CN109908046A - A kind of surfactant and preparation method of the ingredient containing natural citrus - Google Patents
A kind of surfactant and preparation method of the ingredient containing natural citrus Download PDFInfo
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- CN109908046A CN109908046A CN201910136726.0A CN201910136726A CN109908046A CN 109908046 A CN109908046 A CN 109908046A CN 201910136726 A CN201910136726 A CN 201910136726A CN 109908046 A CN109908046 A CN 109908046A
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- citrus
- extract
- aloe
- surfactant
- tangerine oil
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Abstract
The present invention provides the surfactant formulas and preparation method of a kind of ingredient containing natural citrus.Containing active skull cap components such as citrus flavonoids extract, aloe extract, tangerine oils in the formula, natural anti-oxidation and replenishing water and preserving moisture and other effects can be reached, while also cleanable skin inhibits bacteria breed, product itself also possesses the natural orange perfume of citrus.Wherein, citrus flavonoids extract from citrus peel residue, and the prices of raw materials are cheap, and pass it through specially treated and extract the effect of being added in cosmetics, improving cosmetics after beneficiating ingredient, and increase the utilization ways of skin slag, reduce resource waste.
Description
Technical field
The invention belongs to cosmetic fields, and in particular to a kind of surfactant formula of the ingredient containing natural citrus and preparation side
Method.
Background technique
Citrus flavonoids are a kind of compounds with strong bioactivity, research shows that it is as strong oxidizer, freedom
Base scavenger, divalent cation chelators and lipid peroxy agent in anticancer, antiviral, anti-inflammatory, strengthen capillary, anti-mistake
Quick aspect important role.Research is it is also shown that citrus flavonoids have extensive inhibiting effect, such as Staphylococcus aureus to bacterium
Bacterium, Escherichia coli and salmonella typhi；0.005% free isoflavones may also suppress the activity of fungi.
Plants essential oil is the intracorporal secondary metabolites of plant, is made of the relatively small simple compounds of molecular weight,
The oily liquids substance that can be volatilized under room temperature.Tangerine oil is the major class in plants essential oil, colorless and transparent, has tempting tangerine
Fragrance is one of common natural perfume material, is mainly used to deploy food essence, and be used in the daily necessities such as perfume, toothpaste, perfumed soap,
Research shows that tangerine oil have the effects that it is antibacterial, anti-oxidant.
To sum up, in view of antibacterial, the antioxidation of the above citrus flavonoids and tangerine oil, thus there is being developed as
The great potential of cosmetic beneficiating ingredient.
On the other hand, citrus peel residue is the by-product of citrus juicing processing.It is currently used primarily in production fertilizer and feed, it is few
For amount for extracting citrus pectin and flavonoids etc., utilization rate is not high.Increasing skin slag application approach is to solve the wasting of resources, improve skin
Slag utilization rate increases the practical approach that citrus adds the output value.
Summary of the invention
In view of this, the present invention provides a kind of surfactant formula of the ingredient containing natural citrus and the preparation side of Related product
Method contains the active skull cap components such as citrus flavonoids and tangerine oil in the formula, wherein citrus flavonoids extract from orange peel
Slag.
To achieve the above object, the technical solution of the present invention is as follows:
A kind of surfactant of the ingredient containing natural citrus, includes following components by mass parts: 2~10 parts of glycerol, propylene glycol 2
~10 parts, 2~10 parts of dehydrated alcohol, 0.1~4 part of citrus flavonoids extract, 0~2 part of aloe extract, tangerine oil 0.1
~1 part.
Preferably, the surfactant of a kind of ingredient containing natural citrus, includes following components by mass parts: 10 parts of glycerol, the third two
8 parts of alcohol, 6 parts of dehydrated alcohol, 2 parts of citrus flavonoids extract, 1 part of aloe extract, 0.5 part of tangerine oil.
Further, which further includes following components: deionized water, citric acid, sodium hydroxide.Wherein citric acid, hydrogen
Sodium oxide molybdena is for adjusting pH value of solution.
Further, the citrus flavonoids extract includes one of aurantiin, aurantiamarin, polymethoxy flavones or more
Kind.
Further, the ingredient of the tangerine oil include monoterpenes, terpenes, esters it is one or more.
The present invention also provides a kind of preparation methods of the surfactant of ingredient containing natural citrus.
A kind of preparation method of the surfactant of the ingredient containing natural citrus, includes the following steps:
1) glycerol, propylene glycol, dehydrated alcohol are uniformly mixed by above-mentioned mass ratio；
2) citrus flavonoids extract and aloe extract are separately added into the mixture of step 1) by above-mentioned mass ratio；
3) appropriate tangerine oil is taken, is dissolved in the solution of step 2)；
4) it takes appropriate plasma water to be added in the solution of step 3) and is settled to 100ml；
5) citric acid is added and sodium hydroxide adjusts pH to 4.5-7.5；
6) de-soak；4 DEG C of refrigerators, which are stood, to be saved.
The present invention also provides a kind of preparation methods of citrus flavonoids extract.
A kind of preparation method of above-mentioned citrus flavonoids extract, includes the following steps:
1) citrus sample is obtained；
2) it is added 4-5 times of sample volume and measures the ethyl alcohol that mass fraction is 70%-90%, in 70-75 DEG C of extraction 2-3h, reflux
Filtering obtains filtrate；3-4 times is added in filter residue again and measures the ethyl alcohol that mass fraction is 70%-80%, in 70-75 DEG C of extraction 2-
3h, reflux and filter obtain filtrate；Merging filtrate；
3) filtrate being collected into is concentrated through 45-60 DEG C, is concentrated into the 1/3-1/4 of extracting liquid volume, collecting concentrate is
?.
Further, citrus sample is the citrus peel residue by specially treated.
The present invention also provides the composition of the ingredient containing natural citrus and applications.
A kind of composition anti-oxidant for skin, replenishing water and preserving moisture, the composition by glycerol, citrus flavonoids extract,
Tangerine oil, aloe composition, glycerol, citrus flavonoids extract, tangerine oil, aloe mass ratio be 2~10:0.1~4:
0.1~1:2.
It is a kind of for cleaning the composition of sebum, antibacterial anti-acne, the composition is by dehydrated alcohol, tangerine oil, aloe group
Mass ratio at, dehydrated alcohol, tangerine oil, aloe is 2~10:0.1~1:1~2.
Application of the above-mentioned citrus flavonoids extract as natural bacteriostatic agent in cosmetics.
The beneficial effects of the present invention are:
1) present invention is applied in toner using the flavonoids extracted in citrus peel residue as natural, and auxiliary
Using natural essential oil (being obtained in skin slag) as fragrance component.Make this product while moisturizing moisturizing, also cleanable skin inhibits
Bacteria breed, while possessing the natural orange perfume of citrus.
2) using cheap citrus peel residue as raw material, the extract of acquisition is added in cosmetics.By waste
It is converted into skin care raw material, the utilization ways of skin slag is increased, reduces resource waste.
Specific embodiment
The preferred embodiment of the present invention is described in detail below.The experiment of actual conditions is not specified in preferred embodiment
Method, usually according to normal condition, illustrated embodiment are to preferably be illustrated to the contents of the present invention, but are not this
The content of invention is only limitted to illustrated embodiment.So those skilled in the art are according to foregoing invention content to embodiment
Nonessential modifications and adaptations are carried out, protection scope of the present invention is still fallen within.
Embodiment 1
Extract citrus peel residue flavonoids
1) sample preparation.Citrus peel residue is chosen, cleans up and dries.
2) it extracts.It is added 4-5 times of volume of skin slag and measures 70%-90% (v/v) ethyl alcohol, at 70-75 DEG C, extract 2-3h, reflux
Filtering obtains filtrate；3-4 times is added in filter residue again and measures 70%-80% (v/v) ethyl alcohol, and 70-75 DEG C of extraction 2-3h flowed back
Filter obtains filtrate；Merging filtrate.
3) it is concentrated.The filtrate being collected into, 45-60 DEG C of concentration, until being concentrated into extracting liquid volume without concentrate is released after alcohol taste
1/3-1/4, collect concentrate to obtain the final product.
4) ethyl alcohol recycles, and is recycled.
5) it stores.The concentrate freezer of acquisition is saved.
Embodiment 2
Surfactant production technology
1) it is formulated
A phase: glycerol 2%~10%, propylene glycol 2%~10%, dehydrated alcohol 2%~10%；
B phase: citrus flavonoids extract 0.1%~4%, aloe extract 0%~2%；
C phase: tangerine oil 0.1%~1%；
D phase: deionized water surplus；
E phase: citric acid, potassium hydroxide.
2) technique
1. taking A phase reagent, mix；
2. B phase constituent is added sequentially in A phase；
3. taking appropriate essential oil in C phase, it is dissolved in solution；
4. D is added in mixture 3. and is settled to 100ml；
5. E phase is added, pH to 4.5-7.5 is adjusted；
6. de-soak；4 DEG C of refrigerators, which are stood, to be saved.
Embodiment 3
It is preferred that toner formula
Toner is prepared according to the technique of embodiment 2, ingredient lists are as follows:
Table 1
| Ingredient | Account for mass ratio |
| Deionized water | 72.43% |
| Glycerol | 10.00% |
| Propylene glycol | 8.00% |
| Dehydrated alcohol | 6.00% |
| Citrus flavonoids extract | 2.00% |
| Aloe extract | 1.00% |
| Tangerine oil | 0.50% |
| Sodium hydroxide | 0.05% |
| Citric acid | 0.02% |
Embodiment 4
Comparative example 1
Toner is prepared according to the technique of embodiment 2, ingredient lists are as follows:
Table 2
Embodiment 5
Comparative example 2
Toner is prepared according to the technique of embodiment 2, ingredient lists are as follows:
Table 3
| Ingredient | Account for mass ratio |
| Deionized water | 74.43% |
| Glycerol | 10.00% |
| Propylene glycol | 8.00% |
| Dehydrated alcohol | 6.00% |
| Aloe extract | 1.00% |
| Tangerine oil | 0.50% |
| Sodium hydroxide | 0.05% |
| Citric acid | 0.02% |
Experiment investigation is carried out to embodiment 3, comparative example 1~2, main project of investigating is skin moisture content measurement.
1) embodiment 3, the measurement of 1~2 moisturizing antioxidant effect of comparative example
30 volunteers are recruited, women, 18~50 years old, skin of face was relatively dry, was randomly divided into 3 groups.Test item includes:
Skin moisture content test, skin water loss test.Unilateral cheek uses this product 4 weeks.
Table 6
Finally, it is stated that the above examples are only used to illustrate the technical scheme of the present invention and are not limiting, although referring to compared with
Good embodiment describes the invention in detail, those skilled in the art should understand that, it can be to skill of the invention
Art scheme is modified or replaced equivalently, and without departing from the objective and range of technical solution of the present invention, should all be covered at this
In the scope of the claims of invention.
Claims (10)
1. a kind of surfactant of ingredient containing natural citrus, which is characterized in that by mass parts include following components: 2~10 parts of glycerol,
2~10 parts of propylene glycol, 2~10 parts of dehydrated alcohol, 0.1~4 part of citrus flavonoids extract, 0~2 part of aloe extract, citrus
0.1~1 part of essential oil.
2. surfactant according to claim 1, which is characterized in that further include following components: deionized water, citric acid, hydrogen
Sodium oxide molybdena.
3. surfactant according to claim 1, which is characterized in that the citrus flavonoids extract includes aurantiin, orange
One of skin glycosides, polymethoxy flavones are a variety of.
4. surfactant according to claim 1, which is characterized in that the ingredient of the tangerine oil includes monoterpenes, terpenes
Class, esters it is one or more.
5. the preparation method of the surfactant of the ingredient containing natural citrus described in claim any one of 1-4, which is characterized in that including such as
Lower step:
1) glycerol, propylene glycol, dehydrated alcohol are uniformly mixed by above-mentioned mass ratio；
2) citrus flavonoids extract and aloe extract are separately added into the mixture of step 1) by above-mentioned mass ratio；
3) appropriate tangerine oil is taken, is dissolved in the solution of step 2)；
4) it takes appropriate plasma water to be added in the solution of step 3) and is settled to 100ml；
5) citric acid is added and sodium hydroxide adjusts pH to 4.5-7.5；
6) de-soak；4 DEG C of standings save.
6. the preparation method of citrus flavonoids extract described in a kind of claim 3, which comprises the steps of:
1) citrus sample is obtained；
2) ethyl alcohol that 4-5 times of sample volume of addition measures that mass fraction is 70%-90% flowed back in 70-75 DEG C of extraction 2-3h
Filter obtains filtrate；3-4 times is added in filter residue again and measures the ethyl alcohol that mass fraction is 70%-80%, in 70-75 DEG C of extraction 2-3h,
Reflux and filter obtains filtrate, merging filtrate；
3) filtrate being collected into is concentrated through 45-60 DEG C, is concentrated into the 1/3-1/4 of extracting liquid volume, collect concentrate to obtain the final product.
7. preparation method according to claim 6, which is characterized in that the citrus sample is citrus peel residue.
8. a kind of composition anti-oxidant for skin, replenishing water and preserving moisture, which is characterized in that by glycerol, citrus flavonoids extract,
Tangerine oil, aloe composition, glycerol, citrus flavonoids extract, tangerine oil, aloe mass ratio be 2~10:0.1~4:
0.1~1:2.
9. a kind of for cleaning the composition of sebum, antibacterial anti-acne, which is characterized in that by dehydrated alcohol, tangerine oil, aloe group
Mass ratio at, dehydrated alcohol, tangerine oil, aloe is 2~10:0.1~1:1~2.
10. application of the citrus flavonoids extract as natural bacteriostatic agent in cosmetics described in claim 3.
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| CN201910136726.0A CN109908046A (en) | 2019-02-25 | 2019-02-25 | A kind of surfactant and preparation method of the ingredient containing natural citrus |
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|---|---|---|---|
| CN201910136726.0A CN109908046A (en) | 2019-02-25 | 2019-02-25 | A kind of surfactant and preparation method of the ingredient containing natural citrus |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112336780A (en) * | 2019-08-07 | 2021-02-09 | 宁波瀚微国际贸易有限公司 | Citrus bacteriostat and preparation method and application thereof |
| WO2021143096A1 (en) * | 2020-01-19 | 2021-07-22 | 广东药科大学 | Whitening, acne-removing, blackhead-removing and anti-aging composition, and use and preparation thereof |
| CN114306139A (en) * | 2021-12-30 | 2022-04-12 | 海南无限美好智慧科技有限公司 | Natural plant essential oil acne-removing repairing liquid and preparation method thereof |
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| CN107737059A (en) * | 2017-12-04 | 2018-02-27 | 刘晓冰 | A kind of centella whitening lotion |
| CN107789263A (en) * | 2016-08-31 | 2018-03-13 | 张恒元 | A kind of aloe smoothing toner |
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| CN106038340A (en) * | 2016-07-06 | 2016-10-26 | 南方医科大学 | Traditional Chinese medicine component containing bamboo leaf flavonoid and with anti-oxidation function and application of traditional Chinese medicine component to cosmetics |
| CN107789263A (en) * | 2016-08-31 | 2018-03-13 | 张恒元 | A kind of aloe smoothing toner |
| CN107737059A (en) * | 2017-12-04 | 2018-02-27 | 刘晓冰 | A kind of centella whitening lotion |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112336780A (en) * | 2019-08-07 | 2021-02-09 | 宁波瀚微国际贸易有限公司 | Citrus bacteriostat and preparation method and application thereof |
| WO2021143096A1 (en) * | 2020-01-19 | 2021-07-22 | 广东药科大学 | Whitening, acne-removing, blackhead-removing and anti-aging composition, and use and preparation thereof |
| CN114306139A (en) * | 2021-12-30 | 2022-04-12 | 海南无限美好智慧科技有限公司 | Natural plant essential oil acne-removing repairing liquid and preparation method thereof |
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Application publication date: 20190621 |