CN102776069B - Paste microcapsule jasmine essence and preparation method thereof - Google Patents
Paste microcapsule jasmine essence and preparation method thereof Download PDFInfo
- Publication number
- CN102776069B CN102776069B CN 201210288896 CN201210288896A CN102776069B CN 102776069 B CN102776069 B CN 102776069B CN 201210288896 CN201210288896 CN 201210288896 CN 201210288896 A CN201210288896 A CN 201210288896A CN 102776069 B CN102776069 B CN 102776069B
- Authority
- CN
- China
- Prior art keywords
- ethanolic solution
- cream jasmin
- jasmin france
- benzyl
- paste
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Cosmetics (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention discloses a paste microcapsule jasmine essence and a preparation method of the paste microcapsule jasmine essence. The paste microcapsule jasmine essence comprises the following components in percentage by weight: 5-25 percent of jasmine essence, 10-50 percent of beta-cyclodextrin, 0.1-2 percents of xanthan gum and the balance of deionized water. The preparation method comprises thefollowing steps of: uniformly dispersing beta-cyclodextrin into the deionized water to obtain beta-cyclodextrin turbid liquid; and adding the xanthan gum to the obtained beta-cyclodextrin turbid liquid, continuously stirring to ensure that the xanthan gum is dissolved and uniformly dispersed, then adding the jasmine essence, continuously and uniformly stirring to obtain the paste microcapsule jasmine essence. The paste microcapsule jasmine essence prepared by the invention has the advantages of stable fragrance, lasting aroma, high sweet smell strength, high essence content and the like.
Description
Technical field
The present invention relates to a kind of novel paste jasmine slowly-releasing essence, design more specifically a kind of paste microcapsules cream jasmin france and preparation method thereof.
Background technology
Jasmine is one of favorite fresh flower of people because its graceful fragrance forms.In fragrance industry, jasmine fragrance belongs to the bright rhythm of the typical fragrance of a flower, and fragrance is careful and saturating, and pure and fresh sense is arranged.Especially domestic Xiao Hua jasmine fragrance has pure and fresh simple and elegant feature.Therefore, cream jasmin france is widely used in the conglomerate fields such as food, daily chemical products.Because the most of compositions of essence are volatile organic compounds, volatile in direct use procedure, some thermal sensitivity perfume materials and light sensitivity perfume material are unstable, and fragrance remaining time is short, aroma quality is unstable thereby cause.
Microcapsule essence refers to essence as core, selects suitable wall material that essence is coated and forms the essence capsule particulate.Microcapsule essence can greatly improve heat endurance, photostability and the non-oxidizability of essence, can effectively prevent the loss of fragrance component, make the style of essence constant, aroma quality is stable, and can improve the sustained release performance of essence, make things convenient for transportation, storage and the use of essence.
Existing microcapsule essence, usually take converted starch, shitosan, polypropylene acid esters, cyclodextrin etc. as the wall material, generally make the microcapsule essence of emulsion or suspension state, emulsion or suspension are generally unstable, easily layering needs the method such as spray-dried to make the powdery microcapsule essence.
Summary of the invention
One of purpose of the present invention is to provide a kind of paste microcapsules cream jasmin france in order to solve the in stable condition technical problem that exists in the existing microcapsule essence.
The preparation method of a kind of paste microcapsules cream jasmin france that two of purpose of the present invention is to provide above-mentioned.
Know-why of the present invention
Cyclodextrin be by starch obtain through the enzymolysis cyclization by 6 to 8 D-Glucose molecules by the cyclic compound that α-the Isosorbide-5-Nitrae glycoside bond is formed by connecting, the cyclodextrin that wherein is comprised of 7 D-Glucose molecules is called beta-schardinger dextrin-.
Cyclodextrin molecular is cylindric ringwise, surface and hydrophilic outer and inner chamber is hydrophobic, therefore, the cyclodextrin inner chamber can coat the essence molecule, form microcapsule essence, in preparation process, add simultaneously have thickening, the xanthans of stable, emulsification, can obtain the paste microcapsule essence.
Technical scheme of the present invention
A kind of paste microcapsules cream jasmin france counts by weight percentage, and composition and the content of its raw material are as follows:
Cream jasmin france 5-25%
Beta-schardinger dextrin-10-50%
Xanthans 0.1-2%
Surplus is deionized water;
Above-mentioned a kind of paste microcapsules cream jasmin france prepares by the following method, and its preparation process specifically comprises the steps:
(1), in beaker, add beta-schardinger dextrin-, add again deionized water, open to stir, beta-schardinger dextrin-is dispersed in the deionized water uniformly, obtain the beta-schardinger dextrin-suspension;
(2), xanthans is joined in the resulting beta-schardinger dextrin-suspension of step (1), continue to stir, after making the xanthans dissolving and being evenly distributed, add again cream jasmin france, add rear continuation and stir 3-5h, namely get paste microcapsules cream jasmin france.
Used cream jasmin france counts by weight percentage in above-mentioned a kind of paste microcapsules cream jasmin france, and composition and the content of its raw material are as follows:
Benzyl acetate 20-35%
Benzyl propionate 1-3%
α amyl cinnamic aldehyde 5-10%
α n hexyl cinnamic aldehyde 5-15%
10% dihydro jasmone ethanolic solution 0.5-2.5%
MDJ 4-10%
Linalool 10-15%
Bergamio 5-10%
10% benzaldehyde ethanolic solution 0.1-0.4%
10% gamma-undecalactone ethanolic solution 1-1.5%
10% cis-3-hexenol ethanolic solution 1-3.5%
10% Leaf Acetate ethanolic solution 0.5-3%
Phenylacetaldehyde 0.1-0.8%
10% benzopyrrole ethanolic solution 3-6%
10% narceol ethanolic solution 0.5-1%
Terpinol 1-2.5%
Isoeugenol 0.5-1%
Benzyl carbinol 1-5%
Citronellol 1-3%
α-ionone 0.5-1%
Cinnamic alcohol 1-1.5%
Ylang ylang oil 0.1-0.5%
Jasminum sambac absolute 0.1-0.4%
Surplus is ethanol;
Above-mentioned cream jasmin france prepares by the following method:
With ethanol, benzyl acetate, benzyl propionate, α amyl cinnamic aldehyde, α n hexyl cinnamic aldehyde, 10% dihydro jasmone ethanolic solution, MDJ, linalool, bergamio, 10% benzaldehyde ethanolic solution, 10% gamma-undecalactone ethanolic solution, 10% cis-3-hexenol ethanolic solution, 10% Leaf Acetate ethanolic solution, phenylacetaldehyde, 10% benzopyrrole ethanolic solution, 10% narceol ethanolic solution, terpinol, isoeugenol, benzyl carbinol, citronellol, α-ionone, cinnamic alcohol, ylang ylang oil, jasminum sambac absolute evenly mixes, and can mix cream jasmin france.
Beneficial effect of the present invention
A kind of paste microcapsules cream jasmin france of the present invention owing to adopting nontoxic, biodegradable beta-schardinger dextrin-as the wall material, has the xanthans of thickening, stable, emulsification by adding, must arrive the Microencapsulated Slow cream jasmin france of paste.
Further, because the synergy of emulsification, thickening has effectively strengthened stability of system, so the paste microcapsules cream jasmin france that the present invention makes is difficult for layering occurs, and system is more stable.
In addition, the present invention is made paste microcapsules cream jasmin france to smell by Wen Xiangzhi with the cream jasmin france of microencapsulation not and distinguishes analysis, former beginning and end microencapsulation cream jasmin france after 6 days fragrance faint, only can feel the bottom note note of jasmine, and paste microcapsule essence of the present invention still can be felt the whole odor characteristic of obvious jasmine after 21 days.Therefore, the paste microcapsules cream jasmin france fragrance that the present invention makes is stable, and lasting is lasting.
The specific embodiment
Below by embodiment the present invention is further described, but does not affect protection scope of the present invention.Used various raw materials or the specification of reagent and the information of manufacturer see Table 1 in the various embodiments of the present invention.
The specification of table 1, raw material and reagent and manufacturer
Embodiment 1
A kind of paste microcapsules cream jasmin france counts by weight percentage, and composition and the content of its raw material are as follows:
Cream jasmin france 5g(5%)
Beta-schardinger dextrin-10g(10%)
Xanthans 2g (2%)
Deionized water 83g (83%);
Above-mentioned a kind of paste microcapsules cream jasmin france prepares by the following method, and its preparation process specifically comprises the steps:
(1), in the 150ml beaker, add the beta-schardinger dextrin-of 10g, add again the deionized water of 83g, open and stir, beta-schardinger dextrin-is dispersed in the deionized water uniformly, obtain the beta-schardinger dextrin-suspension;
(2), the xanthans of 2g is joined in the beta-schardinger dextrin-suspension of step (1) gained, continue to stir, after making the xanthans dissolving and being evenly distributed, add again the 5g cream jasmin france, add rear continuation and stir 3-5h, namely get paste microcapsules cream jasmin france.
The paste microcapsules cream jasmin france of above-mentioned gained, better mobile, but after leaving standstill for 3 weeks, find that microcapsule essence has sedimentation phenomenon.
Used cream jasmin france counts by weight percentage in above-mentioned a kind of paste microcapsules cream jasmin france, and composition and the content of its raw material are as follows:
Benzyl acetate 20g (20%)
Benzyl propionate 1g (1%)
α amyl cinnamic aldehyde 10g (10%)
α n hexyl cinnamic aldehyde 5g (5%)
10% dihydro jasmone ethanolic solution 2.5g (2.5%)
MDJ 4g (4%)
Linalool 10g (10%)
Bergamio 5g (5%)
10% benzaldehyde ethanolic solution 0.1g (0.1%)
10% gamma-undecalactone ethanolic solution 1g (1%)
10% cis-3-hexenol ethanolic solution 2g (2%)
10% Leaf Acetate ethanolic solution 3g (3%)
Phenylacetaldehyde 0.3g (0.3%)
10% benzopyrrole ethanolic solution 3g (3%)
10% narceol ethanolic solution 1g (1%)
Terpinol 1g (1%)
Isoeugenol 0.5g (0.5%)
Benzyl carbinol 2g (2%)
Citronellol 1g (1%)
α-ionone 0.5g (0.5%)
Cinnamic alcohol 1g (1%)
Ylang ylang oil 0.1g (0.1%)
Jasminum sambac absolute 0.1g (0.1%)
Surplus is ethanol;
Above-mentioned cream jasmin france prepares by the following method:
With ethanol, benzyl acetate, benzyl propionate, α amyl cinnamic aldehyde, α n hexyl cinnamic aldehyde, 10% dihydro jasmone ethanolic solution, MDJ, linalool, bergamio, 10% benzaldehyde ethanolic solution, 10% gamma-undecalactone ethanolic solution, 10% cis-3-hexenol ethanolic solution, 10% Leaf Acetate ethanolic solution, phenylacetaldehyde, 10% benzopyrrole ethanolic solution, 10% narceol ethanolic solution, terpinol, isoeugenol, benzyl carbinol, citronellol, α-ionone, cinnamic alcohol, ylang ylang oil, the even mixing of jasminum sambac absolute namely obtains cream jasmin france.The essence fragrance that obtains is sent out thoroughly, and partially blue or green, turbid perfume (or spice) is laid particular stress on, and has given prominence to the feeling of freshness of jasmine fragrance.
Embodiment 2
A kind of paste microcapsules cream jasmin france counts by weight percentage, and composition and the content of its raw material are as follows:
Cream jasmin france 5g(5%)
Beta-schardinger dextrin-45g(45%)
Xanthans 0.1g (0.1%)
Deionized water 49.9g (49.9%);
Above-mentioned a kind of paste microcapsules cream jasmin france prepares by the following method, and its preparation process specifically comprises the steps:
(1), in the 150ml beaker, add the beta-schardinger dextrin-of 45g, add again the deionized water of 49.9g, open and stir, beta-schardinger dextrin-is dispersed in the deionized water uniformly, obtain the beta-schardinger dextrin-suspension;
(2), the xanthans of 0.1g is joined in the beta-schardinger dextrin-suspension of step (1) gained, continue to stir, after making the xanthans dissolving and being evenly distributed, add again the 5g cream jasmin france, add rear continuation and stir 3-5h, namely get paste microcapsules cream jasmin france.
The paste microcapsules cream jasmin france of above-mentioned gained, thickness relatively, left standstill for 3 weeks after, find slightly sedimentation phenomenon of microcapsule essence.
Used cream jasmin france counts by weight percentage in above-mentioned a kind of paste microcapsules cream jasmin france, and composition and the content of its raw material are as follows:
Benzyl acetate 20g (20%)
Benzyl propionate 1g (1%)
α amyl cinnamic aldehyde 10g (10%)
α n hexyl cinnamic aldehyde 5g (5%)
10% dihydro jasmone ethanolic solution 2.5g (2.5%)
MDJ 4g (4%)
Linalool 10g (10%)
Bergamio 5g (5%)
10% benzaldehyde ethanolic solution 0.1g (0.1%)
10% gamma-undecalactone ethanolic solution 1g (1%)
10% cis-3-hexenol ethanolic solution 2g (2%)
10% Leaf Acetate ethanolic solution 3g (3%)
Phenylacetaldehyde 0.3g (0.3%)
10% benzopyrrole ethanolic solution 3g (3%)
10% narceol ethanolic solution 1g (1%)
Terpinol 1g (1%)
Isoeugenol 0.5g (0.5%)
Benzyl carbinol 2g (2%)
Citronellol 1g (1%)
α-ionone 0.5g (0.5%)
Cinnamic alcohol 1g (1%)
Ylang ylang oil 0.1g (0.1%)
Jasminum sambac absolute 0.1g (0.1%)
Surplus is ethanol;
Above-mentioned cream jasmin france prepares by the following method:
With ethanol, benzyl acetate, benzyl propionate, α amyl cinnamic aldehyde, α n hexyl cinnamic aldehyde, 10% dihydro jasmone ethanolic solution, MDJ, linalool, bergamio, 10% benzaldehyde ethanolic solution, 10% gamma-undecalactone ethanolic solution, 10% cis-3-hexenol ethanolic solution, 10% Leaf Acetate ethanolic solution, phenylacetaldehyde, 10% benzopyrrole ethanolic solution, 10% narceol ethanolic solution, terpinol, isoeugenol, benzyl carbinol, citronellol, α-ionone, cinnamic alcohol, ylang ylang oil, the even mixing of jasminum sambac absolute namely obtains cream jasmin france.The essence fragrance that obtains is sent out thoroughly, and partially blue or green, turbid perfume (or spice) is laid particular stress on, and has given prominence to the feeling of freshness of jasmine fragrance.
Embodiment 3
A kind of paste microcapsules cream jasmin france counts by weight percentage, and composition and the content of its raw material are as follows:
Cream jasmin france 10g(10%)
Beta-schardinger dextrin-25g(25%)
Xanthans 1g (1%)
Deionized water 64g (64%);
Above-mentioned a kind of paste microcapsules cream jasmin france prepares by the following method, and its preparation process specifically comprises the steps:
(1), in the 150ml beaker, add the beta-schardinger dextrin-of 25g, add again the deionized water of 64g, open and stir, beta-schardinger dextrin-is dispersed in the deionized water uniformly, obtain the beta-schardinger dextrin-suspension;
(2), the 1g xanthans is joined in the beta-schardinger dextrin-suspension of step (1) gained, continue to stir, after making the xanthans dissolving and being evenly distributed, add again the 10g cream jasmin france, add rear continuation and stir 3-5h, namely get paste microcapsules cream jasmin france.
The paste microcapsule essence of above-mentioned gained is than stiff, and is mobile relatively poor, but microcapsules cream jasmin france system is more stable, left standstill for 3 weeks after, do not find that microcapsule essence has the sedimentation lamination.
Used cream jasmin france counts by weight percentage in above-mentioned a kind of paste microcapsules cream jasmin france, and composition and the content of its raw material are as follows:
Benzyl acetate 35g (35%)
Benzyl propionate 1g (1%)
α amyl cinnamic aldehyde 5g (5%)
α n hexyl cinnamic aldehyde 5g (5%)
10% dihydro jasmone ethanolic solution 2g (2%)
MDJ 7g (7%)
Linalool 15g (15%)
Bergamio 10g (10%)
10% benzaldehyde ethanolic solution 0.4g (0.4%)
10% gamma-undecalactone ethanolic solution 1.5g (1.5%)
10% cis-3-hexenol ethanolic solution 1g (1%)
10% Leaf Acetate ethanolic solution 3g (3%)
Phenylacetaldehyde 0.1g (0.1%)
10% benzopyrrole ethanolic solution 3g (3%)
10% narceol ethanolic solution 0.5g (0.5%)
Terpinol 1g (1%)
Isoeugenol 0.5g (0.5%)
Benzyl carbinol 3g (3%)
Citronellol 1g (1%)
α-ionone 1g (1%)
Cinnamic alcohol 1g (1%)
Ylang ylang oil 0.1g (0.1%)
Jasminum sambac absolute 0.1g (0.1%)
Surplus is ethanol;
Above-mentioned cream jasmin france is by being prepared as follows the method preparation, and its preparation process specifically comprises the steps:
With ethanol, benzyl acetate, benzyl propionate, α amyl cinnamic aldehyde, α n hexyl cinnamic aldehyde, 10% dihydro jasmone ethanolic solution, MDJ, linalool, bergamio, 10% benzaldehyde ethanolic solution, 10% gamma-undecalactone ethanolic solution, 10% cis-3-hexenol ethanolic solution, 10% Leaf Acetate ethanolic solution, phenylacetaldehyde, 10% benzopyrrole ethanolic solution, 10% narceol ethanolic solution, terpinol, isoeugenol, benzyl carbinol, citronellol, α-ionone, cinnamic alcohol, ylang ylang oil, the even mixing of jasminum sambac absolute namely obtains cream jasmin france.The essence that obtains has the characteristic perfume of jasmine, and slightly with the fruital note.
Embodiment 4
A kind of paste microcapsules cream jasmin france counts by weight percentage, and composition and the content of its raw material are as follows:
Cream jasmin france 10g(10%)
Beta-schardinger dextrin-20g(20%)
Xanthans 1g (1%)
Deionized water 69g (69%);
Above-mentioned a kind of paste microcapsules cream jasmin france prepares by the following method, and its preparation process specifically comprises the steps:
(1), in the 150ml beaker, add the beta-schardinger dextrin-of 20g, add again the deionized water of 69g, open and stir, beta-schardinger dextrin-is dispersed in the deionized water uniformly, obtain the beta-schardinger dextrin-suspension;
(2), the 1g xanthans is joined in the beta-schardinger dextrin-suspension of step (1) gained, continue to stir, after making the xanthans dissolving and being evenly distributed, add again the 10g cream jasmin france, add rear continuation and stir 3-5h, namely get paste microcapsules cream jasmin france.
The paste microcapsule essence of above-mentioned gained is better mobile, and microcapsules cream jasmin france stable system, left standstill for 3 weeks after, do not find that microcapsule essence has the sedimentation lamination.
Used cream jasmin france counts by weight percentage in above-mentioned a kind of paste microcapsules cream jasmin france, and composition and the content of its raw material are as follows:
Benzyl acetate 35g (35%)
Benzyl propionate 1g (1%)
α amyl cinnamic aldehyde 5g (5%)
α n hexyl cinnamic aldehyde 5g (5%)
10% dihydro jasmone ethanolic solution 2g (2%)
MDJ 7g (7%)
Linalool 15g (15%)
Bergamio 10g (10%)
10% benzaldehyde ethanolic solution 0.4g (0.4%)
10% gamma-undecalactone ethanolic solution 1.5g (1.5%)
10% cis-3-hexenol ethanolic solution 1g (1%)
10% Leaf Acetate ethanolic solution 3g (3%)
Phenylacetaldehyde 0.1g (0.1%)
10% benzopyrrole ethanolic solution 3g (3%)
10% narceol ethanolic solution 0.5g (0.5%)
Terpinol 1g (1%)
Isoeugenol 0.5g (0.5%)
Benzyl carbinol 3g (3%)
Citronellol 1g (1%)
α-ionone 1g (1%)
Cinnamic alcohol 1g (1%)
Ylang ylang oil 0.1g (0.1%)
Jasminum sambac absolute 0.1g (0.1%)
Surplus is ethanol;
Above-mentioned cream jasmin france is by being prepared as follows the method preparation, and its preparation process specifically comprises the steps:
With ethanol, benzyl acetate, benzyl propionate, α amyl cinnamic aldehyde, α n hexyl cinnamic aldehyde, 10% dihydro jasmone ethanolic solution, MDJ, linalool, bergamio, 10% benzaldehyde ethanolic solution, 10% gamma-undecalactone ethanolic solution, 10% cis-3-hexenol ethanolic solution, 10% Leaf Acetate ethanolic solution, phenylacetaldehyde, 10% benzopyrrole ethanolic solution, 10% narceol ethanolic solution, terpinol, isoeugenol, benzyl carbinol, citronellol, α-ionone, cinnamic alcohol, ylang ylang oil, the even mixing of jasminum sambac absolute namely obtains cream jasmin france.The essence that obtains has the characteristic perfume of jasmine, and slightly with the fruital note.
Embodiment 5
A kind of paste microcapsules cream jasmin france counts by weight percentage, and composition and the content of its raw material are as follows:
Cream jasmin france 15g(15%)
Beta-schardinger dextrin-20g(20%)
Xanthans 1g (1%)
Deionized water 64g (64%);
Above-mentioned a kind of paste microcapsules cream jasmin france prepares by the following method, and its preparation process specifically comprises the steps:
(1), in the 150ml beaker, add the beta-schardinger dextrin-of 20g, add again the deionized water of 64g, open and stir, beta-schardinger dextrin-is dispersed in the deionized water uniformly, obtain the beta-schardinger dextrin-suspension;
(2), the xanthans of 1g is joined in the beta-schardinger dextrin-suspension of step (1) gained, continue to stir, after making the xanthans dissolving and being evenly distributed, add again the 15g cream jasmin france, add rear continuation and stir 3-5h, namely get paste microcapsules cream jasmin france.
The paste microcapsule essence of above-mentioned gained is than stiff, and is mobile relatively poor, left standstill for 3 weeks after, find that microcapsule essence has sedimentation phenomenon.
Used cream jasmin france counts by weight percentage in above-mentioned a kind of paste microcapsules cream jasmin france, and composition and the content of its raw material are as follows:
Benzyl acetate 25g (25%)
Benzyl propionate 1g (1%)
α amyl cinnamic aldehyde 5g (5%)
α n hexyl cinnamic aldehyde 15g (15%)
10% dihydro jasmone ethanolic solution 1g (1%)
MDJ 10g (10%)
Linalool 10g (10%)
Bergamio 5g (5%)
10% benzaldehyde ethanolic solution 0.1g (0.1%)
10% gamma-undecalactone ethanolic solution 1g (1%)
10% cis-3-hexenol ethanolic solution 2g (2%)
10% Leaf Acetate ethanolic solution 1g (1%)
Phenylacetaldehyde 0.1g (0.1%)
10% benzopyrrole ethanolic solution 4g (4%)
10% narceol ethanolic solution 0.5g (0.5%)
Terpinol 1g (1%)
Isoeugenol 0.5g (0.5%)
Benzyl carbinol 2g (2%)
Citronellol 1g (1%)
α-ionone 0.5g (0.5%)
Cinnamic alcohol 1g (1%)
Ylang ylang oil 0.5g (0.5%)
Jasminum sambac absolute 0.4g (0.4%)
Surplus is ethanol;
Above-mentioned cream jasmin france is by being prepared as follows the method preparation, and its preparation process specifically comprises the steps:
With ethanol, benzyl acetate, benzyl propionate, α amyl cinnamic aldehyde, α n hexyl cinnamic aldehyde, 10% dihydro jasmone ethanolic solution, MDJ, linalool, bergamio, 10% benzaldehyde ethanolic solution, 10% gamma-undecalactone ethanolic solution, 10% cis-3-hexenol ethanolic solution, 10% Leaf Acetate ethanolic solution, phenylacetaldehyde, 10% benzopyrrole ethanolic solution, 10% narceol ethanolic solution, terpinol, isoeugenol, benzyl carbinol, citronellol, α-ionone, cinnamic alcohol, ylang ylang oil, the even mixing of jasminum sambac absolute namely obtains cream jasmin france.The essence fragrance that obtains is pure and fresh elegant, has the characteristic perfume of jasmine, and has stronger natural sense.
In sum, a kind of paste microcapsules cream jasmin france of the present invention is because therefore the synergistic effects such as emulsification, thickening have characteristics in stable condition, that fragrance is coordinated.A kind of paste microcapsules cream jasmin france of gained under the condition of the prescription of embodiment 4 particularly.
Above said content only is the basic explanation of the present invention under conceiving, and any equivalent transformation that technical scheme according to the present invention is done all belongs to the scope of protection of the invention.
Claims (6)
1. a paste microcapsules cream jasmin france is characterized in that counting by weight percentage, and composition and the content of its raw material are as follows:
Cream jasmin france 5-25%
Beta-schardinger dextrin-10-50%
Xanthans 0.1-2%
Surplus is deionized water;
Above-mentioned a kind of paste microcapsules cream jasmin france prepares by the following method, and its preparation process specifically comprises the steps:
(1), in beaker, add beta-schardinger dextrin-, add again deionized water, open to stir, beta-schardinger dextrin-is dispersed in the deionized water uniformly, obtain the beta-schardinger dextrin-suspension;
(2), xanthans is joined in the beta-schardinger dextrin-suspension of step (1) gained, continue to stir, after making the xanthans dissolving and being evenly distributed, add again cream jasmin france and continue to stir, namely get paste microcapsules cream jasmin france;
Described cream jasmin france counts by weight percentage, and composition and the content of its raw material are as follows:
Benzyl acetate 20-35%
Benzyl propionate 1-3%
α amyl cinnamic aldehyde 5-10%
α n hexyl cinnamic aldehyde 5-15%
10% dihydro jasmone ethanolic solution 0.5-2.5%
MDJ 4-10%
Linalool 10-15%
Bergamio 5-10%
10% benzaldehyde ethanolic solution 0.1-0.4%
10% gamma-undecalactone ethanolic solution 1-1.5%
10% cis-3-hexenol ethanolic solution 1-3.5%
10% Leaf Acetate ethanolic solution 0.5-3%
Phenylacetaldehyde 0.1-0.8%
10% benzopyrrole ethanolic solution 3-6%
10% narceol ethanolic solution 0.5-1%
Terpinol 1-2.5%
Isoeugenol 0.5-1%
Benzyl carbinol 1-5%
Citronellol 1-3%
α-ionone 0.5-1%
Cinnamic alcohol 1-1.5%
Ylang ylang oil 0.1-0.5%
Jasminum sambac absolute 0.1-0.4%
Surplus is ethanol;
Above-mentioned cream jasmin france prepares by the following method:
With ethanol, benzyl acetate, benzyl propionate, α amyl cinnamic aldehyde, α n hexyl cinnamic aldehyde, 10% dihydro jasmone ethanolic solution, MDJ, linalool, bergamio, 10% benzaldehyde ethanolic solution, 10% gamma-undecalactone ethanolic solution, 10% cis-3-hexenol ethanolic solution, 10% Leaf Acetate ethanolic solution, phenylacetaldehyde, 10% benzopyrrole ethanolic solution, 10% narceol ethanolic solution, terpinol, isoeugenol, benzyl carbinol, citronellol, α-ionone, cinnamic alcohol, ylang ylang oil, jasminum sambac absolute evenly mixes, and can mix cream jasmin france.
2. a kind of paste microcapsules cream jasmin france as claimed in claim 1 is characterized in that counting by weight percentage, and composition and the content of its raw material are as follows:
Cream jasmin france 5-15%
Beta-schardinger dextrin-10-45%
Xanthans 0.1-2%
Surplus is deionized water.
3. a kind of paste microcapsules cream jasmin france as claimed in claim 2 is characterized in that the cream jasmin france described in the raw material components counts by weight percentage, and composition and the content of its raw material are as follows:
Benzyl acetate 20-35%
Benzyl propionate 1%
α amyl cinnamic aldehyde 5-10%
α n hexyl cinnamic aldehyde 5-15%
10% dihydro jasmone ethanolic solution 1-2.5%
MDJ 4-10%
Linalool 10-15%
Bergamio 5-10%
10% benzaldehyde ethanolic solution 0.1-0.4%
10% gamma-undecalactone ethanolic solution 1-1.5%
10% cis-3-hexenol ethanolic solution 1-2%
10% Leaf Acetate ethanolic solution 1-3%
Phenylacetaldehyde 0.1-0.3%
10% benzopyrrole ethanolic solution 3-4%
10% narceol ethanolic solution 0.5-1%
Terpinol 1%
Isoeugenol 0.5%
Benzyl carbinol 2-3%
Citronellol 1%
α-ionone 0.5-1%
Cinnamic alcohol 1%
Ylang ylang oil 0.1-0.5%
Jasminum sambac absolute 0.1-0.4%
Surplus is ethanol.
4. a kind of paste microcapsules cream jasmin france as claimed in claim 3 is characterized in that counting by weight percentage, and composition and the content of its raw material are as follows:
Cream jasmin france 10%
Beta-schardinger dextrin-20%
Xanthans 1%
Deionized water 69%;
Described cream jasmin france counts by weight percentage, and composition and the content of its raw material are as follows:
Benzyl acetate 35%
Benzyl propionate 1%
α amyl cinnamic aldehyde 5%
α n hexyl cinnamic aldehyde 5%
10% dihydro jasmone ethanolic solution 2%
MDJ 7%
Linalool 15%
Bergamio 10%
10% benzaldehyde ethanolic solution 0.4%
10% gamma-undecalactone ethanolic solution 1.5%
10% cis-3-hexenol ethanolic solution 1%
10% Leaf Acetate ethanolic solution 3%
Phenylacetaldehyde 0.1%
10% benzopyrrole ethanolic solution 3%
10% narceol ethanolic solution 0.5%
Terpinol 1%
Isoeugenol 0.5%
Benzyl carbinol 3%
Citronellol 1%
α-ionone 1%
Cinnamic alcohol 1%
Ylang ylang oil 0.1%
Jasminum sambac absolute 0.1%
Surplus is ethanol.
5. used cream jasmin france in a kind of paste microcapsules cream jasmin france as claimed in claim 1 or 2 is characterized in that counting by weight percentage, and composition and the content of its raw material are as follows:
Benzyl acetate 20-35%
Benzyl propionate 1-3%
α amyl cinnamic aldehyde 5-10%
α n hexyl cinnamic aldehyde 5-15%
10% dihydro jasmone ethanolic solution 0.5-2.5%
MDJ 4-10%
Linalool 10-15%
Bergamio 5-10%
10% benzaldehyde ethanolic solution 0.1-0.4%
10% gamma-undecalactone ethanolic solution 1-1.5%
10% cis-3-hexenol ethanolic solution 1-3.5%
10% Leaf Acetate ethanolic solution 0.5-3%
Phenylacetaldehyde 0.1-0.8%
10% benzopyrrole ethanolic solution 3-6%
10% narceol ethanolic solution 0.5-1%
Terpinol 1-2.5%
Isoeugenol 0.5-1%
Benzyl carbinol 1-5%
Citronellol 1-3%
α-ionone 0.5-1%
Cinnamic alcohol 1-1.5%
Ylang ylang oil 0.1-0.5%
Jasminum sambac absolute 0.1-0.4%
Surplus is ethanol;
Above-mentioned cream jasmin france prepares by the following method:
With ethanol, benzyl acetate, benzyl propionate, α amyl cinnamic aldehyde, α n hexyl cinnamic aldehyde, 10% dihydro jasmone ethanolic solution, MDJ, linalool, bergamio, 10% benzaldehyde ethanolic solution, 10% gamma-undecalactone ethanolic solution, 10% cis-3-hexenol ethanolic solution, 10% Leaf Acetate ethanolic solution, phenylacetaldehyde, 10% benzopyrrole ethanolic solution, 10% narceol ethanolic solution, terpinol, isoeugenol, benzyl carbinol, citronellol, α-ionone, cinnamic alcohol, ylang ylang oil, jasminum sambac absolute evenly mixes, and can mix cream jasmin france.
6. cream jasmin france as claimed in claim 5 is characterized in that counting by weight percentage, and composition and the content of its raw material are as follows:
Benzyl acetate 20-35%
Benzyl propionate 1%
α amyl cinnamic aldehyde 5-10%
α n hexyl cinnamic aldehyde 5-15%
10% dihydro jasmone ethanolic solution 1-2.5%
MDJ 4-10%
Linalool 10-15%
Bergamio 5-10%
10% benzaldehyde ethanolic solution 0.1-0.4%
10% gamma-undecalactone ethanolic solution 1-1.5%
10% cis-3-hexenol ethanolic solution 1-2%
10% Leaf Acetate ethanolic solution 1-3%
Phenylacetaldehyde 0.1-0.3%
10% benzopyrrole ethanolic solution 3-4%
10% narceol ethanolic solution 0.5-1%
Terpinol 1%
Isoeugenol 0.5%
Benzyl carbinol 2-3%
Citronellol 1%
α-ionone 0.5-1%
Cinnamic alcohol 1%
Ylang ylang oil 0.1-0.5%
Jasminum sambac absolute 0.1-0.4%
Surplus is ethanol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210288896 CN102776069B (en) | 2012-08-15 | 2012-08-15 | Paste microcapsule jasmine essence and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210288896 CN102776069B (en) | 2012-08-15 | 2012-08-15 | Paste microcapsule jasmine essence and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102776069A CN102776069A (en) | 2012-11-14 |
| CN102776069B true CN102776069B (en) | 2013-10-16 |
Family
ID=47121181
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201210288896 Expired - Fee Related CN102776069B (en) | 2012-08-15 | 2012-08-15 | Paste microcapsule jasmine essence and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102776069B (en) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5570646B1 (en) * | 2013-09-19 | 2014-08-13 | 小川香料株式会社 | Flavor improver for tea beverages or tea-containing foods |
| CN104359902B (en) * | 2014-11-13 | 2017-05-03 | 上海应用技术学院 | Formaldehyde colour-rendering test paper, and preparation method and application thereof |
| CN106148006A (en) * | 2016-08-03 | 2016-11-23 | 安徽省三环纸业集团香料科技发展有限公司 | A kind of antidepressant joyful type liquid detergent microcapsule essence |
| CN107047813A (en) * | 2017-05-09 | 2017-08-18 | 南京扬子茉莉谷文化科技有限公司 | The preparation method and snowball oil microcapsule powder of a kind of snowball oil microcapsule powder |
| CN114471392A (en) * | 2022-02-09 | 2022-05-13 | 云南中烟工业有限责任公司 | Ring-opened cucurbituril-based cis-jasmone supramolecular capsule and preparation method and application thereof |
| CN117343798B (en) * | 2023-10-24 | 2024-06-18 | 协成香精香料(南通)有限公司 | Jasmine essence and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1073711A (en) * | 1991-12-27 | 1993-06-30 | 昆明五华香料厂 | Microcapsule aromatizing agent and preparation method thereof and purposes |
| WO2008044046A1 (en) * | 2006-10-13 | 2008-04-17 | Reckit Benckiser (Uk) Limited | Perfume compositions |
| WO2009090355A1 (en) * | 2008-01-15 | 2009-07-23 | Reckitt Benckiser (Uk) Limited | Perfume compositions |
| CN101811015A (en) * | 2010-04-15 | 2010-08-25 | 上海应用技术学院 | Preparation method of jasmine sambac essence capsule |
| CN101818100A (en) * | 2010-04-15 | 2010-09-01 | 上海应用技术学院 | Preparation method of polybutylcyanoacrylate-encapsulated jasminum grandiflorum essence capsule |
| CN102553503A (en) * | 2012-02-06 | 2012-07-11 | 陕西师范大学 | Preparation method of sub-micron-scale controlled-release essence microcapsule |
-
2012
- 2012-08-15 CN CN 201210288896 patent/CN102776069B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1073711A (en) * | 1991-12-27 | 1993-06-30 | 昆明五华香料厂 | Microcapsule aromatizing agent and preparation method thereof and purposes |
| WO2008044046A1 (en) * | 2006-10-13 | 2008-04-17 | Reckit Benckiser (Uk) Limited | Perfume compositions |
| WO2009090355A1 (en) * | 2008-01-15 | 2009-07-23 | Reckitt Benckiser (Uk) Limited | Perfume compositions |
| CN101811015A (en) * | 2010-04-15 | 2010-08-25 | 上海应用技术学院 | Preparation method of jasmine sambac essence capsule |
| CN101818100A (en) * | 2010-04-15 | 2010-09-01 | 上海应用技术学院 | Preparation method of polybutylcyanoacrylate-encapsulated jasminum grandiflorum essence capsule |
| CN102553503A (en) * | 2012-02-06 | 2012-07-11 | 陕西师范大学 | Preparation method of sub-micron-scale controlled-release essence microcapsule |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102776069A (en) | 2012-11-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102776071B (en) | Transparent microcapsule flavoring jasmine essence and preparation method thereof | |
| CN102776069B (en) | Paste microcapsule jasmine essence and preparation method thereof | |
| CN102776068A (en) | Paste type microcapsule flavoring rose essence and preparation method thereof | |
| CN102776070A (en) | Transparent microcapsule flavoring rose essence and preparation method thereof | |
| Hambleton et al. | Influence of alginate emulsion-based films structure on its barrier properties and on the protection of microencapsulated aroma compound | |
| CN102776073B (en) | Paste type microcapsule flavoring tuberose essence and preparation method thereof | |
| CN101461534B (en) | Method for preparing antioxidation gelatine membrane containing tea polyphenol nano lipidosome | |
| CN105112162A (en) | Multifunctional essence slow-release carrier and preparation method thereof | |
| CN102985054A (en) | Solid core coacervated capsules | |
| WO2019200675A1 (en) | Method for clathrating tributyrin by means of enzymatic method | |
| CN102807920B (en) | Transparent microcapsule tuberose essence and preparation method thereof | |
| CN102511570A (en) | Olive oil microcapsule and preparation method thereof | |
| CN103409247A (en) | Mosquito-expelling washing powder | |
| CN105540073A (en) | Brittle capsule for cigarettes and preparation method thereof | |
| CN104073346A (en) | Nanometer level microcapsule sweet orange essence and preparing method thereof | |
| CN106074684A (en) | Slow-releasing sachet and preparation method thereof | |
| CN103461988B (en) | High-content alpha-linolenic acid microcapsule and manufacturing method thereof | |
| CN106281676A (en) | A kind of Microencapsulated Slow essence and preparation method thereof | |
| CN107237215A (en) | Fresh-keeping grease proofing food wrapper and preparation method thereof | |
| CN103881400B (en) | Edibility nano flower raw albumen composite membrane and preparation technology thereof | |
| CN101818100B (en) | Preparation method of polybutylcyanoacrylate-encapsulated jasminum grandiflorum essence capsule | |
| CN101811015B (en) | Preparation method of jasmine sambac essence capsule | |
| CN105038387B (en) | Pear essence for water-based inks and preparation method thereof | |
| Dima et al. | Microencapsulation of coriander oil using complex coacervation method | |
| CN110200066A (en) | A kind of capsule of nano antistaling agent and preparation method and application |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131016 Termination date: 20160815 |