CN104381953A - Preparation method of water-soluble zanthoxylum bungeanum oleoresin - Google Patents
Preparation method of water-soluble zanthoxylum bungeanum oleoresin Download PDFInfo
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- CN104381953A CN104381953A CN201410680940.XA CN201410680940A CN104381953A CN 104381953 A CN104381953 A CN 104381953A CN 201410680940 A CN201410680940 A CN 201410680940A CN 104381953 A CN104381953 A CN 104381953A
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- xanthoxylum oleoresin
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Abstract
The invention belongs to the technical field of food additive processing, relates to a new technology for processing and producing water-soluble zanthoxylum bungeanum oleoresin on a large scale, and in particular relates to a preparation method of the water-soluble zanthoxylum bungeanum oleoresin. The method comprises the steps of firstly, selecting oil-soluble zanthoxylum bungeanum oleoresin as a raw material for later use according to the weight and spicy degree of the water-soluble zanthoxylum bungeanum oleoresin to be prepared, selecting Tween 20, propylene glycol and purified water as ingredients for later use, respectively preheating all the ingredients, then sequentially feeding the ingredients into an emulsification kettle filled with the oil-soluble zanthoxylum bungeanum oleoresin, carrying out heat preservation, and stirring for emulsifying; then, continuously homogenizing the emulsified product by a high-pressure homogenizer, then putting the product into a vacuum tank, and vacuumizing to obtain a coarse product; finally, packaging to obtain the product water-soluble zanthoxylum bungeanum oleoresin. The technology is simple in steps, reliable in design principle, good in preparation safety, good in product quality, wide in application scope, long in shelf life and environment-friendly in eating.
Description
Technical field:
The invention belongs to food additives processing technique field, relate to the new technology that a kind of batch machining produces water-soluble xanthoxylum oleoresin, particularly a kind of preparation method of water-soluble xanthoxylum oleoresin.
Background technology:
Chinese prickly ash (Zanthoxylum bungeanum) belongs to Rutaceae (Zanthoxylum L.) Zanthoxylum (Rrutaceae) plant, is distributed in Asia, America, Africa and Oceanian subtropical zone and torrid areas widely; In China, Chinese prickly ash is extensively planted as being a kind of important industrial crops, and xanthoxylum oleoresin adopts organic solvent extractionprocess or supercritical CO
2the oily product of what extraction extracted from Pericarpium Zanthoxyli fruit shell have peculiar flavour, the aroma constituent wherein containing Chinese prickly ash feature and numb taste component, be a kind of edible natural spices, be widely used in the food such as chafing dish, flavouring, instant noodles; Because this product not only has the distinctive fragrance of Chinese prickly ash, mouthfeel, but also have that security is high, stay in grade, can standardize and standardization, the advantages such as addition is few, alternative materials Chinese prickly ash just gradually in the application, accept by increasing consumer, market prospects are very wide.But xanthoxylum oleoresin is oil-soluble product, immiscible with water, only be suitable for oily molten food product environment, be unsuitable for water-soluble food system, and need in food processing link to make the active ingredient in xanthoxylum oleoresin dissolve in water more, therefore, oil-soluble xanthoxylum oleoresin can not use in numerous food product, limits the further expansion of its range of application.So, seek a kind of process preparing water-soluble xanthoxylum oleoresin with the molten xanthoxylum oleoresin of commercially available oil (product specification: numb degree 120 ~ 150), overcome the shortcoming of oily molten xanthoxylum oleoresin, it is made to be suitable for water-soluble food environment, expand its range of application, there are wide market prospects.
Summary of the invention:
The object of the invention is to the defect overcoming prior art existence, seek the preparation technology designing a kind of water-soluble xanthoxylum oleoresin batch production, make xanthoxylum oleoresin be applicable to water-soluble food system, expand the range of application of xanthoxylum oleoresin.
To achieve these goals, main process of the present invention comprise get the raw materials ready, preheating, emulsification, homogeneous, degasification five steps:
(1) get the raw materials ready: according to weight and the numb degree of the water-soluble xanthoxylum oleoresin that will prepare, choose oily molten xanthoxylum oleoresin as raw material for standby, choose polysorbas20, propane diols and pure water for subsequent use as the batching of the water-soluble xanthoxylum oleoresin of preparation, its weight ratio of respectively preparing burden is oily molten xanthoxylum oleoresin: polysorbas20: propane diols: pure water=1:0.8:1:1 ~ 5 simultaneously;
(2) preheating: respectively polysorbas20, propane diols, pure water are heated to 30 DEG C ~ 40 DEG C for subsequent use;
(3) emulsification: molten for oil xanthoxylum oleoresin is inserted in emulsifying kettle, add the above-mentioned polysorbas20 being preheating to 30 ~ 40 DEG C, stir 10 minutes, and then add propane diols and the pure water of preheating successively, stir again at being incubated 30 DEG C ~ 40 DEG C after 20 minutes and stop stirring, mixing speed is 200 ~ 300 revs/min, obtains emulsifying material;
(4) homogeneous: by emulsifying material by high pressure homogenizer continuous homogenizing 2 times under 7500psi-8000psi pressure, obtain homogenous mass;
(5) degasification: again homogenous mass is put into vacuum tank, vacuum condition is bled 10 ~ 20 minutes, after being-0.05Mpa ~-0.07Mpa, then recovering normal pressure and carries out except being so incensed that thick product to vacuum; Then thick product is packed by commercially available needs, obtain the water-soluble xanthoxylum oleoresin of product.
Compared with prior art, its processing step is simple for the inventive method, and design principle is reliable, and manufacture security is good, good product quality, applied range, long shelf-life, edible environmental friendliness.
Detailed description of the invention:
Below by specific embodiment, the present invention is further elaborated.
Embodiment 1:95Kg fiber crops degree is the preparation of the water-soluble xanthoxylum oleoresin of 30, its main process comprise get the raw materials ready, preheating, emulsification, homogeneous, degasification five processing steps:
(1) get the raw materials ready: with commercially available numb degree be 120 the molten xanthoxylum oleoresin of oil prepare the water-soluble xanthoxylum oleoresin that 100Kg fiber crops degree is 20 for raw material, the weight (Kg) of required oily molten xanthoxylum oleoresin is 25Kg, and the weight of polysorbas20 is 20Kg, the weight of propane diols is the weight 25kg of 25Kg, pure water;
(2) preheating: the propane diols of the polysorbas20 of 20Kg, 25Kg, 25kg pure water are inserted three interlayer heating kettles respectively and be heated to 30 DEG C ~ 40 DEG C;
(3) emulsification: molten for the oil of 25Kg xanthoxylum oleoresin (numb degree is 120) is added in emulsifying kettle, add the 20Kg polysorbas20 of preheating, stir 10 minutes, then 25Kg propane diols and the 25kg pure water of preheating is added successively, add Keep agitation in blending process, stir 20 minutes again at remaining on 30 DEG C ~ 40 DEG C, mixing speed is 200 ~ 300 revs/min, and rear stopping is stirred;
(4) homogeneous: by product good for emulsification by high pressure homogenizer, continuous homogenizing 2 times under 7500psi-8000psi pressure;
(5) degasification: by the transferred product after homogeneous in vacuum tank, vacuum condition is bled after 10 ~ 20 minutes (vacuum is-0.05Mpa ~-0.07Mpa), recovers normal pressure, obtains thick product; Then the thick product of degasification is packed by commercially available needs, obtain the water-soluble xanthoxylum oleoresin that 95Kg fiber crops degree is 30.
Embodiment 2:312Kg fiber crops degree be the preparation technology of the water-soluble xanthoxylum oleoresin of 20 comprise get the raw materials ready, preheating, emulsification, homogeneous, degasification five processing steps:
(1) get the raw materials ready: with commercially available numb degree be 150 the molten xanthoxylum oleoresin of oil prepare the water-soluble xanthoxylum oleoresin that 300Kg fiber crops degree is 20 for raw material, the weight (Kg) of required oily molten xanthoxylum oleoresin is 40Kg, and the weight of polysorbas20 is 32Kg, the weight of propane diols is 40Kg, the weight of pure water is 200kg;
(2) preheating: the pure water of the polysorbas20 of 32Kg, the propane diols of 40Kg and 200kg is inserted respectively preheating in three interlayer heating kettles and be heated to 30 DEG C ~ 40 DEG C;
(3) emulsification: the 40Kg molten xanthoxylum oleoresin of oil (numb degree is 150) is added in emulsifying kettle, then the 40Kg polysorbas20 of preheating is added, stir 10 minutes, then 40Kg propane diols and the 200kg pure water of above-mentioned preheating is added successively, Keep agitation is wanted in batching adition process, stir 20 minutes again at remaining on 30 DEG C ~ 40 DEG C, mixing speed is 200 ~ 300 revs/min, and rear stopping is stirred;
(4) homogeneous: by product good for above-mentioned emulsification by high pressure homogenizer, continuous homogenizing 2 times under 8500psi ~ 9000psi pressure;
(5) degasification: the product after homogeneous is put into vacuum tank, vacuum condition is bled after 10 ~ 20 minutes (vacuum is-0.05Mpa ~-0.07Mpa), recovers normal pressure and obtains thick product; Then the water-soluble xanthoxylum oleoresin of degasification is packed by commercially available needs, obtain the water-soluble xanthoxylum oleoresin that product 300Kg fiber crops degree is 20.
Embodiment 3: the technical process of the present embodiment is with embodiment 1 or 2, the weight proportion of its each raw material is: numb degree be 150 the molten xanthoxylum oleoresin of oil be 60Kg, polysorbas20 is 50Kg, and propane diols is 50Kg, pure water is 150Kg, is prepared into water-soluble xanthoxylum oleoresin 310Kg; Obtain product in actual production and be only 306.5Kg, pure water water-holding quantity volatilizees, and does not affect product quality; The application of water-soluble xanthoxylum oleoresin in spicy peanut and shank preparation are produced prepared by the present embodiment has good use mouthfeel and taste.
Claims (1)
1. a preparation method for water-soluble xanthoxylum oleoresin, it is characterized in that main process comprise get the raw materials ready, preheating, emulsification, homogeneous, degasification five steps:
(1) get the raw materials ready: according to weight and the numb degree of the water-soluble xanthoxylum oleoresin that will prepare, choose oily molten xanthoxylum oleoresin as raw material for standby, choose polysorbas20, propane diols and pure water for subsequent use as the batching of the water-soluble xanthoxylum oleoresin of preparation, its weight ratio of respectively preparing burden is oily molten xanthoxylum oleoresin: polysorbas20: propane diols: pure water=1:0.8:1:1 ~ 5 simultaneously;
(2) preheating: respectively polysorbas20, propane diols, pure water are heated to 30 DEG C ~ 40 DEG C for subsequent use;
(3) emulsification: molten for oil xanthoxylum oleoresin is inserted in emulsifying kettle, add the above-mentioned polysorbas20 being preheating to 30 ~ 40 DEG C, stir 10 minutes, and then add propane diols and the pure water of preheating successively, stir again at being incubated 30 DEG C ~ 40 DEG C after 20 minutes and stop stirring, mixing speed is 200 ~ 300 revs/min, obtains emulsifying material;
(4) homogeneous: by emulsifying material by high pressure homogenizer continuous homogenizing 2 times under 7500psi-8000psi pressure, obtain homogenous mass;
(5) degasification: again homogenous mass is put into vacuum tank, vacuum condition is bled 10 ~ 20 minutes, after being-0.05Mpa ~-0.07Mpa, then recovering normal pressure and carries out except being so incensed that thick product to vacuum; Then thick product is packed by commercially available needs, obtain the water-soluble xanthoxylum oleoresin of product.
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| CN201410680940.XA CN104381953B (en) | 2014-11-24 | 2014-11-24 | A kind of preparation method of water-soluble xanthoxylum oleoresin |
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| CN104381953A true CN104381953A (en) | 2015-03-04 |
| CN104381953B CN104381953B (en) | 2016-02-24 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106376905A (en) * | 2016-08-26 | 2017-02-08 | 西南大学 | Preparation method of instant solid pricklyash peel oleoresin |
| CN107048324A (en) * | 2017-05-10 | 2017-08-18 | 上海应用技术大学 | A kind of Chinese prickly ash essence and preparation method thereof |
| CN113142314A (en) * | 2021-03-05 | 2021-07-23 | 四川五丰黎红食品有限公司 | Zanthoxylum oil cake meal resin microcapsule and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101112359A (en) * | 2007-07-31 | 2008-01-30 | 中国农业大学 | Method for preparing transparent water-dispersible concentrated liquor of beta-carotin |
| CN101692890A (en) * | 2009-09-26 | 2010-04-14 | 美科尔(河北)生物科技有限公司 | Method for improving water-soluble chilli extract from oil-soluble chilli extract |
| CN101904480A (en) * | 2009-06-05 | 2010-12-08 | 广州市名花香精香料有限公司 | Method for preparing micro-emulsified essence |
-
2014
- 2014-11-24 CN CN201410680940.XA patent/CN104381953B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101112359A (en) * | 2007-07-31 | 2008-01-30 | 中国农业大学 | Method for preparing transparent water-dispersible concentrated liquor of beta-carotin |
| CN101904480A (en) * | 2009-06-05 | 2010-12-08 | 广州市名花香精香料有限公司 | Method for preparing micro-emulsified essence |
| CN101692890A (en) * | 2009-09-26 | 2010-04-14 | 美科尔(河北)生物科技有限公司 | Method for improving water-soluble chilli extract from oil-soluble chilli extract |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106376905A (en) * | 2016-08-26 | 2017-02-08 | 西南大学 | Preparation method of instant solid pricklyash peel oleoresin |
| CN107048324A (en) * | 2017-05-10 | 2017-08-18 | 上海应用技术大学 | A kind of Chinese prickly ash essence and preparation method thereof |
| CN113142314A (en) * | 2021-03-05 | 2021-07-23 | 四川五丰黎红食品有限公司 | Zanthoxylum oil cake meal resin microcapsule and preparation method thereof |
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| CN104381953B (en) | 2016-02-24 |
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