CN105342932A - All-natural multifunctional hand sanitizer containing carboxymethyl chitosan and production method thereof - Google Patents
All-natural multifunctional hand sanitizer containing carboxymethyl chitosan and production method thereof Download PDFInfo
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- CN105342932A CN105342932A CN201510912095.9A CN201510912095A CN105342932A CN 105342932 A CN105342932 A CN 105342932A CN 201510912095 A CN201510912095 A CN 201510912095A CN 105342932 A CN105342932 A CN 105342932A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention discloses an all-natural multifunctional hand sanitizer containing carboxymethyl chitosan and a production method thereof and relates to the technical field of washing products. Carboxymethyl chitosan is completely dissolved in deionized water firstly, then saponin and tea polyphenol are added, even stirring is conducted, pH is regulated to be 6.0-6.5 with a lemon juice solution after the mixture system is cooled to room temperature, color modulation is conducted with natural pigment, viscosity regulation is conducted with a sodium chloride solution, and then homogenizing, degassing and subpackaging are conducted. According to the method, technological requirements are low, preparation is easy and environmentally friendly, product stability is high, and the functions of decontamination, sterilization and skin moisturizing and care are realized.
Description
Technical field
The present invention relates to articles for washing technical field, particularly relate to the production technical field of handwashing liquid.
Technical background
Handwashing liquid is a kind of daily articles for washing, of a great variety, but handwashing liquid all contains a certain amount of chemosynthesis composition at present.Contacted many materials such as synthetic surfactant, antiseptic, organic solvent, easy chafe, cause the problem such as skin allergy, contact dermatitis, can damage skin, and also can produce necessarily direct or indirect impact to health, having can to environment again, so existing handwashing liquid can not meet people for many-sided demands such as health, antibacterial, healthy, beauty treatment, environmental protection, needs towards green, environmental protection, renewable future development.
Chitosan is unique a large amount of basic amine group polysaccharide existed in natural polysaccharide, and carboxymethyl chitosan is a kind of chitosan derivatives of polyampholyte.Carboxymethyl chitosan not only possesses the advantageous property of chitosan, and also have good water solublity, range of application is more extensive.It has the performances such as excellent antibiotic property, thickening property, dispersibility, emulsibility, moisture retention, film property, gelation; There is many good characteristics such as self zero toxicity, good biocompatibility and degradability; In addition Chitosan-phospholipid complex can also Antifungi, antibacterial and virus growth and breeding, there is good broad-spectrum sterilization.Its carboxyl of carboxymethyl chitosan and amino are all hydrophilic groups, stronger water absorption, 0.25% aqueous solution wettability is suitable with 20% propylene glycol, there is good moisture retention, and it and hyaluronic acid have quite similar molecular structure, its performance is suitable with hyaluronic acid, is expected to alternative hyaluronic acid.
Fructus Gleditsia, has another name called honey locust, is one of China distinctive Caesalpiniaceae Gleditsia seeds, and Qin Han dynasty people just start to carry out washed and hair with Fructus Gleditsia, form convention to Tang of Sui.Gleditisia sinensis Saponin is the triterpene saponin being extensively present in Gleditsia, is the natural non-ionic surface active agent that a class is excellent, is optimal natural cleaning agent.China's Fructus Gleditsia aboundresources, southwest is wild Fructus Gleditsia annual production just ton up to ten thousand only, and containing 15% ~ 32% Saponin in Fructus Gleditsia fruit, so Gleditisia sinensis Saponin has as raw material, source is wide, aboundresources, cheap feature.In addition, Gleditisia sinensis Saponin in neutrality, the strong foaming abundancy of surface activity, nontoxic use safety, non-stimulated to skin, easy degraded do not produce secondary pollution to environment, except there is washing function, also have and keep healthy and sterilizing function.It also has the performances such as emulsibility, dispersibility, solubility, impregnability as plant surface activating agent, is better than any chemical, thus has very high Development volue.
Tea polyphenols is the general name of Polyphenols of Tea, has the formation of shielding of ultraviolet, check melanin; Scavenging free radicals, anti-skin oxidative; Remove greasy, effect such as convergence pore etc., experiment shows, the clearance rate of tea polyphenols to reactive oxygen free radical reaches more than 98%, have well suppress bactericidal property to burst skin ulcer, S.mutans and mucormycosis, penicillium, gibberella, anthrax bacteria, cereuisiae fermentum etc. of bacillus subtilis, staphylococcus aureus, escherichia coli, Fructus Lycopersici esculenti in addition, there is good antisepsis, and free from extraneous odour, the feature such as have no side effect.
Plants essential oil is a class plant source secondary metabolites, is that a class has bioactive chemical substance.Botany is called quintessence oil, commercial title aromatic oil, chemistry and pharmaceutically claim volatile oil.Be made up of chemical moleculars such as aldehyde, alcohol, ketone, phenol, alkene, monoterpene, diterpene and sesquiterpenes, its chemical composition is quite complicated.Have and promote the effect such as lymph circulation, removing toxin, adjustment endo-exocrine gland, the regeneration of promotion histiocyte.The annual quintessence oil total output of China reaches 15000-20000 ton, natural essential oil is exactly one of raw material of daily chemical products for a long time, be commonly used to prepare essence, perfume, but along with going deep into of research, and the raising of people's quality of life and the reinforcement of environmental consciousness, plants essential oil parasite killing, antibacterial and anticorrosion etc. in function, be also day by day subject to concern and the attention of people, therefore the application of plants essential oil also expands gradually.
Summary of the invention
The object of the invention is for the defect existing for current handwashing liquid recited above and the deficiencies in the prior art, propose a kind of containing any chemosynthesis composition, existing clean decontamination, has again antibiotic and sterilizing, moistens the All Pure Nature handwashing liquid of the multi-functional health such as nursing skin, environmental protection.
The present invention includes carboxymethyl chitosan, Saponin, tea polyphenols, natural pigment, sodium chloride, Fructus Citri Limoniae juice and deionized water, described carboxymethyl chitosan account for handwashing liquid gross mass 0.5 ~ 2.0%, Saponin account for handwashing liquid gross mass 6.0 ~ 12.0%, tea polyphenols account for handwashing liquid gross mass 0.2 ~ 1.0%, natural pigment account for handwashing liquid gross mass 0.05 ~ 0.2%, sodium chloride accounts for 0.1 ~ 1.0% of handwashing liquid gross mass.
Superiority of the present invention:
1. the present invention utilizes the functions such as the strong surface activity of natural Saponin, antibacterial, emulsifying; The functions such as carboxymethyl chitosan thickening, antibacterial, moisturizing; Tea polyphenols antioxidation, convergence pore, the function such as antibacterial; Toning effect of natural plant pigment etc., pure natural manufacture, not containing any chemosynthesis compositions such as artificial essence, pigment, synthetic preservative, organic solvents.
2. the present invention has fully clean dirt-removing power, foaming abundancy and stablizing, and easily rinse, the clean result that can have under hard water and normal temperature condition, product has certain viscosity, can stop on hand, the simple and elegant fragrance of abnormal smells from the patient.
3. product subacidity of the present invention, non-stimulated to skin, safe without toxic side effect; Product antibiotic and sterilizing, also have concurrently and moisten nursing and improve skin metabolism, alleviate and prevent functions such as chapping, be applicable to various personage and use.
4. product good biocompatibility of the present invention, environmental protection; Raw material resources are enriched, and price is cheaper.
Further, the present invention also comprises the natural refined plant oil of interpolation, natural plant essential oils or hydrosol.The natural refined plant oil of described interpolation accounts for 0.5 ~ 2.0% of handwashing liquid gross mass.
Refined plant oil has skin protection, the excellent results such as soft and smooth and moist; And plants essential oil has multiple efficacies such as cell regeneration, antibacterial and anticorrosion, light pleasant adjustment odor types.
Another object of the present invention is the production method proposing All Pure Nature multifunctional liquid soap.
The inventive method is: under 40 ~ 65 DEG C of stirrings, first carboxymethyl chitosan is dissolved in deionized water completely, then Saponin is added and tea polyphenols stirs, after system to be mixed is down to room temperature, with Fructus Citri Limoniae juice solution adjustment pH to 6.0 ~ 6.5, with natural pigment toning, adjust viscosity with sodium chloride solution, then homogenizing, degassed, subpackage.Described Saponin account for handwashing liquid always feed intake quality 6.0 ~ 12.0%, carboxymethyl chitosan account for handwashing liquid always feed intake quality 0.5 ~ 2.0%, tea polyphenols account for handwashing liquid always feed intake quality 0.2 ~ 1.0%, natural pigment account for handwashing liquid always feed intake quality 0.05 ~ 0.2%, sodium chloride accounts for handwashing liquid and always to feed intake 0.1 ~ 1.0% of quality.
The inventive method technological requirement is low, and preparation process is simple, environmental protection, and product stability is good.
In addition, when adding Saponin and tea polyphenols, also add natural refined plant oil, described interpolation natural refined plant oil accounts for handwashing liquid and always to feed intake 0.5 ~ 2.0% of quality.
Quintessence oil is made up of, because high fluidity, so be called " oil " chemical moleculars such as terpenes, aldehydes, esters, alcohols; Vegetable oil main component is triglyceride and fatty acid composition, and both have difference in essence.
Vegetable oil, mainly from fruit and the seed of plant, also has part come from leaf, stem, the root of plant and spend.Natural enriched vegetable oil is suitable in various formula, along with people more and more tend to " back to nature advocates green ", and the raising of plant extract and purification technique, the application of crude vegetal progressively becomes focus.In this formula, add vegetable oil mainly play skin protection, the effect such as soft and smooth and moist, wash rear moist.
Natural plant essential oils all has boiling point low and volatile feature.Some of them chemical composition has thermal sensitivity, and especially some lipoid substance thermostabilitys are poor.The present invention adopts and add natural plant essential oils or hydrosol before tune viscosity.
The difference of special instruction natural plant essential oils and natural plants hydrosol:
Hydrosol, also known as crystal's oil, being a kind of 100% saturated distillation stock solution separated when refining quintessence oil, is a kind of side-product of quintessence oil.The composition of multiple preciousness in plant has been incorporated in hydrosol water, and containing have an appointment 0.3 ~ 0.5% quintessence oil water soluble ingredient, so still possess the fragrance of quintessence oil, part curative effect and slight antibiotic property, and containing the unexistent plant essence of quintessence oil (as tannin and flavonoid).Hydrosol has adjustment, purification, antiinflammatory, astriction, controls fat secretion, and make skin sore wound accelerate healing, oiliness, skin sore skin are especially applicable.It and plants essential oil itself have akin effect and effect, and composition is natural pure, and fragrance is light pleasant.Have certain complementary effect between hydrosol and corresponding quintessence oil, collocation use can allow better effects if.
The present invention is as adopted hydrosol, then price is cheap compared with quintessence oil, and production cost has more advantage.
Saponin of the present invention is Gleditisia sinensis Saponin or tea saponin; Described natural pigment be in S. haematocheir Huang, safflower yellow, purple Radix Ipomoeae, Rhizoma Curcumae Longae, cochineal or monascus red pigment at least any one.
Described Fructus Citri Limoniae juice is Fresh Lemon deionized water dilution after squeezing, extracting juice, the supernatant clarified with carboxymethyl chitosan solution.
Described natural refined plant oil is Oleum Vitis viniferae, Radix Oenotherae erythrosepalae oil, Rosehips oil, Semen pruni armeniacae oil, in Oleum Hippophae or Jojoba oil at least any one, described natural plant essential oils or hydrosol be in Camellia sinensis, Herba Menthae, Folium eucalypti globueli (Eucalyptus globulus Labill.), Lignum cinnamomi camphorae, Flos Pelargonii, cypress, Rhizoma Zingiberis Recens quintessence oil or Jiang Chunlu at least any one.
Detailed description of the invention
Further illustrate technical solution of the present invention below in conjunction with detailed description of the invention, embodiment can not be interpreted as it is restriction to technical scheme.
One, preparation technology:
Embodiment 1: take 1kg deionized water and add in flask, be heated to 40 ~ 65 DEG C (this example adopts 55 DEG C), first adding the stirring of 10g carboxymethyl chitosan makes it dissolve completely, add 60.0g Saponin again, 4.0g tea polyphenols stirs, after dropping to room temperature by Fructus Citri Limoniae juice adjustment solution ph to 6.0, to be adjusted to pink with natural lanigerin, 1mL tea tree ethereal oil adjustment odor type, the sodium chloride solution that slowly adds 5% be adjusted to moderate viscosity, then homogenizing, degassed, subpackage.
Embodiment 2: take 8kg deionized water and add in reactor, be heated to 40 ~ 65 DEG C (this example adopts 45 DEG C), first adding the stirring of 0.1kg carboxymethyl chitosan makes it dissolve completely, add 0.9kg Saponin again, 0.05kg tea polyphenols, 60mL Oleum Vitis viniferae stir, after dropping to room temperature by Fructus Citri Limoniae juice adjustment solution ph to 6.5, to be adjusted to neutral red Gardenia Yellow that amber, the natural Peppermint essential oil of 10mL adjusts odor type, the sodium chloride solution that slowly adds 5% is adjusted to moderate viscosity, 10Kg is complemented to deionized water, then homogenizing, degassed, subpackage.
Embodiment 3,4,5,6:
Other condition, with reference to embodiment 2, only adjusts each raw material dosage.
Product main component addition (finished product is in 1kg) of the present invention
In addition, the Saponin in above each example can adopt Gleditisia sinensis Saponin or tea saponin.
Natural pigment can adopt in S. haematocheir Huang, safflower yellow, purple Radix Ipomoeae, Rhizoma Curcumae Longae, cochineal or monascus red pigment at least any one.
Fructus Citri Limoniae juice is Fresh Lemon deionized water dilution after squeezing, extracting juice, the supernatant clarified with carboxymethyl chitosan solution.
Natural refined plant oil is Oleum Vitis viniferae, Radix Oenotherae erythrosepalae oil, Rosehips oil, Semen pruni armeniacae oil, in Oleum Hippophae or Jojoba oil at least any one.
Natural plant essential oils or hydrosol be in Camellia sinensis, Herba Menthae, Folium eucalypti globueli (Eucalyptus globulus Labill.), Lignum cinnamomi camphorae, Flos Pelargonii, cypress, Rhizoma Zingiberis Recens quintessence oil or Jiang Chunlu at least any one.
Two, Product checking result:
Following table is the leading indicator testing result such as sense organ, physicochemical property, microorganism of embodiment 2 product.
Through detecting, this product indices all meets QB2654-2004 relevant national standard.
Carry out indices detection to implement 1,3,4,5,6, result roughly the same.
Claims (10)
1. the All Pure Nature multifunctional liquid soap containing carboxymethyl chitosan, it is characterized in that comprising carboxymethyl chitosan, Saponin, tea polyphenols, natural pigment, sodium chloride, Fructus Citri Limoniae juice and deionized water, described carboxymethyl chitosan account for handwashing liquid gross mass 0.5 ~ 2.0%, Saponin account for handwashing liquid gross mass 6.0 ~ 12.0%, tea polyphenols account for handwashing liquid gross mass 0.2 ~ 1.0%, natural pigment account for handwashing liquid gross mass 0.05 ~ 0.2%, sodium chloride accounts for 0.1 ~ 1.0% of handwashing liquid gross mass.
2. handwashing liquid according to claim 1, characterized by further comprising and add natural refined plant oil, and the natural refined plant oil of described interpolation accounts for 0.5 ~ 2.0% of handwashing liquid gross mass.
3. handwashing liquid according to claim 1 or 2, characterized by further comprising natural plant essential oils or hydrosol.
4. the production method of All Pure Nature multifunctional liquid soap as claimed in claim 1, is characterized in that, under 40 ~ 65 DEG C of stirrings, being first dissolved in completely in deionized water by carboxymethyl chitosan, then adds after Saponin and tea polyphenols stir; After system to be mixed is down to room temperature, with Fructus Citri Limoniae juice solution adjustment pH to 6.0 ~ 6.5, with natural pigment toning, adjust viscosity with sodium chloride solution, then homogenizing, degassed, subpackage; Described carboxymethyl chitosan account for handwashing liquid always feed intake quality 0.5 ~ 2.0%, Saponin account for handwashing liquid always feed intake quality 6.0 ~ 12.0%, tea polyphenols account for handwashing liquid always feed intake quality 0.2 ~ 1.0%, natural pigment account for handwashing liquid always feed intake quality 0.05 ~ 0.2%, sodium chloride accounts for handwashing liquid and always to feed intake 0.1 ~ 1.0% of quality.
5. the production method of All Pure Nature multifunctional liquid soap according to claim 4, is characterized in that when adding Saponin and tea polyphenols, also adds natural refined plant oil, and the natural refined plant oil of described interpolation accounts for handwashing liquid and always to feed intake 0.5 ~ 2.0% of quality.
6. the production method of All Pure Nature multifunctional liquid soap according to claim 4 or 5, is characterized in that, before tune viscosity, adding natural plant essential oils or hydrosol.
7. the production method of All Pure Nature multifunctional liquid soap according to claim 4, is characterized in that described Saponin is Gleditisia sinensis Saponin or tea saponin.
8. the production method of All Pure Nature multifunctional liquid soap according to claim 4, it is characterized in that described natural pigment be in S. haematocheir Huang, safflower yellow, purple Radix Ipomoeae, Rhizoma Curcumae Longae, cochineal or monascus red pigment at least any one.
9. the production method of All Pure Nature multifunctional liquid soap according to claim 4, is characterized in that described Fructus Citri Limoniae juice is Fresh Lemon deionized water dilution after squeezing, extracting juice, the supernatant clarified with carboxymethyl chitosan solution.
10. the production method of All Pure Nature multifunctional liquid soap according to claim 6, it is characterized in that described natural refined plant oil is Oleum Vitis viniferae, Radix Oenotherae erythrosepalae oil, Rosehips oil, Semen pruni armeniacae oil, in Oleum Hippophae or Jojoba oil at least any one, described natural plant essential oils or hydrosol be in Camellia sinensis, Herba Menthae, Folium eucalypti globueli (Eucalyptus globulus Labill.), Lignum cinnamomi camphorae, Flos Pelargonii, cypress, Rhizoma Zingiberis Recens quintessence oil or Jiang Chunlu at least any one.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105997826A (en) * | 2016-07-18 | 2016-10-12 | 鄢海军 | Nano-silver-containing traditional Chinese medicine liquid soap for infants and children |
| CN106265380A (en) * | 2016-10-14 | 2017-01-04 | 柳州立洁科技有限公司 | A kind of handwashing liquid |
| CN106726956A (en) * | 2016-12-23 | 2017-05-31 | 严志海 | A kind of antibacterial skin moistening liquid soap and preparation method thereof |
| CN107496206A (en) * | 2016-06-14 | 2017-12-22 | 中国科学院理化技术研究所 | A kind of chitosan derivatives base children special-purpose non-water hand cleanser and preparation method thereof |
| CN108165378A (en) * | 2017-11-23 | 2018-06-15 | 汪锦川 | A kind of manufacture of pure natural liquid detergent and processing technology |
| CN112391242A (en) * | 2020-11-16 | 2021-02-23 | 四川宸煜林业开发有限责任公司 | Laundry detergent containing camphor oil component and preparation method thereof |
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| CN1696145A (en) * | 2005-04-29 | 2005-11-16 | 北京林业大学 | Technique for preparing saponin of gleditschia horrida and application |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107496206A (en) * | 2016-06-14 | 2017-12-22 | 中国科学院理化技术研究所 | A kind of chitosan derivatives base children special-purpose non-water hand cleanser and preparation method thereof |
| CN105997826A (en) * | 2016-07-18 | 2016-10-12 | 鄢海军 | Nano-silver-containing traditional Chinese medicine liquid soap for infants and children |
| CN106265380A (en) * | 2016-10-14 | 2017-01-04 | 柳州立洁科技有限公司 | A kind of handwashing liquid |
| CN106726956A (en) * | 2016-12-23 | 2017-05-31 | 严志海 | A kind of antibacterial skin moistening liquid soap and preparation method thereof |
| CN108165378A (en) * | 2017-11-23 | 2018-06-15 | 汪锦川 | A kind of manufacture of pure natural liquid detergent and processing technology |
| CN112391242A (en) * | 2020-11-16 | 2021-02-23 | 四川宸煜林业开发有限责任公司 | Laundry detergent containing camphor oil component and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN105342932B (en) | 2019-03-05 |
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