CN115192753A - Essential oil containing sarmentosum bunge and preparation method thereof - Google Patents
Essential oil containing sarmentosum bunge and preparation method thereof Download PDFInfo
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 59
- 241000612118 Samolus valerandi Species 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 43
- 238000000222 aromatherapy Methods 0.000 claims abstract description 36
- 239000000284 extract Substances 0.000 claims abstract description 36
- 239000002562 thickening agent Substances 0.000 claims abstract description 32
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 29
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 29
- 239000002131 composite material Substances 0.000 claims abstract description 28
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000011975 tartaric acid Substances 0.000 claims abstract description 23
- 235000002906 tartaric acid Nutrition 0.000 claims abstract description 23
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims abstract description 21
- 229930195725 Mannitol Natural products 0.000 claims abstract description 21
- 239000000594 mannitol Substances 0.000 claims abstract description 21
- 235000010355 mannitol Nutrition 0.000 claims abstract description 21
- 239000002994 raw material Substances 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims description 67
- 238000000605 extraction Methods 0.000 claims description 47
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 40
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 32
- 239000000843 powder Substances 0.000 claims description 32
- 239000011259 mixed solution Substances 0.000 claims description 30
- 239000003205 fragrance Substances 0.000 claims description 29
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- 239000008107 starch Substances 0.000 claims description 27
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- 240000001724 Piper sarmentosum Species 0.000 claims description 25
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 18
- 239000002002 slurry Substances 0.000 claims description 18
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- 238000002156 mixing Methods 0.000 claims description 17
- 239000011780 sodium chloride Substances 0.000 claims description 17
- 239000001569 carbon dioxide Substances 0.000 claims description 16
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- 239000000287 crude extract Substances 0.000 claims description 14
- 238000000265 homogenisation Methods 0.000 claims description 14
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- 102000004169 proteins and genes Human genes 0.000 claims description 11
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- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 10
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 10
- 235000021302 avocado oil Nutrition 0.000 claims description 10
- 239000008163 avocado oil Substances 0.000 claims description 10
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- 235000011090 malic acid Nutrition 0.000 claims description 10
- PLLBRTOLHQQAQQ-UHFFFAOYSA-N 8-methylnonan-1-ol Chemical compound CC(C)CCCCCCCO PLLBRTOLHQQAQQ-UHFFFAOYSA-N 0.000 claims description 9
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims description 9
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 9
- 239000000194 fatty acid Substances 0.000 claims description 9
- 229930195729 fatty acid Natural products 0.000 claims description 9
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims description 9
- 238000002791 soaking Methods 0.000 claims description 9
- 239000002904 solvent Substances 0.000 claims description 9
- 239000000811 xylitol Substances 0.000 claims description 9
- 235000010447 xylitol Nutrition 0.000 claims description 9
- 229960002675 xylitol Drugs 0.000 claims description 9
- -1 xylitol fatty acid ester Chemical class 0.000 claims description 9
- 238000001035 drying Methods 0.000 claims description 8
- 239000007791 liquid phase Substances 0.000 claims description 8
- 239000006228 supernatant Substances 0.000 claims description 8
- BNXOUFNLXOGIOT-UHFFFAOYSA-N Sarmentose Natural products CC1OC(O)CC(CO)C1O BNXOUFNLXOGIOT-UHFFFAOYSA-N 0.000 claims description 6
- GOYBREOSJSERKM-VQVTYTSYSA-N sarmentose Chemical compound O=CC[C@H](OC)[C@@H](O)[C@@H](C)O GOYBREOSJSERKM-VQVTYTSYSA-N 0.000 claims description 6
- 244000251953 Agaricus brunnescens Species 0.000 claims description 5
- 235000001674 Agaricus brunnescens Nutrition 0.000 claims description 5
- 239000004440 Isodecyl alcohol Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 239000012071 phase Substances 0.000 claims description 5
- 239000006002 Pepper Substances 0.000 claims description 4
- 241000722363 Piper Species 0.000 claims description 4
- 239000000796 flavoring agent Substances 0.000 claims description 4
- 235000013355 food flavoring agent Nutrition 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 235000008390 olive oil Nutrition 0.000 claims description 4
- 239000004006 olive oil Substances 0.000 claims description 4
- 235000002566 Capsicum Nutrition 0.000 claims description 3
- 235000016761 Piper aduncum Nutrition 0.000 claims description 3
- 235000017804 Piper guineense Nutrition 0.000 claims description 3
- 235000008184 Piper nigrum Nutrition 0.000 claims description 3
- 241000345998 Calamus manan Species 0.000 claims description 2
- 235000012950 rattan cane Nutrition 0.000 claims description 2
- 240000008154 Piper betle Species 0.000 claims 5
- 235000008180 Piper betle Nutrition 0.000 claims 5
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- 241000196324 Embryophyta Species 0.000 description 6
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- RKFAZBXYICVSKP-AATRIKPKSA-N alpha-asarone Chemical compound COC1=CC(OC)=C(\C=C\C)C=C1OC RKFAZBXYICVSKP-AATRIKPKSA-N 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
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- 229940116257 pepper extract Drugs 0.000 description 3
- NPNUFJAVOOONJE-ZIAGYGMSSA-N β-(E)-Caryophyllene Chemical compound C1CC(C)=CCCC(=C)[C@H]2CC(C)(C)[C@@H]21 NPNUFJAVOOONJE-ZIAGYGMSSA-N 0.000 description 3
- 206010011224 Cough Diseases 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- FAMPSKZZVDUYOS-UHFFFAOYSA-N alpha-Caryophyllene Natural products CC1=CCC(C)(C)C=CCC(C)=CCC1 FAMPSKZZVDUYOS-UHFFFAOYSA-N 0.000 description 2
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- NVEQFIOZRFFVFW-UHFFFAOYSA-N 9-epi-beta-caryophyllene oxide Natural products C=C1CCC2OC2(C)CCC2C(C)(C)CC21 NVEQFIOZRFFVFW-UHFFFAOYSA-N 0.000 description 1
- 206010010904 Convulsion Diseases 0.000 description 1
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- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
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- 235000019510 Long pepper Nutrition 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
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- 240000004274 Sarcandra glabra Species 0.000 description 1
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- 239000008280 blood Substances 0.000 description 1
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- 230000001914 calming effect Effects 0.000 description 1
- NPNUFJAVOOONJE-UONOGXRCSA-N caryophyllene Natural products C1CC(C)=CCCC(=C)[C@@H]2CC(C)(C)[C@@H]21 NPNUFJAVOOONJE-UONOGXRCSA-N 0.000 description 1
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- QBNFBHXQESNSNP-UHFFFAOYSA-N humulene Natural products CC1=CC=CC(C)(C)CC=C(/C)CCC1 QBNFBHXQESNSNP-UHFFFAOYSA-N 0.000 description 1
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- 235000019633 pungent taste Nutrition 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
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- 230000002195 synergetic effect Effects 0.000 description 1
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- 230000008736 traumatic injury Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2101/00—Chemical composition of materials used in disinfecting, sterilising or deodorising
- A61L2101/32—Organic compounds
- A61L2101/36—Carboxylic acids or derivatives thereof
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Veterinary Medicine (AREA)
- Engineering & Computer Science (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Zoology (AREA)
- Botany (AREA)
- Epidemiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Seasonings (AREA)
Abstract
The invention provides an aromatherapy essential oil containing sarmentosum bunge and a preparation method thereof, wherein the aromatherapy essential oil comprises the following raw materials in parts by weight: 40-60 parts of sarmentosum bungei extract, 10-30 parts of composite tartaric acid, 5-10 parts of mannitol, 2-8 parts of a fragrance-locking agent, 10-26 parts of an emulsifier, 0.1-0.5 part of a thickening agent and 3-10 parts of water.
Description
Technical Field
The invention relates to the technical field of aromatherapy, and in particular relates to an aromatherapy essential oil containing sarmentosum bunge and a preparation method thereof.
Background
The Piper sarmentosum Roxb is perennial herb of Piper of piperceae, also called Piper sarmentosum Roxb, piper sarmentosum Roxb and Piper longum, is widely distributed in Guangxi, guangdong, yunnan, hainan and other provinces in China, has very rich resources, can be harvested all the year round, has pungent taste and warm property, enters stomach and large intestine channels, has the effects of dispelling wind and cold, promoting qi circulation and relieving pain, activating collaterals, reducing swelling and the like, is commonly used for wind-cold cough, abdominal distention, diarrhea dysentery, postpartum foot swelling, traumatic injury and the like, has various pharmacological activities, and has the effects of relieving pain, resisting viruses, inhibiting fungi, resisting tumors, resisting oxidation, resisting inflammation and the like. The piper sarmentosum is rich in various active substances such as acids, ethers, alcohols, terpenes and the like.
The aromatherapy is an aromatherapy which transmits medicinal effects of essential oil and the like by a skin system and a respiratory system, and the aromatic essential oil is quickly blended into blood and lymph of a human body through massage, suction, hot compress, soaking and fumigation, so that the metabolism in the body can be accelerated, the regeneration of living cells can be promoted, the immunity of the body can be enhanced, and further the nervous system, the circulatory system, the endocrine system, muscle tissues, the digestive system, the excretory system and the like of the human body can be adjusted; the active retention components of the prior plant extract essential oil for aromatherapy are less, the fragrance retention time in the use process is short, and the fragrance volatilization is hindered due to the influence of a solid agent when the solid aromatherapy is prepared, so that the use effect of the aromatherapy is greatly influenced.
Disclosure of Invention
In view of the above, the present invention provides an essential oil containing sarmentosum bungei and a preparation method thereof, which solve the above problems.
The technical scheme of the invention is realized as follows: an essential oil containing sarmentosum bungei: the feed comprises the following raw materials in parts by weight: 40 to 60 parts of piper sarmentosum extract, 10 to 30 parts of composite tartaric acid, 5 to 10 parts of mannitol, 2 to 8 parts of a fragrance-locking agent, 10 to 26 parts of an emulsifier, 0.1 to 0.5 part of a thickener and 3 to 10 parts of water.
Further, an essential oil for aromatherapy containing sarmentosum bungei: the feed comprises the following raw materials in parts by weight: 50 parts of piper sarmentosum extract, 20 parts of composite tartaric acid, 8 parts of mannitol, 6 parts of a fragrance locking agent, 18 parts of an emulsifier, 0.3 part of a thickener and 8 parts of water.
Further, the composite fruit acid comprises citric acid, malic acid and citrus acid in a mass ratio of 1-5.
Further, the emulsifier is xylitol fatty acid ester.
Further, the flavor-locking agent is avocado oil or olive oil, and the avocado oil is selected from Ono brand.
Further, the thickening agent is soluble starch slurry and rice bran protein in a mass ratio of 2-6, and the soluble starch slurry is prepared by mixing soluble starch and water according to a mass volume g/mL of 1-5.
Further, the preparation method of the essential oil containing the sarmentosum bungei comprises the following steps:
s1, preparing a sarmentose pepper extract: picking fresh sarmentosum bungei plants, naturally drying in the shade, crushing the sarmentosum bungei plants by 40-80 meshes to obtain sarmentosum bungei powder, soaking the sarmentosum bungei powder in saline water with the volume percentage of 10-50%, wherein the mass volume ratio g/mL of the sarmentosum bungei powder to the saline water is 3-10, heating the sarmentosum bungei powder to 40-60 ℃, putting the sarmentosum bungei powder and the saline water into an extraction kettle, adding an extraction solvent to perform supercritical carbon dioxide low-temperature extraction, wherein the flow rate of the carbon dioxide is 40-60L/h to obtain a crude extraction solution, centrifuging the crude extraction solution, taking a liquid phase, adjusting the pH value to 4.5-4.8, performing secondary low-temperature extraction, and collecting supernatant, namely the sarmentosum bunge extract;
s2, preparing the aromatherapy essential oil: mixing and stirring the piper sarmentosum extract, the composite tartaric acid and the mannitol, controlling the stirring temperature to be 10-20 ℃, the stirring speed to be 200-400rpm, stirring for 20-40 min, and standing for 1-3 h after the stirring is finished to obtain a mixed solution I;
s3, stirring the mixed solution after standing again, adding the fragrance locking agent and water while stirring, raising the temperature to 40-60 ℃, stirring at the speed of 500-600 rpm for 20-30 min to obtain a mixed solution II;
s4, adding an emulsifier and a thickening agent into the obtained mixed liquid II for homogenization, wherein the homogenization conditions are as follows: the essential oil containing the sarmentosum bungei is prepared under the pressure of 16-22 MPa, the temperature of 40-80 ℃ and the time of 15-25 s.
Further, the S1 extraction solvent is a mixed phase of ethanol and isodecyl alcohol, and the volume ratio of the ethanol to the isodecyl alcohol is 5-10: 1 to 4.
Further, the low-temperature extraction temperature of the S1 is 50-55 ℃, the extraction time is 30-50 min, the secondary low-temperature extraction temperature is 40-49 ℃, the extraction time is 15-25 min, and the extraction pressure is 15-40 MPa.
Further, the aromatic essential oil containing the sarmentose pepper is applied to the preparation of aromatic tablets, aromatic candles and rattan aromatherapy.
Compared with the prior art, the invention has the beneficial effects that:
according to the invention, supercritical carbon dioxide extraction is adopted, a mixed phase of ethanol and isodecyl alcohol is prepared as an extraction solvent, extraction process parameters are controlled, the extracted extract liquid maximally preserves sarcandra glabra active ingredients, the contents of alpha-asarone and caryophyllene are high, the alpha-asarone can play roles in relieving cough, eliminating phlegm, relieving asthma, calming, relieving spasm and resisting convulsion, and the caryophyllene has antibacterial, anti-inflammatory, mosquito-repellent, anxiolytic and antidepressant activities; adding compound tartaric acid into the extractive solution to promote fragrance, adding fragrance-locking agent and thickening agent to make fragrance uniform, slowly releasing, and increasing fragrance diffusion time, wherein fragrance concentration reaches 10 μ g/L after 48 hr.
Detailed Description
In order to better understand the technical content of the invention, specific examples are provided below to further illustrate the invention.
The experimental methods used in the examples of the present invention are all conventional methods unless otherwise specified.
The materials, reagents and the like used in the examples of the present invention can be obtained commercially without specific description.
Example 1
The aromatic essential oil containing the sarmentosum bungei comprises the following raw materials in parts by weight: 40 parts of piper sarmentosum extract, 10 parts of composite tartaric acid, 5 parts of mannitol, 2 parts of a fragrance locking agent, 10 parts of an emulsifier, 0.1 part of a thickener and 3 parts of water; the composite fruit acid is citric acid, malic acid and citrus acid in a mass ratio of 1.
Example 2
An aromatherapy essential oil containing sarmentosum bungei comprises the following raw materials in parts by weight: 60 parts of sarmentosum bunge extract, 30 parts of composite tartaric acid, 10 parts of mannitol, 8 parts of a fragrance locking agent, 26 parts of an emulsifier, 0.5 part of a thickening agent and 10 parts of water; the composite fruit acid is citric acid, malic acid and citrus acid in a mass ratio of 1 to 5, the emulsifier is xylitol fatty acid ester, the aroma locking agent is olive oil, the thickener is soluble starch slurry and rice bran protein in a mass ratio of 6 to 1, and the soluble starch slurry is prepared by mixing soluble starch and water according to a mass volume g/mL of 5.
Example 3
An aromatherapy essential oil containing sarmentosum bungei comprises the following raw materials in parts by weight: 50 parts of sarmentosum bungei extract, 20 parts of composite tartaric acid, 8 parts of mannitol, 6 parts of a flavoring agent, 18 parts of an emulsifier, 0.3 part of a thickener and 8 parts of water; the compound fruit acid is citric acid, malic acid and citrus acid in a mass ratio of 1 to 4, the emulsifier is xylitol fatty acid ester, the aroma locking agent is avocado oil, the thickener is soluble starch slurry and rice bran protein in a mass ratio of 4 to 1, and the soluble starch slurry is prepared by mixing soluble starch and water according to a mass volume g/mL of 3;
the aromatherapy essential oil described in the above embodiments 1 to 3 is prepared by the following preparation method:
s1, preparing a sarmentosum bunge extract: picking fresh sarmentosum bungei plants, naturally drying in the shade, crushing the sarmentosum bungei plants through a 60-mesh sieve to obtain sarmentosum bungei powder, soaking the sarmentosum bungei powder in saline water with the volume percentage of 30%, wherein the mass-volume ratio g/mL of the sarmentosum bungei powder to the saline water is 6: 3, performing supercritical carbon dioxide low-temperature extraction at 52 ℃, 33MPa and 50L/h of carbon dioxide flow for 40min to obtain a crude extract, centrifuging the crude extract, taking a liquid phase, adjusting the pH to 4.7, performing secondary low-temperature extraction at 45 ℃, 30MPa and 20min of extraction pressure, and collecting supernatant, namely the piper sarmentosum extract;
s2, preparing the aromatherapy essential oil: mixing and stirring the piper sarmentosum extract, the composite tartaric acid and the mannitol, controlling the stirring temperature to be 15 ℃, the stirring speed to be 300rpm, stirring for 30min, and standing for 2h after stirring to obtain a mixed solution I;
s3, stirring the mixed solution after standing again, adding the fragrance locking agent and water while stirring, raising the temperature to 50 ℃, and stirring at the speed of 550rpm for 25min to obtain a mixed solution II;
s4, adding an emulsifier and a thickening agent into the obtained mixed liquid II for homogenization, wherein the homogenization conditions are as follows: the essential oil containing the sarmentosum is prepared under the pressure of 18MPa and at the temperature of 60 ℃ for 20 s.
Example 4
The aromatic essential oil containing the sarmentosum bungei comprises the following raw materials in parts by weight: 50 parts of piper sarmentosum extract, 20 parts of composite tartaric acid, 8 parts of mannitol, 6 parts of a fragrance locking agent, 18 parts of an emulsifier, 10 parts of a thickener and 8 parts of water; the compound fruit acid is citric acid, malic acid and citrus acid in a mass ratio of 1 to 4, the emulsifier is xylitol fatty acid ester, the aroma locking agent is avocado oil, the thickener is soluble starch slurry and rice bran protein in a mass ratio of 4 to 1, and the soluble starch slurry is prepared by mixing soluble starch and water according to a mass volume g/mL of 3;
the preparation method comprises the following steps:
s1, preparing a sarmentose pepper extract: picking fresh sarmentosum bunge plants, naturally drying in the shade, crushing the sarmentosum bunge plants through a 40-mesh sieve to obtain sarmentosum bunge powder, soaking the sarmentosum bunge powder in saline water with the volume percentage of 10%, wherein the mass-volume ratio g/mL of the sarmentosum bunge powder to the saline water is 3, heating the sarmentosum bunge powder to 40 ℃, filling the sarmentosum bunge powder into an extraction kettle, adding an extraction solvent, wherein the extraction solvent is a mixed phase of ethanol and isodecanol, and the volume ratio of the ethanol to the isodecanol is 5:1, performing supercritical carbon dioxide low-temperature extraction at 50 ℃, 15MPa and 40L/h of carbon dioxide flow for 30min to obtain a crude extract, centrifuging the crude extract, taking a liquid phase, adjusting the pH to 4.5, performing secondary low-temperature extraction at 40 ℃, 15MPa and 15min of extraction pressure, and collecting supernatant, namely the piper sarmentosum extract;
s2, preparing the aromatherapy essential oil: mixing and stirring the piper sarmentosum extractive solution, the composite tartaric acid and the mannitol, controlling the stirring temperature to be 10 ℃, the stirring speed to be 200rpm, stirring for 20min, and standing for 1h after the stirring is finished to obtain a mixed solution I;
s3, stirring the mixed solution after standing again, adding the fragrance locking agent and water while stirring, raising the temperature to 40 ℃, and stirring for 20min at the stirring speed of 500rpm to obtain a mixed solution II;
s4, adding an emulsifier and a thickening agent into the obtained mixed liquid II for homogenization, wherein the homogenization conditions are as follows: the pressure is 16MPa, the temperature is 40 ℃, and the time is 15s, so that the essential oil containing the sarmentosum bunge is prepared.
Example 5
The aromatic essential oil containing the sarmentosum bungei comprises the following raw materials in parts by weight: 50 parts of sarmentosum bungei extract, 20 parts of composite tartaric acid, 8 parts of mannitol, 6 parts of a flavoring agent, 18 parts of an emulsifier, 10 parts of a thickening agent and 8 parts of water; the composite fruit acid is citric acid, malic acid and citrus acid in a mass ratio of 1 to 4, the emulsifier is xylitol fatty acid ester, the aroma locking agent is avocado oil, the thickening agent is soluble starch slurry and rice bran protein in a mass ratio of 4 to 1, and the soluble starch slurry is prepared by mixing soluble starch and water according to a mass volume g/mL of 3;
the preparation method comprises the following steps:
s1, preparing a sarmentose pepper extract: picking fresh sarmentosum bunge plants, naturally drying in the shade, crushing the sarmentosum bunge plants through a 80-mesh sieve to obtain sarmentosum bunge powder, soaking the sarmentosum bunge powder in saline water with the volume percentage of 50%, wherein the mass-volume ratio g/mL of the sarmentosum bunge powder to the saline water is 10, heating the sarmentosum bunge powder to 60 ℃, filling the sarmentosum bunge powder into an extraction kettle, adding an extraction solvent, wherein the extraction solvent is a mixed phase of ethanol and isodecanol, and the volume ratio of the ethanol to the isodecanol is 10:4, performing supercritical carbon dioxide low-temperature extraction at 55 ℃, 40MPa and 60L/h of carbon dioxide flow for 50min to obtain a crude extract, centrifuging the crude extract, taking a liquid phase, adjusting the pH to 4.8, performing secondary low-temperature extraction at 49 ℃, 40MPa and 25min, and collecting supernatant, namely the piper sarmentosum extract;
s2, preparing the aromatherapy essential oil: mixing and stirring the piper sarmentosum extractive solution, the composite tartaric acid and the mannitol, controlling the stirring temperature to be 120 ℃, the stirring speed to be 400rpm, stirring for 40min, and standing for 3h after the stirring is finished to obtain a mixed solution I;
s3, stirring the mixed solution after standing again, adding the fragrance locking agent and water while stirring, raising the temperature to 60 ℃, and stirring for 30min at the stirring speed of 600rpm to obtain a mixed solution II;
at the temperature of 80 ℃ for 25s under 22MPa, the essential oil containing the sarmentosum is prepared.
The essential oils of the aromatherapy prepared in the above examples 1 to 5 are compared in performance, and the content of active ingredients in the piper sarmentosum extract is determined by GC-MS method, wherein the active ingredients account for the percentage of the extract, and the determination results are as follows:
the essential oil of the example 3 is prepared into an aromatherapy candle, the fragrance retaining effect is judged by detecting the fragrance release concentration for 1h, 4h, 8h, 10h, 24h and 48h by using a gas chromatography, and the test results are as follows:
according to the formula raw materials and the preparation method, the extraction content of the active ingredients in the prepared sarmentosum bungei extract is high, the fragrance locking and fixing time of the prepared aromatherapy essential oil is long, the aromatherapy fragrance is uniformly and slowly released, and the diffusion time of the aromatherapy is prolonged.
The following comparative tests were made on the performance and effects of the aromatherapy essential oil prepared in example 3 of the present invention, specifically as follows:
comparative example 1
The difference between the comparative example and the example 3 is that the raw materials are different in proportion, and specifically, the champignon essential oil containing the sarmentosum bunge comprises the following raw materials in parts by weight: 30 parts of sarmentosum bunge extract, 33 parts of composite tartaric acid, 12 parts of mannitol, 1 part of a flavoring agent, 28 parts of an emulsifier, 18 parts of a thickening agent and 12 parts of water; the compound fruit acid is citric acid, malic acid and citrus acid in a mass ratio of 1 to 4, the emulsifier is xylitol fatty acid ester, the aroma locking agent is avocado oil, the thickener is soluble starch slurry and rice bran protein in a mass ratio of 4 to 1, and the soluble starch slurry is prepared by mixing soluble starch and water according to a mass volume g/mL of 3;
the preparation method comprises the following steps:
s1, preparing a sarmentosum bunge extract: picking fresh sarmentosum bungei plants, naturally drying in the shade, crushing the sarmentosum bungei plants through a 60-mesh sieve to obtain sarmentosum bungei powder, soaking the sarmentosum bungei powder in saline water with the volume percentage of 30%, wherein the mass-volume ratio g/mL of the sarmentosum bungei powder to the saline water is 6: 3, performing supercritical carbon dioxide low-temperature extraction at 52 ℃, 33MPa and 50L/h of carbon dioxide flow for 40min to obtain a crude extract, centrifuging the crude extract, taking a liquid phase, adjusting the pH to 4.7, performing secondary low-temperature extraction at 45 ℃, 30MPa and 20min of extraction pressure, and collecting supernatant, namely the piper sarmentosum extract;
s2, preparing the aromatherapy essential oil: mixing and stirring the piper sarmentosum extract, the composite tartaric acid and the mannitol, controlling the stirring temperature to be 15 ℃, the stirring speed to be 300rpm, stirring for 30min, and standing for 2h after stirring to obtain a mixed solution I;
s3, stirring the mixed solution after standing again, adding the fragrance locking agent and water while stirring, raising the temperature to 50 ℃, and stirring at the speed of 550rpm for 25min to obtain a mixed solution II;
s4, adding an emulsifier and a thickening agent into the obtained mixed solution II for homogenization, wherein the homogenization conditions are as follows: the essential oil containing the sarmentosum is prepared under the pressure of 18MPa and at the temperature of 60 ℃ for 20 s.
Comparative example 2
The difference between the comparative example and the example 3 is that the thickening agent in the essential oil raw material is rice bran protein, in particular to champignon essential oil containing sarmentosum, which comprises the following raw materials in parts by weight: 50 parts of piper sarmentosum extract, 20 parts of composite tartaric acid, 8 parts of mannitol, 6 parts of a fragrance locking agent, 18 parts of an emulsifier, 0.3 part of a thickener and 8 parts of water; the composite fruit acid is citric acid, malic acid and citrus acid in a mass ratio of 1 to 4, the emulsifier is xylitol fatty acid ester, the aroma locking agent is avocado oil, the thickener is rice bran protein, and the soluble starch slurry is prepared by mixing soluble starch and water according to a mass volume g/mL of 3;
the preparation method comprises the following steps:
s1, preparing a sarmentosum bunge extract: picking fresh sarmentosum bunge plants, naturally drying in the shade, crushing the sarmentosum bunge plants through a 60-mesh sieve to obtain sarmentosum bunge powder, soaking the sarmentosum bunge powder in saline with the volume percentage of 30%, wherein the mass-volume ratio g/mL of the sarmentosum bunge powder to the saline is 6: 3, performing supercritical carbon dioxide low-temperature extraction at 52 ℃, 33MPa and 50L/h of carbon dioxide flow for 40min to obtain a crude extract, centrifuging the crude extract, taking a liquid phase, adjusting the pH to 4.7, performing secondary low-temperature extraction at 45 ℃, 30MPa and 20min of extraction pressure, and collecting supernatant, namely the piper sarmentosum extract;
s2, preparing the aromatherapy essential oil: mixing and stirring the piper sarmentosum extract, the composite tartaric acid and the mannitol, controlling the stirring temperature to be 15 ℃, the stirring speed to be 300rpm, stirring for 30min, and standing for 2h after stirring to obtain a mixed solution I;
s3, stirring the mixed solution after standing again, adding the fragrance locking agent and water while stirring, raising the temperature to 50 ℃, and stirring at the speed of 550rpm for 25min to obtain a mixed solution II;
s4, adding an emulsifier and a thickening agent into the obtained mixed solution II for homogenization, wherein the homogenization conditions are as follows: the essential oil containing the sarmentosum is prepared under the pressure of 18MPa and at the temperature of 60 ℃ for 20 s.
Comparative example 3
The difference between the comparative example and the example 3 is that no fragrance locking agent is added in the essential oil raw material, and specifically, the essential oil containing sarmentose pepper comprises the following raw materials in parts by weight: 50 parts of sarmentosum bungei extract, 20 parts of composite tartaric acid, 8 parts of mannitol, 18 parts of emulsifier, 0.3 part of thickener and 8 parts of water; the composite fruit acid is citric acid, malic acid and citrus acid in a mass ratio of 1 to 4, the emulsifier is xylitol fatty acid ester, the aroma locking agent is avocado oil, the thickening agent is soluble starch slurry and rice bran protein in a mass ratio of 4 to 1, and the soluble starch slurry is prepared by mixing soluble starch and water according to a mass volume g/mL of 3;
the preparation method comprises the following steps:
s1, preparing a sarmentosum bunge extract: picking fresh sarmentosum bunge plants, naturally drying in the shade, crushing the sarmentosum bunge plants through a 60-mesh sieve to obtain sarmentosum bunge powder, soaking the sarmentosum bunge powder in saline with the volume percentage of 30%, wherein the mass-volume ratio g/mL of the sarmentosum bunge powder to the saline is 6: 3, performing supercritical carbon dioxide low-temperature extraction at 52 ℃, 33MPa and 50L/h of carbon dioxide flow for 40min to obtain a crude extract, centrifuging the crude extract, taking a liquid phase, adjusting the pH to 4.7, performing secondary low-temperature extraction at 45 ℃, 30MPa and 20min, and collecting a supernatant, namely the piper sarmentosum extract;
s2, preparing the aromatherapy essential oil: mixing and stirring the piper sarmentosum extract, the composite tartaric acid and the mannitol, controlling the stirring temperature to be 15 ℃, the stirring speed to be 300rpm, stirring for 30min, and standing for 2h after stirring to obtain a mixed solution I;
s3, stirring the mixed solution after standing again, adding water while stirring, raising the temperature to 50 ℃, and stirring for 25min at the stirring speed of 550rpm to obtain a mixed solution II;
s4, adding an emulsifier and a thickening agent into the obtained mixed solution II for homogenization, wherein the homogenization conditions are as follows: the essential oil containing the sarmentosum is prepared under the pressure of 18MPa and at the temperature of 60 ℃ for 20 s.
The fragrance release concentrations of the fragrance essential oils of the comparative examples 1 to 3 are compared, and the comparison results are as follows:
from the results, the example 3 and the comparative example 1 show that the raw material proportion is in a specific range, the fragrance essential oil can be well released under the synergistic effect, the thickening agent disclosed by the invention is added in the example 3 and the comparative example 2, hydrophobic molecules in soluble starch slurry and rice bran protein interact with hydrophobic molecules in an extracting solution, and then the inclusion effect of essential oil molecules in a mixed solution II can be realized under the external force action of hydrophilic molecules and an aqueous solution in the extracting solution, so that the active ingredients in the fragrance essential oil can be slowly released, the release time of the fragrance essential oil is prolonged, and the fragrance concentration reaches 10 mu g/L after 48 hours; example 3 in comparison with comparative example 3, with the addition of the aroma-locking agent, the avocado oil or olive oil is used as the aroma-locking agent, and high-quality grease molecules can lock active molecules in the mixed solution I and prevent the aroma molecules from losing during release, so that the active substances are preserved.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (10)
1. An essential oil containing sarmentosum bungei, which is characterized in that: the feed comprises the following raw materials in parts by weight: 40 to 60 parts of piper sarmentosum extract, 10 to 30 parts of composite tartaric acid, 5 to 10 parts of mannitol, 2 to 8 parts of a fragrance-locking agent, 10 to 26 parts of an emulsifier, 0.1 to 0.5 part of a thickener and 3 to 10 parts of water.
2. The essential oil for aromatherapy containing sarmentia betel as claimed in claim 1, wherein: the feed comprises the following raw materials in parts by weight: 50 parts of sarmentosum bungei extract, 20 parts of composite tartaric acid, 8 parts of mannitol, 6 parts of a flavoring agent, 18 parts of an emulsifier, 0.3 part of a thickening agent and 8 parts of water.
3. The essential oil for aromatherapy containing sarmentia betel as claimed in claim 1 or 2, wherein: the composite tartaric acid comprises citric acid, malic acid and citrus acid in a mass ratio of 1-5.
4. The essential oil for aromatherapy containing sarmentia betel as claimed in claim 1, wherein: the emulsifier is xylitol fatty acid ester.
5. The essential oil for aromatherapy containing sarmentia betel as claimed in claim 1, wherein: the fragrance-locking agent is avocado oil or olive oil.
6. The essential oil for aromatherapy containing sarmentia betel as claimed in claim 1, wherein: the thickening agent is soluble starch slurry and rice bran protein in a mass ratio of 2-6, and the soluble starch slurry is prepared by mixing soluble starch and water according to a mass volume g/mL of 1-5.
7. The method for preparing laetispicum-containing aromatherapy essential oil according to any one of claims 1 to 6, wherein: the method comprises the following steps:
s1, preparing a sarmentosum bunge extract: picking fresh sarmentosum bunge plants, naturally drying in the shade, crushing the sarmentosum bunge plants by 40-80 meshes to obtain sarmentosum bunge powder, soaking the sarmentosum bunge powder in saline water with the volume percentage of 10-50%, wherein the mass-volume ratio g/mL of the sarmentosum bunge powder to the saline water is 3-10, heating the sarmentosum bunge powder to 40-60 ℃, putting the sarmentosum bunge powder to an extraction kettle, adding an extraction solvent, performing supercritical carbon dioxide low-temperature extraction, controlling the flow of the carbon dioxide to be 40-60L/h to obtain a crude extract, centrifuging the crude extract, taking a liquid phase, adjusting the pH to be 4.5-4.8, performing secondary low-temperature extraction, and collecting supernatant, namely sarmentosum bunge extract;
s2, preparing the aromatherapy essential oil: mixing and stirring the piper sarmentosum extract, the composite tartaric acid and the mannitol, controlling the stirring temperature to be 10-20 ℃, the stirring speed to be 200-400rpm, stirring for 20-40 min, and standing for 1-3 h after the stirring is finished to obtain a mixed solution I;
s3, stirring the mixed solution after standing again, adding the fragrance locking agent and water while stirring, raising the temperature to 40-60 ℃, stirring at the speed of 500-600 rpm for 20-30 min to obtain a mixed solution II;
s4, adding an emulsifier and a thickening agent into the obtained mixed solution II for homogenization, wherein the homogenization conditions are as follows: the essential oil containing the sarmentose pepper is prepared under the pressure of 16-22 MPa and the temperature of 40-80 ℃ for 15-25 s.
8. The preparation method of the laetispicum-containing aromatherapy essential oil according to claim 7, wherein the preparation method comprises the following steps: the S1 extraction solvent is a mixed phase of ethanol and isodecyl alcohol, and the volume ratio of the ethanol to the isodecyl alcohol is 5-10: 1 to 4.
9. The method for preparing essential oil of aromatherapy containing sarmentia pubescens as claimed in claim 7, wherein: the low-temperature extraction temperature of the S1 is 50-55 ℃, the extraction time is 30-50 min, the secondary low-temperature extraction temperature is 40-49 ℃, the extraction time is 15-25 min, and the extraction pressure is 15-40 MPa.
10. Use of the essential oil of champignon-pepper-containing as claimed in any one of claims 1 to 6 for the preparation of champignon tablets, champignon candles, rattan champignon.
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