CN103409247A - Mosquito-expelling washing powder - Google Patents
Mosquito-expelling washing powder Download PDFInfo
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- CN103409247A CN103409247A CN2013103726966A CN201310372696A CN103409247A CN 103409247 A CN103409247 A CN 103409247A CN 2013103726966 A CN2013103726966 A CN 2013103726966A CN 201310372696 A CN201310372696 A CN 201310372696A CN 103409247 A CN103409247 A CN 103409247A
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Abstract
The invention relates to mosquito-expelling washing powder and belongs to the technical field of daily washing products. The mosquito-expelling washing powder comprises the following ingredients: 5-15% of mozzie buster essential oil micro capsule, 10-25% of sodium dodecyl benzene sulfonate, 6-8% of sodium silicate, 1-7% of sodium sulphate, 2-10% of fatty alcohol-polyoxyethylene ether, 0.2-0.7% of fluorescent whitening agent, 0.5-1% of essence and 5-10% of water. A cyclodextrin micro capsule wrapping technology is adopted for preparing a mozzie buster slow release sac, production cost is low, a mosquito-expelling effect is good, mosquito-expelling essence can be slowly released, and the aim of continuously and effectively expelling mosquitoes can be reached.
Description
Technical field
The present invention relates to a kind of mosquito repellent washing powder.Belong to daily articles for washing technical field.
Background technology
Washing powder is articles for washing common in people's daily life.Along with the development of modern science and technology, the soil removability of washing powder is more and more stronger, and its taste emerges in an endless stream especially.But existing these washing powder are all relatively paid attention to soil removability, and its function can be more single, on market, need a kind of washing powder of effective mosquito repellent, meet people's demand.
Investigators also constantly carry out the research of mosquito repellent washing powder.
Application for a patent for invention numbers 201210459031.4, a kind of mosquito repellent washing powder, this invention is by following composition: too acetate is 0.2-4 parts; Tremble 0.5-3 parts of hydrochlorates; Spices is appropriate; 8-16 parts of Witco 1298 Soft Acids; 2-4 parts of ethanol; 5-8 parts, Tetranthera citrata blade; 6-10 parts of melia toosendan skins.This washing powder has stronger soil removability, but the actual effect of mosquito repellent is short, does not reach the desirable mosquito repellent time.
Cyclodextrin is by seven Glucopyranose units, to be connected the ring molecule formed by α-Isosorbide-5-Nitrae glycosidic link, and it can be divided into alpha-cylodextrin, beta-cyclodextrin, γ-cyclodextrin.Cyclodextrin itself has interior hydrophobic, outer hydrophilic special molecular structure, and the different compound of energy Borrow, form inclusion complex, is a kind of sorbing material of excellent property.Adopt cyclodextrin, by carrier, it is wrapped to thing and carry out the micro-capsule capsule, can play good protection and slow releasing function.Wherein beta-cyclodextrin solubleness is low, can well coat some VITAMIN or aromatic oil, and easily crystallization, separation, purification, and cost is low, manufactures the microcapsule controlled-release effect.
Summary of the invention
The present invention, for meeting the need of market, provides a kind of mosquito repellent washing powder preparation formula, and the present invention adopts cyclodextrin micro-capsule technique for packing to prepare Mozzie buster slowly-releasing capsule, not only production cost is low, and repelling effect is good, can slowly discharge, reach the purpose that effectively continues mosquito repellent.
A kind of mosquito repellent washing powder, by following composition: QUWENCAO JINGYOU micro-capsule 5-15%, Sodium dodecylbenzene sulfonate 10-25%, water glass 6-8%, sodium sulfate 1-7%, fatty alcohol-polyoxyethylene ether 2-10%, white dyes 0.2-0.7%, essence 0.5-1%, water 5-10%.
In the present invention, the preparation method of QUWENCAO JINGYOU micro-capsule is, take QUWENCAO JINGYOU and tween-80, mass ratio is 1:4, quick homogeneous emulsification, then get in proportion a certain amount of water, under agitation be heated to 80 ℃, add the beta-cyclodextrin of suitable proportion that it is dissolved fully, water and beta-cyclodextrin mass ratio are 100:15, then drip the uniform QUWENCAO JINGYOU of above-mentioned emulsification, QUWENCAO JINGYOU and beta-cyclodextrin mass ratio are 3:5-15, inclusion 3.0h under 50 ℃ of stirrings.Naturally cool to room temperature, essence is put 24h, and the microcapsule of formation are from solution, separating out, and through separating, concussion is dry, obtains the QUWENCAO JINGYOU micro-capsule.
After deliberation, QUWENCAO JINGYOU and beta-cyclodextrin mass ratio are 3:10, and the packing effect is better, can slowly effectively discharge mosquito-repellent essential oil, therefore the optimum proportion that the present invention selects is 3:10.
In formula of the present invention, find that through the mosquito repellent experimental study Mozzie buster micro-capsule massfraction 10% repelling effect is good.
The washing powder of the present invention's formula not only has stronger soil removability, and has mosquito repellent function, safety, nontoxicity, stable performance.
Embodiment 1
A kind of mosquito repellent washing powder, comprise the raw material of following quality: QUWENCAO JINGYOU micro-capsule 5%, Sodium dodecylbenzene sulfonate 20%, water glass 8%, sodium sulfate 6%, fatty alcohol-polyoxyethylene ether 10%, white dyes 0.5%, essence 1%, water 10%.
Embodiment 2
A kind of mosquito repellent washing powder, comprise the raw material of following quality: QUWENCAO JINGYOU micro-capsule 10%, Sodium dodecylbenzene sulfonate 20%, water glass 8%, sodium sulfate 7%, fatty alcohol-polyoxyethylene ether 10%, white dyes 0.5%, essence 1%, water 10%.
Embodiment 2
A kind of mosquito repellent washing powder, comprise the raw material of following quality: QUWENCAO JINGYOU micro-capsule 15%, Sodium dodecylbenzene sulfonate 20%, water glass 8%, sodium sulfate 7%, fatty alcohol-polyoxyethylene ether 10%, white dyes 0.5%, essence 1%, water 10%.
The mosquito repellent test: choose 20 rats, cropping exposes the skin of belly 3cm * 3 cm, will test with sample and reference substance and evenly smear by 2.0mg/cm, and rest part tightly hides.The mosquito repellent detergent liquid is the repellent group, and deionized water is the blank group.After painting water, after 1 h, rat is put into to mosquito cage 5 min of 100, observe and have or not mosquito to stop dropping on the epidermis of exposure, per hour test 1 time later, namely sentence inefficacy as long as there is 1 mosquito to stop falling.Revision test 3 times, the average effective mosquito repellent time and effective mosquito repellent rate of recording sample.
| ? | Blank group | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Effective mosquito repellent time | 0 | 74% | 100% | 100% |
| Effective mosquito repellent rate | 0 | 4h | 10h | 10h |
The mosquito repellent test-results shows, the Mozzie buster mass percent is in 10% left and right, and the effect of mosquito repellent is best, and the mosquito repellent time is better.
Claims (2)
1. mosquito repellent washing powder, it is characterized in that being formed by the component of following mass percent meter: QUWENCAO JINGYOU micro-capsule 5-15%, Sodium dodecylbenzene sulfonate 10-25%, water glass 6-8%, sodium sulfate 1-7%, fatty alcohol-polyoxyethylene ether 2-10%, white dyes 0.2-0.7%, essence 0.5-1%, water 5-10%.
2. a kind of mosquito repellent washing powder according to claim 1, is characterized in that the preparation method of described QUWENCAO JINGYOU micro-capsule is, (1) takes QUWENCAO JINGYOU and tween-80, and mass ratio is 1:4, quick homogeneous emulsification; (2) water intaking in proportion again, be heated to 80 ℃, add beta-cyclodextrin that it is dissolved fully, water and beta-cyclodextrin mass ratio are 100:15, (3) then drip the uniform QUWENCAO JINGYOU of above-mentioned emulsification to cyclodextrin aqueous solution, QUWENCAO JINGYOU and beta-cyclodextrin mass ratio are 3:5-15, inclusion 3.0h under 50 ℃ of stirrings; Naturally cool to room temperature, essence is put 24h, and the microcapsule of formation are from solution, separating out, and through separating, concussion is dry, obtains the QUWENCAO JINGYOU micro-capsule.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013103726966A CN103409247A (en) | 2013-08-23 | 2013-08-23 | Mosquito-expelling washing powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013103726966A CN103409247A (en) | 2013-08-23 | 2013-08-23 | Mosquito-expelling washing powder |
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| CN103409247A true CN103409247A (en) | 2013-11-27 |
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| CN2013103726966A Withdrawn CN103409247A (en) | 2013-08-23 | 2013-08-23 | Mosquito-expelling washing powder |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105002011A (en) * | 2015-07-23 | 2015-10-28 | 安徽省三环纸业集团香料科技发展有限公司 | Perfume with nerve soothing and sleep aiding functions for detergent and preparing method thereof |
| CN105039016A (en) * | 2015-07-23 | 2015-11-11 | 安徽省三环纸业集团香料科技发展有限公司 | Spice used for antimicrobial and acarus killing washing powder and preparation method of spice |
| CN105039018A (en) * | 2015-07-23 | 2015-11-11 | 安徽省三环纸业集团香料科技发展有限公司 | Detergent fragrance with anti-anxiety and refreshing functions and preparing method thereof |
| CN105062713A (en) * | 2015-07-23 | 2015-11-18 | 安徽省三环纸业集团香料科技发展有限公司 | Spice used for mosquito repellent detergent powder and preparation method for spice |
| CN105132207A (en) * | 2015-07-23 | 2015-12-09 | 安徽省三环纸业集团香料科技发展有限公司 | Sleep-improving perfume used in laundry detergent powder and preparation method thereof |
| CN108893205A (en) * | 2018-06-21 | 2018-11-27 | 界首市洁净日用品有限公司 | A kind of capsule-type powder laundry detergent |
| CN110423654A (en) * | 2019-08-02 | 2019-11-08 | 唐铁君 | Clean piece of the mosquito-proof laundry of one kind and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1350054A (en) * | 2000-10-20 | 2002-05-22 | 孙逸龙 | Non-toxic washing powder with long-acting scenting and mosquito repelling effect and its prepn |
| CN1680519A (en) * | 2004-04-05 | 2005-10-12 | 新疆芳香植物科技开发股份有限公司 | Microcapsules of essential oil from fragrant plants and preparation thereof |
| US20080214497A1 (en) * | 2007-02-15 | 2008-09-04 | Bioactives, Llc | Water dispersible policosanol cyclodextrin complex and method of its production |
| CN102776070A (en) * | 2012-08-15 | 2012-11-14 | 上海应用技术学院 | Transparent microcapsule flavoring rose essence and preparation method thereof |
-
2013
- 2013-08-23 CN CN2013103726966A patent/CN103409247A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1350054A (en) * | 2000-10-20 | 2002-05-22 | 孙逸龙 | Non-toxic washing powder with long-acting scenting and mosquito repelling effect and its prepn |
| CN1680519A (en) * | 2004-04-05 | 2005-10-12 | 新疆芳香植物科技开发股份有限公司 | Microcapsules of essential oil from fragrant plants and preparation thereof |
| US20080214497A1 (en) * | 2007-02-15 | 2008-09-04 | Bioactives, Llc | Water dispersible policosanol cyclodextrin complex and method of its production |
| CN102776070A (en) * | 2012-08-15 | 2012-11-14 | 上海应用技术学院 | Transparent microcapsule flavoring rose essence and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105002011A (en) * | 2015-07-23 | 2015-10-28 | 安徽省三环纸业集团香料科技发展有限公司 | Perfume with nerve soothing and sleep aiding functions for detergent and preparing method thereof |
| CN105039016A (en) * | 2015-07-23 | 2015-11-11 | 安徽省三环纸业集团香料科技发展有限公司 | Spice used for antimicrobial and acarus killing washing powder and preparation method of spice |
| CN105039018A (en) * | 2015-07-23 | 2015-11-11 | 安徽省三环纸业集团香料科技发展有限公司 | Detergent fragrance with anti-anxiety and refreshing functions and preparing method thereof |
| CN105062713A (en) * | 2015-07-23 | 2015-11-18 | 安徽省三环纸业集团香料科技发展有限公司 | Spice used for mosquito repellent detergent powder and preparation method for spice |
| CN105132207A (en) * | 2015-07-23 | 2015-12-09 | 安徽省三环纸业集团香料科技发展有限公司 | Sleep-improving perfume used in laundry detergent powder and preparation method thereof |
| CN108893205A (en) * | 2018-06-21 | 2018-11-27 | 界首市洁净日用品有限公司 | A kind of capsule-type powder laundry detergent |
| CN110423654A (en) * | 2019-08-02 | 2019-11-08 | 唐铁君 | Clean piece of the mosquito-proof laundry of one kind and preparation method thereof |
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Application publication date: 20131127 |