CN109957449A - A kind of soluble perfume and preparation method thereof - Google Patents
A kind of soluble perfume and preparation method thereof Download PDFInfo
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- CN109957449A CN109957449A CN201711500068.6A CN201711500068A CN109957449A CN 109957449 A CN109957449 A CN 109957449A CN 201711500068 A CN201711500068 A CN 201711500068A CN 109957449 A CN109957449 A CN 109957449A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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Abstract
The present invention relates to flavors and fragrances products, more particularly to a kind of soluble perfume and preparation method thereof, the soluble perfume is prepared using 10~60 parts by weight of oil soluble perfume, 0.1~2 parts by weight of converted starch, 15~50 parts by weight of emulsifier, 5~25 parts by weight of assistant for emulsifying agent, 0.05~0.4 parts by weight of thickener, 0.01~0.1 parts by weight of citric acid, 0.02~0.08 parts by weight of potassium sorbate, 1~5 parts by weight of distilled water through self-emulsification approach.Specific aim of the present invention solves oil soluble perfume and is difficult to the technical issues of being dissolved in the water, and oil soluble perfume is enable quickly and easily to be dissolved in water, and for cigarette filter gel flavoring, cigarette paper flavoring and tobacco perfuming etc., assigns the specific aromatic style of cigarette product.Preparation method simple process of the invention, equipment requirement is low, is easy to industrialization.
Description
Technical field
The present invention relates to flavors and fragrances product processing technique fields, more particularly, to a kind of soluble perfume and its system
Preparation Method.
Technical background
Variation with the increasingly developed and consumer of low tar Less harmful cigarette to cigarette style demand, perfuming cigarette add
The research and development and application of material have become one of the key technology that cigarette fragrant smell is kept in work of reducing tar and reducing harm.Domestic production of cigarettes enterprise
Industry is carrying out correlative study work, preferably to meet the needs of tobacco consumer.Meanwhile with the substantially drop of tar content
Low, the flavouring essence quality that tobacco leaf itself has certainly will be affected, and traditional flavoring and casing technology cannot better meet mesh
The requirement of preceding cigarette industry development, fragrance of the cigarette in suction is obviously insufficient, the needs for the person that is not able to satisfy cigarette consumption.Cause
This, the development of tobacco industry proposes new higher requirement to cigarette composition and flavoring and casing technology, and there is an urgent need to adapt to mesh
The exploitation and corresponding compensating aroma technology of the new fragrance of preceding cigarette industry development.
There are many ways to perfuming cigarette, can be conventional method and be directly added into pipe tobacco, can also be added in cigarette
In other auxiliary materials such as filter tip, cigarette paper and packaging material.In recent years, reported cigarette filter gel flavoring, cigarette paper and cigarette
The modes such as box aluminum foil lining paper flavoring, but these novel flavoring modes require that essence used can be dissolved in well
In water, the most of dissolubility in water of essence spice for cigarette used in tradition flavoring is poor at present, limits these flavoring sides
The application of formula, and result in that the fragrance release in suction of the cigarette of institute's flavoring is uneven, and hamony and stability are poor.Institute
With, transformation and improves the dissolubility in water of essence spice for cigarette used in traditional flavoring and solubility and just become new cigarette
Flavoring industry research and focus technology problem urgently to be solved.
Summary of the invention
The purpose of the present invention is provide a kind of soluble easily in water, steady for drawbacks described above existing for essence spice for cigarette now
Qualitative good, fragrance discharges uniform soluble perfume, can be used for cigarette filter gel flavoring, cigarette paper flavoring and tobacco perfuming
Deng the imparting specific aromatic style of cigarette product.
In addition a kind of simple, easy to operate, the easy industrialization of preparation process and the free of contamination water solubility of production process are also provided
The preparation method of essence.
The purpose of the present invention is achieved by the following technical programs:
A kind of soluble perfume is provided, is prepared using each group lease making self-emulsifying of following parts by weight:
Preferably, the soluble perfume is prepared using each group lease making self-emulsifying of following parts by weight:
Oil soluble perfume of the present invention is any in dissolubility poor natural essence or preparing essence in water
One kind, including but not limited to sweet orange oil essence, grapefruit oil essence, flavoring orange oil essence, flavoring lemon oil essence, Fruity type essence, the fragrance of a flower
Type essence, spicy essence, hay flavor essence, tobacco this flavor essence, green grows flavor essence, milk flavoured type at Costus essence
Essence, baking flavor essence in any one；The converted starch is crosslinked starch；The emulsifier be sucrose ester and
Polyglycerol ester, the weight proportion of the two are sucrose ester: polyglycerol ester=1: 1~1: 10；The assistant for emulsifying agent is ethyl alcohol, the third two
Alcohol, glycerol, any one in polyethylene glycol；The thickener is xanthan gum, any one in Arabic gum.
Invention also provides the preparation methods of the soluble perfume, comprising the following steps:
S1. oil soluble perfume, converted starch, emulsifier and assistant for emulsifying agent are weighed according to the ratio, distilled water are added, in 40~60
Under DEG C water-bath and machine mixer, 50~200r/min of speed stirs 5~15min, carries out self-emulsifying to being uniformly dissolved, is made
Oil soluble perfume emulsified body；
S2. thickener, citric acid and potassium sorbate are weighed according to the ratio, and distilled water is then added, at 40~60 DEG C of water-bath,
The mixture aqueous solutions such as thickener are made in stirring and dissolving；
S3. the oil soluble perfume emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as thickener, emulsification pretreatment is extremely
Soluble perfume is made in uniformly one.
More specifically, preparation method of the invention the following steps are included:
S1. 10~60 parts by weight oil soluble perfumes, 0.1~2 parts by weight converted starch, 15~50 parts by weight are weighed according to the ratio
0.5~2.5 parts by weight distilled water is added, in 40~60 DEG C of water-baths and mechanical stirring in emulsifier and 5~25 parts by weight assistant for emulsifying agents
Under machine, 50~200r/min of speed stirs 5~15min, carries out self-emulsifying to being uniformly dissolved, oil soluble perfume emulsified body is made；
S2. 0.05~0.4 parts by weight of thickening agent, 0.01~0.1 parts by weight of lemon acid and 0.02~0.08 are weighed according to the ratio
Then 0.5~2.5 parts by weight distilled water is added in parts by weight potassium sorbate, at 40~60 DEG C of water-bath, stirring and dissolving is made and increases
Thick dose of equal mixture aqueous solutions；
S3. the oil soluble perfume emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as thickener, emulsification pretreatment is extremely
Soluble perfume is made in uniformly one.
Raw material oil soluble perfume can be according to cigarette consumption person to fragrance in soluble perfume formula in above-mentioned technical proposal
Different demands, choose at random the essence with different aromas style with preparation cost invention soluble perfume.
Self-emulsifying technology refers to being formed by oily phase, nonionic surfactant and assistant for emulsifying agent in terms of medicine uniform
Solid or liquid preparation transparent and that include drug, in the case where environment temperature (usually 37 DEG C) and gentle agitation, due to
The presence of surfactant, spontaneous emulsification form partial size in the emulsion of 100~500nm, referred to as self-emulsifying drug delivery system.And as parent
Aqueous tenside (HLB > 12) content higher (>=40%, w/w) or surfactant add assistant for emulsifying agent, can be light
Finer solution (partial size < 100nm), referred to as self-micro-emulsification medicine-releasing system are made under micro- agitation.Self-emulsifying technology has emulsification
Temperature is low, generally in room temperature or 40 DEG C or less；Equipment requirement is low, only needs conventional mechanical stirring；Emulsion is dissolved in water and is formed
A kind of emulsification system the advantages that being transparent or semitransparent, low viscosity, isotropy and thermodynamically stable micro emulsion.Mesh
Before, it yet there are no at home and soluble perfume prepared with self-emulsifying technology.
The present invention experiments verify that, the partial size of the soluble perfume belongs to self-emulsifying emulsion or from micro- in 50~500nm
Emulsify emulsion；It is soluble easily in water, it has good stability, soluble perfume of the present invention is dissolved in the water with 5% (w/w), can must be dissolved
Clear solution；Under 4000r/min, it is centrifuged 10min, there are no lamination；For cigarette filter gel flavoring, this is sent out
Bright soluble perfume is dissolved in the gel of melting with 2% (w/w), is then injected into cigarette filter, and injection dosage is cigarette
0.05% (w/w) of weight, and smoked panel test by member of smoking, fragrance release uniformly, assigns the specific aromatic style of cigarette product.
The beneficial effects of the present invention are:
The present invention provides a kind of soluble perfumes, first by optimizing the compatibility and ratio of emulsifier and assistant for emulsifying agent,
The partial size of prepared soluble perfume is set to be in Nano grade, it is soluble easily in water to form a kind of transparent or semitransparent, low viscosity
, isotropy and thermodynamically stable micro emulsion, specific aim solve oil soluble perfume and be difficult to the technical issues of being dissolved in the water；
Secondly using the converted starch of crosslinking, the gap with three-dimensional space network structure has certain encapsulation to aroma substance,
It is more uniform to play fragrance release；Third use thickener, citric acid and potassium sorbate, improve soluble perfume stability and
Anti-corrosive properties.
Method of the present invention, equipment requirement is low, implements simply, operation is controllable, easy to industrialized production.
Specific embodiment
Combined with specific embodiments below, the present invention is described in further details.Unless stated otherwise, the present invention uses
Raw material and equipment are the raw material for meeting the perhaps workable additive list of food additives requirement or tobacco product of regular market purchase
With the conventional use of equipment of the art.Following embodiment is only for further specific descriptions of the invention, and not
It is for the restriction to the claimed scope of the invention.
Embodiment 1
S1. 30 parts by weight sweet orange oil essences, 1 parts by weight converted starch, 35 parts by weight Emulsifier (sucrose esters are weighed according to the ratio
: with 20 parts by weight of ethanol, 1 parts by weight distilled water, under 40 DEG C of water-baths and machine mixer, speed polyglycerol ester=1: 4) is added
50r/min stirs 10min, carries out self-emulsifying to being uniformly dissolved, sweet orange oil essence emulsified body is made；
S2. 0.1 parts by weight xanthan gum, 0.05 parts by weight of lemon acid and 0.05 parts by weight potassium sorbate are weighed according to the ratio, so
After 1 parts by weight distilled water is added, at 40 DEG C of water-bath, the mixture aqueous solutions such as xanthan gum are made in stirring and dissolving；
S3. the sweet orange oil essence emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as xanthan gum, emulsification pretreatment is extremely
Water solubility sweet orange oil essence is made in uniformly one.
Embodiment 2
S1. 10 parts by weight grapefruit oil essences, 0.1 parts by weight converted starch, 15 parts by weight Emulsifier (sucrose are weighed according to the ratio
Ester: polyglycerol ester=1: 2) with 5 parts by weight of ethanol, being added 0.5 parts by weight distilled water, under 45 DEG C of water-baths and machine mixer,
Speed 100r/min stirs 5min, carries out self-emulsifying to being uniformly dissolved, grapefruit oil essence emulsified body is made；
S2. 0.05 parts by weight xanthan gum, 0.01 parts by weight of lemon acid and 0.02 parts by weight potassium sorbate are weighed according to the ratio, so
After 0.5 parts by weight distilled water is added, at 45 DEG C of water-bath, the mixture aqueous solutions such as xanthan gum are made in stirring and dissolving；
S3. the grapefruit oil essence emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as xanthan gum, emulsification pretreatment is extremely
Water solubility grapefruit oil essence is made in uniformly one.
Embodiment 3
S1. 15 parts by weight flavoring orange oil essences, 0.2 parts by weight converted starch, 18 parts by weight Emulsifier (sucrose are weighed according to the ratio
Ester: polyglycerol ester=1: 3) with 10 parts by weight of ethanol, being added 1.2 parts by weight distilled water, under 50 DEG C of water-baths and machine mixer,
Speed 150r/min stirs 15min, carries out self-emulsifying to being uniformly dissolved, flavoring orange oil essence emulsified body is made；
S2. 0.2 parts by weight Arabic gum, 0.02 parts by weight of lemon acid and 0.04 parts by weight potassium sorbate are weighed according to the ratio,
Then 1.8 parts by weight distilled water are added, at 50 DEG C of water-bath, the mixture aqueous solutions such as Arabic gum are made in stirring and dissolving；
S3. the flavoring orange oil essence emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as Arabic gum, emulsification pretreatment
To uniform one, water solubility flavoring orange oil essence is made.
Embodiment 4
S1. 40 parts by weight of lemon oil essences, 1.5 parts by weight converted starches, 40 parts by weight Emulsifier (sucrose are weighed according to the ratio
Ester: polyglycerol ester=1: 9) with 15 parts by weight of ethanol, being added 2.5 parts by weight distilled water, under 55 DEG C of water-baths and machine mixer,
Speed 200r/min stirs 15min, carries out self-emulsifying to being uniformly dissolved, flavoring lemon oil essence emulsified body is made；
S2. 0.4 parts by weight Arabic gum, 0.1 parts by weight of lemon acid and 0.08 parts by weight potassium sorbate are weighed according to the ratio, so
After 2.5 parts by weight distilled water are added, at 55 DEG C of water-bath, the mixture aqueous solutions such as Arabic gum are made in stirring and dissolving；
S3. the flavoring lemon oil essence emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as Arabic gum, emulsification pretreatment
To uniform one, water-soluble lemon oil essence is made.
Embodiment 5
S1. 60 parts by weight Fruity type essence, 2 parts by weight converted starches, 16 parts by weight Emulsifier (sucrose esters are weighed according to the ratio
: polyglycerol ester=1: 4) with 5 parts by weight of propylene glycol, being added 2.5 parts by weight distilled water, under 60 DEG C of water-baths and machine mixer,
Speed 150r/min stirs 10min, carries out self-emulsifying to being uniformly dissolved, Fruity type essence emulsified body is made；
S2. 0.3 parts by weight Arabic gum, 0.04 parts by weight of lemon acid and 0.06 parts by weight potassium sorbate are weighed according to the ratio,
Then 2 parts by weight distilled water are added, at 60 DEG C of water-bath, the mixture aqueous solutions such as Arabic gum are made in stirring and dissolving；
S3. the Fruity type essence emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as Arabic gum, emulsification pretreatment
To uniform one, water solubility Fruity type essence is made.
Embodiment 6
S1. 40 parts by weight bouquet type compositions, 0.8 parts by weight converted starch, 50 parts by weight Emulsifier (sucrose are weighed according to the ratio
Ester: polyglycerol ester=1: 7) with 25 parts by weight of propylene glycol, being added 2 parts by weight distilled water, under 45 DEG C of water-baths and machine mixer,
Speed 100r/min stirs 10min, carries out self-emulsifying to being uniformly dissolved, bouquet type composition emulsified body is made；
S2. 0.25 parts by weight xanthan gum, 0.03 parts by weight of lemon acid and 0.04 parts by weight potassium sorbate are weighed according to the ratio, so
After 1.5 parts by weight distilled water are added, at 45 DEG C of water-bath, the mixture aqueous solutions such as xanthan gum are made in stirring and dissolving；
S3. the bouquet type composition emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as xanthan gum, emulsification pretreatment is extremely
Water solubility bouquet type composition is made in uniformly one.
Embodiment 7
S1. 50 parts by weight Costus essences, 0.5 parts by weight converted starch, 33 parts by weight Emulsifier (sucrose are weighed according to the ratio
Ester: polyglycerol ester=1: 10) with 17 parts by weight of glycerin, 1.5 parts by weight distilled water are added, in 50 DEG C of water-baths and machine mixer
Under, speed 150r/min stirs 5min, carries out self-emulsifying to being uniformly dissolved, Costus essence emulsified body is made；
S2. 0.08 parts by weight xanthan gum, 0.06 parts by weight of lemon acid and 0.07 parts by weight potassium sorbate are weighed according to the ratio, so
After 2 parts by weight distilled water are added, at 50 DEG C of water-bath, the mixture aqueous solutions such as xanthan gum are made in stirring and dissolving；
S3. the Costus essence emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as xanthan gum, emulsification pretreatment is extremely
Water solubility Costus essence is made in uniformly one.
Embodiment 8
S1. 20 parts by weight spicy essences, 1.2 parts by weight converted starches, 24 parts by weight Emulsifier (sucrose are weighed according to the ratio
Ester: polyglycerol ester=1: 5) with 6 parts by weight polyethylene glycol, 2.5 parts by weight distilled water are added, in 60 DEG C of water-baths and machine mixer
Under, speed 200r/min stirs 15min, carries out self-emulsifying to being uniformly dissolved, spicy essence emulsified body is made；
S2. 0.15 parts by weight xanthan gum, 0.08 parts by weight of lemon acid and 0.08 parts by weight potassium sorbate are weighed according to the ratio, so
After 2.5 parts by weight distilled water are added, at 60 DEG C of water-bath, the mixture aqueous solutions such as xanthan gum are made in stirring and dissolving；
S3. the spicy essence emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as xanthan gum, emulsification pretreatment is extremely
Water solubility spicy essence is made in uniformly one.
Embodiment 9
S1. 25 parts by weight hay flavor essences, 0.1 parts by weight converted starch, 25 parts by weight Emulsifier (sugarcanes are weighed according to the ratio
Sugar ester: polyglycerol ester=1: 1) with 12 parts by weight polyethylene glycol, 2 parts by weight distilled water are added, in 55 DEG C of water-baths and mechanical stirring
Under machine, speed 50r/min stirs 10min, carries out self-emulsifying to being uniformly dissolved, hay flavor essence emulsified body is made；
S2. 0.35 parts by weight Arabic gum, 0.03 parts by weight of lemon acid and 0.04 parts by weight potassium sorbate are weighed according to the ratio,
Then 2 parts by weight distilled water are added, at 55 DEG C of water-bath, the mixture aqueous solutions such as Arabic gum are made in stirring and dissolving；
S3. the hay flavor essence emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as Arabic gum, shearing cream
Change to uniform one, water solubility hay flavor essence is made.
Embodiment 10
S1. 20 parts by weight tobacco this flavor essence, 1.6 parts by weight converted starches, 45 parts by weight Emulsifier are weighed according to the ratio
(sucrose ester: polyglycerol ester=1: 4) and 12 parts by weight help propylene glycol, 1.5 parts by weight distilled water are added, in 60 DEG C of water-baths and machinery
Under blender, speed 100r/min stirs 15min, carries out self-emulsifying to being uniformly dissolved, the emulsification of this flavor essence of tobacco is made
Body；
S2. 0.25 parts by weight are weighed according to the ratio increases xanthan gum, 0.1 parts by weight of lemon acid and 0.08 parts by weight potassium sorbate,
Then 2.5 parts by weight distilled water are added, at 60 DEG C of water-bath, the mixture aqueous solutions such as xanthan gum are made in stirring and dissolving；
S3. this flavor essence of the tobacco of step S1 emulsified body is added at a slow speed the mixture aqueous solutions such as xanthan gum, shearing cream
Change to uniform one, this flavor essence of water solubility tobacco is made.
Embodiment 11
S1. 18 parts by weight blueness are weighed according to the ratio grows flavor essence, 0.15 parts by weight converted starch, 32 parts by weight Emulsifier
(sucrose ester: polyglycerol ester=1: 3) and 10 parts by weight of ethanol, 1 parts by weight distilled water is added, in 45 DEG C of water-baths and machine mixer
Under, speed 150r/min stirs 10min, carries out self-emulsifying to being uniformly dissolved, is made green and grows flavor essence emulsified body；
S2. 0.18 parts by weight Arabic gum, 0.02 parts by weight of lemon acid and 0.03 parts by weight potassium sorbate are weighed according to the ratio,
Then 1.5 parts by weight distilled water are added, at 45 DEG C of water-bath, the mixture aqueous solutions such as Arabic gum are made in stirring and dissolving；
S3. the green flavor essence emulsified body of growing of step S1 is added at a slow speed the mixture aqueous solutions such as Arabic gum, shearing cream
Change to uniform one, water-soluble green taste flavor essence is made.
Embodiment 12
S1. 10 parts by weight milk flavoured type essence, 2 parts by weight converted starches, 20 parts by weight Emulsifier (sucrose esters are weighed according to the ratio
: polyglycerol ester=1: 5) with 15 parts by weight of propylene glycol, being added 2.5 parts by weight distilled water, under 60 DEG C of water-baths and machine mixer,
Speed 200r/min stirs 15min, carries out self-emulsifying to being uniformly dissolved, milk flavoured type essence emulsified body is made；
S2. 0.3 parts by weight Arabic gum, 0.03 parts by weight of lemon acid and 0.06 parts by weight potassium sorbate are weighed according to the ratio,
Then 2.5 parts by weight distilled water are added, at 60 DEG C of water-bath, the mixture aqueous solutions such as Arabic gum are made in stirring and dissolving；
S3. the milk flavoured type essence emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as Arabic gum, emulsification pretreatment
To uniform one, water solubility milk flavoured type essence is made.
Embodiment 13
S1. 35 parts by weight baking flavor essence, 0.8 parts by weight converted starch, 28 parts by weight Emulsifier (sugarcanes are weighed according to the ratio
Sugar ester: polyglycerol ester=1: 6) with 22 parts by weight of propylene glycol, 2.5 parts by weight distilled water are added, in 55 DEG C of water-baths and mechanical stirring
Under machine, speed 100r/min stirs 10min, carries out self-emulsifying to being uniformly dissolved, baking flavor essence emulsified body is made；
S2. 0.25 parts by weight xanthan gum, 0.02 parts by weight of lemon acid and 0.03 parts by weight potassium sorbate are weighed according to the ratio, so
After 1.5 parts by weight distilled water are added, at 55 DEG C of water-bath, the mixture aqueous solutions such as xanthan gum are made in stirring and dissolving；
S3. the baking flavor essence emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as xanthan gum, emulsification pretreatment
To uniform one, water-soluble baking flavor essence is made.
Embodiment 14
Soluble perfume of the present invention is compared with the performance of oil soluble perfume before self-emulsifying
The superior function of soluble perfume in order to better illustrate the present invention, by any one in above-described embodiment 1~13
Dissolubility, stability and the cigarette filter gel perfumed applications effect of oil soluble perfume in water before soluble perfume and self-emulsifying
It is compared, experimental result is as follows:
Soluble perfume: it is soluble easily in water, it can must dissolve clear solution；It has good stability, under 4000r/min, centrifugation
10min there are no lamination；It can be dissolved in the gel of melting, be used for cigarette filter gel flavoring, fragrance release is uniform,
Assign the specific aromatic style of cigarette product.
Oil soluble perfume: being insoluble in water, there is insoluble oil droplet；Stability is poor, under 4000r/min, is centrifuged 10min, sees
Obvious grease lamination；It being difficult to be dissolved in the gel of melting, is used for cigarette filter gel flavoring, fragrance release is uneven,
Effect is poor.
It can be seen that soluble perfume of the present invention has good dissolubility and stability, preferable application effect.
Claims (8)
1. a kind of soluble perfume, which is characterized in that be prepared using each group lease making self-emulsifying of following parts by weight:
2. soluble perfume according to claim 1, which is characterized in that the oil soluble perfume is dissolubility in water
Any one in poor natural essence or preparing essence, including but not limited to sweet orange oil essence, grapefruit oil essence, citrus seed oil
Essence, flavoring lemon oil essence, Fruity type essence, bouquet type composition, Costus essence, spicy essence, hay flavor essence, tobacco
This flavor essence, any one green grown in flavor essence, milk flavoured type essence, baking flavor essence etc..
3. soluble perfume according to claim 1, which is characterized in that the converted starch is crosslinked starch.
4. soluble perfume according to claim 1, which is characterized in that the emulsifier is sucrose ester and polyglycereol
Ester, the weight proportion of the two are sucrose ester: polyglycerol ester=1: 1~1: 10.
5. soluble perfume according to claim 1, which is characterized in that the assistant for emulsifying agent is ethyl alcohol, propylene glycol, sweet
Oil, any one in polyethylene glycol.
6. soluble perfume according to claim 1, which is characterized in that the thickener is xanthan gum, Arabic gum
In any one.
7. a kind of preparation method of claim 1~6 soluble perfume, which comprises the following steps:
S1. oil soluble perfume, converted starch, emulsifier and assistant for emulsifying agent are weighed according to the ratio, distilled water are added, in 40~60 DEG C of water
Under bath and machine mixer, 50~200r/min of speed stirs 5~15min, carries out self-emulsifying to being uniformly dissolved, it is molten that oil is made
Property essence emulsified body；
S2. thickener, citric acid and potassium sorbate are weighed according to the ratio, and distilled water is then added, at 40~60 DEG C of water-bath, stirring
The mixture aqueous solutions such as thickener are made in dissolution；
S3. the oil soluble perfume emulsified body of step S1 is added at a slow speed the mixture aqueous solutions such as thickener, emulsification pretreatment is to uniform
Soluble perfume is made in one.
8. the soluble perfume that preparation method described in claim 7 is prepared.
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| CN110338389A (en) * | 2019-08-19 | 2019-10-18 | 珠海雅富兴源食品工业有限公司 | A kind of new type water-solubility natural lemon essence and preparation method thereof |
| CN110754598A (en) * | 2019-11-27 | 2020-02-07 | 翟文娟 | Lemon-flavored emulsified essence and preparation process thereof |
| CN110760388A (en) * | 2019-11-27 | 2020-02-07 | 安徽香杰香精科技有限公司 | Production formula and preparation method of electronic cigarette emulsified essence |
| CN113403154A (en) * | 2021-07-23 | 2021-09-17 | 广州芬豪香精有限公司 | Preparation method of smooth washing essence |
| CN113444574A (en) * | 2021-07-03 | 2021-09-28 | 广州芬豪香精有限公司 | Preparation method of water-soluble essence |
| CN114908574A (en) * | 2021-10-13 | 2022-08-16 | 深圳市华宝生物材料科技有限公司 | Water-based essence microcapsule and preparation method thereof |
| CN115192753A (en) * | 2022-07-07 | 2022-10-18 | 保亭海农农业开发有限公司 | Essential oil containing sarmentosum bunge and preparation method thereof |
| CN115211548A (en) * | 2022-07-25 | 2022-10-21 | 四川欣逸食品有限公司 | Water-soluble litchi essence and preparation method thereof |
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| CN110338389A (en) * | 2019-08-19 | 2019-10-18 | 珠海雅富兴源食品工业有限公司 | A kind of new type water-solubility natural lemon essence and preparation method thereof |
| CN110338389B (en) * | 2019-08-19 | 2022-05-17 | 珠海雅富兴源食品工业有限公司 | Water-soluble natural lemon essence and preparation method thereof |
| CN110754598A (en) * | 2019-11-27 | 2020-02-07 | 翟文娟 | Lemon-flavored emulsified essence and preparation process thereof |
| CN110760388A (en) * | 2019-11-27 | 2020-02-07 | 安徽香杰香精科技有限公司 | Production formula and preparation method of electronic cigarette emulsified essence |
| CN113444574A (en) * | 2021-07-03 | 2021-09-28 | 广州芬豪香精有限公司 | Preparation method of water-soluble essence |
| CN113403154A (en) * | 2021-07-23 | 2021-09-17 | 广州芬豪香精有限公司 | Preparation method of smooth washing essence |
| CN114908574A (en) * | 2021-10-13 | 2022-08-16 | 深圳市华宝生物材料科技有限公司 | Water-based essence microcapsule and preparation method thereof |
| CN114908574B (en) * | 2021-10-13 | 2023-06-16 | 深圳市华宝生物材料科技有限公司 | Water-based essence microcapsule and preparation method thereof |
| CN115192753A (en) * | 2022-07-07 | 2022-10-18 | 保亭海农农业开发有限公司 | Essential oil containing sarmentosum bunge and preparation method thereof |
| CN115192753B (en) * | 2022-07-07 | 2023-11-28 | 保亭海农农业开发有限公司 | Aromatherapy essential oil containing sarmentosum and preparation method thereof |
| CN115211548A (en) * | 2022-07-25 | 2022-10-21 | 四川欣逸食品有限公司 | Water-soluble litchi essence and preparation method thereof |
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