CN101904480A - Method for preparing micro-emulsified essence - Google Patents
Method for preparing micro-emulsified essence Download PDFInfo
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- CN101904480A CN101904480A CN2009100400060A CN200910040006A CN101904480A CN 101904480 A CN101904480 A CN 101904480A CN 2009100400060 A CN2009100400060 A CN 2009100400060A CN 200910040006 A CN200910040006 A CN 200910040006A CN 101904480 A CN101904480 A CN 101904480A
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- Edible Oils And Fats (AREA)
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Abstract
The invention relates to technology in the field of food and beverage processing, in particular to an oil-in-water essence system, and the prepared micro-emulsified essence can be widely applied to the food industry. An oil-soluble essence base and a food-grade emulsifier are taken as raw materials, and the method comprises the following steps of: mixing glycerol, propylene glycol, Tween, glycerol diacetate, ethoxylated glyceride, polyglycerol and sucrose ester, stirring at the temperature of between 50 and 60 DEG C for 20 to 30 min, adding the oil-soluble essence base, stirring at the room temperature for 10 min, adding an SSL/CSL, adding alcohol serving as a cocatalyst, and simultaneously eliminating bubbles generated in the stirring process. The whole stirring process is mildly performed, and the finished product is the transparent micro-emulsified essence with certain viscosity and high concentration.
Description
Technical field
The present invention relates to the technology of bag and bottle manufacture field, specifically is a kind of oil-in-water essence systems of research and development, and prepared micro-emulsified essence can be widely used in each food service industry.
Background technology
Present preparation to emulsifying essence normally is distributed to by surfactant and emulsifying device water-fast oil soluble perfume with it makes emulsion in distilled water, this essence can make all kinds of oil-soluble spices use in water quality, and can delay the evaporation rate and the aroma-keeping time of essence, but this emulsifying essence is owing to oil, water two-phase are in the thermodynamic instability state, the essence system is damaged easily, produce lamination, cause product normally not use.And the perfume base concentration in this emulsifying essence can only be at 5%-10%, and excessive concentration also can cause water-oil separating, so its use is subjected to significant limitation.
Micro-emulsified essence is to adopt emulsifying agent and assistant for emulsifying agent to prepare a kind of oil-in-water transparent microemulsified system, overcomes the deficiency of emulsifying essence in the past, has both had temperature tolerance, has cold resistance again.When being used for replacing existing milkiness shape emulsifying essence, have higher anti-stability and good opacity, can be at-20 ℃, also can be 50 ℃ of uses, it can be for a long time under adverse circumstances normal use the and can not produce and decompose precipitation.And the maximum concentration of the perfume base of this emulsifying essence can reach about 40%, is 4-8 times of the emulsifying essence concentration of use at present.Save spendings such as transportation, packing and warehousing costs in a large number, thereby saved production cost.Micro-emulsified essence has been broken the idea that emulsifying essence production must be passed through high pressure, high speed homogenization especially, thereby the same with present water quality, oily essence, becomes simple blending and mixes the infiltrate journey.
The object of the present invention is to provide a kind of micro-emulsion technology of essence, it is characterized in that it possesses high emulsifying capacity, perfume base concentration can reach about 40% in the emulsifying essence, can be used as that water/oily both sexes are widely used in ice cream, bake, in the industry such as beverage and roasted seeds and nuts.
Summary of the invention
Problem to be solved by this invention is that a kind of stability of preparation is high, and performance is good, the micro-emulsified essence product that concentration is high, and the manufacture craft of this product is provided.
This method prepares micro-emulsified essence by the following technical solutions:
The present invention's prescription is: glycerine, 20-25%; Propane diols, 7-10%; Polysorbas20,10-15%; SSL/CSL, 0.2-1%; Diacetine, 3-5%; Ethyoxyl glyceride, 1-3%; Polyglycerol ester, 2-4%; Sucrose ester, 10-15%; The oil-soluble perfume base, 35-42%; Ethanol, 1-3%.
The preparation method is as follows: with oil-soluble perfume base, food grade emulsifier is raw material, earlier with glycerine, and 20-25kg; Propane diols, 7-10kg; Polysorbas20,10-15kg; Diacetine, 2-3kg; Ethyoxyl glyceride, 3-5kg; Polyglycerol ester, 2-4kg and sucrose ester, 10-15kg mixes, 60 ℃ are stirred 30min, add oil-soluble perfume base 35-42kg again, stirring at room 10min, add SSL/CSL 0.2-1kg then, add ethanol 1-3kg at last, eliminate the bubble that produces in the whipping process simultaneously as co-catalyst.Whole whipping process keeps leniently carrying out, and final products present certain viscosity, high concentration and transparent micro-emulsified essence.
The prepared microemulsified perfume (or spice) of the present invention has following characteristics:
1. the product design height, has been saved costs such as packing, stores keeping and transportation by the high 4-8 of perfume base concentration of uncommon emulsifying essence product times.
2. have good emulsion stability and thickening property, and high temperature resistant (100 ℃) and low temperature (20 ℃).High-speed separation is difficult for situations such as water-oil separating, layering or oil spill.
3. solubility property is better, stirs at normal temperatures and just can dissolve immediately.
The specific embodiment
Provide specific embodiment further to set forth technical scheme of the present invention below, but technology of the present invention application is not limited only to embodiment.
Embodiment 1: the fresh milk micro-emulsified essence
Prescription:
Cream hydrolysate 40kg
Glycerine: 21kg
Propane diols: 9kg
Polysorbas20: 10kg
SSL/CSL：0.2kg
Diacetine: 3kg
Ethyoxyl glyceride: 2kg
Polyglycerol ester: 3kg
Sucrose ester: 10.8kg
Ethanol: 2kg
The preparation method: with oil-soluble perfume base, food grade emulsifier is raw material, earlier glycerine, propane diols, polysorbas20, diacetine, ethyoxyl glyceride, polyglycerol ester and sucrose ester are mixed, 50-60 ℃ is stirred 30min, add the cream hydrolysate again, stirring at room 10min, add SSL/CSL then, add ethanol at last, eliminate the bubble that produces in the whipping process simultaneously as co-catalyst.Whole whipping process keeps leniently carrying out, and final products present certain viscosity, high concentration and transparent micro-emulsified essence.
Embodiment 2: the butter micro-emulsified essence
Prescription:
Cream alcoholysate 38kg
Glycerine: 20kg
Propane diols: 10kg
Polysorbas20: 9kg
SSL/CSL：0.2kg
Diacetine: 3kg
Ethyoxyl glyceride: 2kg
Polyglycerol ester: 3kg
Sucrose ester: 12.8kg
Ethanol: 2kg
The preparation method: with oil-soluble perfume base, food grade emulsifier is raw material, earlier glycerine, propane diols, polysorbas20, diacetine, ethyoxyl glyceride, polyglycerol ester and sucrose ester are mixed, 50-60 ℃ is stirred 30min, add the cream alcoholysate again, stirring at room 10min, add SSL/CSL then, add ethanol at last, eliminate the bubble that produces in the whipping process simultaneously as co-catalyst.Whole whipping process keeps leniently carrying out, and final products present certain viscosity, high concentration and transparent micro-emulsified essence.
Claims (3)
1. the present invention relates to the technology of bag and bottle manufacture field, specifically be a kind of oil-in-water essence systems of research and development, its raw material is made up of glycerine, propane diols, polysorbas20, SSL/CSL, diacetine, ethyoxyl glyceride, polyglycerol ester, sucrose ester and oil-soluble perfume base.
2. according to claim 1, optimum formula of the present invention is: glycerine, 20-25%; Propane diols, 7-10%; Polysorbas20,10-15%; SSL/CSL, 0.2-1%; Diacetine, 3-5%; Ethyoxyl glyceride, 1-3%; Polyglycerol ester, 2-4%; Sucrose ester, 10-15%; The oil-soluble perfume base, 35-42%; Ethanol, 1-3%.
3. adopt prescription as claimed in claim 2, preparation method of the present invention is: with oil-soluble perfume base, food grade emulsifier is raw material, earlier glycerine, propane diols, polysorbas20, diacetine, ethyoxyl glyceride, polyglycereol and sucrose ester are mixed, 50-60 ℃ is stirred 30min, add the oil-soluble perfume base again, stirring at room 10min adds SSL/CSL then, add ethanol at last as co-catalyst, eliminate the bubble that produces in the whipping process simultaneously.Whole process keeps gentle agitation, and final products present certain viscosity, high concentration and transparent micro-emulsified essence.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100400060A CN101904480B (en) | 2009-06-05 | 2009-06-05 | Method for preparing micro-emulsified essence |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100400060A CN101904480B (en) | 2009-06-05 | 2009-06-05 | Method for preparing micro-emulsified essence |
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| Publication Number | Publication Date |
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| CN101904480A true CN101904480A (en) | 2010-12-08 |
| CN101904480B CN101904480B (en) | 2013-11-06 |
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| CN2009100400060A Active CN101904480B (en) | 2009-06-05 | 2009-06-05 | Method for preparing micro-emulsified essence |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102140388A (en) * | 2011-01-20 | 2011-08-03 | 深圳市如烟生物科技有限公司 | Preparation method for solid essence for tobaccos |
| CN103320226A (en) * | 2013-06-03 | 2013-09-25 | 吴江市利达上光制品有限公司 | Essence compound emulsifier and preparation method |
| CN104305119A (en) * | 2014-09-26 | 2015-01-28 | 杭州杭曼香精有限公司 | Microemulsified essence and preparing method thereof |
| CN104381953A (en) * | 2014-11-24 | 2015-03-04 | 青岛大学 | Preparation method of water-soluble zanthoxylum bungeanum oleoresin |
| CN106962879A (en) * | 2017-05-27 | 2017-07-21 | 徐学 | A kind of emulsified transparent essence and preparation method |
| CN109957449A (en) * | 2017-12-25 | 2019-07-02 | 广州华芳烟用香精有限公司 | A kind of soluble perfume and preparation method thereof |
| CN117143668A (en) * | 2023-11-01 | 2023-12-01 | 山东九一生物科技股份有限公司 | Preparation method and application of jasmine essence for biological deodorization |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104082703A (en) * | 2014-07-17 | 2014-10-08 | 天宁香料（江苏）有限公司 | Preparation method of micro-emulsified citrus shatangju essence and application of essence to beverages |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1395858A (en) * | 2002-09-03 | 2003-02-12 | 韦大文 | Pure gum for emulsifying essence and its preparing process |
| CN101283774A (en) * | 2008-04-28 | 2008-10-15 | 广东富味制果厂有限公司 | Microcapsule essence and its preparation method |
| CN101411459A (en) * | 2008-11-17 | 2009-04-22 | 广州市名花香料有限公司 | Milk fat element |
| CN101411457A (en) * | 2008-11-17 | 2009-04-22 | 广州市名花香料有限公司 | Cream essence |
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2009
- 2009-06-05 CN CN2009100400060A patent/CN101904480B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1395858A (en) * | 2002-09-03 | 2003-02-12 | 韦大文 | Pure gum for emulsifying essence and its preparing process |
| CN101283774A (en) * | 2008-04-28 | 2008-10-15 | 广东富味制果厂有限公司 | Microcapsule essence and its preparation method |
| CN101411459A (en) * | 2008-11-17 | 2009-04-22 | 广州市名花香料有限公司 | Milk fat element |
| CN101411457A (en) * | 2008-11-17 | 2009-04-22 | 广州市名花香料有限公司 | Cream essence |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102140388A (en) * | 2011-01-20 | 2011-08-03 | 深圳市如烟生物科技有限公司 | Preparation method for solid essence for tobaccos |
| CN103320226A (en) * | 2013-06-03 | 2013-09-25 | 吴江市利达上光制品有限公司 | Essence compound emulsifier and preparation method |
| CN104305119A (en) * | 2014-09-26 | 2015-01-28 | 杭州杭曼香精有限公司 | Microemulsified essence and preparing method thereof |
| CN104381953A (en) * | 2014-11-24 | 2015-03-04 | 青岛大学 | Preparation method of water-soluble zanthoxylum bungeanum oleoresin |
| CN104381953B (en) * | 2014-11-24 | 2016-02-24 | 青岛大学 | A kind of preparation method of water-soluble xanthoxylum oleoresin |
| CN106962879A (en) * | 2017-05-27 | 2017-07-21 | 徐学 | A kind of emulsified transparent essence and preparation method |
| CN109957449A (en) * | 2017-12-25 | 2019-07-02 | 广州华芳烟用香精有限公司 | A kind of soluble perfume and preparation method thereof |
| CN117143668A (en) * | 2023-11-01 | 2023-12-01 | 山东九一生物科技股份有限公司 | Preparation method and application of jasmine essence for biological deodorization |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101904480B (en) | 2013-11-06 |
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Address after: 510440 Guangdong Province, Guangzhou Baiyun Avenue North Street No. 1 Dongfeng Road East Applicant after: Guangzhou Minghua Perfume Co., Ltd. Address before: 510440 Guangdong Province, Guangzhou Baiyun Avenue North Street No. 1 Dongfeng Road East Applicant before: Guangzhou Flower Flavours & Fragrances Co., Ltd. |
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Free format text: CORRECT: APPLICANT; FROM: GUANGZHOU FLOWER FLAVOUR + FRAGRANCES CO., LTD. TO: GUANGZHOU FLOWER FLAVOURS AND FRAGRANCES CO., LTD. |
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