CN108893205A - A kind of capsule-type powder laundry detergent - Google Patents
A kind of capsule-type powder laundry detergent Download PDFInfo
- Publication number
- CN108893205A CN108893205A CN201810643633.2A CN201810643633A CN108893205A CN 108893205 A CN108893205 A CN 108893205A CN 201810643633 A CN201810643633 A CN 201810643633A CN 108893205 A CN108893205 A CN 108893205A
- Authority
- CN
- China
- Prior art keywords
- capsule
- alkyl glycosides
- camphorated oil
- laundry detergent
- microballoon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/001—Softening compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38609—Protease or amylase in solid compositions only
Abstract
The invention discloses a kind of capsule-type powder laundry detergents, powdery is made in liquid detergent, and capsule is further made, it is not easy to control to not only solve traditional liquid detergent dosage, easily reveals, packed and transported problem at high cost, simultaneously, laundry detergents clean effect of the present invention is good, mild, energy conservation and environmental protection, easy to use, and can assign clothing Vermins-proof and mosquito-driving, anti-mould and anti-moth, flexibility, antistatic property and certain fluffy degree.
Description
Technical field
The invention belongs to articles for washing technical fields, and in particular to a kind of capsule-type powder laundry detergent.
Background technique
Traditional liquid detergent is a kind of liquid detergent, the component design for the purpose of fabric decontaminating, with traditional washing powder and
Laundry soap is compared, and belongs to novel fabric detergent, market development is rapid nearly ten years.Liquid detergent is mild with neutrality, does not hurt
Clothing, do not stimulate skin, be hard water resistance, not add phosphorus and solid filler, production and use process waste discharge few etc. numerous
Advantage, therefore, substituting traditional washing powder, laundry soap with liquid detergent can economize on resources, reduces environmental pollution, and have good
Economic and social benefit.
However, traditional liquid laundry liquid is usually bottled, measuring cup is needed to measure when taking, and be easy when toppling over
Cause liquid detergent to be revealed, meanwhile, liquid laundry liquid consumes a large amount of packaging material, traffic condition is required it is harsh, cause product at
Originally, the increase of transportation cost and carbon emission.
Summary of the invention
In view of the above-mentioned problems, the present invention is intended to provide a kind of usage amount easy to control, easy to package, and there is Vermins-proof and mosquito-driving effect
Capsule-type powder laundry detergent.
The invention is realized by the following technical scheme：
A kind of capsule-type powder laundry detergent, is made of powder laundry detergent and capsule, the capsule be it is water-soluble, the powdery is washed
Clothing agent is made of raw material from the following weight：Protease 1-2, amylase 1-3, alkyl glycosides-camphorated oil microballoon 5-10, dodecane
Base benzene sulfonic acid sodium salt 20-30, sodium chloride 3-5.
Further, the alkyl glycosides-camphorated oil microballoon preparation method is：By alkyl glycosides and camphorated oil in 500-
It is stirred in the blender of 900rpm, obtains mixture, then, under the stirring condition of 800-1500rpm, to β-ring paste
Tween-80 is added in the saturated aqueous solution of essence, continues after stirring 20-30min, said mixture is added dropwise, is stirred to react 1-2h, so
Cooling, suction filtration is placed in ice-water bath, and washing is dry to get alkyl glycosides-camphorated oil microballoon.
Further, the capsule is made of one of gelatin, polyvinyl alcohol, beta-cyclodextrin.
Further, the drying condition is 30-40 DEG C.
Further, the saturated aqueous solution temperature of the beta-cyclodextrin is 80-96 DEG C.
Beneficial effects of the present invention：Powdery is made in liquid detergent by the present invention, and capsule is further made, and not only solves biography
Liquid detergent dosage of uniting is not easy to control, easily reveals, packed and transported problem at high cost, meanwhile, laundry detergents decontamination effect of the present invention
Fruit is good, mild, energy conservation and environmental protection, easy to use, and can assign clothing Vermins-proof and mosquito-driving, anti-mould and anti-moth, flexibility, antistatic
Property and certain fluffy degree；Cladding is carried out to alkyl glycosides and camphorated oil using cyclodextrin and forms microballoon, with surfactant one
Play synergistic effect, it is possible to reduce stimulation of the surfactant to skin also improves the ability of the grease stain on removal fabric.
Specific embodiment
Illustrate the present invention with specific embodiment below, but is not limitation of the present invention.
Embodiment 1
A kind of capsule-type powder laundry detergent, is made of powder laundry detergent and capsule, the capsule be it is water-soluble, the powdery is washed
Clothing agent is made of raw material from the following weight：Protease 1, amylase 1, alkyl glycosides-camphorated oil microballoon 5, detergent alkylate sulphur
Sour sodium 20, sodium chloride 3.
Further, the alkyl glycosides-camphorated oil microballoon preparation method is：Alkyl glycosides and camphorated oil are existed
It is stirred in the blender of 500rpm, obtains mixture, then, under the stirring condition of 800rpm, to beta-cyclodextrin
Tween-80 is added in saturated aqueous solution, continues after stirring 20min, said mixture is added dropwise, is stirred to react 1h, is subsequently placed in ice
It is cooling in water-bath, it filters, washing, it is dry to get alkyl glycosides-camphorated oil microballoon.
Further, the capsule is made of one of gelatin, polyvinyl alcohol, beta-cyclodextrin.
Further, the drying condition is 30 DEG C.
Further, the saturated aqueous solution temperature of the beta-cyclodextrin is 80 DEG C.
Embodiment 2
A kind of capsule-type powder laundry detergent, is made of powder laundry detergent and capsule, the capsule be it is water-soluble, the powdery is washed
Clothing agent is made of raw material from the following weight：Protease 2, amylase 2, alkyl glycosides-camphorated oil microballoon 8, detergent alkylate sulphur
Sour sodium 25, sodium chloride 4.
Further, the alkyl glycosides-camphorated oil microballoon preparation method is：Alkyl glycosides and camphorated oil are existed
It is stirred in the blender of 700rpm, obtains mixture, then, under the stirring condition of 1000rpm, to beta-cyclodextrin
Tween-80 is added in saturated aqueous solution, continues after stirring 25min, said mixture is added dropwise, is stirred to react 2h, is subsequently placed in ice
It is cooling in water-bath, it filters, washing, it is dry to get alkyl glycosides-camphorated oil microballoon.
Further, the capsule is made of one of gelatin, polyvinyl alcohol, beta-cyclodextrin.
Further, the drying condition is 35 DEG C.
Further, the saturated aqueous solution temperature of the beta-cyclodextrin is 85 DEG C.
Embodiment 3
A kind of capsule-type powder laundry detergent, is made of powder laundry detergent and capsule, the capsule be it is water-soluble, the powdery is washed
Clothing agent is made of raw material from the following weight：Protease 2, amylase 3, alkyl glycosides-camphorated oil microballoon 10, detergent alkylate sulphur
Sour sodium 30, sodium chloride 5.
Further, the alkyl glycosides-camphorated oil microballoon preparation method is：Alkyl glycosides and camphorated oil are existed
It is stirred in the blender of 900rpm, obtains mixture, then, under the stirring condition of 1500rpm, to beta-cyclodextrin
Tween-80 is added in saturated aqueous solution, continues after stirring 30min, said mixture is added dropwise, is stirred to react 2h, is subsequently placed in ice
It is cooling in water-bath, it filters, washing, it is dry to get alkyl glycosides-camphorated oil microballoon.
Further, the capsule is made of one of gelatin, polyvinyl alcohol, beta-cyclodextrin.
Further, the drying condition is 40 DEG C.
Further, the saturated aqueous solution temperature of the beta-cyclodextrin is 96 DEG C.
Comparative example 1
The addition of alkyl glycosides is omitted compared to embodiment 1 in this comparative example, and method and step in addition to this is all the same.
Comparative example 2
The addition of camphorated oil is omitted compared to embodiment 1 in this comparative example, and method and step in addition to this is all the same.
Comparative example 3
The addition of alkyl glycosides-camphorated oil microballoon, method in addition to this is omitted compared to embodiment 1 in this comparative example
Step is all the same.
Experiment：
Detergency test：Hard water is prepared according to GB/T13174-2,008 7.1.Each group sample is matched using prepared hard water
At the solution of 0.1 %, detergency is tested by GB/T13174-2008 with Terg-O-Tometer and standard soiled cloth.Test result is such as
Shown in table 1：
Table 1
As can be seen from Table 1, present invention gained laundry detergents have good dirt-removing power.
Antistatic property：By several pieces of terylene side's cloth（Side length is 10 cm）, rinsed with clear water spare to still rear naturally dry.
Sample to be tested is respectively made into 100 mL of aqueous solution of 0.1 % concentration, is heated to 30 DEG C, and 4 pieces of each sample solution addition is processed to wash
Synthetic fibre side's cloth takes out and dries after stirring 3 min, places into relative humidity to be surveyed in 65% drier equipped with sodium bromide after 2 h
Its sheet resistance value, the average value of every group of 4 pieces of cloth are test result of the sample under the concentration, and resistance value reduction is bigger,
Illustrate that antistatic property is better.It is that antistatic property is good as Rs >=1013；It is good as Rs=1 012~1011；When
It is general when Rs=1010；Work as Rs<It is poor when 1009.
Fungicidal properties test：The fabric for preparing 6 parts of equivalent respectively washes a fabric with each group sample, and the fabric washed is not
It is directly placed into the case where drying in closed polybag, then does solarizing test, pass through the big of artificial nasil musty after 15 days
It is small and then compare its anti-mold effect.
Test result is as shown in table 2：
Table 2
As can be seen from Table 2, present invention gained sample has good antistatic property and mould proof characteristic.
Claims (5)
1. a kind of capsule-type powder laundry detergent, which is characterized in that be made of powder laundry detergent and capsule, the capsule is water solubility
, the powder laundry detergent is made of raw material from the following weight：Protease 1-2, amylase 1-3, alkyl glycosides-camphorated oil are micro-
Ball 5-10, neopelex 20-30, sodium chloride 3-5.
2. a kind of capsule-type Powdered laundry liquid according to claim 1, which is characterized in that the alkyl glycosides-camphorated oil
The preparation method of microballoon is：Alkyl glycosides and camphorated oil are stirred in the blender of 500-900rpm, must be mixed
Then object under the stirring condition of 800-1500rpm, is added Tween-80 into the saturated aqueous solution of beta-cyclodextrin, continues to stir
After mixing 20-30min, said mixture being added dropwise, is stirred to react 1-2h, is subsequently placed in ice-water bath cooling, suction filtration, washing is dry,
Up to alkyl glycosides-camphorated oil microballoon.
3. a kind of capsule-type Powdered laundry liquid according to claim 1, which is characterized in that the capsule is by gelatin, gathers
One of vinyl alcohol, beta-cyclodextrin are made.
4. alkyl glycosides according to claim 2-camphorated oil microballoon preparation method, which is characterized in that the dried strip
Part is 30-40 DEG C.
5. alkyl glycosides according to claim 2-camphorated oil microballoon preparation method, which is characterized in that the β-ring paste
The saturated aqueous solution temperature of essence is 80-96 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810643633.2A CN108893205A (en) | 2018-06-21 | 2018-06-21 | A kind of capsule-type powder laundry detergent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810643633.2A CN108893205A (en) | 2018-06-21 | 2018-06-21 | A kind of capsule-type powder laundry detergent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108893205A true CN108893205A (en) | 2018-11-27 |
Family
ID=64345257
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810643633.2A Pending CN108893205A (en) | 2018-06-21 | 2018-06-21 | A kind of capsule-type powder laundry detergent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108893205A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1426456A (en) * | 2000-04-28 | 2003-06-25 | 宝洁公司 | Pouched compositions |
| CN101002720A (en) * | 2000-03-01 | 2007-07-25 | Pvaxx研究和开发有限公司 | Method and apparatus for blowmolding capsules of polyvinylalcohol and blowmolded polyvinylalcohol capsules |
| CN103409247A (en) * | 2013-08-23 | 2013-11-27 | 吴江市利达上光制品有限公司 | Mosquito-expelling washing powder |
| CN104403849A (en) * | 2014-10-28 | 2015-03-11 | 江南大学 | Solid washing-agent composition packaged by water-soluble membrane |
| CN105886169A (en) * | 2014-12-15 | 2016-08-24 | 上海和黄白猫有限公司 | Powder detergent bag and preparation method thereof |
| CN106675881A (en) * | 2016-12-06 | 2017-05-17 | 钦州市高新技术产业服务中心 | Powdered detergent bag and preparation method thereof |
| CN108531298A (en) * | 2018-04-10 | 2018-09-14 | 上海应用技术大学 | A kind of washing powder and preparation method thereof containing gold bergamot essential oil microcapsules |
-
2018
- 2018-06-21 CN CN201810643633.2A patent/CN108893205A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101002720A (en) * | 2000-03-01 | 2007-07-25 | Pvaxx研究和开发有限公司 | Method and apparatus for blowmolding capsules of polyvinylalcohol and blowmolded polyvinylalcohol capsules |
| CN1426456A (en) * | 2000-04-28 | 2003-06-25 | 宝洁公司 | Pouched compositions |
| CN103409247A (en) * | 2013-08-23 | 2013-11-27 | 吴江市利达上光制品有限公司 | Mosquito-expelling washing powder |
| CN104403849A (en) * | 2014-10-28 | 2015-03-11 | 江南大学 | Solid washing-agent composition packaged by water-soluble membrane |
| CN105886169A (en) * | 2014-12-15 | 2016-08-24 | 上海和黄白猫有限公司 | Powder detergent bag and preparation method thereof |
| CN106675881A (en) * | 2016-12-06 | 2017-05-17 | 钦州市高新技术产业服务中心 | Powdered detergent bag and preparation method thereof |
| CN108531298A (en) * | 2018-04-10 | 2018-09-14 | 上海应用技术大学 | A kind of washing powder and preparation method thereof containing gold bergamot essential oil microcapsules |
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|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20181127 |
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| RJ01 | Rejection of invention patent application after publication |