CN108714117B - Long-acting perfume and preparation method thereof - Google Patents
Long-acting perfume and preparation method thereof Download PDFInfo
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- CN108714117B CN108714117B CN201810733761.6A CN201810733761A CN108714117B CN 108714117 B CN108714117 B CN 108714117B CN 201810733761 A CN201810733761 A CN 201810733761A CN 108714117 B CN108714117 B CN 108714117B
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- 239000002304 perfume Substances 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 69
- 239000000341 volatile oil Substances 0.000 claims abstract description 52
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 51
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- CAULGCQHVOVVRN-UHFFFAOYSA-N (3Z,9E)-Germacra-3,7(11),9-trien-6-on Natural products CC(C)=C1CC=C(C)CCC=C(C)CC1=O CAULGCQHVOVVRN-UHFFFAOYSA-N 0.000 claims abstract description 23
- CAULGCQHVOVVRN-SWZPTJTJSA-N (E,E)-germacrone Chemical compound CC(C)=C1C\C=C(C)\CC\C=C(C)\CC1=O CAULGCQHVOVVRN-SWZPTJTJSA-N 0.000 claims abstract description 23
- ZVSZHMFUICOVPY-UHFFFAOYSA-N Germacrone Natural products CC(=C)C1CC=C(/C)CCC=C(/C)CC1=O ZVSZHMFUICOVPY-UHFFFAOYSA-N 0.000 claims abstract description 23
- 241000220317 Rosa Species 0.000 claims abstract description 21
- 235000009508 confectionery Nutrition 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims description 19
- 230000032683 aging Effects 0.000 claims description 10
- 239000012467 final product Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 3
- 239000003205 fragrance Substances 0.000 abstract description 33
- 230000007423 decrease Effects 0.000 abstract description 2
- 238000009776 industrial production Methods 0.000 abstract description 2
- 230000002045 lasting effect Effects 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 9
- 230000014759 maintenance of location Effects 0.000 description 8
- 241000196324 Embryophyta Species 0.000 description 6
- 238000001704 evaporation Methods 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 241001313734 Dictyophora Species 0.000 description 4
- 238000004821 distillation Methods 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 238000000227 grinding Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 241000779599 Malpighia Species 0.000 description 3
- 244000242564 Osmanthus fragrans Species 0.000 description 3
- 235000019083 Osmanthus fragrans Nutrition 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 241000736285 Sphagnum Species 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 241000411851 herbal medicine Species 0.000 description 3
- 238000002791 soaking Methods 0.000 description 3
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 description 2
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 2
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 2
- 235000011613 Pinus brutia Nutrition 0.000 description 2
- 241000018646 Pinus brutia Species 0.000 description 2
- 235000005324 Typha latifolia Nutrition 0.000 description 2
- 239000002250 absorbent Substances 0.000 description 2
- 230000002745 absorbent Effects 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 244000118869 coast club rush Species 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 description 2
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 description 2
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 description 2
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000661 sodium alginate Substances 0.000 description 2
- 235000010413 sodium alginate Nutrition 0.000 description 2
- 229940005550 sodium alginate Drugs 0.000 description 2
- 229940045920 sodium pyrrolidone carboxylate Drugs 0.000 description 2
- HYRLWUFWDYFEES-UHFFFAOYSA-M sodium;2-oxopyrrolidine-1-carboxylate Chemical compound [Na+].[O-]C(=O)N1CCCC1=O HYRLWUFWDYFEES-UHFFFAOYSA-M 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 241000880938 Bryomaltaea obtusifolia Species 0.000 description 1
- 229920001661 Chitosan Polymers 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- 235000011201 Ginkgo Nutrition 0.000 description 1
- 244000194101 Ginkgo biloba Species 0.000 description 1
- 235000008100 Ginkgo biloba Nutrition 0.000 description 1
- 241001669657 Odontobutis Species 0.000 description 1
- 241000881171 Zygodon Species 0.000 description 1
- 229940124532 absorption promoter Drugs 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 229940104299 cimicifugae rhizoma Drugs 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 229930000044 secondary metabolite Natural products 0.000 description 1
- 230000008786 sensory perception of smell Effects 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- -1 terpene hydrocarbons Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9739—Bryophyta [mosses]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a long-acting perfume and a preparation method thereof. The composition comprises the following components in parts by weight: 5-8 parts of rose essential oil, 6-10 parts of iris essential oil, 1-3 parts of germacrone, 30-80 parts of ethanol, 5-10 parts of glycerol and 150 parts of water. The perfume prepared by the invention has sweet fragrance type fragrance, can be stored for a long time, has no fragrance decline, can be sprayed on skin to retain fragrance for more than 3 days, has lasting effect, and solves the problem of short fragrance retaining time commonly existing in the field of perfumes. The preparation method is simple and feasible, and the prepared perfume has stable fragrance and is suitable for large-scale industrial production.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to perfume capable of keeping sweet flower fragrance slowly-released and a preparation method thereof.
Background
Perfume, mainly made by blending plant essential oil and alcohol, the essential oil is a very important secondary metabolite synthesized by the organs of aromatic plants. These oily substances with characteristic fragrance are obtained from flower, leaf, and bark of aromatic plant by steam distillation, squeezing, solvent extraction, adsorption, etc. They are mixtures of many compounds, mainly composed of esters, alcohols, aromatic hydrocarbons, terpene hydrocarbons, ethers, ketones, aldehydes, phenols, and the like.
The perfume prepared from the plant essential oil has the advantages of natural fragrance maintenance, mellow fragrance and inaccurate odor regulation, and has the disadvantages of different flavors and difficult unification due to complex components of the plant essential oil and different preparation methods, and the fragrance substance extracted from the natural plant has short fragrance retention time, generally retains fragrance for 1-3 days and has poor use experience.
Patent 201510219452.3 discloses a pine needle perfume, which comprises the following raw materials by volume: 10-18 parts of pine needle essential oil, 8-15 parts of sweet osmanthus essential oil, 6-8 parts of fructus cnidii essential oil and 70-80 parts of solvent; the solvent consists of 55-65 v% ethanol and 35-45 v% propylene glycol. The perfume can effectively cover the medicinal smell of fructus Cnidii essential oil, but has short fragrance-retaining time and fast fragrance decreasing speed.
Patent 201510576560.6 discloses a perfume for tranquilization, which is prepared from essential oil obtained from Chinese medicinal herbs for tranquilization, ethanol, glycerol, distilled water, sodium alginate, Chinese medicinal herb absorption promoter N-octyl chitosan, hydroxypropyl methylcellulose and sodium pyrrolidone carboxylate; 3-6 parts of essential oil obtained from nerve-soothing Chinese herbal medicines, 15-25 parts of ethanol, 2-5 parts of glycerol, 95-105 parts of distilled water, 1-3 parts of sodium alginate, 0.5-1.5 parts of Chinese herbal medicine absorbent, 0.5-1.5 parts of hydroxypropyl methyl cellulose and 3-6 parts of sodium pyrrolidone carboxylate; the tranquilizing Chinese herbal medicine is prepared from folium Ginkgo, lignum Aquilariae Resinatum, rhizoma Gastrodiae, fructus Schisandrae chinensis, fructus Gardeniae, pericarpium Citri Tangerinae, herba Cymbopogonis Cistanchis, cimicifugae rhizoma, herba Pileae Scriptae, flos Osmanthi Fragrantis, herba Potentillae Discoloris, rhizoma Polygoni Cuspidati, Coptidis rhizoma, caulis Polygoni Multiflori, Saviae Miltiorrhizae radix, and herba Menthae. The perfume has the effect of soothing the nerves, but the raw material components are complex, and the original smell is strong in irritation.
Disclosure of Invention
The invention aims to provide a long-acting perfume and a preparation method thereof.
The long-acting perfume comprises the following components in parts by weight: 5-8 parts of rose essential oil, 6-10 parts of iris essential oil, 1-3 parts of germacrone, 30-80 parts of ethanol, 5-10 parts of glycerol and 150 parts of water.
The long-acting perfume has sweet floral type fragrance.
The long-acting perfume also comprises 3-8 parts of a dictyophora blume extract.
The extraction method of the dictyophora blume extract comprises the following steps: taking the sphagnum crenatum, drying in the sun, grinding into coarse powder, putting into a distillation container, adding 3-8 times of water by weight, and infiltrating for 0.5-2 hours; heating rapidly to boil, maintaining for 10-40min, connecting reflux condenser tube, collecting condensate to obtain distillate, and evaporating distillate to obtain powdery substance.
The long-acting perfume also comprises 1-3 parts of cangzhinone.
The preparation method of the long-acting perfume comprises the following steps:
(1) under the condition of room temperature, taking 5-8 parts of rose essential oil and 6-10 parts of iris essential oil by weight, and dissolving in 30-80 parts of ethanol;
(2) adding 5-10 parts of glycerol and 150 parts of water, and stirring for 20-30 min;
(3) adding 1-3 parts of germacrone, stirring for 20-30min, placing in a sealed container, and aging for 25-35 days to obtain the final product.
3-8 parts of a dictyophora blume extract is also added in the step (1).
1-3 parts of canodoketone is also added in the step (2).
The invention has the beneficial effects that: the perfume prepared by the invention has sweet fragrance type fragrance, can be stored for a long time, has no fragrance decline, can be sprayed on skin to retain fragrance for more than 3 days, has lasting effect, and solves the problem of short fragrance retaining time commonly existing in the field of perfumes. The preparation method is simple and feasible, and the prepared perfume has stable fragrance and is suitable for large-scale industrial production.
Detailed Description
The present invention is further illustrated by the following specific examples.
Example 1
The long-acting perfume comprises the following components in parts by weight: 6g of rose essential oil, 8g of iris essential oil, 2g of germacrone, 50g of ethanol, 8g of glycerol and 120g of water.
The preparation method of the long-acting perfume comprises the following steps:
(1) dissolving 6g of rose essential oil and 8g of iris essential oil in 50g of ethanol at room temperature according to parts by weight;
(2) adding 8g of glycerol and 120g of water, and stirring for 25 min;
(3) adding 2g of germacrone, stirring for 25min, placing into a sealed container, and aging for 30 days to obtain the product.
Example 2
The long-acting perfume comprises the following components in parts by weight: 5g of rose essential oil, 6g of iris essential oil, 1g of germacrone, 30g of ethanol, 5g of glycerol and 100g of water.
The preparation method of the long-acting perfume comprises the following steps:
(1) under the condition of room temperature, taking 5g of rose essential oil and 6g of iris essential oil according to parts by weight, and dissolving in 30g of ethanol;
(2) adding 5g of glycerol and 100g of water, and stirring for 20 min;
(3) adding germacrone 1g, stirring for 20min, placing in a sealed container, aging for 25 days, and making into the final product.
Example 3
The long-acting perfume comprises the following components in parts by weight: 8g of rose essential oil, 10g of iris essential oil, 3g of germacrone, 80g of ethanol, 10g of glycerol and 150g of water.
The preparation method of the long-acting perfume comprises the following steps:
(1) under the condition of room temperature, taking 8g of rose essential oil and 10g of iris essential oil according to parts by weight, and dissolving in 80g of ethanol;
(2) adding 10g of glycerol and 150g of water, and stirring for 30 min;
(3) adding germacrone 3g, stirring for 30min, placing in a sealed container, aging for 35 days, and making into the final product.
Example 4
The long-acting perfume comprises the following components in parts by weight: 6g of rose essential oil, 8g of iris essential oil, 2g of germacrone, 50g of ethanol, 8g of glycerol, 5g of odontophyllum dulcis extract and 120g of water.
The extraction method of the dictyophora blume extract comprises the following steps: taking the sphagnum crenatum (Zygodon obtusifolius hook.), drying in the sun, grinding into coarse powder, putting into a distillation container, adding 5 times of water by weight, and soaking for 1 hour; heating rapidly to boil, maintaining for 30min, connecting reflux condenser tube, collecting condensate to obtain distillate, and evaporating distillate to obtain powdery substance.
The preparation method of the long-acting perfume comprises the following steps:
(1) dissolving 6g of rose essential oil, 8g of iris essential oil and 5g of sphagnum blume extract in 50g of ethanol at room temperature according to parts by weight;
(2) adding 8g of glycerol and 120g of water, and stirring for 25 min;
(3) adding 2g of germacrone, stirring for 25min, placing into a sealed container, and aging for 30 days to obtain the product.
Example 5
The long-acting perfume comprises the following components in parts by weight: 6g of rose essential oil, 8g of iris essential oil, 2g of germacrone, 50g of ethanol, 8g of glycerol, 5g of odontobutis brevicaulis extract and 120g of water.
The extraction method of the malpighia brevicaulis extract comprises the following steps: taking short-dentate malpighia (Zygodon brevicetus wils. ex mitt.), drying in the sun, grinding into coarse powder, placing in a distillation container, adding 5 times of water by weight, and soaking for 1 hour; heating rapidly to boil, maintaining for 30min, connecting reflux condenser tube, collecting condensate to obtain distillate, and evaporating distillate to obtain powdery substance.
The preparation method of the long-acting perfume comprises the following steps:
(1) dissolving 6g of rose essential oil, 8g of iris essential oil and 5g of malpighia brevicaulis extract in 50g of ethanol at room temperature according to parts by weight;
(2) adding 8g of glycerol and 120g of water, and stirring for 25 min;
(3) adding 2g of germacrone, stirring for 25min, placing into a sealed container, and aging for 30 days to obtain the product.
Example 6
The long-acting perfume comprises the following components in parts by weight: 6g of rose essential oil, 8g of iris essential oil, 2g of germacrone, 2g of canodoxolone, 50g of ethanol, 8g of glycerol and 120g of water.
The preparation method of the long-acting perfume comprises the following steps:
(1) dissolving 6g of rose essential oil and 8g of iris essential oil in 50g of ethanol at room temperature according to parts by weight;
(2) adding 8g of glycerol, 2g of cangzhinone and 120g of water, and stirring for 25 min;
(3) adding 2g of germacrone, stirring for 25min, placing into a sealed container, and aging for 30 days to obtain the product.
Example 7
The long-acting perfume comprises the following components in parts by weight: 6g of rose essential oil, 8g of iris essential oil, 2g of germacrone, 50g of ethanol, 8g of glycerol, 5g of bulrush extract and 120g of water.
The extraction method of the burley wood extract comprises the following steps: taking brevifolius (Breedeyera microphylla (Griseb.) Hieron), drying in the sun, grinding into coarse powder, placing in a distillation container, adding 5 times of water by weight, and soaking for 1 hour; heating rapidly to boil, maintaining for 30min, connecting reflux condenser tube, collecting condensate to obtain distillate, and evaporating distillate to obtain powdery substance.
The preparation method of the long-acting perfume comprises the following steps:
(1) dissolving 6g of rose essential oil, 8g of iris essential oil and 5g of bulrush extract in 50g of ethanol at room temperature according to parts by weight;
(2) adding 8g of glycerol and 120g of water, and stirring for 25 min;
(3) adding 2g of germacrone, stirring for 25min, placing into a sealed container, and aging for 30 days to obtain the product.
Comparative example 1
The long-acting perfume comprises the following components in parts by weight: 6g of rose essential oil, 8g of iris essential oil, 50g of ethanol, 8g of glycerol and 120g of water.
The preparation method of the long-acting perfume comprises the following steps:
(1) dissolving 6g of rose essential oil and 8g of iris essential oil in 50g of ethanol at room temperature according to parts by weight;
(2) adding glycerol 8g and water 120g, stirring for 25min, placing in a sealed container, and aging for 30 days to obtain the final product.
Experimental example 1: aroma duration evaluation method
A weight loss method: the absorbent paper with the weight of 264g per square meter is used as a supporter, the supporter is cut into strips with the length of 15.0 multiplied by 1.0cm, and the positions 2.0cm away from the front ends of the strips are wetted by the liquid to be measured. And weighing the scented paper by using an accurate analytical balance after every 30min, and calculating the volatilization amount of the perfume in unit volume. The results of the experiment are shown in table 1:
TABLE 1 perfume volatile amount per unit volume (g/mL)
Note: represents P <0.05 compared to the example 1 group.
As can be seen from Table 1, the perfumes of examples 1-3 have equivalent volatilization amounts which are higher than those of comparative example 1, and the comparative example 1 has the same conditions as the comparative example 1, only the addition of the germacrone in the comparative example 1 is less, so that the germacrone has good fragrance retention effect; the perfume of example 4, example 6 and example 7 has a significantly lower evaporation rate than that of example 1, and the perfume of example 5 has an evaporation rate equivalent to that of example 1.
Olfaction method: selecting 15 fragrance smelling persons, wherein the group of fragrance smelling persons are screened by a fragrance smelling experiment in advance, and can easily distinguish deionized water, acetic acid with the mass concentration of 1% and 1% beta-phenylethyl alcohol, so that the persons can smell and distinguish osmanthus fragrans essence ethanol solution dropped on fragrance smelling paper at intervals in rooms with the same temperature and humidity conditions until the fragrance disappears, namely the retention time of the osmanthus fragrans essence fragrance. The results of the experiment are shown in table 2:
TABLE 2 determination of perfume fragrance retention time by sniffing
Note: represents P <0.05 compared to the example 1 group; p < 0.01.
As can be seen from Table 2, the perfume fragrance retention time of the perfumes of the examples 1-3 is equivalent and is remarkably higher than that of the perfume of the comparative example 1(P <0.01), compared with the perfume of the comparative example 1, the perfume of the comparative example 1 has the same conditions, only the perfume of the comparative example 1 is added with little germacrone, and the fact that the germacrone has good fragrance retention effect is proved; the perfume of example 4, example 6 and example 7 has a significantly higher fragrance retention time than example 1, and the perfume of example 5 has a fragrance retention time comparable to example 1.
Claims (3)
1. The long-acting perfume is characterized by comprising the following components in parts by weight: 5-8 parts of rose essential oil, 6-10 parts of iris essential oil, 1-3 parts of germacrone, 30-80 parts of ethanol, 5-10 parts of glycerol and 150 parts of water.
2. The long-acting perfume of claim 1, wherein the long-acting perfume has a sweet floral scent.
3. A process for the preparation of a long-acting perfume according to claim 1, characterized in that it is carried out according to the following steps:
(1) under the condition of room temperature, taking 5-8 parts of rose essential oil and 6-10 parts of iris essential oil by weight, and dissolving in 30-80 parts of ethanol;
(2) adding 5-10 parts of glycerol and 150 parts of water, and stirring for 20-30 min;
(3) adding 1-3 parts of germacrone, stirring for 20-30min, placing in a sealed container, and aging for 25-35 days to obtain the final product.
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| CN112891259B (en) * | 2021-02-25 | 2022-09-30 | 蔓莎(苏州)工艺制品有限公司 | Plant perfume and preparation method thereof |
| CN113893195A (en) * | 2021-10-27 | 2022-01-07 | 海南省守护者科技有限公司 | Perfume with fatigue relieving effect and preparation method thereof |
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| CN101817806A (en) * | 2010-05-13 | 2010-09-01 | 苏州派腾生物医药科技有限公司 | Method for preparing atractylon |
| CN102058568A (en) * | 2010-12-24 | 2011-05-18 | 海南碧凯药业有限公司 | Application of germacrone |
| JP2012001467A (en) * | 2010-06-15 | 2012-01-05 | Naris Cosmetics Co Ltd | Skin external preparation |
| CN102763692A (en) * | 2012-08-15 | 2012-11-07 | 李国� | Mosquito-repellent incense |
| CN105237378A (en) * | 2015-09-30 | 2016-01-13 | 浙江工业大学 | Method for separating germacrone from Curcuma wenyujin volatile oil |
| CN106491398A (en) * | 2016-11-07 | 2017-03-15 | 广西大学 | Slow release long-acting perfume and preparation method thereof |
| CN106580746A (en) * | 2016-12-24 | 2017-04-26 | 杭州心悦化妆品有限公司 | Perfume with long fragrance holding time |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1916307B1 (en) * | 2001-09-17 | 2014-02-26 | Dafra Pharma Research & Development BVBA | Plant enzymes for bioconversion |
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