CN102776069A - Paste microcapsule jasmine essence and preparation method thereof - Google Patents
Paste microcapsule jasmine essence and preparation method thereof Download PDFInfo
- Publication number
- CN102776069A CN102776069A CN2012102888969A CN201210288896A CN102776069A CN 102776069 A CN102776069 A CN 102776069A CN 2012102888969 A CN2012102888969 A CN 2012102888969A CN 201210288896 A CN201210288896 A CN 201210288896A CN 102776069 A CN102776069 A CN 102776069A
- Authority
- CN
- China
- Prior art keywords
- ethanolic soln
- cream jasmin
- jasmin france
- jiguiquan
- cyclodextrin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Cosmetics (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention discloses a paste microcapsule jasmine essence and a preparation method of the paste microcapsule jasmine essence. The paste microcapsule jasmine essence comprises the following components in percentage by weight: 5-25 percent of jasmine essence, 10-50 percent of beta-cyclodextrin, 0.1-2 percents of xanthan gum and the balance of deionized water. The preparation method comprises the following steps of: uniformly dispersing beta-cyclodextrin into the deionized water to obtain beta-cyclodextrin turbid liquid; and adding the xanthan gum to the obtained beta-cyclodextrin turbid liquid, continuously stirring to ensure that the xanthan gum is dissolved and uniformly dispersed, then adding the jasmine essence, continuously and uniformly stirring to obtain the paste microcapsule jasmine essence. The paste microcapsule jasmine essence prepared by the invention has the advantages of stable fragrance, lasting aroma, high sweet smell strength, high essence content and the like.
Description
Technical field
The present invention relates to a kind of novel paste jasmine slowly-releasing essence, design a kind of paste microcapsule cream jasmin france and preparation method thereof more specifically.
Background technology
Flower of Arabian Jasmine is one of favorite fresh flower of people because of its graceful fragrance forms.In fragrance industry, jasmine fragrance belongs to the bright rhythm of the typical fragrance of a flower, and fragrance is careful and pass through and send out, and pure and fresh sense is arranged.Especially domestic Xiao Hua jasmine fragrance has pure and fresh simple and elegant characteristic.Therefore, cream jasmin france is widely used in conglomerate fields such as food, daily chemical products.Because the most of compositions of essence are volatile organic cpds, volatile in direct use, some thermo-sensitivity perfume materials and photosensitivity perfume material are unstable, and fragrance remaining time is short, aroma quality is unstable thereby cause.
Microcapsule essence is meant essence as core, selects for use suitable wall material that essence is coated and forms the essence capsule particulate.Microcapsule essence can greatly improve thermostability, light stability and the oxidation-resistance of essence; Can prevent the loss of aroma component effectively, make the style of essence constant, aroma quality is stable; And can improve the sustained release performance of essence, make things convenient for transportation, storage and the use of essence.
Existing microcapsule essence; Usually be the wall material with modified starch, chitosan, polypropylene acid esters, Schardinger dextrins etc., generally make the microcapsule essence of milk sap or suspension liquid state, milk sap or suspension liquid are generally unstable; Be prone to layering, need method such as spray-dried to make the powdery microcapsule essence.
Summary of the invention
One of the object of the invention is in order to solve the in stable condition technical problem that exists in the existing microcapsule essence a kind of paste microcapsule cream jasmin france to be provided.
The preparation method of a kind of paste microcapsule cream jasmin france that two of the object of the invention is to provide above-mentioned.
Know-why of the present invention
Schardinger dextrins is to pass through the ring compound that α-1,4 glycoside bond is formed by connecting by what starch obtained through the enzymolysis cyclization by 6 to 8 D-glucose molecules, and the Schardinger dextrins of wherein being made up of 7 D-glucose molecules is called beta-cyclodextrin.
Cyclodextrin molecular is cylindric ringwise, surface and hydrophilic outer and inner chamber is hydrophobic, therefore; The Schardinger dextrins inner chamber can coat the essence molecule; Form microcapsule essence, in the preparation process, add simultaneously have thickening, the XG 550 of stable, emulsifying effect, can obtain the paste microcapsule essence.
Technical scheme of the present invention
A kind of paste microcapsule cream jasmin france is counted by weight percentage, and the composition and the content of its raw material are following:
Cream jasmin france 5-25%
Beta-cyclodextrin 10-50%
XG 550 0.1-2%
Surplus is a deionized water;
Above-mentioned a kind of paste microcapsule cream jasmin france prepares through following method, and its preparation process specifically comprises the steps:
(1), in beaker, add beta-cyclodextrin, add deionized water again, open to stir, beta-cyclodextrin is dispersed in the deionized water uniformly, obtain the beta-cyclodextrin suspension liquid;
(2), XG 550 is joined in the resulting beta-cyclodextrin suspension liquid of step (1), continue to stir, after making the XG 550 dissolving and being evenly distributed, add cream jasmin france again, add continued and stir 3-5h, promptly get paste microcapsule cream jasmin france.
Used cream jasmin france is counted by weight percentage in above-mentioned a kind of paste microcapsule cream jasmin france, and the composition and the content of its raw material are following:
Jasmal 20-35%
Benzyl propionate 1-3%
α-Wu Jiguiquan 5-10%
α-Ji Jiguiquan 5-15%
10% Dihydrojasmone ethanolic soln 0.5-2.5%
Methyl dihydrojasmonate 4-10%
Phantol 10-15%
Phanteine 5-10%
10% phenyl aldehyde ethanolic soln 0.1-0.4%
10% γ-Shi Yineizhi ethanolic soln 1-1.5%
10% cis-3-hexenol ethanolic soln 1-3.5%
10% acetate leaf-alcohol ester ethanolic soln 0.5-3%
Phenylacetic aldehyde 0.1-0.8%
10% benzopyrrole ethanolic soln 3-6%
10% p-cresyl acetate ethanolic soln 0.5-1%
Terpineol 350 1-2.5%
Isoeugenol 0.5-1%
Phenylethyl alcohol 1-5%
Geraniol 1-3%
α-Zi Luolantong 0.5-1%
Cinnamic alcohol 1-1.5%
Ylang ylang oil 0.1-0.5%
Jasminum sambac absolute 0.1-0.4%
Surplus is an ethanol;
Above-mentioned cream jasmin france prepares through following method:
With ethanol, jasmal, benzyl propionate, α-Wu Jiguiquan, α-Ji Jiguiquan, 10% Dihydrojasmone ethanolic soln, methyl dihydrojasmonate, phantol, phanteine, 10% phenyl aldehyde ethanolic soln, 10% γ-Shi Yineizhi ethanolic soln, 10% cis-3-hexenol ethanolic soln, 10% acetate leaf-alcohol ester ethanolic soln, phenylacetic aldehyde, 10% benzopyrrole ethanolic soln, 10% p-cresyl acetate ethanolic soln, Terpineol 350, isoeugenol, phenylethyl alcohol, geraniol, α-Zi Luolantong, cinnamic alcohol, ylang ylang oil, jasminum sambac absolute uniform mixing, can mix cream jasmin france.
Beneficial effect of the present invention
A kind of paste microcapsule cream jasmin france of the present invention owing to adopt nontoxic, biodegradable beta-cyclodextrin as the wall material, through the XG 550 that adding has thickening, stable, emulsifying effect, must arrive the microcapsule slowly-releasing cream jasmin france of paste.
Further, because the synergy of emulsification, thickening has effectively strengthened the stability of system, so the paste microcapsule cream jasmin france that the present invention makes is difficult for layering takes place, and system is more stable.
In addition; The present invention is made paste microcapsule cream jasmin france to smell through Wen Xiangzhi with the cream jasmin france of micro encapsulation not and distinguishes analysis; Former beginning and end micro encapsulation cream jasmin france after 6 days fragrance faint; Only can feel the bottom note note of jasmine, and paste microcapsule essence of the present invention still can be felt the whole odour characteristics of obvious jasmine after 21 days.Therefore, the paste microcapsule cream jasmin france fragrance that the present invention makes is stable, and lasting is lasting.
Embodiment
Through embodiment the present invention is done explanation further below, but do not influence protection scope of the present invention.The used various raw materials or the specification of reagent and the information of manufacturer are seen table 1 in the various embodiments of the present invention.
The specification of table 1, raw material and reagent and manufacturer
Embodiment 1
A kind of paste microcapsule cream jasmin france is counted by weight percentage, and the composition and the content of its raw material are following:
Cream jasmin france 5g (5%)
Beta-cyclodextrin 10g (10%)
XG 550 2g (2%)
Deionized water 83g (83%);
Above-mentioned a kind of paste microcapsule cream jasmin france prepares through following method, and its preparation process specifically comprises the steps:
(1), in the 150ml beaker, add the beta-cyclodextrin of 10g, add the deionized water of 83g again, open and stir, beta-cyclodextrin is dispersed in the deionized water uniformly, obtain the beta-cyclodextrin suspension liquid;
(2), the XG 550 of 2g is joined in the beta-cyclodextrin suspension liquid of step (1) gained, continue to stir, after making the XG 550 dissolving and being evenly distributed, add the 5g cream jasmin france again, add continued and stir 3-5h, promptly get paste microcapsule cream jasmin france.
The paste microcapsule cream jasmin france of above-mentioned gained, better mobile, but after leaving standstill for 3 weeks, find that microcapsule essence has sedimentation phenomenon.
Used cream jasmin france is counted by weight percentage in above-mentioned a kind of paste microcapsule cream jasmin france, and the composition and the content of its raw material are following:
Jasmal 20g (20%)
Benzyl propionate 1g (1%)
α-Wu Jiguiquan 10g (10%)
α-Ji Jiguiquan 5g (5%)
10% Dihydrojasmone ethanolic soln 2.5g (2.5%)
Methyl dihydrojasmonate 4g (4%)
Phantol 10g (10%)
Phanteine 5g (5%)
10% phenyl aldehyde ethanolic soln 0.1g (0.1%)
10% γ-Shi Yineizhi ethanolic soln 1g (1%)
10% cis-3-hexenol ethanolic soln 2g (2%)
10% acetate leaf-alcohol ester ethanolic soln 3g (3%)
Phenylacetic aldehyde 0.3g (0.3%)
10% benzopyrrole ethanolic soln 3g (3%)
10% p-cresyl acetate ethanolic soln 1g (1%)
Terpineol 350 1g (1%)
Isoeugenol 0.5g (0.5%)
Phenylethyl alcohol 2g (2%)
Geraniol 1g (1%)
α-Zi Luolantong 0.5g (0.5%)
Cinnamic alcohol 1g (1%)
Ylang ylang oil 0.1g (0.1%)
Jasminum sambac absolute 0.1g (0.1%)
Surplus is an ethanol;
Above-mentioned cream jasmin france prepares through following method:
With ethanol; Jasmal; Benzyl propionate; α-Wu Jiguiquan; α-Ji Jiguiquan; 10% Dihydrojasmone ethanolic soln; Methyl dihydrojasmonate; Phantol; Phanteine; 10% phenyl aldehyde ethanolic soln; 10% γ-Shi Yineizhi ethanolic soln; 10% cis-3-hexenol ethanolic soln; 10% acetate leaf-alcohol ester ethanolic soln; Phenylacetic aldehyde; 10% benzopyrrole ethanolic soln; 10% p-cresyl acetate ethanolic soln; Terpineol 350; Isoeugenol; Phenylethyl alcohol; Geraniol; α-Zi Luolantong; Cinnamic alcohol; Ylang ylang oil; The jasminum sambac absolute uniform mixing promptly obtains cream jasmin france.The essence fragrance that obtains passes through to be sent out, and blue or green partially, turbid perfume (or spice) is laid particular stress on, and has given prominence to the feeling of freshness of jasmine fragrance.
Embodiment 2
A kind of paste microcapsule cream jasmin france is counted by weight percentage, and the composition and the content of its raw material are following:
Cream jasmin france 5g (5%)
Beta-cyclodextrin 45g (45%)
XG 550 0.1g (0.1%)
Deionized water 49.9g (49.9%);
Above-mentioned a kind of paste microcapsule cream jasmin france prepares through following method, and its preparation process specifically comprises the steps:
(1), in the 150ml beaker, add the beta-cyclodextrin of 45g, add the deionized water of 49.9g again, open and stir, beta-cyclodextrin is dispersed in the deionized water uniformly, obtain the beta-cyclodextrin suspension liquid;
(2), the XG 550 of 0.1g is joined in the beta-cyclodextrin suspension liquid of step (1) gained, continue to stir, after making the XG 550 dissolving and being evenly distributed, add the 5g cream jasmin france again, add continued and stir 3-5h, promptly get paste microcapsule cream jasmin france.
The paste microcapsule cream jasmin france of above-mentioned gained, thickness relatively, left standstill for 3 weeks after, find slightly sedimentation phenomenon of microcapsule essence.
Used cream jasmin france is counted by weight percentage in above-mentioned a kind of paste microcapsule cream jasmin france, and the composition and the content of its raw material are following:
Jasmal 20g (20%)
Benzyl propionate 1g (1%)
α-Wu Jiguiquan 10g (10%)
α-Ji Jiguiquan 5g (5%)
10% Dihydrojasmone ethanolic soln 2.5g (2.5%)
Methyl dihydrojasmonate 4g (4%)
Phantol 10g (10%)
Phanteine 5g (5%)
10% phenyl aldehyde ethanolic soln 0.1g (0.1%)
10% γ-Shi Yineizhi ethanolic soln 1g (1%)
10% cis-3-hexenol ethanolic soln 2g (2%)
10% acetate leaf-alcohol ester ethanolic soln 3g (3%)
Phenylacetic aldehyde 0.3g (0.3%)
10% benzopyrrole ethanolic soln 3g (3%)
10% p-cresyl acetate ethanolic soln 1g (1%)
Terpineol 350 1g (1%)
Isoeugenol 0.5g (0.5%)
Phenylethyl alcohol 2g (2%)
Geraniol 1g (1%)
α-Zi Luolantong 0.5g (0.5%)
Cinnamic alcohol 1g (1%)
Ylang ylang oil 0.1g (0.1%)
Jasminum sambac absolute 0.1g (0.1%)
Surplus is an ethanol;
Above-mentioned cream jasmin france prepares through following method:
With ethanol; Jasmal; Benzyl propionate; α-Wu Jiguiquan; α-Ji Jiguiquan; 10% Dihydrojasmone ethanolic soln; Methyl dihydrojasmonate; Phantol; Phanteine; 10% phenyl aldehyde ethanolic soln; 10% γ-Shi Yineizhi ethanolic soln; 10% cis-3-hexenol ethanolic soln; 10% acetate leaf-alcohol ester ethanolic soln; Phenylacetic aldehyde; 10% benzopyrrole ethanolic soln; 10% p-cresyl acetate ethanolic soln; Terpineol 350; Isoeugenol; Phenylethyl alcohol; Geraniol; α-Zi Luolantong; Cinnamic alcohol; Ylang ylang oil; The jasminum sambac absolute uniform mixing promptly obtains cream jasmin france.The essence fragrance that obtains passes through to be sent out, and blue or green partially, turbid perfume (or spice) is laid particular stress on, and has given prominence to the feeling of freshness of jasmine fragrance.
Embodiment 3
A kind of paste microcapsule cream jasmin france is counted by weight percentage, and the composition and the content of its raw material are following:
Cream jasmin france 10g (10%)
Beta-cyclodextrin 25g (25%)
XG 550 1g (1%)
Deionized water 64g (64%);
Above-mentioned a kind of paste microcapsule cream jasmin france prepares through following method, and its preparation process specifically comprises the steps:
(1), in the 150ml beaker, add the beta-cyclodextrin of 25g, add the deionized water of 64g again, open and stir, beta-cyclodextrin is dispersed in the deionized water uniformly, obtain the beta-cyclodextrin suspension liquid;
(2), the 1g XG 550 is joined in the beta-cyclodextrin suspension liquid of step (1) gained, continue to stir, after making the XG 550 dissolving and being evenly distributed, add the 10g cream jasmin france again, add continued and stir 3-5h, promptly get paste microcapsule cream jasmin france.
The paste microcapsule essence of above-mentioned gained is than stiff, and is mobile relatively poor, but microcapsule cream jasmin france system is more stable, left standstill for 3 weeks after, do not find that microcapsule essence has the sedimentation demixing phenomenon.
Used cream jasmin france is counted by weight percentage in above-mentioned a kind of paste microcapsule cream jasmin france, and the composition and the content of its raw material are following:
Jasmal 35g (35%)
Benzyl propionate 1g (1%)
α-Wu Jiguiquan 5g (5%)
α-Ji Jiguiquan 5g (5%)
10% Dihydrojasmone ethanolic soln 2g (2%)
Methyl dihydrojasmonate 7g (7%)
Phantol 15g (15%)
Phanteine 10g (10%)
10% phenyl aldehyde ethanolic soln 0.4g (0.4%)
10% γ-Shi Yineizhi ethanolic soln 1.5g (1.5%)
10% cis-3-hexenol ethanolic soln 1g (1%)
10% acetate leaf-alcohol ester ethanolic soln 3g (3%)
Phenylacetic aldehyde 0.1g (0.1%)
10% benzopyrrole ethanolic soln 3g (3%)
10% p-cresyl acetate ethanolic soln 0.5g (0.5%)
Terpineol 350 1g (1%)
Isoeugenol 0.5g (0.5%)
Phenylethyl alcohol 3g (3%)
Geraniol 1g (1%)
α-Zi Luolantong 1g (1%)
Cinnamic alcohol 1g (1%)
Ylang ylang oil 0.1g (0.1%)
Jasminum sambac absolute 0.1g (0.1%)
Surplus is an ethanol;
Above-mentioned cream jasmin france is through being prepared as follows the method preparation, and its preparation process specifically comprises the steps:
With ethanol; Jasmal; Benzyl propionate; α-Wu Jiguiquan; α-Ji Jiguiquan; 10% Dihydrojasmone ethanolic soln; Methyl dihydrojasmonate; Phantol; Phanteine; 10% phenyl aldehyde ethanolic soln; 10% γ-Shi Yineizhi ethanolic soln; 10% cis-3-hexenol ethanolic soln; 10% acetate leaf-alcohol ester ethanolic soln; Phenylacetic aldehyde; 10% benzopyrrole ethanolic soln; 10% p-cresyl acetate ethanolic soln; Terpineol 350; Isoeugenol; Phenylethyl alcohol; Geraniol; α-Zi Luolantong; Cinnamic alcohol; Ylang ylang oil; The jasminum sambac absolute uniform mixing promptly obtains cream jasmin france.The essence that obtains has the characteristic perfume of jasmine, and slightly has the fruital note.
Embodiment 4
A kind of paste microcapsule cream jasmin france is counted by weight percentage, and the composition and the content of its raw material are following:
Cream jasmin france 10g (10%)
Beta-cyclodextrin 20g (20%)
XG 550 1g (1%)
Deionized water 69g (69%);
Above-mentioned a kind of paste microcapsule cream jasmin france prepares through following method, and its preparation process specifically comprises the steps:
(1), in the 150ml beaker, add the beta-cyclodextrin of 20g, add the deionized water of 69g again, open and stir, beta-cyclodextrin is dispersed in the deionized water uniformly, obtain the beta-cyclodextrin suspension liquid;
(2), the 1g XG 550 is joined in the beta-cyclodextrin suspension liquid of step (1) gained, continue to stir, after making the XG 550 dissolving and being evenly distributed, add the 10g cream jasmin france again, add continued and stir 3-5h, promptly get paste microcapsule cream jasmin france.
The paste microcapsule essence of above-mentioned gained is better mobile, and microcapsule cream jasmin france system is stable, left standstill for 3 weeks after, do not find that microcapsule essence has the sedimentation demixing phenomenon.
Used cream jasmin france is counted by weight percentage in above-mentioned a kind of paste microcapsule cream jasmin france, and the composition and the content of its raw material are following:
Jasmal 35g (35%)
Benzyl propionate 1g (1%)
α-Wu Jiguiquan 5g (5%)
α-Ji Jiguiquan 5g (5%)
10% Dihydrojasmone ethanolic soln 2g (2%)
Methyl dihydrojasmonate 7g (7%)
Phantol 15g (15%)
Phanteine 10g (10%)
10% phenyl aldehyde ethanolic soln 0.4g (0.4%)
10% γ-Shi Yineizhi ethanolic soln 1.5g (1.5%)
10% cis-3-hexenol ethanolic soln 1g (1%)
10% acetate leaf-alcohol ester ethanolic soln 3g (3%)
Phenylacetic aldehyde 0.1g (0.1%)
10% benzopyrrole ethanolic soln 3g (3%)
10% p-cresyl acetate ethanolic soln 0.5g (0.5%)
Terpineol 350 1g (1%)
Isoeugenol 0.5g (0.5%)
Phenylethyl alcohol 3g (3%)
Geraniol 1g (1%)
α-Zi Luolantong 1g (1%)
Cinnamic alcohol 1g (1%)
Ylang ylang oil 0.1g (0.1%)
Jasminum sambac absolute 0.1g (0.1%)
Surplus is an ethanol;
Above-mentioned cream jasmin france is through being prepared as follows the method preparation, and its preparation process specifically comprises the steps:
With ethanol; Jasmal; Benzyl propionate; α-Wu Jiguiquan; α-Ji Jiguiquan; 10% Dihydrojasmone ethanolic soln; Methyl dihydrojasmonate; Phantol; Phanteine; 10% phenyl aldehyde ethanolic soln; 10% γ-Shi Yineizhi ethanolic soln; 10% cis-3-hexenol ethanolic soln; 10% acetate leaf-alcohol ester ethanolic soln; Phenylacetic aldehyde; 10% benzopyrrole ethanolic soln; 10% p-cresyl acetate ethanolic soln; Terpineol 350; Isoeugenol; Phenylethyl alcohol; Geraniol; α-Zi Luolantong; Cinnamic alcohol; Ylang ylang oil; The jasminum sambac absolute uniform mixing promptly obtains cream jasmin france.The essence that obtains has the characteristic perfume of jasmine, and slightly has the fruital note.
Embodiment 5
A kind of paste microcapsule cream jasmin france is counted by weight percentage, and the composition and the content of its raw material are following:
Cream jasmin france 15g (15%)
Beta-cyclodextrin 20g (20%)
XG 550 1g (1%)
Deionized water 64g (64%);
Above-mentioned a kind of paste microcapsule cream jasmin france prepares through following method, and its preparation process specifically comprises the steps:
(1), in the 150ml beaker, add the beta-cyclodextrin of 20g, add the deionized water of 64g again, open and stir, beta-cyclodextrin is dispersed in the deionized water uniformly, obtain the beta-cyclodextrin suspension liquid;
(2), the XG 550 of 1g is joined in the beta-cyclodextrin suspension liquid of step (1) gained, continue to stir, after making the XG 550 dissolving and being evenly distributed, add the 15g cream jasmin france again, add continued and stir 3-5h, promptly get paste microcapsule cream jasmin france.
The paste microcapsule essence of above-mentioned gained is than stiff, and is mobile relatively poor, left standstill for 3 weeks after, find that microcapsule essence has sedimentation phenomenon.
Used cream jasmin france is counted by weight percentage in above-mentioned a kind of paste microcapsule cream jasmin france, and the composition and the content of its raw material are following:
Jasmal 25g (25%)
Benzyl propionate 1g (1%)
α-Wu Jiguiquan 5g (5%)
α-Ji Jiguiquan 15g (15%)
10% Dihydrojasmone ethanolic soln 1g (1%)
Methyl dihydrojasmonate 10g (10%)
Phantol 10g (10%)
Phanteine 5g (5%)
10% phenyl aldehyde ethanolic soln 0.1g (0.1%)
10% γ-Shi Yineizhi ethanolic soln 1g (1%)
10% cis-3-hexenol ethanolic soln 2g (2%)
10% acetate leaf-alcohol ester ethanolic soln 1g (1%)
Phenylacetic aldehyde 0.1g (0.1%)
10% benzopyrrole ethanolic soln 4g (4%)
10% p-cresyl acetate ethanolic soln 0.5g (0.5%)
Terpineol 350 1g (1%)
Isoeugenol 0.5g (0.5%)
Phenylethyl alcohol 2g (2%)
Geraniol 1g (1%)
α-Zi Luolantong 0.5g (0.5%)
Cinnamic alcohol 1g (1%)
Ylang ylang oil 0.5g (0.5%)
Jasminum sambac absolute 0.4g (0.4%)
Surplus is an ethanol;
Above-mentioned cream jasmin france is through being prepared as follows the method preparation, and its preparation process specifically comprises the steps:
With ethanol; Jasmal; Benzyl propionate; α-Wu Jiguiquan; α-Ji Jiguiquan; 10% Dihydrojasmone ethanolic soln; Methyl dihydrojasmonate; Phantol; Phanteine; 10% phenyl aldehyde ethanolic soln; 10% γ-Shi Yineizhi ethanolic soln; 10% cis-3-hexenol ethanolic soln; 10% acetate leaf-alcohol ester ethanolic soln; Phenylacetic aldehyde; 10% benzopyrrole ethanolic soln; 10% p-cresyl acetate ethanolic soln; Terpineol 350; Isoeugenol; Phenylethyl alcohol; Geraniol; α-Zi Luolantong; Cinnamic alcohol; Ylang ylang oil; The jasminum sambac absolute uniform mixing promptly obtains cream jasmin france.The essence fragrance that obtains is pure and fresh elegant, has the characteristic perfume of jasmine, and has stronger natural sense.
In sum, a kind of paste microcapsule cream jasmin france of the present invention is because therefore synergistic effects such as emulsification, thickening have characteristics in stable condition, that fragrance is coordinated.A kind of paste microcapsule cream jasmin france of gained under the condition of the prescription of embodiment 4 particularly.
The above content is merely the basic explanation of the present invention under conceiving, and according to any equivalent transformation that technical scheme of the present invention is done, all belongs to the scope of the present invention's protection.
Claims (7)
1. a paste microcapsule cream jasmin france is characterized in that counting by weight percentage, and the composition and the content of its raw material are following:
Cream jasmin france 5-25%
Beta-cyclodextrin 10-50%
XG 550 0.1-2%
Surplus is a deionized water;
Above-mentioned a kind of paste microcapsule cream jasmin france prepares through following method, and its preparation process specifically comprises the steps:
(1), in beaker, add beta-cyclodextrin, add deionized water again, open to stir, beta-cyclodextrin is dispersed in the deionized water uniformly, obtain the beta-cyclodextrin suspension liquid;
(2), XG 550 is joined in the beta-cyclodextrin suspension liquid of step (1) gained, continue to stir, after making the XG 550 dissolving and being evenly distributed, add cream jasmin france again and continue to stir, promptly get paste microcapsule cream jasmin france.
2. a kind of paste microcapsule cream jasmin france as claimed in claim 1 is characterized in that counting by weight percentage, and the composition and the content of its raw material are following:
Cream jasmin france 5-15%
Beta-cyclodextrin 10-45%
XG 550 0.1-2%
Surplus is a deionized water.
3. according to claim 1 or claim 2 a kind of paste microcapsule cream jasmin france is characterized in that the cream jasmin france described in the feed composition counts by weight percentage, and the composition and the content of its raw material are following:
Jasmal 20-35%
Benzyl propionate 1-3%
α-Wu Jiguiquan 5-10%
α-Ji Jiguiquan 5-15%
10% Dihydrojasmone ethanolic soln 0.5-2.5%
Methyl dihydrojasmonate 4-10%
Phantol 10-15%
Phanteine 5-10%
10% phenyl aldehyde ethanolic soln 0.1-0.4%
10% γ-Shi Yineizhi ethanolic soln 1-1.5%
10% cis-3-hexenol ethanolic soln 1-3.5%
10% acetate leaf-alcohol ester ethanolic soln 0.5-3%
Phenylacetic aldehyde 0.1-0.8%
10% benzopyrrole ethanolic soln 3-6%
10% p-cresyl acetate ethanolic soln 0.5-1%
Terpineol 350 1-2.5%
Isoeugenol 0.5-1%
Phenylethyl alcohol 1-5%
Geraniol 1-3%
α-Zi Luolantong 0.5-1%
Cinnamic alcohol 1-1.5%
Ylang ylang oil 0.1-0.5%
Jasminum sambac absolute 0.1-0.4%
Surplus is an ethanol;
Above-mentioned cream jasmin france prepares through following method:
With ethanol, jasmal, benzyl propionate, α-Wu Jiguiquan, α-Ji Jiguiquan, 10% Dihydrojasmone ethanolic soln, methyl dihydrojasmonate, phantol, phanteine, 10% phenyl aldehyde ethanolic soln, 10% γ-Shi Yineizhi ethanolic soln, 10% cis-3-hexenol ethanolic soln, 10% acetate leaf-alcohol ester ethanolic soln, phenylacetic aldehyde, 10% benzopyrrole ethanolic soln, 10% p-cresyl acetate ethanolic soln, Terpineol 350, isoeugenol, phenylethyl alcohol, geraniol, α-Zi Luolantong, cinnamic alcohol, ylang ylang oil, jasminum sambac absolute uniform mixing, can mix cream jasmin france.
4. a kind of paste microcapsule cream jasmin france as claimed in claim 3 is characterized in that the cream jasmin france described in the feed composition counts by weight percentage, and the composition and the content of its raw material are following:
Jasmal 20-35%
Benzyl propionate 1%
α-Wu Jiguiquan 5-10%
α-Ji Jiguiquan 5-15%
10% Dihydrojasmone ethanolic soln 1-2.5%
Methyl dihydrojasmonate 4-10%
Phantol 10-15%
Phanteine 5-10%
10% phenyl aldehyde ethanolic soln 0.1-0.4%
10% γ-Shi Yineizhi ethanolic soln 1-1.5%
10% cis-3-hexenol ethanolic soln 1-2%
10% acetate leaf-alcohol ester ethanolic soln 1-3%
Phenylacetic aldehyde 0.1-0.3%
10% benzopyrrole ethanolic soln 3-4%
10% p-cresyl acetate ethanolic soln 0.5-1%
Terpineol 350 1%
Isoeugenol 0.5%
Phenylethyl alcohol 2-3%
Geraniol 1%
α-Zi Luolantong 0.5-1%
Cinnamic alcohol 1%
Ylang ylang oil 0.1-0.5%
Jasminum sambac absolute 0.1-0.4%
Surplus is an ethanol.
5. a kind of paste microcapsule cream jasmin france as claimed in claim 4 is characterized in that counting by weight percentage, and the composition and the content of its raw material are following:
Cream jasmin france 10%
Beta-cyclodextrin 20%
XG 550 1%
Deionized water 69%;
Described cream jasmin france is counted by weight percentage, and the composition and the content of its raw material are following:
Jasmal 35%
Benzyl propionate 1%
α-Wu Jiguiquan 5%
α-Ji Jiguiquan 5%
10% Dihydrojasmone ethanolic soln 2%
Methyl dihydrojasmonate 7%
Phantol 15%
Phanteine 10%
10% phenyl aldehyde ethanolic soln 0.4%
10% γ-Shi Yineizhi ethanolic soln 1.5%
10% cis-3-hexenol ethanolic soln 1%
10% acetate leaf-alcohol ester ethanolic soln 3%
Phenylacetic aldehyde 0.1%
10% benzopyrrole ethanolic soln 3%
10% p-cresyl acetate ethanolic soln 0.5%
Terpineol 350 1%
Isoeugenol 0.5%
Phenylethyl alcohol 3%
Geraniol 1%
α-Zi Luolantong 1%
Cinnamic alcohol 1%
Ylang ylang oil 0.1%
Jasminum sambac absolute 0.1%
Surplus is an ethanol.
6. used cream jasmin france in according to claim 1 or claim 2 a kind of paste microcapsule cream jasmin france is characterized in that counting by weight percentage, and the composition and the content of its raw material are following:
Jasmal 20-35%
Benzyl propionate 1-3%
α-Wu Jiguiquan 5-10%
α-Ji Jiguiquan 5-15%
10% Dihydrojasmone ethanolic soln 0.5-2.5%
Methyl dihydrojasmonate 4-10%
Phantol 10-15%
Phanteine 5-10%
10% phenyl aldehyde ethanolic soln 0.1-0.4%
10% γ-Shi Yineizhi ethanolic soln 1-1.5%
10% cis-3-hexenol ethanolic soln 1-3.5%
10% acetate leaf-alcohol ester ethanolic soln 0.5-3%
Phenylacetic aldehyde 0.1-0.8%
10% benzopyrrole ethanolic soln 3-6%
10% p-cresyl acetate ethanolic soln 0.5-1%
Terpineol 350 1-2.5%
Isoeugenol 0.5-1%
Phenylethyl alcohol 1-5%
Geraniol 1-3%
α-Zi Luolantong 0.5-1%
Cinnamic alcohol 1-1.5%
Ylang ylang oil 0.1-0.5%
Jasminum sambac absolute 0.1-0.4%
Surplus is an ethanol;
Above-mentioned cream jasmin france prepares through following method:
With ethanol, jasmal, benzyl propionate, α-Wu Jiguiquan, α-Ji Jiguiquan, 10% Dihydrojasmone ethanolic soln, methyl dihydrojasmonate, phantol, phanteine, 10% phenyl aldehyde ethanolic soln, 10% γ-Shi Yineizhi ethanolic soln, 10% cis-3-hexenol ethanolic soln, 10% acetate leaf-alcohol ester ethanolic soln, phenylacetic aldehyde, 10% benzopyrrole ethanolic soln, 10% p-cresyl acetate ethanolic soln, Terpineol 350, isoeugenol, phenylethyl alcohol, geraniol, α-Zi Luolantong, cinnamic alcohol, ylang ylang oil, jasminum sambac absolute uniform mixing, can mix cream jasmin france.
7. cream jasmin france as claimed in claim 6 is characterized in that counting by weight percentage, and the composition and the content of its raw material are following:
Jasmal 20-35%
Benzyl propionate 1%
α-Wu Jiguiquan 5-10%
α-Ji Jiguiquan 5-15%
10% Dihydrojasmone ethanolic soln 1-2.5%
Methyl dihydrojasmonate 4-10%
Phantol 10-15%
Phanteine 5-10%
10% phenyl aldehyde ethanolic soln 0.1-0.4%
10% γ-Shi Yineizhi ethanolic soln 1-1.5%
10% cis-3-hexenol ethanolic soln 1-2%
10% acetate leaf-alcohol ester ethanolic soln 1-3%
Phenylacetic aldehyde 0.1-0.3%
10% benzopyrrole ethanolic soln 3-4%
10% p-cresyl acetate ethanolic soln 0.5-1%
Terpineol 350 1%
Isoeugenol 0.5%
Phenylethyl alcohol 2-3%
Geraniol 1%
α-Zi Luolantong 0.5-1%
Cinnamic alcohol 1%
Ylang ylang oil 0.1-0.5%
Jasminum sambac absolute 0.1-0.4%
Surplus is an ethanol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210288896 CN102776069B (en) | 2012-08-15 | 2012-08-15 | Paste microcapsule jasmine essence and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210288896 CN102776069B (en) | 2012-08-15 | 2012-08-15 | Paste microcapsule jasmine essence and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102776069A true CN102776069A (en) | 2012-11-14 |
| CN102776069B CN102776069B (en) | 2013-10-16 |
Family
ID=47121181
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201210288896 Expired - Fee Related CN102776069B (en) | 2012-08-15 | 2012-08-15 | Paste microcapsule jasmine essence and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102776069B (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104359902A (en) * | 2014-11-13 | 2015-02-18 | 上海应用技术学院 | Formaldehyde colour-rendering test paper, and preparation method and application thereof |
| CN105246345A (en) * | 2013-09-19 | 2016-01-13 | 小川香料株式会社 | Flavor-improving agent for tea beverage or tea-containing food product |
| CN106148006A (en) * | 2016-08-03 | 2016-11-23 | 安徽省三环纸业集团香料科技发展有限公司 | A kind of antidepressant joyful type liquid detergent microcapsule essence |
| CN107047813A (en) * | 2017-05-09 | 2017-08-18 | 南京扬子茉莉谷文化科技有限公司 | The preparation method and snowball oil microcapsule powder of a kind of snowball oil microcapsule powder |
| CN114471392A (en) * | 2022-02-09 | 2022-05-13 | 云南中烟工业有限责任公司 | Ring-opened cucurbituril-based cis-jasmone supramolecular capsule and preparation method and application thereof |
| CN117343798A (en) * | 2023-10-24 | 2024-01-05 | 协成香精香料(南通)有限公司 | Jasmine essence and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1073711A (en) * | 1991-12-27 | 1993-06-30 | 昆明五华香料厂 | Microcapsule aromatizing agent and preparation method thereof and purposes |
| WO2008044046A1 (en) * | 2006-10-13 | 2008-04-17 | Reckit Benckiser (Uk) Limited | Perfume compositions |
| WO2009090355A1 (en) * | 2008-01-15 | 2009-07-23 | Reckitt Benckiser (Uk) Limited | Perfume compositions |
| CN101811015A (en) * | 2010-04-15 | 2010-08-25 | 上海应用技术学院 | Preparation method of jasmine sambac essence capsule |
| CN101818100A (en) * | 2010-04-15 | 2010-09-01 | 上海应用技术学院 | Preparation method of polybutylcyanoacrylate-encapsulated jasminum grandiflorum essence capsule |
| CN102553503A (en) * | 2012-02-06 | 2012-07-11 | 陕西师范大学 | Preparation method of sub-micron-scale controlled-release essence microcapsule |
-
2012
- 2012-08-15 CN CN 201210288896 patent/CN102776069B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1073711A (en) * | 1991-12-27 | 1993-06-30 | 昆明五华香料厂 | Microcapsule aromatizing agent and preparation method thereof and purposes |
| WO2008044046A1 (en) * | 2006-10-13 | 2008-04-17 | Reckit Benckiser (Uk) Limited | Perfume compositions |
| WO2009090355A1 (en) * | 2008-01-15 | 2009-07-23 | Reckitt Benckiser (Uk) Limited | Perfume compositions |
| CN101811015A (en) * | 2010-04-15 | 2010-08-25 | 上海应用技术学院 | Preparation method of jasmine sambac essence capsule |
| CN101818100A (en) * | 2010-04-15 | 2010-09-01 | 上海应用技术学院 | Preparation method of polybutylcyanoacrylate-encapsulated jasminum grandiflorum essence capsule |
| CN102553503A (en) * | 2012-02-06 | 2012-07-11 | 陕西师范大学 | Preparation method of sub-micron-scale controlled-release essence microcapsule |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105246345A (en) * | 2013-09-19 | 2016-01-13 | 小川香料株式会社 | Flavor-improving agent for tea beverage or tea-containing food product |
| CN104359902A (en) * | 2014-11-13 | 2015-02-18 | 上海应用技术学院 | Formaldehyde colour-rendering test paper, and preparation method and application thereof |
| CN106148006A (en) * | 2016-08-03 | 2016-11-23 | 安徽省三环纸业集团香料科技发展有限公司 | A kind of antidepressant joyful type liquid detergent microcapsule essence |
| CN107047813A (en) * | 2017-05-09 | 2017-08-18 | 南京扬子茉莉谷文化科技有限公司 | The preparation method and snowball oil microcapsule powder of a kind of snowball oil microcapsule powder |
| CN114471392A (en) * | 2022-02-09 | 2022-05-13 | 云南中烟工业有限责任公司 | Ring-opened cucurbituril-based cis-jasmone supramolecular capsule and preparation method and application thereof |
| CN117343798A (en) * | 2023-10-24 | 2024-01-05 | 协成香精香料(南通)有限公司 | Jasmine essence and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102776069B (en) | 2013-10-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102776068A (en) | Paste type microcapsule flavoring rose essence and preparation method thereof | |
| CN102776071A (en) | Transparent microcapsule flavoring jasmine essence and preparation method thereof | |
| CN102776069A (en) | Paste microcapsule jasmine essence and preparation method thereof | |
| CN102776070A (en) | Transparent microcapsule flavoring rose essence and preparation method thereof | |
| CN104277249B (en) | A kind of antimicrobial packaging film and preparation method thereof | |
| CN105395373A (en) | Flake microcapsule | |
| CN102776073A (en) | Paste type microcapsule flavoring tuberose essence and preparation method thereof | |
| CN104666275B (en) | Starch-based plant empty capsule | |
| CN104923134B (en) | Preparation method for lavender nanocapsule | |
| CN109957449A (en) | A kind of soluble perfume and preparation method thereof | |
| CN107712543A (en) | A kind of deflocculation curcumin microcapsule, preparation method and applications | |
| CN103316616A (en) | Osmanthus essence nanocapsule and preparation method | |
| CN105540073A (en) | Brittle capsule for cigarettes and preparation method thereof | |
| CN102924942A (en) | Modified plant fiber material type glass moldproof parting powder | |
| CN106074684A (en) | Slow-releasing sachet and preparation method thereof | |
| CN102807920A (en) | Transparent microcapsule tuberose essence and preparation method thereof | |
| CN103409247A (en) | Mosquito-expelling washing powder | |
| CN104073346A (en) | Nanometer level microcapsule sweet orange essence and preparing method thereof | |
| CN102846494A (en) | Perfume | |
| CN107237215B (en) | Fresh-keeping grease proofing food wrapper and preparation method thereof | |
| CN106281676A (en) | A kind of Microencapsulated Slow essence and preparation method thereof | |
| CN103461988B (en) | High-content alpha-linolenic acid microcapsule and manufacturing method thereof | |
| CN103849466B (en) | A kind of weather-proof long-acting type of resistance to migration microcapsule essence and preparation method thereof | |
| CN103881400B (en) | Edibility nano flower raw albumen composite membrane and preparation technology thereof | |
| CN101818100B (en) | Preparation method of polybutylcyanoacrylate-encapsulated jasminum grandiflorum essence capsule |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131016 Termination date: 20160815 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |