beta-cyclodextrin into the deionized water to form a beta-cyclodextrin turbid liquid; adding the xanthan gum into the obtained beta-cyclodextrin turbid liquid, and continuously stirring to ensure that the xanthan gum is dissolved and uniformly distributed; and then adding the flavoring rose essence, and continuously and uniformly stirring to obtain the paste type microcapsule flavoring rose essence. The prepared paste type microcapsule flavoring rose essence is stable in fragrance, keeps fragrance for a long time, and has the characteristics of high fragrance strength, high essence content and the like.
Description
Technical field
The present invention relates to a kind of paste rose slowly-releasing essence, particularly a kind of paste microcapsule rose compound and preparation method thereof.
Background technology
Rose fragrance belongs to the fragrance of a flower, sweet rhythm, the fragrant and sweet as honey of Rose, and that its sweet rhythm comprises is pure and sweet, beeswax is sweet and it is sweet to make, and fragrance overflows, and the good reputation of the hat of the fragrance of a flower is arranged.Fields such as the high-grade daily chemical products of rose compound widespread use, food, tobacco.Because the most of compositions of essence are volatile organic cpds, volatile in direct use, some thermo-sensitivity perfume materials and photosensitivity perfume material are unstable, and fragrance remaining time is short, aroma quality is unstable thereby cause.
Microcapsule essence is meant essence as core, selects for use suitable wall material that essence is coated and forms the essence capsule particulate.Microcapsule essence can greatly improve thermostability, light stability and the oxidation-resistance of essence; Can prevent the loss of aroma component effectively, make the style of essence constant, aroma quality is stable; And can improve the sustained release performance of essence, make things convenient for transportation, storage and the use of essence.
Existing microcapsule essence is the wall material with modified starch, chitosan, polypropylene acid esters, Schardinger dextrins etc. usually; Make the microcapsule essence of milk sap or suspension liquid state; Methods such as milk sap or suspension liquid are generally unstable, are prone to layering, and need are spray-dried make the powdery microcapsule essence.
Summary of the invention
One of the object of the invention is in order to solve the in stable condition technical problem that exists in the existing microcapsule essence a kind of paste microcapsule rose compound to be provided.
The preparation method of a kind of paste microcapsule rose compound that two of the object of the invention is to provide above-mentioned.
Know-why of the present invention
Schardinger dextrins is to pass through the ring compound that α-1,4 glycoside bond is formed by connecting by what starch obtained through the enzymolysis cyclization by 6 to 8 D-glucose molecules, and the Schardinger dextrins of wherein being made up of 7 D-glucose molecules is called beta-cyclodextrin.
Cyclodextrin molecular is cylindric ringwise, surface and hydrophilic outer and inner chamber is hydrophobic, therefore; The Schardinger dextrins inner chamber can coat the essence molecule; Form microcapsule essence, in the preparation process, add simultaneously have thickening, the XG 550 of stable, emulsifying effect, can obtain the paste microcapsule essence.
Technical scheme of the present invention
A kind of paste microcapsule rose compound is counted by weight percentage, and the composition and the content of its raw material are following:
Rose compound 5-25%
Beta-cyclodextrin 10-50%
XG 550 0.1-2%
Surplus is a deionized water;
Above-mentioned a kind of paste microcapsule rose compound is through following preparation method, and its concrete preparation process comprises the steps:
(1), in beaker, add beta-cyclodextrin, add deionized water again, open to stir, beta-cyclodextrin is dispersed in the deionized water uniformly, form the beta-cyclodextrin suspension liquid;
(2), XG 550 is slowly joined in the resulting beta-cyclodextrin suspension liquid of step (1), continue to stir, make the XG 550 dissolving and be evenly distributed, and then add rose compound, add continued and stir, promptly get paste microcapsule rose compound.
Rose compound in above-mentioned a kind of paste microcapsule rose compound feed composition is counted by weight percentage, and the composition and the content of its raw material are following:
Geraniol 20-50%
Phenylethyl alcohol 20-40%
Geraniol 10-30%
10% aldehyde C-9 ethanolic soln 1-2%
Wine oil 0.5-3%
Eugenol 2-5%
Jononeionone 2-8%
Cinnamic alcohol 1-5%
Meraneine 1-5%
Citronellyl acetate 1-5%
Phantol 2-6%
Phanteine 2-4%
10% rose oxide ethanolic soln 0.5-1%
Itral 1-2%
Jasmal 0-3%
Laurine 0-1%
Patchouli oil 0-1.5%
Surplus is an ethanol;
Above-mentioned rose compound prepares through following method, and this preparation process steps is following:
With ethanol, Geraniol, phenylethyl alcohol, geraniol, 10% aldehyde C-9 ethanolic soln, wine oil, Eugenol, jononeionone, cinnamic alcohol, meraneine, citronellyl acetate, phantol, phanteine, 10% rose oxide ethanolic soln, itral, jasmal, laurine and patchouli oil uniform mixing, promptly get rose compound.
Beneficial effect of the present invention
A kind of paste microcapsule rose compound of the present invention owing to adopt nontoxic, biodegradable beta-cyclodextrin as the wall material, through the XG 550 that adding has thickening, stable, emulsifying effect, therefore finally obtains the microcapsule slowly-releasing essence of paste.
Further, because the synergy of emulsification, thickening has effectively strengthened the stability of system, so the paste microcapsule rose compound that the present invention makes is difficult for layering takes place, and system is more stable.
In addition; The present invention is made the paste microcapsule essence to smell through Wen Xiangzhi with the rose compound of micro encapsulation not and distinguishes analysis; Former beginning and end micro encapsulation rose compound after 5 days fragrance faint; Only can feel the bottom note note of rose, and paste microcapsule essence of the present invention still can be felt the whole odour characteristics of obvious rose after 21 days.Therefore, the paste microcapsule rose compound fragrance that the present invention makes is stable, and lasting is lasting.
Embodiment
Through embodiment the present invention is done explanation further below, but do not influence protection scope of the present invention.The used various raw materials or the specification of reagent and the information of manufacturer are seen table 1 in the various embodiments of the present invention.
The specification of table 1, raw material and reagent and manufacturer
Embodiment 1
A kind of paste microcapsule rose compound is counted by weight percentage, and the composition and the content of its raw material are following:
Rose compound 5g (5%)
Beta-cyclodextrin 10g (10%)
XG 550 2g (2%)
Deionized water 83g (83%);
Above-mentioned a kind of paste microcapsule rose compound is through following preparation method, and its concrete preparation process comprises the steps:
(1), in the 150ml beaker, add the beta-cyclodextrin of 10g, add the deionized water of 83g again, open and stir, beta-cyclodextrin is dispersed in the deionized water uniformly, form the beta-cyclodextrin suspension liquid;
(2), the 2g XG 550 is joined in the beta-cyclodextrin suspension liquid of step (1) gained, continue to stir, make the XG 550 dissolving and be evenly distributed, and then add the 5g rose compound, continuation stirring 3-5h again after having added promptly gets paste microcapsule rose compound.
The paste microcapsule rose compound of above-mentioned gained, better mobile, but after leaving standstill for 3 weeks, find that microcapsule essence has sedimentation phenomenon.
Rose compound in above-mentioned a kind of paste microcapsule rose compound feed composition is counted by weight percentage, and the composition and the content of its raw material are following:
Geraniol 25g (25%)
Phenylethyl alcohol 20g (20%)
Geraniol 13.9g (13.9%)
10% aldehyde C-9 ethanolic soln 1g (1%)
Wine oil 0.5g (0.5%)
Eugenol 5g (5%)
Jononeionone 4g (4%)
Cinnamic alcohol 2g (2%)
Meraneine 3g (3%)
Citronellyl acetate 5g (5%)
Phantol 5g (5%)
Phanteine 4g (4%)
10% rose oxide ethanolic soln 1g (1%)
Itral 1g (1%)
Jasmal 0.3g (0.3%)
Laurine 0.2g (0.2%)
Patchouli oil 0.1g (0.1%)
Surplus is an ethanol;
Above-mentioned rose compound prepares through following method, and this preparation process steps is following:
With ethanol, Geraniol, phenylethyl alcohol, geraniol, 10% aldehyde C-9 ethanolic soln, wine oil, Eugenol, jononeionone, cinnamic alcohol, meraneine, citronellyl acetate, phantol, phanteine, 10% rose oxide ethanolic soln, itral, jasmal, laurine and patchouli oil uniform mixing, promptly get rose compound.The essence fragrance that obtains passes through to be sent out, and fragrance is thicker, hot sweet partially, has the characteristic perfume of Rose.
Embodiment 2
A kind of paste microcapsule rose compound is counted by weight percentage, and the composition and the content of its raw material are following:
Rose compound 5g (5%)
Beta-cyclodextrin 45g (45%)
XG 550 0.1g (0.1%)
Deionized water 49.9g (49.9%).
Above-mentioned a kind of paste microcapsule rose compound is through following preparation method, and its concrete preparation process comprises the steps:
(1), in the 150ml beaker, add the beta-cyclodextrin of 45g, add the deionized water of 49.9g again, open and stir, beta-cyclodextrin is dispersed in the deionized water uniformly, form the beta-cyclodextrin suspension liquid;
(2), the 0.1g XG 550 is joined in the beta-cyclodextrin suspension liquid of step (1) gained; Continue to stir, make the XG 550 dissolving and be evenly distributed, and then add the 5g rose compound; Continue again after having added to stir 3-5h, promptly get paste microcapsule rose compound.
The paste microcapsule rose compound of above-mentioned gained, thickness relatively, left standstill for 3 weeks after, find slightly sedimentation phenomenon of microcapsule essence.
Rose compound in above-mentioned a kind of paste microcapsule rose compound feed composition is counted by weight percentage, and the composition and the content of its raw material are following:
Geraniol 25g (25%)
Phenylethyl alcohol 20g (20%)
Geraniol 13.9g (13.9%)
10% aldehyde C-9 ethanolic soln 1g (1%)
Wine oil 0.5g (0.5%)
Eugenol 5g (5%)
Jononeionone 4g (4%)
Cinnamic alcohol 2g (2%)
Meraneine 3g (3%)
Citronellyl acetate 5g (5%)
Phantol 5g (5%)
Phanteine 4g (4%)
10% rose oxide ethanolic soln 1g (1%)
Itral 1g (1%)
Jasmal 0.3g (0.3%)
Laurine 0.2g (0.2%)
Patchouli oil 0.1g (0.1%)
Surplus is an ethanol;
Above-mentioned rose compound prepares through following method, and this preparation process steps is following:
With ethanol, Geraniol, phenylethyl alcohol, geraniol, 10% aldehyde C-9 ethanolic soln, wine oil, Eugenol, jononeionone, cinnamic alcohol, meraneine, citronellyl acetate, phantol, phanteine, 10% rose oxide ethanolic soln, itral, jasmal, laurine and patchouli oil uniform mixing, promptly get rose compound.The essence fragrance that obtains passes through to be sent out, and fragrance is thicker, hot sweet partially, has the characteristic perfume of Rose.
Embodiment 3
A kind of paste microcapsule rose compound is counted by weight percentage, and the composition and the content of its raw material are following:
Rose compound 10g (10%)
Beta-cyclodextrin 25g (25%)
XG 550 1g (1%)
Deionized water 64g (64%).
Above-mentioned a kind of paste microcapsule rose compound is through following preparation method, and its concrete preparation process comprises the steps:
(1), in the 150ml beaker, add the beta-cyclodextrin of 25g, add the deionized water of 64g again, open and stir, beta-cyclodextrin is dispersed in the deionized water uniformly, form the beta-cyclodextrin suspension liquid;
(2), the XG 550 with 1.0g joins in the beta-cyclodextrin suspension liquid of step (1) gained; Continue to stir, make the XG 550 dissolving and be evenly distributed, and then add the 10g rose compound; Continue again after having added to stir 3-5h, promptly get paste microcapsule rose compound.
The paste microcapsule rose compound of above-mentioned gained is than stiff, and is mobile relatively poor, but microcapsule rose compound system is more stable, left standstill for 3 weeks after, do not find that microcapsule essence has the sedimentation demixing phenomenon.
Rose compound in above-mentioned a kind of paste microcapsule rose compound feed composition is counted by weight percentage, and the composition and the content of its raw material are following:
Geraniol 30g (30%)
Phenylethyl alcohol 25g (25%)
Geraniol 20.5g (20.5%)
10% aldehyde C-9 ethanolic soln 1g (1%)
Wine oil 3g (3%)
Eugenol 2g (2%)
Jononeionone 3g (3%)
Cinnamic alcohol 2g (2%)
Meraneine 3g (3%)
Citronellyl acetate 3g (3%)
Phantol 2g (2%)
Phanteine 2g (2%)
10% rose oxide ethanolic soln 0.5g (0.5%)
Itral 1g (1%)
Jasmal 0.1g (0.1%)
Laurine 0.1g (0.1%)
Patchouli oil 0.1g (0.1%)
Surplus is an ethanol;
Above-mentioned rose compound prepares through following method, and this preparation process steps is following:
With ethanol, Geraniol, phenylethyl alcohol, geraniol, 10% aldehyde C-9 ethanolic soln, wine oil, Eugenol, jononeionone, cinnamic alcohol, meraneine, citronellyl acetate, phantol, phanteine, 10% rose oxide ethanolic soln, itral, jasmal, laurine and patchouli oil uniform mixing, promptly get rose compound.The essence that obtains has the characteristic perfume of rose, and fragrance is fine and smooth, and it is outstanding to make fragrant and sweet rhythm.
Embodiment 4
A kind of paste microcapsule rose compound is counted by weight percentage, and the composition and the content of its raw material are following:
Rose compound 10g (10%)
Beta-cyclodextrin 20g (20%)
XG 550 1g (1%)
Deionized water 69g (69%).
Above-mentioned a kind of paste microcapsule rose compound is through following preparation method, and its concrete preparation process comprises the steps:
(1), in the 150ml beaker, add the beta-cyclodextrin of 20g, add the deionized water of 69g again, open and stir, beta-cyclodextrin is dispersed in the deionized water uniformly, form the beta-cyclodextrin suspension liquid;
(2), the 1.0g XG 550 is joined in the beta-cyclodextrin suspension liquid of step (1) gained; Continue to stir, make the XG 550 dissolving and be evenly distributed, and then add the 10g rose compound; Continue again after having added to stir 3-5h, promptly get paste microcapsule rose compound.
The paste microcapsule essence of above-mentioned gained is better mobile, and paste microcapsule rose compound system is stable, left standstill for 3 weeks after, do not find that microcapsule essence has the sedimentation demixing phenomenon.
Rose compound in above-mentioned a kind of paste microcapsule rose compound feed composition is counted by weight percentage, and the composition and the content of its raw material are following:
Geraniol 40g (40%)
Phenylethyl alcohol 30g (30%)
Geraniol 12.7g (12.7%)
10% aldehyde C-9 ethanolic soln 2g (2%)
Wine oil 0.5g (0.5%)
Eugenol 2g (2%)
Jononeionone 2g (2%)
Cinnamic alcohol 1g (1%)
Meraneine 1g (1%)
Citronellyl acetate 2g (2%)
Phantol 2g (2%)
Phanteine 2g (2%)
10% rose oxide ethanolic soln 0.5g (0.5%)
Itral 1g (1%)
Jasmal 0.1g (0.1%)
Laurine 0.1g (0.1%)
Patchouli oil 0.1g (0.1%)
Surplus is an ethanol;
Above-mentioned rose compound prepares through following method, and this preparation process steps is following:
With ethanol, Geraniol, phenylethyl alcohol, geraniol, 10% aldehyde C-9 ethanolic soln, wine oil, Eugenol, jononeionone, cinnamic alcohol, meraneine, citronellyl acetate, phantol, phanteine, 10% rose oxide ethanolic soln, itral, jasmal, laurine and patchouli oil uniform mixing, promptly get rose compound.The essence that obtains has the characteristic perfume of Rose, and the fragrant note of adipocere is outstanding.
Embodiment 5
A kind of paste microcapsule rose compound is counted by weight percentage, and the composition and the content of its raw material are following:
Rose compound 15g (15%)
Beta-cyclodextrin 20g (20%)
XG 550 1g (1%)
Deionized water 64g (64%).
Above-mentioned a kind of paste microcapsule rose compound is through following preparation method, and its concrete preparation process comprises the steps:
(1), in the 150ml beaker, add the beta-cyclodextrin of 20g, add the deionized water of 64g again, open and stir, beta-cyclodextrin is dispersed in the deionized water uniformly, form the beta-cyclodextrin suspension liquid;
(2), the 1g XG 550 is joined in the beta-cyclodextrin suspension liquid of step (1) gained, continue to stir, make the XG 550 dissolving and be evenly distributed, and then add the 15g rose compound, continuation stirring 3-5h again after having added promptly gets paste microcapsule rose compound.
The paste microcapsule rose compound of above-mentioned gained is than stiff, and is mobile relatively poor, left standstill for 3 weeks after, find that microcapsule essence has sedimentation phenomenon.
Rose compound in above-mentioned a kind of paste microcapsule rose compound feed composition is counted by weight percentage, and the composition and the content of its raw material are following:
Geraniol 40g (40%)
Phenylethyl alcohol 30g (30%)
Geraniol 12.7g (12.7%)
10% aldehyde C-9 ethanolic soln 2g (2%)
Wine oil 0.5g (0.5%)
Eugenol 2g (2%)
Jononeionone 2g (2%)
Cinnamic alcohol 1g (1%)
Meraneine 1g (1%)
Citronellyl acetate 2g (2%)
Phantol 2g (2%)
Phanteine 2g (2%)
10% rose oxide ethanolic soln 0.5g (0.5%)
Itral 1g (1%)
Jasmal 0.1g (0.1%)
Laurine 0.1g (0.1%)
Patchouli oil 0.1g (0.1%)
Surplus is an ethanol;
Above-mentioned rose compound prepares through following method, and this preparation process steps is following:
With ethanol, Geraniol, phenylethyl alcohol, geraniol, 10% aldehyde C-9 ethanolic soln, wine oil, Eugenol, jononeionone, cinnamic alcohol, meraneine, citronellyl acetate, phantol, phanteine, 10% rose oxide ethanolic soln, itral, jasmal, laurine and patchouli oil uniform mixing, promptly get rose compound.The essence that obtains has the characteristic perfume of Rose, and the fragrant note of adipocere is outstanding.
In sum, a kind of paste microcapsule rose compound of the present invention is because therefore synergistic effects such as emulsification, thickening have characteristics in stable condition, that fragrance is coordinated.A kind of paste microcapsule rose compound of gained under the condition of the prescription of embodiment 4 particularly, essence system good fluidity, in stable condition, fragrance is coordinated.
The above content is merely the basic explanation of the present invention under conceiving, and according to any equivalent transformation that technical scheme of the present invention is done, all belongs to the scope of the present invention's protection.
Claims (7)
1. a paste microcapsule rose compound is characterized in that counting by weight percentage, and the composition and the content of its raw material are following:
Rose compound 5-25%
Beta-cyclodextrin 10-50%
XG 550 0.1-2%
Surplus is a deionized water;
Above-mentioned a kind of paste microcapsule rose compound obtains through following preparation method, and its concrete preparation process comprises the steps:
(1), in beaker, add beta-cyclodextrin, add deionized water again, open to stir, beta-cyclodextrin is dispersed in the deionized water uniformly, form the beta-cyclodextrin suspension liquid;
(2), XG 550 is joined in the resulting beta-cyclodextrin suspension liquid of step (1), continue to stir, make the XG 550 dissolving and be evenly distributed, add rose compound then and continue to stir, promptly get paste microcapsule rose compound.
2. a kind of paste microcapsule rose compound as claimed in claim 1 is characterized in that counting by weight percentage, and the composition and the content of its raw material are following:
Rose compound 5-15%
Beta-cyclodextrin 10-45%
XG 550 0.1-2%
Surplus is a deionized water.
3. according to claim 1 or claim 2 a kind of paste microcapsule rose compound is characterized in that the rose compound described in the feed composition counts by weight percentage, and the composition and the content of its raw material are following:
Geraniol 20-50%
Phenylethyl alcohol 20-40%
Geraniol 10-30%
10% aldehyde C-9 ethanolic soln 1-2%
Wine oil 0.5-3%
Eugenol 2-5%
Jononeionone 2-8%
Cinnamic alcohol 1-5%
Meraneine 1-5%
Citronellyl acetate 1-5%
Phantol 2-6%
Phanteine 2-4%
10% rose oxide ethanolic soln 0.5-1%
Itral 1-2%
Jasmal 0-3%
Laurine 0-1%
Patchouli oil 0-1.5%
Surplus is an ethanol;
Above-mentioned rose compound prepares through following method, and this preparation process steps is following:
With ethanol, Geraniol, phenylethyl alcohol, geraniol, 10% aldehyde C-9 ethanolic soln, wine oil, Eugenol, jononeionone, cinnamic alcohol, meraneine, citronellyl acetate, phantol, phanteine, 10% rose oxide ethanolic soln, itral, jasmal, laurine and patchouli oil uniform mixing, promptly get rose compound.
4. a kind of paste microcapsule rose compound as claimed in claim 3 is characterized in that the rose compound described in the feed composition counts by weight percentage, and the composition and the content of its raw material are following:
Geraniol 25-40%
Phenylethyl alcohol 20-30%
Geraniol 12.7-20.5%
10% aldehyde C-9 ethanolic soln 1-2%
Wine oil 0.5-3%
Eugenol 2-5%
Jononeionone 2-4%
Cinnamic alcohol 1-2%
Meraneine 1-3%
Citronellyl acetate 2-5%
Phantol 2-5%
Phanteine 2-4%
10% rose oxide ethanolic soln 0.5-1%
Itral 1%
Jasmal 0.1-0.3%
Laurine 0.1-0.2%
Patchouli oil 0.1%
Surplus is an ethanol.
5. a kind of paste microcapsule rose compound as claimed in claim 4 is characterized in that counting by weight percentage, and the composition and the content of its raw material are following:
Rose compound 10%
Beta-cyclodextrin 20%
XG 550 1%
Deionized water 69%
Described rose compound is counted by weight percentage, and the composition and the content of its raw material are following:
Geraniol 40%
Phenylethyl alcohol 30%
Geraniol 12.7%
10% aldehyde C-9 ethanolic soln 2%
Wine oil 0.5%
Eugenol 2%
Jononeionone 2%
Cinnamic alcohol 1%
Meraneine 1%
Citronellyl acetate 2%
Phantol 2%
Phanteine 2%
10% rose oxide ethanolic soln 0.5%
Itral 1%
Jasmal 0.1%
Laurine 0.1%
Patchouli oil 0.1%
Surplus is an ethanol.
6. according to claim 1 or claim 2 the used rose compound of a kind of paste microcapsule rose compound is characterized in that counting by weight percentage, and the composition and the content of its raw material are following:
Geraniol 20-50%
Phenylethyl alcohol 20-40%
Geraniol 10-30%
10% aldehyde C-9 ethanolic soln 1-2%
Wine oil 0.5-3%
Eugenol 2-5%
Jononeionone 2-8%
Cinnamic alcohol 1-5%
Meraneine 1-5%
Citronellyl acetate 1-5%
Phantol 2-6%
Phanteine 2-4%
10% rose oxide ethanolic soln 0.5-1%
Itral 1-2%
Jasmal 0-3%
Laurine 0-1%
Patchouli oil 0-1.5%
Surplus is an ethanol;
Above-mentioned rose compound prepares through following method, and this preparation process steps is following:
With ethanol, Geraniol, phenylethyl alcohol, geraniol, 10% aldehyde C-9 ethanolic soln, wine oil, Eugenol, jononeionone, cinnamic alcohol, meraneine, citronellyl acetate, phantol, phanteine, 10% rose oxide ethanolic soln, itral, jasmal, laurine and patchouli oil uniform mixing, promptly get rose compound.
7. rose compound as claimed in claim 6 is characterized in that counting by weight percentage, and the composition and the content of its raw material are following:
Geraniol 25-40%
Phenylethyl alcohol 20-30%
Geraniol 12.7-20.5%
10% aldehyde C-9 ethanolic soln 1-2%
Wine oil 0.5-3%
Eugenol 2-5%
Jononeionone 2-4%
Cinnamic alcohol 1-2%
Meraneine 1-3%
Citronellyl acetate 2-5%
Phantol 2-5%
Phanteine 2-4%
10% rose oxide ethanolic soln 0.5-1%
Itral 1%
Jasmal 0.1-0.3%
Laurine 0.1-0.2%
Patchouli oil 0.1%
Surplus is an ethanol.
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| CN108743999A (en) * | 2018-06-04 | 2018-11-06 | 上海应用技术大学 | A kind of solid shoes tablet and preparation method thereof with citris aromas |
| CN109674667A (en) * | 2019-01-25 | 2019-04-26 | 广州积美国际贸易有限公司 | A kind of hair washing essence that fragrance retention is lasting |
| CN111500368A (en) * | 2020-06-15 | 2020-08-07 | 上海应用技术大学 | Watermelon slow-release essence and preparation method thereof |
| CN111592934A (en) * | 2020-06-15 | 2020-08-28 | 上海应用技术大学 | Jasmine slow-release essence and preparation method thereof |
| CN115595209A (en) * | 2022-11-02 | 2023-01-13 | 云南中烟工业有限责任公司（Cn） | Rose-characteristic essence formula, preparation method and application thereof |
| CN115886226A (en) * | 2022-11-02 | 2023-04-04 | 江西省华宝孔雀食品科技发展有限公司 | Microcapsule paste essence and preparation method thereof |
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| CN109674667B (en) * | 2019-01-25 | 2022-01-21 | 毓美生物科技(广州)有限公司 | Shampoo essence with lasting fragrance retention |
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