CN108714117A - A kind of long-acting perfume and preparation method thereof - Google Patents
A kind of long-acting perfume and preparation method thereof Download PDFInfo
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- CN108714117A CN108714117A CN201810733761.6A CN201810733761A CN108714117A CN 108714117 A CN108714117 A CN 108714117A CN 201810733761 A CN201810733761 A CN 201810733761A CN 108714117 A CN108714117 A CN 108714117A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- 239000000341 volatile oil Substances 0.000 claims abstract description 51
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 47
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 46
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 29
- 235000019441 ethanol Nutrition 0.000 claims abstract description 27
- CAULGCQHVOVVRN-UHFFFAOYSA-N (3Z,9E)-Germacra-3,7(11),9-trien-6-on Natural products CC(C)=C1CC=C(C)CCC=C(C)CC1=O CAULGCQHVOVVRN-UHFFFAOYSA-N 0.000 claims abstract description 23
- CAULGCQHVOVVRN-SWZPTJTJSA-N (E,E)-germacrone Chemical compound CC(C)=C1C\C=C(C)\CC\C=C(C)\CC1=O CAULGCQHVOVVRN-SWZPTJTJSA-N 0.000 claims abstract description 23
- ZVSZHMFUICOVPY-UHFFFAOYSA-N Germacrone Natural products CC(=C)C1CC=C(/C)CCC=C(/C)CC1=O ZVSZHMFUICOVPY-UHFFFAOYSA-N 0.000 claims abstract description 23
- 235000011187 glycerol Nutrition 0.000 claims abstract description 23
- 239000003205 fragrance Substances 0.000 claims abstract description 22
- 241000220317 Rosa Species 0.000 claims abstract description 21
- 235000009508 confectionery Nutrition 0.000 claims abstract description 5
- 241001122767 Theaceae Species 0.000 claims abstract 2
- 238000003756 stirring Methods 0.000 claims description 19
- 239000000284 extract Substances 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 11
- 238000007789 sealing Methods 0.000 claims description 10
- 150000002576 ketones Chemical class 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 5
- 238000004821 distillation Methods 0.000 claims description 5
- 238000010992 reflux Methods 0.000 claims description 5
- 239000000126 substance Substances 0.000 claims description 5
- 230000002045 lasting effect Effects 0.000 abstract description 7
- -1 can long storage Substances 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 230000007423 decrease Effects 0.000 abstract description 2
- 238000009776 industrial production Methods 0.000 abstract description 2
- 238000003860 storage Methods 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 7
- 241000196324 Embryophyta Species 0.000 description 5
- 241000411851 herbal medicine Species 0.000 description 5
- 230000002936 tranquilizing effect Effects 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 230000035943 smell Effects 0.000 description 4
- 239000002023 wood Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 235000019082 Osmanthus Nutrition 0.000 description 3
- 241000333181 Osmanthus Species 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 244000269722 Thea sinensis Species 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 description 2
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 2
- 235000011613 Pinus brutia Nutrition 0.000 description 2
- 241000018646 Pinus brutia Species 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 description 2
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 description 2
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 description 2
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000661 sodium alginate Substances 0.000 description 2
- 235000010413 sodium alginate Nutrition 0.000 description 2
- 229940005550 sodium alginate Drugs 0.000 description 2
- 241000271309 Aquilaria crassna Species 0.000 description 1
- 241000734626 Bredemeyera microphylla Species 0.000 description 1
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- 229920001661 Chitosan Polymers 0.000 description 1
- 241000005787 Cistanche Species 0.000 description 1
- 244000247747 Coptis groenlandica Species 0.000 description 1
- 235000002991 Coptis groenlandica Nutrition 0.000 description 1
- 241001643874 Cymbopogon distans Species 0.000 description 1
- 244000111489 Gardenia augusta Species 0.000 description 1
- 235000018958 Gardenia augusta Nutrition 0.000 description 1
- 235000011201 Ginkgo Nutrition 0.000 description 1
- 244000194101 Ginkgo biloba Species 0.000 description 1
- 235000008100 Ginkgo biloba Nutrition 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 244000242564 Osmanthus fragrans Species 0.000 description 1
- 235000019083 Osmanthus fragrans Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 244000292697 Polygonum aviculare Species 0.000 description 1
- 235000006386 Polygonum aviculare Nutrition 0.000 description 1
- 244000153955 Reynoutria sachalinensis Species 0.000 description 1
- 235000003202 Reynoutria sachalinensis Nutrition 0.000 description 1
- 240000006079 Schisandra chinensis Species 0.000 description 1
- 235000008422 Schisandra chinensis Nutrition 0.000 description 1
- 241000881171 Zygodon Species 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 230000008365 organ synthesis Effects 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 150000004040 pyrrolidinones Chemical class 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 229930000044 secondary metabolite Natural products 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 230000002459 sustained effect Effects 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 208000016261 weight loss Diseases 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9739—Bryophyta [mosses]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of long-acting perfumes and preparation method thereof.Include the component of following parts by weight：5-8 parts of rose ethereal oil, 6-10 parts of iris flower essential oil, 1-3 parts of germacrone, 30-80 parts of ethyl alcohol, 5-10 parts of glycerine, 100-150 parts of water.Perfume prepared by the present invention has sweet tea floral type fragrance, can long storage, fragrance do not decline, be sprayed onto on skin can lasting 3 days or more, effect is lasting, solves the problems, such as that the fragrance remaining time of perfume area generally existing is short.Preparation method is simple by the present invention, and the perfume odor type of preparation is stablized, and large-scale industrial production is suitble to.
Description
Technical field
The invention belongs to cosmetic technical fields, and in particular to it is a kind of can keep the sweet tea fragrance of a flower be sustained perfume and its preparation side
Method.
Background technology
Perfume is mainly made of plants essential oil and alcohol reconciliation, essential oil be the organ synthesis of fragrant plant it is a kind of very
Important secondary metabolite.The positions such as flower, leaf, skin from fragrant plant extract by steam distillation, squeezing method, solvent
It follows the example of, the means such as the absorption method oily mater with characteristic perfume that obtains these.They are the mixtures of many compounds, mainly
By material compositions such as esters, alcohols, arene, terpene hydrocarbons, ethers, ketone, aldehydes and phenols.
Plants essential oil prepares the advantages of perfume and is to maintain natural fragrance, and fragrance is mellow, the disadvantage is that smell adjust it is inaccurate,
Due to the complicated component of plants essential oil, the difference of each preparation method causes the taste of fragrance variant, it is difficult to and it is unified, in addition,
The fragrance matter fragrance remaining time of extracted form natural plant is short, and general lasting 1-3 days, usage experience is poor.
Patent 201510219452.3 discloses a kind of pine needle perfume, includes the raw material composition of following volumes part：Pine needle essence
10-18 parts oily, 8-15 parts of osmanthus essential oil, 6-8 parts of frutus cnidii essential oil, 70-80 parts of solvent；The solvent is by 55-65v% ethyl alcohol
It is formed with 35-45v% propylene glycol.Although the perfume can effectively cover the flavour of a drug of frutus cnidii essential oil, fragrance remaining time is short, fragrant
Taste decline rate is fast.
Patent 201510576560.6 discloses a kind of tranquilizing the mind perfume, essential oil that raw material is obtained by tranquilizing the mind Chinese herbal medicine, ethyl alcohol,
Glycerine, distilled water, sodium alginate, Chinese herbal medicine absorption enhancers N- octyls chitosan, hydroxypropyl methyl cellulose and pyrrolidones
Carboxylic acid sodium is constituted；- 6 parts by weight of 3 parts by weight of essential oil of tranquilizing the mind Chinese herbal medicine acquisition, -25 parts by weight of 15 parts by weight of ethyl alcohol, glycerine 2
- 5 parts by weight of parts by weight, -105 parts by weight of 95 parts by weight of distilled water, -3 parts by weight of 1 parts by weight of sodium alginate, Chinese herbal medicine promote to absorb
- 1.5 parts by weight of 0.5 parts by weight of agent, -1.5 parts by weight of 0.5 parts by weight of hydroxypropyl methyl cellulose, pyrrolidone sodium carboxylate 3-6
Part；The raw material of the tranquilizing the mind Chinese herbal medicine is by ginkgo leaf, agalloch eaglewood, Rhizoma Gastrodiae, Schisandra chinensis, cape jasmine, dried orange peel, cymbopogon distans, Herba Cistanches, liter
Fiber crops, bean cotyledon perfume, sweet osmanthus, night fragrant flower, giant knotweed, the coptis, the vine of multiflower knotweed, Radix Salviae Miltiorrhizae, peppermint are constituted.Although the perfume has the effect of tranquilizing the mind,
But its material composition is complicated, it is just stronger with feeling Odor stimulation.
Invention content
The purpose of the present invention is to provide a kind of long-acting perfumes and preparation method thereof.
A kind of long-acting perfume includes the component of following parts by weight：5-8 parts of rose ethereal oil, 6-10 parts of iris flower essential oil,
1-3 parts of germacrone, 30-80 parts of ethyl alcohol, 5-10 parts of glycerine, 100-150 parts of water.
The long-acting perfume has sweet tea floral type fragrance.
The long-acting perfume further includes that blunt leaf becomes 3-8 parts of tooth moss extract.
The blunt leaf become the extracting method of tooth moss extract into：It takes blunt leaf to become tooth moss, dries, it is coarse powder to beat, and is placed in distillation
In container, add the water of 3-8 times of parts by weight, infiltrates 0.5-2 hours；Boiling is quickly heated up to, 10-40min, connection reflux are kept
Condenser pipe collects condensate liquid, obtains distillate, is evaporated distillate, obtain powdered substance, is made.
The long-acting perfume further includes 1-3 parts of storehouse art ketone.
The preparation method of above-mentioned long-acting perfume carries out in accordance with the following steps：
(1) at ambient temperature, according to parts by weight, 5-8 parts of rose ethereal oil, 6-10 parts of iris flower essential oil, dissolving are taken
In 30-80 parts of ethyl alcohol；
(2) 5-10 parts of glycerine is added, 100-150 parts of water stirs 20-30min；
(3) 1-3 parts of germacrone is added, stirs 20-30min, is put into sealing container, is aged 25-35 days, is made.
It is additionally added blunt leaf in step (1) and becomes 3-8 parts of tooth moss extract.
1-3 parts of storehouse art ketone is additionally added in step (2).
Beneficial effects of the present invention：Perfume prepared by the present invention has sweet tea floral type fragrance, can long storage, fragrance do not subtract
Move back, be sprayed onto on skin can lasting 3 days or more, effect is lasting, and the fragrance remaining time for solving perfume area generally existing short is asked
Topic.Preparation method is simple by the present invention, and the perfume odor type of preparation is stablized, and large-scale industrial production is suitble to.
Specific implementation mode
With reference to specific embodiment, the present invention will be further described.
Embodiment 1
A kind of long-acting perfume includes the component of following parts by weight：Rose ethereal oil 6g, iris flower essential oil 8g, germacrone
2g, ethyl alcohol 50g, glycerine 8g, water 120g.
The preparation method of above-mentioned long-acting perfume carries out in accordance with the following steps：
(1) at ambient temperature, according to parts by weight, rose ethereal oil 6g, iris flower essential oil 8g is taken to be dissolved in 50g second
In alcohol；
(2) glycerine 8g, water 120g is added, stirs 25min；
(3) germacrone 2g is added, stirs 25min, is put into sealing container, is aged 30 days, is made.
Embodiment 2
A kind of long-acting perfume includes the component of following parts by weight：Rose ethereal oil 5g, iris flower essential oil 6g, germacrone
1g, ethyl alcohol 30g, glycerine 5g, water 100g.
The preparation method of above-mentioned long-acting perfume carries out in accordance with the following steps：
(1) at ambient temperature, according to parts by weight, rose ethereal oil 5g, iris flower essential oil 6g is taken to be dissolved in 30g second
In alcohol；
(2) glycerine 5g, water 100g is added, stirs 20min；
(3) germacrone 1g is added, stirs 20min, is put into sealing container, is aged 25 days, is made.
Embodiment 3
A kind of long-acting perfume includes the component of following parts by weight：Rose ethereal oil 8g, iris flower essential oil 10g, germacrone
3g, ethyl alcohol 80g, glycerine 10g, water 150g.
The preparation method of above-mentioned long-acting perfume carries out in accordance with the following steps：
(1) at ambient temperature, according to parts by weight, rose ethereal oil 8g, iris flower essential oil 10g is taken to be dissolved in 80g second
In alcohol；
(2) glycerine 10g, water 150g is added, stirs 30min；
(3) germacrone 3g is added, stirs 30min, is put into sealing container, is aged 35 days, is made.
Embodiment 4
A kind of long-acting perfume includes the component of following parts by weight：Rose ethereal oil 6g, iris flower essential oil 8g, germacrone
2g, ethyl alcohol 50g, glycerine 8g, blunt leaf become tooth moss extract 5g, water 120g.
The blunt leaf become the extracting method of tooth moss extract into：Blunt leaf is taken to become tooth moss (Zygodon obtusifolius
Hook.), dry, it is coarse powder to beat, and is placed in distillation container, adds the water of 5 times of parts by weight, infiltrates 1 hour；Quickly heat up to boiling
It rises, 30min, connection reflux condensing tube is kept to collect condensate liquid, obtain distillate, be evaporated distillate, obtain powdered substance, make
At.
The preparation method of above-mentioned long-acting perfume carries out in accordance with the following steps：
(1) at ambient temperature, according to parts by weight, rose ethereal oil 6g, iris flower essential oil 8g, blunt leaf is taken to become tooth moss and carry
Object 5g is taken, is dissolved in 50g ethyl alcohol；
(2) glycerine 8g, water 120g is added, stirs 25min；
(3) germacrone 2g is added, stirs 25min, is put into sealing container, is aged 30 days, is made.
Embodiment 5
A kind of long-acting perfume includes the component of following parts by weight：Rose ethereal oil 6g, iris flower essential oil 8g, germacrone
2g, ethyl alcohol 50g, glycerine 8g, short tooth become tooth moss extract 5g, water 120g.
The short tooth become the extracting method of tooth moss extract into：Short tooth is taken to become tooth moss (Zygodon brevisetus
Wils.ex mitt.), it dries, it is coarse powder to beat, and is placed in distillation container, adds the water of 5 times of parts by weight, infiltrates 1 hour；Quickly
It is heated to boiling, 30min, connection reflux condensing tube is kept to collect condensate liquid, obtain distillate, be evaporated distillate, obtain powder
Shape substance, is made.
The preparation method of above-mentioned long-acting perfume carries out in accordance with the following steps：
(1) at ambient temperature, according to parts by weight, rose ethereal oil 6g, iris flower essential oil 8g, short tooth is taken to become tooth moss and carry
Object 5g is taken, is dissolved in 50g ethyl alcohol；
(2) glycerine 8g, water 120g is added, stirs 25min；
(3) germacrone 2g is added, stirs 25min, is put into sealing container, is aged 30 days, is made.
Embodiment 6
A kind of long-acting perfume includes the component of following parts by weight：Rose ethereal oil 6g, iris flower essential oil 8g, germacrone
2g, storehouse art ketone 2g, ethyl alcohol 50g, glycerine 8g, water 120g.
The preparation method of above-mentioned long-acting perfume carries out in accordance with the following steps：
(1) at ambient temperature, according to parts by weight, rose ethereal oil 6g, iris flower essential oil 8g is taken to be dissolved in 50g second
In alcohol；
(2) glycerine 8g, storehouse art ketone 2g, water 120g is added, stirs 25min；
(3) germacrone 2g is added, stirs 25min, is put into sealing container, is aged 30 days, is made.
Embodiment 7
A kind of long-acting perfume includes the component of following parts by weight：Rose ethereal oil 6g, iris flower essential oil 8g, germacrone
2g, ethyl alcohol 50g, glycerine 8g, leaflet mine-laying wood extract 5g, water 120g.
The extracting method of the leaflet mine-laying wood extract is：Take leaflet mine-laying wood (Bredemeyera microphylla
(Griseb.) Hieron), it dries, it is coarse powder to beat, and is placed in distillation container, adds the water of 5 times of parts by weight, infiltrates 1 hour；Soon
Speed is heated to boiling, and 30min, connection reflux condensing tube is kept to collect condensate liquid, obtain distillate, be evaporated distillate, obtain powder
Last shape substance, is made.
The preparation method of above-mentioned long-acting perfume carries out in accordance with the following steps：
(1) at ambient temperature, according to parts by weight, rose ethereal oil 6g, iris flower essential oil 8g, leaflet mine-laying wood is taken to carry
Object 5g is taken, is dissolved in 50g ethyl alcohol；
(2) glycerine 8g, water 120g is added, stirs 25min；
(3) germacrone 2g is added, stirs 25min, is put into sealing container, is aged 30 days, is made.
Comparative example 1
A kind of long-acting perfume includes the component of following parts by weight：Rose ethereal oil 6g, iris flower essential oil 8g, ethyl alcohol
50g, glycerine 8g, water 120g.
The preparation method of above-mentioned long-acting perfume carries out in accordance with the following steps：
(1) at ambient temperature, according to parts by weight, rose ethereal oil 6g, iris flower essential oil 8g is taken to be dissolved in 50g second
In alcohol；
(2) glycerine 8g, water 120g is added, stirs 25min, is put into sealing container, is aged 30 days, is made.
Experimental example 1：Perfume substantiation evaluation method
Weight-loss method：It uses the blotting paper of every weight per square meter 264g as carrier, the paper slip of 15.0 × 1.0cm is cut into, by paper slip
It is soaked with testing liquid at the 2.0cm of front end.After 30min Wen Xiangzhi, unit of account volume are weighed with accurate assay balance
Interior volatilizing perfume amount.Experimental result is as shown in table 1：
Volatilizing perfume amount (g/mL) in 1 unit volume of table
Note：* the P compared with 1 group of embodiment is represented<0.05.
As can be seen from Table 1, the volatilizing perfume amount of embodiment 1-3 is suitable, is above comparative example 1, comparative example 1 and embodiment
1 compares, and other conditions are identical, and only comparative example 1 adds germacrone less, it was demonstrated that germacrone has good lasting effect；
The volatilizing perfume amount of embodiment 4, embodiment 6 and embodiment 7 is substantially less than embodiment 1, volatilizing perfume amount and the implementation of embodiment 5
Example 1 is suitable.
Smell the method for distinguishing：15 Wen Xiang personnel are chosen, this group is heard fragrant personnel and is all crossed in advance by hearing fragrant experiment screening, he
Can tell easily deionized water, mass concentration be 1% acetic acid and 1% bata-phenethyl alcohol, allow they respectively temperature,
In the identical room of damp condition, smell distinguishing to hearing dripped osmanthus flower fragrance ethanol solution on fragrant paper at regular intervals, until
Fragrance disappears, as osmanthus essential oil fragrance retention time.Experimental result is as shown in table 2：
Table 2 smells method of distinguishing and measures perfume fragrance remaining time
Note：* the P compared with 1 group of embodiment is represented<0.05；**P<0.01.
As can be seen from Table 2, the perfume fragrance remaining time of embodiment 1-3 is suitable, is all remarkably higher than 1 (P of comparative example<0.01),
Compared with Example 1, other conditions are identical for comparative example 1, and only comparative example 1 adds germacrone less, it was demonstrated that germacrone has
Good lasting effect；The perfume fragrance remaining time of embodiment 4, embodiment 6 and embodiment 7 is significantly higher than embodiment 1, embodiment 5
Perfume fragrance remaining time and embodiment 1 it is suitable.
Claims (8)
1. a kind of long-acting perfume, which is characterized in that include the component of following parts by weight：5-8 parts of rose ethereal oil, iris anthosin
It is 6-10 parts oily, 1-3 parts of germacrone, 30-80 parts of ethyl alcohol, 5-10 parts of glycerine, 100-150 parts of water.
2. long-acting perfume according to claim 1, which is characterized in that the long-acting perfume has sweet tea floral type fragrance.
3. long-acting perfume according to claim 1, which is characterized in that the long-acting perfume further includes that blunt leaf becomes tooth moss extract
3-8 parts.
4. long-acting perfume according to claim 1, which is characterized in that the blunt leaf become the extracting method of tooth moss extract into：
It takes blunt leaf to become tooth moss, dries, it is coarse powder to beat, and is placed in distillation container, adds the water of 3-8 times of parts by weight, infiltrates 0.5-2 hours；
Boiling is quickly heated up to, 10-40min, connection reflux condensing tube is kept to collect condensate liquid, obtain distillate, be evaporated distillate, obtain
To powdered substance, it is made.
5. long-acting perfume according to claim 1, which is characterized in that the long-acting perfume further includes 1-3 parts of storehouse art ketone.
6. the preparation method of long-acting perfume described in claim 1, which is characterized in that carry out in accordance with the following steps：
(1) at ambient temperature, according to parts by weight, 5-8 parts of rose ethereal oil, 6-10 parts of iris flower essential oil is taken to be dissolved in 30-
In 80 parts of ethyl alcohol；
(2) 5-10 parts of glycerine is added, 100-150 parts of water stirs 20-30min；
(3) 1-3 parts of germacrone is added, stirs 20-30min, is put into sealing container, is aged 25-35 days, is made.
7. the preparation method of long-acting perfume according to claim 1, which is characterized in that be additionally added blunt leaf in step (1) and become tooth
3-8 parts of moss extract.
8. the preparation method of long-acting perfume according to claim 1, which is characterized in that be additionally added storehouse art ketone 1-3 in step (2)
Part.
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