CN104388192B - For the Rose type essence of Ms's cigarette and its application - Google Patents
For the Rose type essence of Ms's cigarette and its application Download PDFInfo
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- CN104388192B CN104388192B CN201410729584.6A CN201410729584A CN104388192B CN 104388192 B CN104388192 B CN 104388192B CN 201410729584 A CN201410729584 A CN 201410729584A CN 104388192 B CN104388192 B CN 104388192B
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- 241000220317 Rosa Species 0.000 title claims abstract description 66
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 60
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 55
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 37
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 claims abstract description 22
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 claims abstract description 22
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims abstract description 22
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 22
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 22
- 235000004936 Bromus mango Nutrition 0.000 claims abstract description 14
- 244000119298 Emblica officinalis Species 0.000 claims abstract description 14
- 235000015489 Emblica officinalis Nutrition 0.000 claims abstract description 14
- 235000008100 Ginkgo biloba Nutrition 0.000 claims abstract description 14
- 244000194101 Ginkgo biloba Species 0.000 claims abstract description 14
- 235000014826 Mangifera indica Nutrition 0.000 claims abstract description 14
- 235000009184 Spondias indica Nutrition 0.000 claims abstract description 14
- 239000000341 volatile oil Substances 0.000 claims abstract description 14
- 235000013599 spices Nutrition 0.000 claims abstract description 13
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 11
- 239000001605 (5-methyl-2-propan-2-ylcyclohexyl) acetate Substances 0.000 claims abstract description 11
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 11
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000005711 Benzoic acid Substances 0.000 claims abstract description 11
- XHXUANMFYXWVNG-UHFFFAOYSA-N D-menthyl acetate Natural products CC(C)C1CCC(C)CC1OC(C)=O XHXUANMFYXWVNG-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000005792 Geraniol Substances 0.000 claims abstract description 11
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 claims abstract description 11
- ZOZIRNMDEZKZHM-UHFFFAOYSA-N Phenethyl phenylacetate Chemical compound C=1C=CC=CC=1CCOC(=O)CC1=CC=CC=C1 ZOZIRNMDEZKZHM-UHFFFAOYSA-N 0.000 claims abstract description 11
- 240000004760 Pimpinella anisum Species 0.000 claims abstract description 11
- 235000012550 Pimpinella anisum Nutrition 0.000 claims abstract description 11
- 244000250129 Trigonella foenum graecum Species 0.000 claims abstract description 11
- 235000001484 Trigonella foenum graecum Nutrition 0.000 claims abstract description 11
- 235000010233 benzoic acid Nutrition 0.000 claims abstract description 11
- 239000001902 eugenia caryophyllata l. bud oil Substances 0.000 claims abstract description 11
- 229940113087 geraniol Drugs 0.000 claims abstract description 11
- 235000012907 honey Nutrition 0.000 claims abstract description 11
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 11
- 239000004310 lactic acid Substances 0.000 claims abstract description 11
- 229930007744 linalool Natural products 0.000 claims abstract description 11
- 239000003921 oil Substances 0.000 claims abstract description 11
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims abstract description 11
- 235000001019 trigonella foenum-graecum Nutrition 0.000 claims abstract description 11
- YKVWPZJHENXDAJ-VOTSOKGWSA-N Megastigmatrienone Chemical compound CC1=CC(=O)CC(C)(C)C1\C=C\C=C YKVWPZJHENXDAJ-VOTSOKGWSA-N 0.000 claims abstract description 10
- 240000007228 Mangifera indica Species 0.000 claims abstract description 4
- 244000126002 Ziziphus vulgaris Species 0.000 claims abstract description 4
- 244000061176 Nicotiana tabacum Species 0.000 claims abstract 5
- -1 isobutyl Acetoacetic ester Chemical compound 0.000 claims description 3
- 235000011201 Ginkgo Nutrition 0.000 claims description 2
- 150000002576 ketones Chemical class 0.000 claims description 2
- 240000004784 Cymbopogon citratus Species 0.000 claims 1
- 235000017897 Cymbopogon citratus Nutrition 0.000 claims 1
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 abstract description 20
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 18
- 239000003546 flue gas Substances 0.000 abstract description 18
- 239000002304 perfume Substances 0.000 abstract description 15
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 abstract description 10
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 abstract description 10
- 235000000484 citronellol Nutrition 0.000 abstract description 10
- 235000019640 taste Nutrition 0.000 abstract description 10
- AYJXHIDNNLJQDT-UHFFFAOYSA-N 2,6,6-Trimethyl-2-cyclohexene-1,4-dione Chemical compound CC1=CC(=O)CC(C)(C)C1=O AYJXHIDNNLJQDT-UHFFFAOYSA-N 0.000 abstract description 7
- WDAXFOBOLVPGLV-UHFFFAOYSA-N ethyl isobutyrate Chemical compound CCOC(=O)C(C)C WDAXFOBOLVPGLV-UHFFFAOYSA-N 0.000 abstract description 6
- 241000208125 Nicotiana Species 0.000 description 32
- 239000000243 solution Substances 0.000 description 21
- 239000002994 raw material Substances 0.000 description 16
- 241001247821 Ziziphus Species 0.000 description 12
- 239000003205 fragrance Substances 0.000 description 12
- 241001093152 Mangifera Species 0.000 description 10
- KQNPFQTWMSNSAP-UHFFFAOYSA-N isobutyric acid Chemical compound CC(C)C(O)=O KQNPFQTWMSNSAP-UHFFFAOYSA-N 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 238000000605 extraction Methods 0.000 description 5
- 238000001914 filtration Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
- 230000000391 smoking effect Effects 0.000 description 4
- HNAGHMKIPMKKBB-UHFFFAOYSA-N 1-benzylpyrrolidine-3-carboxamide Chemical compound C1C(C(=O)N)CCN1CC1=CC=CC=C1 HNAGHMKIPMKKBB-UHFFFAOYSA-N 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
- OBNCKNCVKJNDBV-UHFFFAOYSA-N butanoic acid ethyl ester Natural products CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 244000269722 Thea sinensis Species 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 230000003694 hair properties Effects 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 240000009087 Crescentia cujete Species 0.000 description 1
- 235000005983 Crescentia cujete Nutrition 0.000 description 1
- 235000009797 Lagenaria vulgaris Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 235000014676 Phragmites communis Nutrition 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 150000002561 ketenes Chemical class 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000874 microwave-assisted extraction Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000000199 molecular distillation Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- MTZWHHIREPJPTG-UHFFFAOYSA-N phorone Chemical compound CC(C)=CC(=O)C=C(C)C MTZWHHIREPJPTG-UHFFFAOYSA-N 0.000 description 1
- 229930193351 phorone Natural products 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 235000019643 salty taste Nutrition 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 238000009777 vacuum freeze-drying Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Toxicology (AREA)
- General Health & Medical Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of Rose type essence for Ms's cigarette, it is mixed by following components：1.0~2.5% rose ethereal oil, 0.1~0.5% clove bud oil, 0.01~0.1% aniseed oil, 1.5~3.0% citronellol, 0.1~0.5% geraniol, 0.2~0.5% linalool, 0.5~1.5% benzyl carbinol, 0.1~1.0% ethyl isobutyrate, 0.2~1.5% phenylethyl phenylacetate, 0.1~0.3% menthyl acetate, 0.5~1.0% ginkgo biloba p.e, 0.1~1.0% mango extract, 0.05~0.5% coffee-extract, 0.1~1.0% emblic extract, 1.0~2.0% smoked plum extractive, 0.5~1.0% jujube medicinal extract, 0.01~0.05% fenugreek concrete, 0.5~1.5% spices tobacco extract, 0.01~0.1% lactic acid, 0.02~0.08% benzoic acid, 0.02~0.05% ketoisophorone, 0.5~1.0% Megastigmatrienone, 0.5~1.0% honey, 40.0~60.0% 70% ethanol, remaining is propane diols.Be added into using Rose type essence in pipe tobacco, roll into cigarette, it has the advantages that, and soft flue gas exquisiteness, comfortable taste, pleasant impression are clean, inhale taste alcohol and, cigarette perfume coordinates.
Description
Technical field
The invention belongs to technical field of cigarette flavors, specifically refer to a kind of Rose type essence for Ms's cigarette and its
Using.
Technical background
Because " smoking and health " problem is more and more paid close attention to by society, produced with " high fragrance, low tar, less harmful "
Turn into the direction of tobacco industry survival and development for the cigarette product of main feature.But, while reducing tar and reducing harm, often
Cigarette odor-absorbing composition can be caused largely to lose, fragrance substantially weakens, it is difficult to meet consumer demand.Therefore, carry out fragrance to mend
Repay technical research and the exploitation of essence and flavoring agent, it has also become an urgent demand of cigarette industry.For example, domestic many tobacco companies exist
While allocating cigarette composition, mostly again using the method for additional various spices or essence, to make up the deficiency of cigarette fragrance.Together
When, in order to protrude the style and features of brand, flavouring essence for tobacco of the exploitation with feature odor type is for example various floral types, Fruity type, salty
Taste type essence, it has also become major tobacco enterprises endeavour the target of research.
Ms's cigarette is also known as " female's cigarette ", refers to the cigarette designed the need for being directed to female smoker, and its outward appearance typically compares
Very thin, exquisiteness, is packed based on fashion bright colors lines, and it aspirates taste and carries fruit aroma or flowery odour mostly, compares
It is fresh and clean.In recent years, continuing to develop with China's economic, the continuous enhancing of the independent consciousness of women shows women
Property age arrive, smoke no longer be man patent, a part of high salary white collar and the women of individual character of following the fashion also are added
To this ranks.Due to physiology and psychological difference, male and female embodies completely different in cigarette consumption demand
Feature.Flue gas is fine and smooth, elegant in smell, inhale taste alcohol and, pleasant impression is pure, comfortable taste cigarette often enjoys female smoker to welcome,
This specifies direction for the adjustment and exploitation of Ms's cigarette perfume extract formula.It is existing with the popularization of " Smoking is harmful to your health " this idea
For women smoker following the fashion, individual character while, more focus on the health and safety problem of cigarette, low-harm type cigarette product
The object increasingly paid close attention to as female smoker.
The content of the invention
The characteristics of it is an object of the invention to be liked deeply by Ms according to rose, there is provided a kind of Rose type for Ms's cigarette
Essence and its application, it can assign Ms's cigarette graceful naturally rose characteristic perfume, with flue gas exquisiteness is soft, mouthfeel is relaxed
Suitable, pleasant impression is clean, inhale taste alcohol and, cigarette perfume is the advantages of coordinate, while the thorn that flue gas is caused to throat when can effectively mitigate suction
Property is swashed, with potential harm reduction effect.
To achieve the above object, a kind of Rose type essence for Ms's cigarette designed by the present invention, it is by following groups
Divide and mix by weight percentage：1.0~2.5% rose ethereal oil, 0.1~0.5% clove bud oil, 0.01~
0.1% aniseed oil, 1.5~3.0% citronellol, 0.1~0.5% geraniol, 0.2~0.5% linalool, 0.5
~1.5% benzyl carbinol, 0.1~1.0% ethyl isobutyrate, 0.2~1.5% phenylethyl phenylacetate, 0.1~0.3%
Menthyl acetate, 0.5~1.0% ginkgo biloba p.e, 0.1~1.0% mango extract, 0.05~0.5% coffee
Extract, 0.1~1.0% emblic extract, 1.0~2.0% smoked plum extractive, 0.5~1.0% jujube medicinal extract,
0.01~0.05% fenugreek concrete, 0.5~1.5% spices tobacco extract, 0.01~0.1% lactic acid, 0.02~
0.08% benzoic acid, 0.02~0.05% ketoisophorone, 0.5~1.0% Megastigmatrienone, 0.5~1.0%
Honey, 40.0~60.0% 70% ethanol, remaining is propane diols.
Preferably, it is mixed by weight percentage by following components：1.5~2.0% rose ethereal oil,
0.2~0.3% clove bud oil, 0.01~0.05% aniseed oil, 1.5~2.5% citronellol, 0.1~0.3%
Geraniol, 0.2~0.5% linalool, 0.5~1.0% benzyl carbinol, 0.1~0.5% ethyl isobutyrate, 0.5~
1.0% phenylethyl phenylacetate, 0.1~0.2% menthyl acetate, 0.7~1.0% ginkgo biloba p.e, 0.5~
1.0% mango extract, 0.2~0.4% coffee-extract, 0.2~0.8% emblic extract, 1.0~1.5%
Smoked plum extractive, 0.5~0.8% jujube medicinal extract, 0.03~0.05% fenugreek concrete, 0.6~1.2% Turkish tobaccos
Extract, 0.05~0.1% lactic acid, 0.03~0.06% benzoic acid, 0.02~0.05% ketoisophorone, 0.5
~0.7% Megastigmatrienone, 0.6~0.8% honey, 45.0~55.0% 70% ethanol, remaining is propane diols.
Yet further, the volume fraction of ethanol is 70%.
The preparation method is that by said components raw material according to being stirred after percentage by weight dispensing in container
Mixing.
The present invention also provides a kind of application for the Rose type essence of Ms's cigarette in Ms's cigarette：Comprise the following steps：
Rose type essence is weighed to be dissolved in volume fraction in 70% ethanol solution, to obtain the rose that mass fraction is 10~70%
It, is then uniformly sprayed on Ms's cigarette blank pipe tobacco by rare type fragrance solution, and rolls into cigarette, wherein, Rose type essence
Addition be pipe tobacco weight 0.01~0.05%.
Advantage of the present invention is as follows：
1st, the present invention is based on the alcohols monomer perfume rich in rose suggestion, and independent development has simultaneously used various plants
Natural extract, while abundant tobacco aromaticss range of choice so that the allotment for the Rose type essence of Ms's cigarette is obtained
Compared with quantum jump.
2nd, plant containing natural extract and traditional monomer cigarette flavor are passed through scientific and rational compatibility by the present invention,
Allotment obtains a kind of Rose type essence for Ms's cigarette, can assign Ms's cigarette graceful naturally rose characteristic perfume, have
Flue gas exquisiteness is soft, comfortable taste, pleasant impression are clean, inhale taste alcohol and, cigarette perfume is the advantages of coordinate, while when effectively can mitigate suction
The excitant that flue gas is caused to throat, with potential harm reduction effect.
3rd, the present invention has the advantages that preparation method is simple, economical and practical, raw material is easily obtained.
Embodiment
Method of the present invention is described in further detail with reference to specific embodiment.
Embodiment 1
Weigh following raw material components (based on 100g formulas)：2g rose ethereal oil, 0.2g clove bud oil, 0.02g
Aniseed oil, 2g citronellol, 0.4g geraniol, 0.2g linalool, 1.0g benzyl carbinol, 0.6g isobutyric acid second
Ester, 0.7g phenylethyl phenylacetate, 0.1g menthyl acetate, 1g ginkgo biloba p.e, 0.5g mango extract, 0.2g
Coffee-extract, 0.5g emblic extract, 1.0g smoked plum extractive, 0.5g jujube medicinal extract, 0.02g faenum graecum
Medicinal extract, 1.0g spices tobacco extract, 0.02g lactic acid, 0.06g benzoic acid, 0.03g ketoisophorone, 0.8g
Megastigmatrienone, 0.5g honey, 50g volume fraction are 70% ethanol, and remaining is propane diols.By above-mentioned raw materials in container
Stir and produce Rose type essence 1.Appropriate Rose type essence 1 is taken to be dissolved in volume fraction in 70% ethanol solution, to obtain
Mass fraction is 10% Rose type fragrance solution, and then it be uniformly sprayed to Yellow Crane Tower " heart is blue " Ms's cigarette blank pipe tobacco
On, and roll into cigarette.The addition of Rose type essence is the 0.01% of pipe tobacco weight.
Embodiment 2
Weigh following raw material components (based on 100g formulas)：1.5g rose ethereal oil, 0.3g clove bud oil,
0.05g aniseed oil, 1.5g citronellol, 0.5g geraniol, 0.4g linalool, 0.8g benzyl carbinol, 0.4g it is different
Ethyl butyrate, 1.0g phenylethyl phenylacetate, 0.3g menthyl acetate, 0.8g ginkgo biloba p.e, 1.0g mango are carried
Take thing, 0.3g coffee-extract, 0.3g emblic extract, 1.5g smoked plum extractive, 0.8g jujube medicinal extract,
0.05g fenugreek concrete, 0.8g spices tobacco extract, 0.1g lactic acid, 0.02g benzoic acid, the 0.04g different Buddhist of oxo
That ketone, 0.5g Megastigmatrienone, 0.7g honey, 40g volume fraction are 70% ethanol, and remaining is propane diols.Will be above-mentioned
Raw material uniformly produces Rose type essence 2 in container for stirring.Appropriate Rose type essence 2 is taken to be dissolved in volume fraction for 70% ethanol
In solution, the Rose type fragrance solution that mass fraction is 70% is obtained, then it be uniformly sprayed to Yellow Crane Tower " heart is blue " Ms
On cigarette blank pipe tobacco, and roll into cigarette.The addition of Rose type essence is the 0.05% of pipe tobacco weight.
Embodiment 3
Weigh following raw material components (based on 100g formulas)：1.8g rose ethereal oil, 0.5g clove bud oil, 0.1g
Aniseed oil, 2.5g citronellol, 0.2g geraniol, 0.3g linalool, 1.2g benzyl carbinol, 0.6g isobutyric acid second
Ester, 1.2g phenylethyl phenylacetate, 0.25g menthyl acetate, 0.5g ginkgo biloba p.e, 0.7g mango extract,
0.2g coffee-extract, 0.5g emblic extract, 1.2g smoked plum extractive, 0.6g jujube medicinal extract, 0.04g calabash
Reed bar medicinal extract, 1.0g spices tobacco extract, 0.05g lactic acid, 0.04g benzoic acid, 0.05g ketoisophorone,
0.6g Megastigmatrienone, 0.6g honey, 60g volume fraction are 70% ethanol, and remaining is propane diols.Above-mentioned raw materials are existed
Container for stirring uniformly produces Rose type essence 3.Appropriate Rose type essence 3 is taken to be dissolved in volume fraction for 70% ethanol solution
In, the Rose type fragrance solution that mass fraction is 50% is obtained, then it is uniformly sprayed to Yellow Crane Tower " heart is blue " Ms's cigarette empty
On white cigarette silk, and roll into cigarette.The addition of Rose type essence is the 0.03% of pipe tobacco weight.
Embodiment 4
Weigh following raw material components (based on 100g formulas)：1.8g rose ethereal oil, 0.3g clove bud oil,
0.08g aniseed oil, 2.5g citronellol, 0.4g geraniol, 0.5g linalool, 0.8g benzyl carbinol, 0.4g it is different
Ethyl butyrate, 0.8g phenylethyl phenylacetate, 0.15g menthyl acetate, 0.6g ginkgo biloba p.e, 0.8g mango are carried
Take thing, 0.15g coffee-extract, 0.8g emblic extract, 1.5g smoked plum extractive, 0.8g jujube medicinal extract,
0.02g fenugreek concrete, 0.8g spices tobacco extract, 0.08g lactic acid, 0.02g benzoic acid, 0.03g oxo it is different
Phorone, 0.7g Megastigmatrienone, 0.5g honey, 55g volume fraction are 70% ethanol, and remaining is propane diols.Will be upper
State raw material and uniformly produce Rose type essence 4 in container for stirring.Appropriate Rose type essence 4 is taken to be dissolved in volume fraction for 70% second
In alcoholic solution, the Rose type fragrance solution that mass fraction is 50% is obtained, then it be uniformly sprayed to Yellow Crane Tower " heart is blue " female
On scholar's cigarette blank pipe tobacco, and roll into cigarette.The addition of Rose type essence is the 0.02% of pipe tobacco weight.
Embodiment 5
Weigh following raw material components (based on 100g formulas)：2.5g rose ethereal oil, 0.1g clove bud oil,
0.01g aniseed oil, 1.8g citronellol, 0.1g geraniol, 0.3g linalool, 0.5g benzyl carbinol, 0.1g it is different
Ethyl butyrate, 0.2g phenylethyl phenylacetate, 0.2g menthyl acetate, 0.7g ginkgo biloba p.e, 0.1g mango are carried
Take thing, 0.05g coffee-extract, 0.1g emblic extract, 2g smoked plum extractive, 1g jujube medicinal extract, 0.01g
Fenugreek concrete, 0.5g spices tobacco extract, 0.01g lactic acid, 0.03g benzoic acid, 0.02g ketoisophorone,
1g Megastigmatrienone, 1g honey, 45g volume fraction are 70% ethanol, and remaining is propane diols.By above-mentioned raw materials in container
Inside stir and produce Rose type essence 5.Appropriate Rose type essence 5 is taken to be dissolved in volume fraction in 70% ethanol solution, to obtain
To the Rose type fragrance solution that mass fraction is 20%, then it be uniformly sprayed to Yellow Crane Tower " heart is blue " Ms's cigarette blank pipe tobacco
On, and roll into cigarette.The addition of Rose type essence is the 0.01% of pipe tobacco weight.
Embodiment 6
Weigh following raw material components (based on 100g formulas)：1g rose ethereal oil, 0.25g clove bud oil, 0.03g
Aniseed oil, 1.7g citronellol, 0.3g geraniol, 0.3g linalool, 1.5g benzyl carbinol, 1g isobutyric acid second
Ester, 1.5g phenylethyl phenylacetate, 0.3g menthyl acetate, 1g ginkgo biloba p.e, 0.6g mango extract, 0.4g
Coffee-extract, 1g emblic extract, 1.4g smoked plum extractive, 0.7g jujube medicinal extract, 0.03g faenum graecum leaching
Cream, 1.5g spices tobacco extract, 0.05g lactic acid, 0.08g benzoic acid, 0.04g ketoisophorone, 0.5g it is huge
The ketenes of beans three, 0.8g honey, 52g volume fraction are 70% ethanol, and remaining is propane diols.Above-mentioned raw materials are stirred in container
Mix and uniformly produce Rose type essence 6.Appropriate Rose type essence 6 is taken to be dissolved in volume fraction in 70% ethanol solution, to obtain matter
The Rose type fragrance solution that fraction is 60% is measured, is then uniformly sprayed at it on Yellow Crane Tower " heart is blue " Ms's cigarette blank pipe tobacco,
And roll into cigarette.The addition of Rose type essence is the 0.05% of pipe tobacco weight.
Embodiment 7
Weigh following raw material components (based on 100g formulas)：1.8g rose ethereal oil, 0.28g clove bud oil,
0.04g aniseed oil, 3g citronellol, 0.2g geraniol, 0.4g linalool, 1.3g benzyl carbinol, 0.5g isobutyl
Acetoacetic ester, 0.5g phenylethyl phenylacetate, 0.2g menthyl acetate, 0.8g ginkgo biloba p.e, 0.8g mango are extracted
Thing, 0.5g coffee-extract, 0.2g emblic extract, 1.2g smoked plum extractive, 0.5g jujube medicinal extract, 0.05g
Fenugreek concrete, 1.2g spices tobacco extract, 0.08g lactic acid, 0.02g benzoic acid, the 0.03g different Fo Er of oxo
Ketone, 0.7g Megastigmatrienone, 0.7g honey, 48g volume fraction are 70% ethanol, and remaining is propane diols.By above-mentioned original
Material uniformly produces Rose type essence 7 in container for stirring.Appropriate Rose type essence 7 is taken to be dissolved in volume fraction molten for 70% ethanol
In liquid, the Rose type fragrance solution that mass fraction is 40% is obtained, then it be uniformly sprayed to Yellow Crane Tower " heart is blue " Ms's cigarette
On blank pipe tobacco, and roll into cigarette.The addition of Rose type essence is the 0.02% of pipe tobacco weight.
In embodiment 1~7, rose ethereal oil is to handle rose through vacuum freeze drying, after pulverizing and sieving, using super
Critical CO2The essential oil product that abstraction technique is prepared.
Ginkgo biloba p.e is after the ginkgo leaf dried is crushed, to carry out backflow using 50~80% ethanol solution and carry
Take, then the extract through filtering, being concentrated to give.
Mango extract is after the pulp of mango is crushed through squeezing, to carry out backflow using 30~70% ethanol solution and carry
Take, then the extract through filtering, being concentrated to give.
Coffee-extract is that after coffee is crushed, sieve, refluxing extraction is carried out with the aqueous solution, then through filtering, being concentrated to give
Extract.
Emblic extract is after emblic is crushed, sieve, Microwave Extraction to be used after being stayed overnight with aqueous solution soaking, then pass through
The extract filter, being concentrated to give.
Smoked plum extractive is to carry out refluxing extraction after dry dark plum is stayed overnight using 40~75% alcohol solution dipping, then is passed through
The extract filter, being concentrated to give.
Jujube medicinal extract is will to obtain jujube powder particle after dry jujube pretreatment, after 50~70% alcohol solution dippings
Ultrasonic wave extraction is carried out, then rotated evaporation and concentration obtains jujube medicinal extract.
Fenugreek concrete be by faenum graecum seed through parch, pulverize after, refluxing extraction is carried out with 60~80% ethanol solutions, then
Through filtering, being concentrated to give fenugreek concrete.
Spices tobacco extract is after Turkish tobaccos are handled through chopping, to carry out refluxing extraction with 50~70% ethanol solutions, adopt
The extract prepared with molecular distillation technique.
Remaining raw material used is commercially available.
Sensory evaluating smoking's effect of several plant natural extract：
Rose ethereal oil：Feature rose suggestion, soft, fine and smooth flue gas, cigarette perfume is coordinated, and pleasant impression is comfortable.
Ginkgo biloba p.e：Abundant cigarette perfume, saturating smoke gas increases sweet tea sense.
Mango extract：Abundant cigarette perfume, reduction is stimulated, and pleasant impression is comfortable, and flue gas is fine and smooth, soft.
Coffee-extract：Reducing throat stimulates, and soft flue gas increases flue gas sweet tea sense.
Emblic extract：Hair property thoroughly is improved, soft flue gas slightly improves pleasant impression, slightly reduction is stimulated.
Smoked plum extractive：Soft flue gas, reduction throat stimulates, and increases flue gas concentration.
Jujube medicinal extract：Abundant cigarette perfume, improves hair property, enrichment flue gas thoroughly.
Fenugreek concrete：Abundant cigarette perfume, slightly increases flue gas concentration, and reduction is stimulated, and covers miscellaneous gas.
Spices tobacco extract：Increase perfume quantity, improve flue gas concentration.
Sensory evaluating smoking's result shows：Rose type essence 1~7 can assign Ms's cigarette graceful naturally rose characteristic perfume,
Have the advantages that soft flue gas exquisiteness, comfortable taste, pleasant impression are clean, inhale taste alcohol and, cigarette perfume coordinate, taken out while can effectively mitigate
The excitant that flue gas is caused to throat during suction, with potential harm reduction effect.
Claims (2)
1. a kind of Rose type essence for Ms's cigarette, it is mixed by weight percentage by following components：1.5~2.0%
Rose ethereal oil, 0.2~0.3% clove bud oil, 0.01~0.05% aniseed oil, 1.5~2.5% lemongrass
Alcohol, 0.1~0.3% geraniol, 0.2~0.5% linalool, 0.5~1.0% benzyl carbinol, 0.1~0.5% isobutyl
Acetoacetic ester, 0.5~1.0% phenylethyl phenylacetate, 0.1~0.2% menthyl acetate, 0.7~1.0% ginkgo leaf are extracted
Thing, 0.5~1.0% mango extract, 0.2~0.4% coffee-extract, 0.2~0.8% emblic extract, 1.0
~1.5% smoked plum extractive, 0.5~0.8% jujube medicinal extract, 0.03~0.05% fenugreek concrete, 0.6~1.2%
Spices tobacco extract, 0.05~0.1% lactic acid, 0.03~0.06% benzoic acid, the different Buddhist of 0.02~0.05% oxo
That ketone, 0.5~0.7% Megastigmatrienone, 0.6~0.8% honey, the second that 45.0~55.0% volume fraction is 70%
Alcohol, remaining is propane diols.
2. it is used for application of the Rose type essence of Ms's cigarette in Ms's cigarette described in a kind of claim 1：It is characterized in that：Including
Following steps：
Weigh Rose type essence to be dissolved in the ethanol solution of volume fraction 70%, obtain the Rose type that mass fraction is 10~70% fragrant
It, is then uniformly sprayed on Ms's cigarette blank pipe tobacco by smart solution, and rolls into cigarette, wherein, the addition of Rose type essence
Measure as the 0.01~0.05% of pipe tobacco weight.
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| RU2593966C1 (en) * | 2015-04-20 | 2016-08-10 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| RU2594041C1 (en) * | 2015-04-20 | 2016-08-10 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| RU2593094C1 (en) * | 2015-04-20 | 2016-07-27 | Олег Иванович Квасенков | Method for production of hookah smoking composition |
| CN105199851B (en) * | 2015-10-21 | 2019-03-08 | 河南中烟工业有限责任公司 | A kind of cream odor type flavouring essence for tobacco |
| CN106433972A (en) * | 2016-10-31 | 2017-02-22 | 湖北中烟工业有限责任公司 | Flavoring rose essence for cigarette paper |
| CN109222212A (en) * | 2017-07-10 | 2019-01-18 | 中国烟草总公司广东省公司 | A kind of fragrance-enhancing tobacco agent containing faenum graecum essential oil |
| CN107586612A (en) * | 2017-10-10 | 2018-01-16 | 广东长利香精香料有限公司 | A kind of lemongrass mango essential oil |
| CN108035195B (en) * | 2017-12-12 | 2020-11-17 | 江西中烟工业有限责任公司 | Tipping paper containing composite natural plant extract and preparation method thereof |
| CN109439435B (en) * | 2018-12-14 | 2022-06-21 | 湖北中烟工业有限责任公司 | Preparation method and application of smoking extract and tobacco essence containing smoking extract |
| CN112760169A (en) * | 2020-12-02 | 2021-05-07 | 桂林理工大学 | Acer truncatum seed essential oil, and preparation method and application thereof |
| CN114703020B (en) * | 2022-05-23 | 2023-06-02 | 茂名华美实业有限公司 | Essence composition for producing coffee-flavored tobacco and preparation method thereof |
| CN115595209B (en) * | 2022-11-02 | 2024-03-26 | 云南中烟工业有限责任公司 | Essence formula with rose characteristics, preparation method and application thereof |
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| EP2088877B1 (en) * | 2006-11-29 | 2018-08-01 | Imperial Tobacco Canada Limited | Cigarette filter with flavored particles |
| CN101396169B (en) * | 2007-09-29 | 2010-12-29 | 上海百润香精香料股份有限公司 | Cured tobacco perfume formulation |
| CN101215805A (en) * | 2008-01-07 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Cigarette perfuming agent and its preparation method and application |
| CN102304423B (en) * | 2011-03-17 | 2013-06-05 | 广州市澳键丰泽生物科技有限公司 | Fragrance-enhancing tobacco essence |
| CN102925289B (en) * | 2012-11-21 | 2013-11-20 | 红塔烟草(集团)有限责任公司 | Rose type cigarette essence, preparation method and application thereof |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
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