CN103405359B - Natural chionanthus retusus flower perfume and preparation method thereof - Google Patents

Natural chionanthus retusus flower perfume and preparation method thereof Download PDF

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CN103405359B
CN103405359B CN201310297312.9A CN201310297312A CN103405359B CN 103405359 B CN103405359 B CN 103405359B CN 201310297312 A CN201310297312 A CN 201310297312A CN 103405359 B CN103405359 B CN 103405359B
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flower
natural
perfume
oil
essential oil
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CN103405359A (en
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尹卫平
刘普
范文瑞
高嘉屿
李欣
牛兰岚
李海迪
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Henan University of Science and Technology
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Henan University of Science and Technology
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Abstract

The invention provides natural chionanthus retusus flower perfume and a preparation method thereof, relating to the perfume. The natural chionanthus retusus flower perfume is composed of following components in parts by volume: 1.4-2.8 parts of chionanthus retusus flower natural essential oil, 0.05-0.12 part of sandalwood essential oil, 0.05-0.13 part of rosemary essential oil, 0.05-0.10 part of tea tree oil, 0.08-0.2 part of geranium essential oil, 0.08-0.17 part of bergamot essential oil, 0.15-0.23 part of sweet orange oil and 96.25-98.14 parts of ethanol with the volume concentration of 95%, wherein all the components are mixed uniformly, and then are aged and filtered to obtain the natural chionanthus retusus flower perfume. The natural chionanthus retusus flower perfume provided by the invention is clear is color and luster, smooth and soft in aroma and reasonable in formula; the dispersion of aromas of all spice components in the perfume is harmonious and stable; a special rich flower aroma of a chionanthus retusus flower is kept; a main aroma of a single flower aroma type perfume is highlighted and the aroma keeping time can be up to 3-5 days.

Description

A kind of natural Diffuse Coptosapelta flower perfume and preparation method thereof
Technical field
The present invention relates to a kind of perfume, be specially a kind of natural Diffuse Coptosapelta flower perfume and preparation method thereof.
Background technology
Chionanthus retusa Lindl et Paxt is Oleaceae Diffuse Coptosapelta platymiscium, defoliation small arbor or shrub, and Chinese Second Class Key Protected Plant, views and admires species for excellent.In time early summer, full tree spends a thousand li drifting fragrance in vain, as covered frost lid snow, luicd and elegant pleasant, suitablely plants in building surrounding, or by Zhong Chi side, park and trade.Diffuse Coptosapelta tender leaf can make beverage for Folium Camelliae sinensis, fruit rich in oil, can extract oil, and for industrial, timber heavily fortified point is heavy careful, can manufacturing appliance.Bud, the leaf of chionanthus retusa Lindl et Paxt also have medical value.Diffuse Coptosapelta is used for folk medicine in medicinal, has the effect of relieving heat and thirst, the tender leaf of Diffuse Coptosapelta and flower among the people make tea to drink also can be used for preventing and treating chronic hepatopathy.Therefore cultivated plant Diffuse Coptosapelta, has Development volue in China.
Spend the volatile oil fragrance of middle extraction pure from Diffuse Coptosapelta, for the typical fragrance of a flower, after measured containing tens kinds of fragrance components, mainly contain benzyl alcohol, phenethanol, p-methoxybenzene ethanol, p-hydroxyphenylethanol, ethyl anisate, trans-(+)-nerolidol, hexyl-benzoate, (E)-2-hexyl-benzoate, myristic aldehyde, farnesol, benzyl benzoate, linalool oxide, eugenol, p-methoxybenzene ethanol, trans-jasmone, a large amount of natural flavoring ingredients such as dehydrogenation ionol, not only can be used as essence but also can be used as natural perfume material application, especially can be used in the preparation of specific single floral type perfume.Current single floral type perfume is mostly the common fragrance of a flower perfume such as Flos Rosae Rugosae, jasmine, and there is not been reported so far with the Diffuse Coptosapelta flower natural single floral type perfume that is main note.
Summary of the invention
Object of the present invention is just to provide one with the Diffuse Coptosapelta fragrance of a flower for main note, natural single floral type Diffuse Coptosapelta flower perfume being equipped with other auxiliary fragrance material and preparation method thereof, prepared perfume fragrance exquisiteness is soft, each spice fragrance distribute harmony, stable, and the main note gas of Diffuse Coptosapelta flower can be given prominence to, guarantor's fragrant time is longer.
To achieve these goals, technical scheme of the present invention is: a kind of natural Diffuse Coptosapelta flower perfume, by volume number meter its consist of: Diffuse Coptosapelta flower natural essential oil 1.4 ~ 2.8 parts, sandalwood essential oil 0.05 ~ 0.12 part, rosemary ethereal oil 0.05 ~ 0.13 part, tea tree oil 0.05 ~ 0.10 part, Geranium Essential 0.08 ~ 0.2 part, Bergamot 0.08 ~ 0.17 part, oleum Citri sinensis 0.15 ~ 0.23 part and volumetric concentration are the ethanol 96.25 ~ 98.14 parts of 95%.
As preferably, Diffuse Coptosapelta flower natural essential oil 2.5 parts, sandalwood essential oil 0.08 part, rosemary ethereal oil 0.08 part, tea tree oil 0.08 part, Geranium Essential 0.15 part, Bergamot 0.14 part, oleum Citri sinensis 0.21 part and volumetric concentration are the ethanol 96.76 parts of 95%.
The preparation method of described natural Diffuse Coptosapelta flower perfume is:
(1), the preparation of natural Diffuse Coptosapelta flower essential oil: spend nature to dry in the shade Diffuse Coptosapelta, pulverize and be placed in distil container, adopt steam distillation distillation 6 ~ 7 hours, gained distillate through extraction, filter after namely obtain natural Diffuse Coptosapelta flower essential oil;
(2), the modulation of perfume: by volume number, get Diffuse Coptosapelta flower natural essential oil 1.4 ~ 2.8 parts, rosemary ethereal oil 0.05 ~ 0.13 part, Geranium Essential 0.08 ~ 0.2 part, Bergamot 0.08 ~ 0.17 part and oleum Citri sinensis 0.15 ~ 0.23 part, above-mentioned spice mix homogeneously is kept in Dark Place 3 ~ 5 days, and then add sandalwood essential oil 0.05 ~ 0.12 part, tea tree oil 0.05 ~ 0.10 part and volumetric concentration are the ethanol 96.25 ~ 98.14 parts of 95%, mixed liquor is obtained after mix homogeneously, above-mentioned mixed liquor is placed 40 ~ 60 days at 0 ~ 5 DEG C, then disgorging is filtered, gained filtrate is natural Diffuse Coptosapelta flower perfume.
Beneficial effect: natural Diffuse Coptosapelta flower perfume color and luster of the present invention is limpid, and fragrance exquisiteness is soft, and formula is reasonable, in perfume, each fragrance component fragrance distributes harmony, stable, remain Diffuse Coptosapelta and spend distinctive foundation for heavy florals breath, highlight the main note taste of single floral type perfume, fragrance remaining time can reach 3 ~ 5 days.In perfume of the present invention, select spice oleum Citri sinensis fragrant as head, add there is happiness, that Bergamot that is nice and cool, aromatic odour is used for modifying head is fragrant.Natural Diffuse Coptosapelta flower essential oil as body note, and comes to be in harmonious proportion body note with Flos Pelargonii and Herba Rosmarini Officinalis, and with the main note taste of outstanding Diffuse Coptosapelta flower, Herba Rosmarini Officinalis also plays antiseptical function simultaneously.Bottom note selects the Lignum Santali Albi of woody note, both remained the Diffuse Coptosapelta fragrance of a flower strong turn increase wooden pure and fresh, form a kind of fresh scent of uniqueness, and the effect of slow-release fragrance is played together with tea tree oil, to coordinate the volatility of each spice, each spice fragrance emission is become slowly, harmonious stable, make perfume fragrance more lasting simultaneously, extend fragrance remaining time.
In addition, in the modulation process of perfume of the present invention, first several spice mixed and preserve, add bottom note spice again and ethanol is fully in harmonious proportion, then ageing is carried out, this can make the fragrant and body note of the head of perfume become in the distributing of fragrance to be connected and to coordinate, and the fragrance of perfume becomes more fine and smooth soft, and fragrance emissions is more stable, lastingly.
Detailed description of the invention
A kind of natural Diffuse Coptosapelta flower perfume, by volume number meter its consist of: Diffuse Coptosapelta flower natural essential oil 1.4 ~ 2.8 parts, sandalwood essential oil 0.05 ~ 0.12 part, rosemary ethereal oil 0.05 ~ 0.13 part, tea tree oil 0.05 ~ 0.10 part, Geranium Essential 0.08 ~ 0.2 part, Bergamot 0.08 ~ 0.17 part, oleum Citri sinensis 0.15 ~ 0.23 part and volumetric concentration are the ethanol 96.25 ~ 98.14 parts of 95%.
The preparation method of described natural Diffuse Coptosapelta flower perfume is:
(1), the preparation of natural Diffuse Coptosapelta flower essential oil: spend nature to dry in the shade Diffuse Coptosapelta, pulverize and be placed in distil container, adopt steam distillation distillation 6 ~ 7 hours, gained distillate through extraction, filter after namely obtain natural Diffuse Coptosapelta flower essential oil;
(2), the modulation of perfume: by volume number, get Diffuse Coptosapelta flower natural essential oil 1.4 ~ 2.8 parts, rosemary ethereal oil 0.05 ~ 0.13 part, Geranium Essential 0.08 ~ 0.2 part, Bergamot 0.08 ~ 0.17 part and oleum Citri sinensis 0.15 ~ 0.23 part, above-mentioned spice mix homogeneously is kept in Dark Place 3 ~ 5 days, and then add sandalwood essential oil 0.05 ~ 0.12 part, tea tree oil 0.05 ~ 0.10 part and volumetric concentration are the ethanol 96.25 ~ 98.14 parts of 95%, mixed liquor is obtained after mix homogeneously, above-mentioned mixed liquor is placed 40 ~ 60 days at 0 ~ 5 DEG C, then disgorging is filtered, gained filtrate is natural Diffuse Coptosapelta flower perfume.
Embodiment 1
A kind of natural Diffuse Coptosapelta flower perfume, by volume number meter its consist of: Diffuse Coptosapelta flower natural essential oil 1.4 parts, sandalwood essential oil 0.05 part, rosemary ethereal oil 0.05 part, tea tree oil 0.05 part, Geranium Essential 0.08 part, Bergamot 0.08 part, oleum Citri sinensis 0.15 part and volumetric concentration are the ethanol 98.14 parts of 95%.
Embodiment 2
A kind of natural Diffuse Coptosapelta flower perfume, by volume number meter its consist of: Diffuse Coptosapelta flower natural essential oil 2.5 parts, sandalwood essential oil 0.08 part, rosemary ethereal oil 0.08 part, tea tree oil 0.08 part, Geranium Essential 0.15 part, Bergamot 0.14 part, oleum Citri sinensis 0.21 part and volumetric concentration are the ethanol 96.76 parts of 95%.
Embodiment 3
A kind of natural Diffuse Coptosapelta flower perfume, by volume number meter its consist of: Diffuse Coptosapelta flower natural essential oil 2.8 parts, sandalwood essential oil 0.12 part, rosemary ethereal oil 0.13 part, tea tree oil 0.1 part, Geranium Essential 0.2 part, Bergamot 0.17 part, oleum Citri sinensis 0.23 part and volumetric concentration are the ethanol 96.25 parts of 95%.
Embodiment 4
A kind of natural Diffuse Coptosapelta flower perfume, by volume number meter its consist of: Diffuse Coptosapelta flower natural essential oil 2.0 parts, sandalwood essential oil 0.1 part, rosemary ethereal oil 0.1 part, tea tree oil 0.1 part, Geranium Essential 0.2 part, Bergamot 0.17 part, oleum Citri sinensis 0.23 part and volumetric concentration are the ethanol 97.1 parts of 95%.

Claims (3)

1. a natural Diffuse Coptosapelta flower perfume, is characterized in that: by volume number meter its consist of: Diffuse Coptosapelta flower natural essential oil 1.4 ~ 2.8 parts, sandalwood essential oil 0.05 ~ 0.12 part, rosemary ethereal oil 0.05 ~ 0.13 part, tea tree oil 0.05 ~ 0.10 part, Geranium Essential 0.08 ~ 0.2 part, Bergamot 0.08 ~ 0.17 part, oleum Citri sinensis 0.15 ~ 0.23 part and volumetric concentration are the ethanol 96.25 ~ 98.14 parts of 95%;
The preparation method of described natural Diffuse Coptosapelta flower perfume is: by volume number, get Diffuse Coptosapelta flower natural essential oil 1.4 ~ 2.8 parts, rosemary ethereal oil 0.05 ~ 0.13 part, Geranium Essential 0.08 ~ 0.2 part, Bergamot 0.08 ~ 0.17 part and oleum Citri sinensis 0.15 ~ 0.23 part, above-mentioned spice mix homogeneously is kept in Dark Place 3 ~ 5 days, and then add sandalwood essential oil 0.05 ~ 0.12 part, tea tree oil 0.05 ~ 0.10 part and volumetric concentration are the ethanol 96.25 ~ 98.14 parts of 95%, mixed liquor is obtained after mix homogeneously, above-mentioned mixed liquor is placed 40 ~ 60 days at 0 ~ 5 DEG C, then disgorging is filtered, gained filtrate is natural Diffuse Coptosapelta flower perfume.
2. a kind of natural Diffuse Coptosapelta flower perfume as claimed in claim 1, is characterized in that: by volume number meter its consist of: Diffuse Coptosapelta flower natural essential oil 2.5 parts, sandalwood essential oil 0.08 part, rosemary ethereal oil 0.08 part, tea tree oil 0.08 part, Geranium Essential 0.15 part, Bergamot 0.14 part, oleum Citri sinensis 0.21 part and volumetric concentration be 95% ethanol 96.76 parts.
3. a kind of natural Diffuse Coptosapelta flower perfume as claimed in claim 1, it is characterized in that: the preparation method of described Diffuse Coptosapelta flower natural essential oil is: spend nature to dry in the shade Diffuse Coptosapelta, pulverize and be placed in distil container, adopt steam distillation distillation 6 ~ 7 hours, namely gained distillate obtains Diffuse Coptosapelta flower natural essential oil after extraction, filtration.
CN201310297312.9A 2013-07-16 2013-07-16 Natural chionanthus retusus flower perfume and preparation method thereof Active CN103405359B (en)

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CN104274369A (en) * 2014-09-28 2015-01-14 青岛康合伟业商贸有限公司 Mixed flower type perfume
CN108117768B (en) * 2017-12-12 2020-04-24 湖北中烟工业有限责任公司 Nano catalytic material for essence package and preparation method and application thereof
CN109248112A (en) * 2018-11-07 2019-01-22 长沙浩然医疗科技有限公司 A kind of lasting refreshing perfume and preparation method thereof
CN109288732A (en) * 2018-11-26 2019-02-01 金玛瑙香水(明光)有限公司 A kind of natural Yilan perfume
CN115322831A (en) * 2022-08-15 2022-11-11 泉州威士登香精香料有限公司 Mint essence with lasting cool feeling release function and preparation method thereof

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