JPH07126129A - Hair-growing agent and cosmetic for hair containing the same - Google Patents
Hair-growing agent and cosmetic for hair containing the sameInfo
- Publication number
- JPH07126129A JPH07126129A JP5274686A JP27468693A JPH07126129A JP H07126129 A JPH07126129 A JP H07126129A JP 5274686 A JP5274686 A JP 5274686A JP 27468693 A JP27468693 A JP 27468693A JP H07126129 A JPH07126129 A JP H07126129A
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- JP
- Japan
- Prior art keywords
- hair
- citrus
- seeds
- extract
- cosmetic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
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- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
Description
【０００１】[0001]
【産業上の利用分野】本発明は、育毛剤及びこれを含有
する頭髪用化粧料に関し、詳しくは、柑橘類種子の圧搾
物及び／又は抽出物からなる育毛剤及びこれを含有する
頭髪用化粧料に関する。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a hair restorer and a cosmetic for hair containing the same, and more specifically, a hair restorer comprising a pressed product and / or an extract of citrus seeds and a cosmetic for hair containing the same. Regarding
【０００２】[0002]
【従来の技術】いつまでも豊富で黒く美しい頭髪を保持
することは、老若男女を問わず、多くの人の願いであっ
た。しかしながら、社会的なストレスや対人関係でのス
トレス等、ストレスの多い現代社会においては、かかる
ストレスが頭髪へ悪影響を及ぼし、脱毛症などの頭髪に
係わるトラブルを抱える人の数は、毎年うなぎ登りに増
大している。2. Description of the Related Art It has been a wish of many people, regardless of age or sex, to keep abundant and beautiful black hair forever. However, in today's stressful society such as social stress and interpersonal stress, the stress adversely affects the hair, and the number of people who have troubles related to hair such as alopecia is increased every year. It is increasing.
【０００３】この様な状況を反映して、これまでに、ヨ
クイニン、イチョウ、ショウガなどの生薬抽出エキス、
ビタミンＥやアロキサジン、アデノシン−３’、５’−
サイクリックモノホスフェ−ト（ｃ−ＡＭＰ）などが養
毛剤として開発されてきた。Reflecting such a situation, the herbal medicine extracts such as Yokuinin, Ginkgo, and Ginger have been used so far,
Vitamin E, alloxazine, adenosine-3 ', 5'-
Cyclic monophosphate (c-AMP) and the like have been developed as a hair restorer.
【０００４】しかしながら、これらの養毛剤は、いずれ
も養毛作用が今一つである上、なかには、ブームを呼ん
だいわゆる１０１の様に、皮膚炎などの副作用を起こす
等、安全上好ましくないものもあり、今のところ、実用
に耐えるものは得られていない。そこで、養毛効果に優
れ、且つ、安全性にも優れた養毛剤の開発が望まれてい
た。However, all of these hair nourishing agents have a poor hair nourishing action, and some of them are unfavorable for safety such as side effects such as dermatitis such as so-called 101, which has been booming. So far, nothing has been obtained that can be put to practical use. Therefore, there has been a demand for the development of a hair nourishing agent which is excellent in the hair-growth effect and also excellent in safety.
【０００５】ところで、柑橘類の抽出物については、ユ
ズ抽出物が化粧料用の基剤として利用されている。ま
た、柑橘類種子の抽出物については、浴用剤での使用が
知られている。しかし、柑橘類種子の抽出物または圧搾
物が育毛作用を有することは、全く知られておらず、ま
た、これを頭髪用化粧料に配合して育毛効果を持たせる
という報告は、未だされていない。By the way, as for citrus extracts, Yuzu extract is used as a base for cosmetics. In addition, the use of citrus seed extracts in bath agents is known. However, it is not known at all that a citrus seed extract or a squeezed product has a hair-growing action, and no report has been made yet to add this to hair cosmetics to have a hair-growing effect. .
【０００６】[0006]
【発明が解決しようとする課題】本発明は、上記観点よ
りなされたものであり、育毛効果に優れ、且つ、高い安
全性を有する育毛剤及びこれを含有する頭髪用化粧料を
提供することを課題とする。SUMMARY OF THE INVENTION The present invention has been made from the above viewpoints, and provides a hair-growth agent having an excellent hair-growth effect and high safety, and a hair cosmetic composition containing the same. It is an issue.
【０００７】[0007]
【課題を解決するための手段】本発明者らは、上記課題
を解決するために、植物の構成成分及び抽出物につい
て、育毛作用を指標に、広くスクリーニングを重ねた結
果、柑橘類の種子中に、優れた発毛促進作用を有すると
共に白髪改善作用をも併せ持つ成分が存在することを見
出し、本発明を完成するに至った。[Means for Solving the Problems] In order to solve the above problems, the present inventors have extensively screened plant constituents and extracts using hair-growth action as an index, and found that the citrus seeds were It was found that there is a component which has an excellent hair growth promoting action as well as a gray hair improving action, and has completed the present invention.
【０００８】すなわち、本発明は、柑橘類種子の圧搾物
及び／又は抽出物からなる育毛剤及びこれを含有する頭
髪用化粧料である。以下、本発明を詳細に説明する。That is, the present invention is a hair-growing agent comprising a pressed product and / or an extract of citrus seeds and a hair cosmetic containing the same. Hereinafter, the present invention will be described in detail.
【０００９】＜１＞本発明の育毛剤 本発明の育毛剤は、柑橘類種子の圧搾物及び／又は抽出
物よりなる。ここで、本発明で言う柑橘類とは、ミカン
科ミカン亜科に属するミカン属、キンカン属、カラタチ
属の３属の植物の総称である。このような植物として
は、例えば、ミカン科ミカン属に属するウンシュウミカ
ン、ナツミカン、オレンジ、ハッサク、イヨカン、グレ
ープフルーツ、ユコウ、スダチ、カボス、ポンカン等
や、ミカン科キンカン属に属するキンカン、キンズ、マ
ルキンカン、ナガキンカン等、あるいはミカン科カラタ
チ属に属するカラタチ等が挙げられる。<1> Hair Growth Agent of the Present Invention The hair growth agent of the present invention comprises a pressed product and / or an extract of citrus seeds. Here, the citrus fruits referred to in the present invention are a general term for plants of three genera belonging to the citrus family Citrus genus, quince genus, and karata genus belonging to the Rutaceae subfamily Citrus. Such plants include, for example, Unshu mandarin oranges belonging to the citrus family Rutaceae, Natsumikan, orange, hassaku, yokan, grapefruit, Yuko, Sudachi, Kabosu, ponkan, etc. , Nagakinkan, etc., or Karatachi belonging to the Rutaceae genus Karatachi.
【００１０】上記ミカン科に属する３属の植物のうち、
本発明においては特に、ミカン科ミカン属に属する植物
が好ましく用いられ、更に好ましくは、ウンシュウミカ
ン、ナツミカン、オレンジ、グレープフルーツ、ユコ
ウ、スダチが用いられる。また、本発明においては、こ
れらの柑橘類の種子の１種を単独で用いてもよく、ある
いは２種以上を混合して用いてもよい。Of the three genus plants belonging to the Rutaceae family,
In the present invention, plants belonging to the citrus genus Citrus are particularly preferably used, and more preferably Unshu mandarin orange, natsumi mandarin orange, grapefruit, yuko and Sudachi are used. Further, in the present invention, one kind of these citrus seeds may be used alone, or two or more kinds may be mixed and used.
【００１１】上記柑橘類の種子には、発毛促進作用を有
すると共に白髪改善作用を併せ持つ成分が含まれてお
り、この成分を本発明の育毛剤として用いるには、種子
を圧搾したり、種子より前記成分を抽出物として取り出
して用いることが好ましい。また、これら圧搾物と抽出
物の混合物を用いてもよい。更に、これらの圧搾物、抽
出物から、上記作用を有する成分を分離精製して用いて
もよい。The above-mentioned citrus seeds contain a component that has both a hair growth promoting action and a gray hair improving action. To use this component as a hair restorer of the present invention, the seeds are squeezed or seeds are used. It is preferable to extract and use the above components as an extract. Moreover, you may use the mixture of these pressed products and extracts. Furthermore, the components having the above-mentioned action may be separated and purified from these pressed products and extracts, and then used.
【００１２】柑橘類種子の圧搾は、室温下あるいは加温
下で、通常の圧搾機を用いて常法により行えばよいが、
効率の面を考えると加温下で行う方が好ましい。また、
圧搾に先立ち、柑橘類種子に乾燥等の前処理を施しても
よい。The citrus seeds may be squeezed at room temperature or under heating by an ordinary squeezing machine by a conventional method.
Considering the efficiency, it is preferable to carry out the heating. Also,
Prior to pressing, citrus seeds may be subjected to a pretreatment such as drying.
【００１３】柑橘類種子の抽出処理は、有機溶媒を用い
て、連続式あるいはバッチ式で、常法通り行う。例え
ば、生または乾燥した柑橘類種子を粉砕し、これの１〜
１００倍量の有機溶剤を加え、室温で数日間、または、
沸点付近の温度で数時間、撹拌しながら浸漬する。さら
に、必要に応じて溶媒を完全に留去して乾固するかまた
は凍結乾燥させる。The extraction process of citrus seeds is carried out in a continuous manner or a batch manner using an organic solvent in a usual manner. For example, crush fresh or dried citrus seeds,
Add 100 times the amount of organic solvent and leave it at room temperature for several days, or
Immerse at a temperature near the boiling point for several hours with stirring. Further, if necessary, the solvent is completely distilled off to dryness or freeze-drying.
【００１４】抽出に用いられる有機溶媒としては、例え
ば、メタノール、エタノール等のアルコール類、アセト
ン、メチルエチルケトン等のケトン類、アセトニトリル
等のニトリル類、テトラヒドロフラン等のフラン類、ク
ロロホルム、塩化メチレン等のハロゲン化炭化水素類、
ジエチルエーテル、イソプロピルエーテル等のエーテル
類、ノルマルヘキサン、石油エーテル等の炭化水素類等
が挙げられ、これらを単独または２種以上混合して用い
てもよい。Examples of the organic solvent used for extraction include alcohols such as methanol and ethanol, ketones such as acetone and methyl ethyl ketone, nitriles such as acetonitrile, furans such as tetrahydrofuran, halogenated compounds such as chloroform and methylene chloride. Hydrocarbons,
Examples thereof include ethers such as diethyl ether and isopropyl ether, hydrocarbons such as normal hexane and petroleum ether, and these may be used alone or in combination of two or more kinds.
【００１５】＜２＞本発明の頭髪用化粧料 本発明の頭髪用化粧料は、上記柑橘類種子の圧搾物及び
／又は抽出物を育毛剤として配合したものである。配合
量は、化粧料全量に対して、０．０１〜１０重量％であ
ることが好ましい。配合量が０．０１重量％未満では、
十分な発毛促進効果が期待できず、１０重量％を越えて
も効果は頭打ちになり経済的でない。<2> Cosmetic for Hair of the Present Invention The cosmetic for hair of the present invention contains the above-mentioned pressed product and / or extract of citrus seeds as a hair restorer. The blending amount is preferably 0.01 to 10% by weight based on the total amount of the cosmetic. If the blending amount is less than 0.01% by weight,
A sufficient effect of promoting hair growth cannot be expected, and even if the amount exceeds 10% by weight, the effect reaches the ceiling and is not economical.
【００１６】本発明の頭髪用化粧料の剤型は、特に限定
されるものではなく、例えば、ヘアトニック、シャンプ
ー、リンス、ポマード、ヘアローション、ヘアクリー
ム、ヘアトリートメント等の通常、頭髪用化粧料として
用いられているものが挙げられる。これらの頭髪用化粧
料は、柑橘類種子の圧搾物及び／又は抽出物を配合する
以外は、通常の頭髪用化粧料と同様の方法で製造するこ
とができる。The dosage form of the cosmetic for hair of the present invention is not particularly limited, and for example, it is usually a cosmetic for hair such as hair tonic, shampoo, conditioner, pomade, hair lotion, hair cream and hair treatment. What is used as. These cosmetics for hair can be manufactured by the same method as that for ordinary cosmetics for hair, except that the pressed product and / or extract of citrus seeds are blended.
【００１７】また、本発明の頭髪用化粧料には、通常、
頭髪用化粧料に適用される炭化水素類、ロウ類、油脂
類、エステル類、高級脂肪酸、高級アルコール、界面活
性剤、香料、色素、防腐剤、抗酸化剤、紫外線防御剤、
アルコール類、ｐＨ調整剤、及び各種目的に応じた種々
の薬効成分などが適宜選択されて調製される。更に、本
発明の発毛促進成分である柑橘類種子の圧搾物及び／又
は抽出物以外の発毛、育毛成分、例えば、卵胞ホルモ
ン、抹消血管血流促進剤、局所刺激剤、角質溶解剤、抗
脂漏剤、殺菌剤、代謝賦活剤、酸素活性阻害剤、消炎
剤、栄養剤、保湿剤等を柑橘類種子の圧搾物及び／又は
抽出物と併わせて用いることもできる。The hair cosmetic composition of the present invention usually contains
Hydrocarbons, waxes, oils and fats, esters, higher fatty acids, higher alcohols, surfactants, fragrances, dyes, preservatives, antioxidants, UV protection agents, which are applied to hair cosmetics.
Alcohols, pH adjusters, and various medicinal components suitable for various purposes are appropriately selected and prepared. Furthermore, hair growth other than the pressed product and / or extract of citrus seeds, which is the hair growth-promoting component of the present invention, hair-growth components, such as estrogen, peripheral vascular blood flow promoter, local stimulant, keratolytic agent, anti A seborrheic agent, a bactericidal agent, a metabolic activator, an oxygen activity inhibitor, an anti-inflammatory agent, a nutritional agent, a moisturizing agent, etc. can be used in combination with the pressed and / or extracted citrus seeds.
【００１８】[0018]
【実施例】以下に、本発明の実施例を説明する。はじめ
に、柑橘類種子の圧搾物及び／又は抽出物からなる本発
明の育毛剤の実施例を説明する。EXAMPLES Examples of the present invention will be described below. First, an example of the hair-growing agent of the present invention comprising a pressed product and / or an extract of citrus seeds will be described.
【００１９】[0019]
【実施例１】ウンシュウミカンの種子の乾燥物１ｋｇを
圧搾機に入れ、１００℃に加熱しながら、徐々に加圧し
６０ｋｇ／ｃｍ2まで加圧して、圧搾物５８ｇを淡黄色
の液体として得た。このウンシュウみかん種子の圧搾物
をそのまま育毛剤とした。Example 1 1 kg of dried mandarin orange seeds was placed in a press and gradually heated while being heated to 100 ° C. to 60 kg / cm 2 to obtain 58 g of a pressed product as a pale yellow liquid. . This pressed product of Unshu mandarin orange seeds was used as it was as a hair restorer.
【００２０】[0020]
【実施例２】ウンシュウミカンの種子の乾燥物１ｋｇを
細かく砕いた後、ノルマルヘキサン２ｌを加え、撹拌し
ながら加熱還流し、濾過、減圧濃縮を行い、抽出物１８
９ｇを淡黄色液体として得た。このウンシュウミカン種
子の抽出物をそのまま育毛剤とした。Example 2 1 kg of dried mandarin orange seeds was finely crushed, 2 l of normal hexane was added, the mixture was heated to reflux with stirring, filtered, and concentrated under reduced pressure to obtain extract 18
9 g was obtained as a pale yellow liquid. The extract of Unshiu mandarin orange seeds was directly used as a hair restorer.
【００２１】[0021]
【実施例３】ナツミカンの種子の乾燥物１ｋｇを細かく
砕いた後、ジクロロメタン２ｌを加え、撹拌しながら加
熱還流し、濾過、減圧濃縮を行い、抽出物１５２ｇを淡
黄色液体として得た。このナツミカン種子の抽出物をそ
のまま育毛剤とした。[Example 3] 1 kg of dried nutsipe seeds was finely crushed, 2 l of dichloromethane was added, the mixture was heated under reflux with stirring, filtered and concentrated under reduced pressure to obtain 152 g of an extract as a pale yellow liquid. The extract of Natsumikan seeds was directly used as a hair restorer.
【００２２】[0022]
【実施例４】オレンジの種子の乾燥物１ｋｇを細かく砕
いた後、ジエチルエーテル２ｌを加え、撹拌しながら加
熱還流し、濾過、減圧濃縮を行い、抽出物１９５ｇを淡
黄色液体として得た。このオレンジ種子の抽出物をその
まま育毛剤とした。Example 4 1 kg of dried orange seeds was finely crushed, 2 l of diethyl ether was added, the mixture was heated under reflux with stirring, filtered and concentrated under reduced pressure to obtain 195 g of an extract as a pale yellow liquid. This orange seed extract was directly used as a hair restorer.
【００２３】[0023]
【実施例５】グレープフルーツの種子の乾燥物１ｋｇを
細かく砕いた後、アセトン２ｌを加え、撹拌しながら加
熱還流し、濾過、減圧濃縮を行い、抽出物１４３ｇを淡
黄色液体として得た。このグレープフルーツ種子の抽出
物をそのまま育毛剤とした。Example 5 1 kg of a dried product of grapefruit seeds was finely crushed, 2 l of acetone was added, the mixture was heated under reflux with stirring, filtered and concentrated under reduced pressure to obtain 143 g of an extract as a pale yellow liquid. This grapefruit seed extract was used as it was as a hair restorer.
【００２４】[0024]
【実施例６】ユコウの種子の乾燥物１ｋｇを細かく砕い
た後、５０％エタノールクロロホルム溶液２ｌを加え、
撹拌しながら加熱還流し、濾過、減圧濃縮を行い、抽出
物２０１ｇを淡黄色液体として得た。このユコウ種子の
抽出物をそのまま育毛剤とした。Example 6 1 kg of dried Yuko seeds was crushed finely, and then 2 l of 50% ethanol-chloroform solution was added,
The mixture was heated under reflux with stirring, filtered and concentrated under reduced pressure to obtain 201 g of an extract as a pale yellow liquid. This extract of Yuko seeds was directly used as a hair restorer.
【００２５】[0025]
【実施例７】スダチの種子の乾燥物１ｋｇを細かく砕い
た後、５０％ノルマルヘキサンジエチルエーテル溶液２
ｌを加え、撹拌しながら加熱還流し、濾過、減圧濃縮を
行い、抽出物２０１ｇを淡黄色液体として得た。このス
ダチ種子の抽出物をそのまま育毛剤とした。Example 7 1 kg of a dried product of Sudachi seeds was finely crushed and then 50% normal hexane diethyl ether solution 2
l was added, the mixture was heated under reflux with stirring, filtered, and concentrated under reduced pressure to obtain 201 g of an extract as a pale yellow liquid. The extract of this Sudachi seed was used as it was as a hair restorer.
【００２６】＜本発明の育毛剤の評価＞上記実施例１〜
７で得られた育毛剤について、安全性、発毛促進作用、
白髪改善作用に関する評価を行った。<Evaluation of the hair restorer of the present invention> Examples 1 to 1 above
Regarding the hair restorer obtained in 7, the safety, hair growth promoting action,
The effect of improving gray hair was evaluated.
【００２７】（１）急性毒性試験 ６匹づつ７群のＩＣＲマウス（雄性、５週齢、体重２５
〜３５ｇ）に、上記各実施例で得られた育毛剤をそれぞ
れ１ｇ／ｋｇ経口投与した。投与後１４日目に生死を判
定しＬＤ50値を求めた。その結果、何れのマウスも死亡
例を認めず、ＬＤ50値は１ｇ／ｋｇ以上であることがわ
かった。これより本発明の育毛剤の安全性が高いことが
わかる。(1) Acute toxicity test 6 groups of 7 ICR mice (male, 5 weeks old, weight 25)
˜35 g), 1 g / kg of the hair restorer obtained in each of the above examples was orally administered. On the 14th day after the administration, life or death was judged and the LD 50 value was calculated. As a result, no death was observed in any of the mice, and it was found that the LD 50 value was 1 g / kg or more. This shows that the hair restorer of the present invention is highly safe.
【００２８】（２）経皮刺激試験（局所毒性試験） ６匹づつ７群のハートレー系白色種モルモットの背部を
３ｃｍ四方に剃毛し、この部分に上記各実施例で得られ
た育毛剤の１０％流動パラフィン溶液を１日１回、０．
０５ｍｌづつ５日間連続投与した。投与開始後６日目
に、以下に示す本邦パッチテスト基準（日本皮膚科学
会）により、経皮刺激性を評価した。(2) Transdermal Irritation Test (Local Toxicity Test) The backs of 6 groups of 7 Hartley white guinea pigs were shaved on 3 cm squares, and the hair-growth agents obtained in each of the above Examples were applied to this part. A 10% liquid paraffin solution was added once a day to 0.1.
The solution was continuously administered in an amount of 05 ml for 5 days. On the 6th day after the start of administration, the dermal irritation was evaluated by the following Japanese patch test standards (Japanese Dermatological Association).
【００２９】−：無反応 ±：疑陽性反応 ＋：陽性反応 ＋＋：浮腫を伴った反応 結果は全ての動物が−（無反応）を示した。これより、
本発明の育毛剤である実施例１〜７の育毛剤は安全性に
優れていることが判る。-: No reaction ±: False positive reaction +: Positive reaction ++: Reaction with edema As a result, all animals showed-(no reaction). Than this,
It can be seen that the hair restorers of Examples 1 to 7, which are the hair restorers of the present invention, are excellent in safety.
【００３０】（３）発毛促進作用 １群５匹づつ１０週齢のＣ３Ｈマウスの背部を２ｃｍ四
方に剃毛し、翌日、上記各実施例で得られた育毛剤を表
１に示す様な各種濃度で含有するエタノール溶液を、比
較例としてビタミンＥを２重量％含有するエタノール溶
液を、コントロールとしてエタノールを、それぞれ各群
のマウスの剃毛部に０．０５ｍｌづつ塗布した。塗布後
１４日目に、毛成長度のレベルを以下に示す基準によ
り、肉眼判定した。(3) Hair growth promoting action The backs of 10-week-old C3H mice (5 mice per group) were shaved in a 2 cm square, and the next day, the hair-growth agents obtained in each of the above-mentioned Examples were as shown in Table 1. An ethanol solution containing various concentrations, an ethanol solution containing 2% by weight of vitamin E as a comparative example, and ethanol as a control were each applied to the shaved portion of each group of mice in an amount of 0.05 ml. On the 14th day after application, the level of hair growth was visually judged according to the following criteria.
【００３１】−：コントロール群のマウスの毛の生え方
と同じ ±：コントロール群のマウスの毛の生え方よりわずかに
早い ＋：コントロール群のマウスの毛の生え方より明らかに
早い ＋＋：コントロール群のマウスの毛の生え方より著しく
早い 結果を表１に示す。-: Same as hair growth of mice in control group ±: Slightly earlier than hair growth of mice in control group +: Clearly earlier than hair growth of mice in control group ++: Control group Table 1 shows the results which are significantly faster than the hair growth of the mouse.
【００３２】[0032]
【表１】 [Table 1]
【００３３】この結果より本発明の育毛剤は、発毛促進
効果に優れていることが明らかである。From these results, it is clear that the hair restorer of the present invention is excellent in the hair growth promoting effect.
【００３４】（４）白髪改善効果 １群１０匹づつの白髪の混じる１年齢Ｂ５７ブラックマ
ウスに、上記各実施例で得られた育毛剤の２重量％エタ
ノール溶液を、比較としてビタミンＥの２重量％エタノ
ール溶液を、それぞれ背部１面に０．１ｍｌづつ１日１
回３０日間連続投与した。投与終了後７日目に白髪を１
匹につき１０本抜毛し、根元の黒化したものの数を数え
た。結果を１０匹の平均として表２に示す。(4) Effect of improving gray hair To 1-year-old B57 black mice with 10 gray hairs per group, 2% by weight ethanol solution of the hair-growth agent obtained in each of the above-mentioned examples was compared with 2 weight% of vitamin E. % Ethanol solution, 0.1 ml per back surface, 1 day per day
Administration was repeated once for 30 days. 1 gray hair on the 7th day after administration
Ten hairs were removed from each animal and the number of blackened roots was counted. The results are shown in Table 2 as an average of 10 animals.
【００３５】[0035]
【表２】 [Table 2]
【００３６】この結果より本発明の育毛剤が、毛の黒化
を促して白髪化を改善していることがわかる。次に、上
記実施例で得られた育毛剤を含有する本発明の頭髪用化
粧料の実施例を示す。尚、以下に用いる配合量は全て重
量部である。From these results, it can be seen that the hair restorer of the present invention promotes blackening of hair and improves graying. Next, examples of the cosmetic for hair of the present invention containing the hair-growth agent obtained in the above-mentioned examples will be shown. In addition, all compounding amounts used below are parts by weight.
【００３７】[0037]
【実施例８】 ヘアローション 表３に示す処方成分を秤りとり、室温で撹拌し可溶化し
て、ヘアローションを得た。Example 8 Hair Lotion The formulation components shown in Table 3 were weighed and stirred at room temperature for solubilization to obtain a hair lotion.
【００３８】[0038]
【表３】 [Table 3]
【００３９】[0039]
【実施例９】 ヘアトニック 表４に示す処方成分を秤りとり、室温で撹拌し可溶化し
て、ヘアトニックを得た。Example 9 Hair Tonic The formulation components shown in Table 4 were weighed and stirred at room temperature for solubilization to obtain a hair tonic.
【００４０】[0040]
【表４】 [Table 4]
【００４１】[0041]
【実施例１０】 ヘアクリーム 表５のＡ成分、Ｂ成分をそれぞれ８０℃に加熱溶解し、
Ａ成分にＢ成分を撹拌しながら、徐々に加え、更にＣ成
分を加えた後、冷却してヘアクリームを得た。Example 10 Hair Cream Components A and B in Table 5 were dissolved by heating at 80 ° C.,
The component B was gradually added to the component A while stirring, and the component C was further added, followed by cooling to obtain a hair cream.
【００４２】[0042]
【表５】 [Table 5]
【００４３】[0043]
【実施例１１】 ヘアトートメント 表６のＡ成分、Ｂ成分をそれぞれ８０℃に加熱溶解し、
Ａ成分にＢ成分を撹拌しながら、徐々に加え、更にＣ成
分を加えた後、冷却してヘアトリートメントを得た。Example 11 Hair Totment Components A and B in Table 6 were dissolved by heating at 80 ° C.,
The component B was gradually added to the component A while stirring, and the component C was further added, followed by cooling to obtain a hair treatment.
【００４４】[0044]
【表６】 [Table 6]
【００４５】[0045]
【実施例１２】表７に示す処方成分を秤取り、８０℃で
加熱溶解した後、冷却してシャンプーを得た。Example 12 The ingredients shown in Table 7 were weighed out, dissolved by heating at 80 ° C., and cooled to obtain a shampoo.
【００４６】[0046]
【表７】 [Table 7]
【００４７】[0047]
【発明の効果】本発明の育毛剤は、優れた育毛作用を有
すると共に安全性も高い。また、本発明の頭髪用化粧料
は、この育毛剤を含有することで、育毛作用に優れるば
かりでなく、長期間連続して安全に使用することができ
る。The hair-growing agent of the present invention has an excellent hair-growing action and is highly safe. Further, the hair cosmetic composition of the present invention not only has an excellent hair-growth effect by containing this hair-growth agent, but can be safely used continuously for a long period of time.
───────────────────────────────────────────────────── フロントページの続き (72)発明者 村松 宣江 神奈川県横浜市神奈川区高島台27番地１号 ポーラ化成工業株式会社横浜研究所内 (72)発明者 福田 寿之 神奈川県横浜市戸塚区柏尾町560ポーラ化 成工業株式会社戸塚研究所内 (72)発明者 八木 正喜 神奈川県横浜市戸塚区柏尾町560ポーラ化 成工業株式会社戸塚研究所内 ─────────────────────────────────────────────────── ─── Continuation of the front page (72) Nobue Muramatsu No. 1, Takashimadai, Kanagawa-ku, Yokohama, Kanagawa 27, No. 1, Yokohama Research Laboratory, Pola Chemical Industry Co., Ltd. (72) Toshiyuki Fukuda 560, Kashio-cho, Totsuka-ku, Yokohama, Kanagawa (72) Inventor Masaki Yagi 560 Kashio-cho, Totsuka-ku, Yokohama-shi, Kanagawa Pola Chemical Industry Co., Ltd.
Claims (5)
らなる育毛剤。1. A hair restorer comprising a pressed product and / or an extract of citrus seeds.
植物から選ばれることを特徴とする請求項１記載の育毛
剤。2. The hair restorer according to claim 1, wherein the citrus fruits are selected from plants belonging to the citrus family of the citrus family.
ンシュウミカン、ナツミカン、オレンジ、グレープフル
ーツ、ユコウ、スダチから選ばれる１種または２種以上
である請求項１又は２記載の育毛剤。3. The hair restorer according to claim 1 or 2, wherein the plant belonging to the citrus family Rutaceae is one or more selected from Unshu mandarin orange, natsuki mandarin orange, orange, grapefruit, yuko, and sudachi.
化粧料。4. A hair cosmetic containing the hair restorer according to claim 1.
して０．１〜１０重量％であることを特徴とする請求項
４記載の頭髪用化粧料。5. The hair cosmetic composition according to claim 4, wherein the content of the hair restorer is 0.1 to 10% by weight based on the total amount of the cosmetic composition.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP27468693A JP3171515B2 (en) | 1993-11-02 | 1993-11-02 | Hair cosmetics |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP27468693A JP3171515B2 (en) | 1993-11-02 | 1993-11-02 | Hair cosmetics |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH07126129A true JPH07126129A (en) | 1995-05-16 |
| JP3171515B2 JP3171515B2 (en) | 2001-05-28 |
Family
ID=17545152
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP27468693A Expired - Fee Related JP3171515B2 (en) | 1993-11-02 | 1993-11-02 | Hair cosmetics |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP3171515B2 (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001226278A (en) * | 2000-02-15 | 2001-08-21 | Maruzen Pharmaceut Co Ltd | Antiandrogen agent |
| JP2002173416A (en) * | 2000-12-06 | 2002-06-21 | Kao Corp | Hair cosmetic |
| JP2003313113A (en) * | 2002-04-22 | 2003-11-06 | Noevir Co Ltd | Hair grower |
| JP2009530369A (en) * | 2006-03-21 | 2009-08-27 | ヘオング ゲオン チョイ | Natural herbal hair growth promoting composition and method for producing the same |
| JP2013136525A (en) * | 2011-12-28 | 2013-07-11 | Konnyakuya Honpo Kk | Cosmetic |
| WO2013159790A1 (en) * | 2012-04-26 | 2013-10-31 | Petitjean Max W | "regeneration composition and method for natural hair recoloration and stimulation of hair growth by processed makroot fruit extract" |
Families Citing this family (1)
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|---|---|---|---|---|
| KR102294905B1 (en) | 2020-01-20 | 2021-08-30 | 주식회사 한샘 | Furniture falling prevention device |
-
1993
- 1993-11-02 JP JP27468693A patent/JP3171515B2/en not_active Expired - Fee Related
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001226278A (en) * | 2000-02-15 | 2001-08-21 | Maruzen Pharmaceut Co Ltd | Antiandrogen agent |
| JP4585073B2 (en) * | 2000-02-15 | 2010-11-24 | 丸善製薬株式会社 | Anti-androgen, hair nourishing cosmetics, prostate hypertrophy inhibitor, external preparation and food and drink |
| JP2002173416A (en) * | 2000-12-06 | 2002-06-21 | Kao Corp | Hair cosmetic |
| JP2003313113A (en) * | 2002-04-22 | 2003-11-06 | Noevir Co Ltd | Hair grower |
| JP2009530369A (en) * | 2006-03-21 | 2009-08-27 | ヘオング ゲオン チョイ | Natural herbal hair growth promoting composition and method for producing the same |
| JP2013136525A (en) * | 2011-12-28 | 2013-07-11 | Konnyakuya Honpo Kk | Cosmetic |
| WO2013159790A1 (en) * | 2012-04-26 | 2013-10-31 | Petitjean Max W | "regeneration composition and method for natural hair recoloration and stimulation of hair growth by processed makroot fruit extract" |
| CN104379219A (en) * | 2012-04-26 | 2015-02-25 | 马克斯·W·佩提特金 | regeneration composition and method for natural hair recoloration and stimulation of hair growth by processed makroot fruit extract |
| US9173834B2 (en) | 2012-04-26 | 2015-11-03 | Max W. Petitjean | Regeneration composition and method for natural hair recoloration and stimulation of hair growth by processed Makroot fruit extract |
Also Published As
| Publication number | Publication date |
|---|---|
| JP3171515B2 (en) | 2001-05-28 |
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| LAPS | Cancellation because of no payment of annual fees |