CN103146483A - Pelargonium roseum extract and application of extract in cigarette - Google Patents
Pelargonium roseum extract and application of extract in cigarette Download PDFInfo
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- CN103146483A CN103146483A CN2013100925987A CN201310092598A CN103146483A CN 103146483 A CN103146483 A CN 103146483A CN 2013100925987 A CN2013100925987 A CN 2013100925987A CN 201310092598 A CN201310092598 A CN 201310092598A CN 103146483 A CN103146483 A CN 103146483A
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Abstract
The invention discloses a pelargonium roseum extract and application of extract in a cigarette, and belongs to the field of a tobacco additive. The aromatic plant pelargonium roseum (pelargonium graveolens L'Herit) is taken as a material and extracted by a supercritical CO2 extraction technology combined with a molecular distillation technology to prepare the tobacco additive. The natural plant extract comprises the main ingredients such as citronellol, geraniol, linalool, citronellyl formate and pulegone. The extract has the effects of increasing fresh and sweet flavor and fineness, reducing thrill, covering offensive odor and improving the comfort after the extract is added to the cigarette.
Description
Technical field
The invention belongs to the technical field of cigarette additive, specifically relate to a kind of preparation of Pelargonium gravelens extract, simultaneously, the invention still further relates to the application of described Pelargonium gravelens extract in tobacco processing.
Background technology
In tobacco product, the fragrance of tobacco and jealous be vital, along with the reduction of tar content in cigarette in recent years, low-coke tar cigarette exists smoke thin out, fragrance weakens, cigarette product loses original style, is difficult to the problem of being accepted by the human consumer.So when Jiao fell in Harm reduction techniques, cigarette flavouring and raising flue gas concentration were key issues.Perfuming cigarette is reinforced is one of core technology of tobacco industry.Mode by flavoring and casing can make up the insufficient fragrance on cigarette tobacco leaf formulation, eliminates assorted gas, makes the cigarette perfume (or spice) of cigarette product more abundant, sufficient, thereby inhaling flavor, smelling and have individual style on perfume (or spice), strengthens the feature of cigarette product.
Preparing by different way essence spice for cigarette makes an addition to and reaches the method that promotes cigarette smoking quality in cigarette and appear in the newspapers.The people such as Yang Lihua are take natural mushroom mushroom as raw material, adopt conventional extraction method, enzymolysis process and Maillard reaction method development of new tobacco aromatics using, and carry out perfuming cigarette experiment, result shows that enzyme process gained spices gives cigarette special note, has the effect that improves the flue gas comfort level.Deng state guests etc. utilize the microorganism aroma former to make the fresh iris spices of fresh iris preparation fermentation, and the absolute oil of preparation is carried out perfuming cigarette for kinds of cigarettes leaf group, experimental result shows that the fresh orris absolute of fermentation is better than without adding of the fresh orris absolute of biological fermentation of fragrant effect at the perfuming successful aspect fragrance, assorted gas and comfortableness.Zhu Baokun etc. have analyzed the impact of the humectants such as glycerine, propylene glycol, sorbyl alcohol, honey on cigarette Oranoleptic indicators such as stimulation, pleasant impression, dry sensations, result shows, the humectant consumption promotes " cloud and mist " product sensory remarkably influenced, and has determined the broiler diets of four kinds of humectants; The different humectants such as glycerine, propylene glycol, sorbyl alcohol, honey have remarkably influenced to the pungency of " cloud and mist " product, and the propylene glycol consumption is its pungency of cigarette of 0.4% less than the cigarette that has added 0.7% glycerine, 0.7% sorbyl alcohol, 0.7% honey.Ji Xiaoming etc. extract volatile oil take Flower of Chinese Globeflower as raw material, use GC-MS to analyze volatile oil component, and carry out perfuming cigarette and test, result shows the appropriate Flower of Chinese Globeflower volatile oil of interpolation in pipe tobacco, can improve fragrance matter and the perfume quantity of cigarette smoke, reduce pungency, improve pleasant impression, its main aroma component is alpha, beta-lonone, dioxy actinidia lactone etc.The reports such as Duan Binbin, carry out the perfuming experiment as material extraction volatile oil and in cigarette take the bosom chrysanthemum, result shows, this volatile oil can be modified cigarette flavor, improve that flue gas is submissive, fine and smooth degree, reduce pungency and improve pleasant impression, its key odorant composition is p-ymene, α-pinene, β-phellandrene, farnesol etc.
Report to some extent with the research that promotes the cigarette organoleptic quality although be applied in cigarette with plant milk extract, adopt supercritical CO
2Abstraction technique and molecular distillation technique coupling prepare the method that the Pelargonium gravelens extract is used for the tobacco aromatics using aspect and there is not yet report.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of cigarette Pelargonium gravelens extract is provided, be applied to perfuming cigarette to promote the flue gas quality.
The present invention also aims to provide the concrete application method of described Pelargonium gravelens extract in perfuming cigarette.
Purpose of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage ratio that adopts in the present invention is mass percent.
A kind of Pelargonium gravelens extract is prepared by following method:
(1) the Pelargonium gravelens raw material is packed in extraction kettle, add the ethanol of 10% concentration 95%, with the CO of supercritical state
2Injecting extraction kettle, is 20～40MPa in extracting pressure, extracts 1～3h under the condition that extraction temperature is 30～50 ℃, is dissolved with the CO of aroma component
2Fluid enters separating still, heats up by step-down the aroma component of Pelargonium gravelens is separated;
(2) with supercritical CO
2The material that extracts carries out molecular distillation, is that 150～200 g/h, knifing speed are that 600～700 r/min, distillation temperature are that 40～60 ℃, distillation pressure are to separate under 250～350 Pa conditions to obtain volatile oil in input speed;
(3) with after 50 times of volatile oil dilutions, obtain required Pelargonium gravelens extract.
Wherein, Pelargonium gravelens (Pelargonium graveolens L ' Herit) is Mang ox seedling section per nnial herb, and using part is its over-ground part.
The Pelargonium gravelens extract that makes with aforesaid method is a kind of faint yellow transparent oily liquids, has peculiar fragrance.Being used in conjunction chromatographic instrument through makings analyzes to such an extent that its main component is: firpene, eucalyptus alcohol, amphene, limonene, phantol, camphor, borneol, Terpineol 350, Bornyl acetate etc.
The concrete application method of described Pelargonium gravelens extract in cigarette: described Pelargonium gravelens extract is added in pipe tobacco with 0.25%～0.75% ratio, and then technology is made cigarette routinely.
The experimental result of smokeing panel test shows, compared with the control, described Pelargonium gravelens extract has and promotes perfume quantity and fragrance matter, increases fine and smooth sense, reduces the effect that stimulates, covers assorted gas, promotes comfortableness.
Compared with prior art, the present invention has following beneficial effect:
(1) select the scented plants Pelargonium gravelens to study as raw material, be conducive to improve the economic use value of scented plants;
(2) interpolation of Pelargonium gravelens extract in cigarette when obviously increasing sweet sense, has the effect of enriching cigarette perfume (or spice), reducing to stimulate, promote comfortableness;
(3) production technique operability and standardization are strong, can realize suitability for industrialized production, have good development prospect.
Embodiment
In order to make purpose of the present invention, technical scheme and advantage clearer, the present invention is described in further detail by the following examples.Should be appreciated that specific embodiment described herein is only in order to explain the present invention, the protection domain that is not intended to limit the present invention.
Embodiment 1---the preparation of Pelargonium gravelens extract and use 1
1. the preparation of extract
(1) the Pelargonium gravelens raw material is packed in extraction kettle, add 10% to carry agent (95% ethanol), with the CO of supercritical state
2Injecting extraction kettle, is 20 MPa in extracting pressure, extracts 3 h under the condition that extraction temperature is 30 ℃, is dissolved with the CO of aroma component
2Fluid enters separating still, heats up by step-down the aroma component of Pelargonium gravelens is separated;
(2) with supercritical CO
2The material that extracts carries out molecular distillation, is that 150 g/h, knifing speed are that 600 r/min, distillation temperature are that 40 ℃, distillation pressure are that the light constituent that separates under 250 Pa conditions to obtain is as the volatile oil that uses in input speed.
(3) with after 50 times of volatile oil dilutions, obtain the perfuming extract.
2. perfuming cigarette experiment
The natural plant extracts that utilization prepares is processed tobacco leaf leaf group, and the adding proportion according to 0.75% makes an addition to the leaf group as treatment group, and with the leaf group of not adding extract as a control group.
3. the experiment of smokeing panel test
After the pipe tobacco for the treatment of group and control group is put into climatic chamber inner equilibrium 24 h, make cigarette, sample and contrast random number, the group of smokeing panel test that is comprised of the expert who possesses the qualification of smokeing panel test carries out the sensory evaluating smoking.
4. effect evaluation
Add the experimental result of smokeing panel test and show in pipe tobacco, the interpolation of this natural plant extracts has increases fresh and sweet note, enrich cigarette perfume (or spice), reduce the effect that stimulates, covers assorted gas, promotes comfortableness.
Embodiment 2---the preparation of Pelargonium gravelens extract and use 2
1. the preparation of extract
(1) the Pelargonium gravelens raw material is packed in extraction kettle, add 10% to carry agent (95% ethanol), with the CO of supercritical state
2Injecting extraction kettle, is 40 MPa in extracting pressure, extracts 1 h under the condition that the extraction temperature is 50 ℃, is dissolved with the CO of aroma component
2Fluid enters separating still, heats up by step-down the aroma component of Pelargonium gravelens is separated;
(2) with supercritical CO
2The material that extracts carries out molecular distillation, is that 200 g/h, knifing speed are that 700 r/min, distillation temperature are that 60 ℃, distillation pressure are that the light constituent that separates under 350 Pa conditions to obtain is as the volatile oil that uses in input speed.
(3) with after 50 times of volatile oil dilutions, obtain the perfuming extract.
2. perfuming cigarette experiment
The natural plant extracts that utilization prepares is processed tobacco leaf leaf group, makes an addition to the leaf group as treatment group according to the adding proportion of 0.25 %, and with the leaf group of not adding extract as a control group.
3. the experiment of smokeing panel test
After the pipe tobacco for the treatment of group and control group is put into climatic chamber inner equilibrium 24 h, make cigarette, sample and contrast random number, the group of smokeing panel test that is comprised of the expert who possesses the qualification of smokeing panel test carries out the sensory evaluating smoking.
4. effect evaluation
Add the experimental result of smokeing panel test and show in pipe tobacco, the interpolation of this natural plant extracts can promote fragrance matter, reduces stimulation, cover assorted gas, can increase fresh and sweet rhythm simultaneously.
Embodiment 3---the preparation of Pelargonium gravelens extract and use 3
1. the preparation of extract
(1) the Pelargonium gravelens raw material is packed in extraction kettle, add 10% to carry agent (95% ethanol), with the CO of supercritical state
2Injecting extraction kettle, is 30 MPa in extracting pressure, extracts 2 h under the condition that extraction temperature is 40 ℃, is dissolved with the CO of aroma component
2Fluid enters separating still, heats up by step-down the aroma component of Pelargonium gravelens is separated;
(2) with supercritical CO
2The material that extracts carries out molecular distillation, is that 150 g/h, knifing speed are that 600 r/min, distillation temperature are that 50 ℃, distillation pressure are that the light constituent that separates under 300 Pa conditions to obtain is as the volatile oil that uses in input speed.
(3) with after 50 times of volatile oil dilutions, obtain the perfuming extract.
2. perfuming cigarette experiment
The natural plant extracts that utilization prepares is processed tobacco leaf leaf group, and the adding proportion according to 0.50% makes an addition to the leaf group as treatment group, and with the leaf group of not adding extract as a control group.
3. the experiment of smokeing panel test
After the pipe tobacco for the treatment of group and control group is put into climatic chamber inner equilibrium 24 h, make cigarette, sample and contrast random number, the group of smokeing panel test that is comprised of the expert who possesses the qualification of smokeing panel test carries out the sensory evaluating smoking.
4. effect evaluation
Add the experimental result of smokeing panel test and show in pipe tobacco, the interpolation of this natural plant extracts can increase fresh and sweet note, reduce stimulation, promotes comfort.
The above is only preferred embodiment of the present invention, not in order to limiting the present invention, all any modifications of doing within the spirit and principles in the present invention, is equal to and replaces and improvement etc., within all should being included in protection scope of the present invention.
Claims (2)
1. Pelargonium gravelens extract is prepared by following method:
(1) the Pelargonium gravelens raw material is packed in extraction kettle, add the ethanol of 10% concentration 95%, with the CO of supercritical state
2Injecting extraction kettle, is 20～40MPa in extracting pressure, extracts 1～3h under the condition that extraction temperature is 30～50 ℃, is dissolved with the CO of aroma component
2Fluid enters separating still, heats up by step-down the aroma component of Pelargonium gravelens is separated;
(2) with supercritical CO
2The material that extracts carries out molecular distillation, is that 150～200 g/h, knifing speed are that 600～700 r/min, distillation temperature are that 40～60 ℃, distillation pressure are to separate under 250～350 Pa conditions to obtain volatile oil in input speed;
(3) with after 50 times of volatile oil dilutions, obtain required Pelargonium gravelens extract.
2. the concrete application method of Pelargonium gravelens extract claimed in claim 1 in cigarette: described Pelargonium gravelens extract is added in pipe tobacco with 0.25%～0.75% ratio, and then technology is made cigarette routinely.
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| CN2013100925987A CN103146483A (en) | 2013-03-21 | 2013-03-21 | Pelargonium roseum extract and application of extract in cigarette |
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| CN2013100925987A CN103146483A (en) | 2013-03-21 | 2013-03-21 | Pelargonium roseum extract and application of extract in cigarette |
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Cited By (8)
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| CN104531356A (en) * | 2015-01-19 | 2015-04-22 | 川渝中烟工业有限责任公司 | Honeyed-sweet additive and electronic cigarette liquid with same |
| CN105062682A (en) * | 2015-08-27 | 2015-11-18 | 湖北中烟工业有限责任公司 | Camphor tree seed cigarette spice and preparation method thereof |
| CN105272824A (en) * | 2015-11-17 | 2016-01-27 | 鹰潭华宝香精香料有限公司 | Preparation method of natural cinnamomum camphora aromatic material |
| CN105581374A (en) * | 2016-03-18 | 2016-05-18 | 云南中烟工业有限责任公司 | Glycerol triacetate extract of pelargonium graveolens L'Herit. and application of extract in cigarettes |
| CN106433980A (en) * | 2016-08-28 | 2017-02-22 | 广西灏源盛世生物科技有限公司 | Extraction method of geranium essential oil |
| CN109111993A (en) * | 2018-10-10 | 2019-01-01 | 湖北中烟工业有限责任公司 | A kind of preparation method of the effective component of cigarette wild jujube and its application in cigarette |
| CN110129124A (en) * | 2019-05-07 | 2019-08-16 | 青岛科技大学 | A kind of extracting method of geranium oil |
| CN110684599A (en) * | 2019-10-24 | 2020-01-14 | 江西中烟工业有限责任公司 | Preparation method of azalea absolute oil suitable for cigarettes |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104531356A (en) * | 2015-01-19 | 2015-04-22 | 川渝中烟工业有限责任公司 | Honeyed-sweet additive and electronic cigarette liquid with same |
| CN105062682A (en) * | 2015-08-27 | 2015-11-18 | 湖北中烟工业有限责任公司 | Camphor tree seed cigarette spice and preparation method thereof |
| CN105062682B (en) * | 2015-08-27 | 2019-03-19 | 湖北中烟工业有限责任公司 | A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof |
| CN105272824A (en) * | 2015-11-17 | 2016-01-27 | 鹰潭华宝香精香料有限公司 | Preparation method of natural cinnamomum camphora aromatic material |
| CN105272824B (en) * | 2015-11-17 | 2017-06-30 | 鹰潭华宝香精有限公司 | A kind of preparation method of natural linalool spices |
| CN105581374A (en) * | 2016-03-18 | 2016-05-18 | 云南中烟工业有限责任公司 | Glycerol triacetate extract of pelargonium graveolens L'Herit. and application of extract in cigarettes |
| CN106433980A (en) * | 2016-08-28 | 2017-02-22 | 广西灏源盛世生物科技有限公司 | Extraction method of geranium essential oil |
| CN109111993A (en) * | 2018-10-10 | 2019-01-01 | 湖北中烟工业有限责任公司 | A kind of preparation method of the effective component of cigarette wild jujube and its application in cigarette |
| CN109111993B (en) * | 2018-10-10 | 2022-01-14 | 湖北中烟工业有限责任公司 | Preparation method of wild jujube effective component for cigarettes and application of wild jujube effective component in cigarettes |
| CN110129124A (en) * | 2019-05-07 | 2019-08-16 | 青岛科技大学 | A kind of extracting method of geranium oil |
| CN110684599A (en) * | 2019-10-24 | 2020-01-14 | 江西中烟工业有限责任公司 | Preparation method of azalea absolute oil suitable for cigarettes |
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Application publication date: 20130612 |