CN103405360B - Natural syringa microphylla flower perfume - Google Patents
Natural syringa microphylla flower perfume Download PDFInfo
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- CN103405360B CN103405360B CN201310297440.3A CN201310297440A CN103405360B CN 103405360 B CN103405360 B CN 103405360B CN 201310297440 A CN201310297440 A CN 201310297440A CN 103405360 B CN103405360 B CN 103405360B
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Abstract
The invention provides natural syringa microphylla flower perfume and relates to single flower aroma type natural syringa microphylla flower perfume. The natural syringa microphylla flower perfume is composed of the following components in parts by volume: 0.9-4.5 parts of syringa microphylla natural essential oil, 0.07-0.4 part of sweet orange oil, 0.05-0.33 part of geranium essential oil, 0.05-0.33 part of rosemary essential oil, 0.05-0.33 part of tea tree oil, 0.09-0.45 part of sandalwood essential oil and 93.66-98.79 parts of ethanol with the volume concentration of 95%, wherein the syringa microphylla natural essential oil is extracted from syringa microphylla flowers by adopting a water steam distillation method. The natural syringa microphylla flower perfume provided by the invention is clear is color and luster, and smooth and soft in aroma; the dispersion of aromas of all spice components in the perfume is harmonious and stable; a main aroma of the syringa microphylla flowers is highlighted in the single flower aroma type natural syringa microphylla flower perfume; the aroma keeping time can be up to 3-5 days.
Description
Technical field
The present invention relates to a kind of perfume, relate in particular to a kind of native leaflet Flos Caryophylli perfume of single floral type.
Background technology
Oleaceae (Oleaceae) Genus Syringa (Syringa) plant resources is abundant, and the genus syringa whole world approximately has 40 kinds, is distributed in Europe and Asia, and China has 23 kinds, all has distribution from China northeast to southwestern each province.At present the utilization to genus syringa resource, is taking cultivating and growing as main, and wild resource is auxiliary, and in addition, root it is documented and the achievement in research of recent year, and the medical value of the Flos Caryophylli to Oleaceae Genus Syringa has had than more comprehensive understanding and utilized.The common lilac (syringa) cultivar of China mainly contains Korea Flos Caryophylli, Syringa oblata Lindl., foreign Flos Caryophylli, and other still have Syringa pubescens, Chinese lilac, syringa reticulata var mandshurica, spend Korea Flos Caryophylli, Faeces Passeris etc. in vain.Sytingamicrophylla (
syringa pubescens,turca) be Oleaceae genus syringa, shrub, has another name called hair (leaf) Flos Caryophylli, tongue of sparrow flower, and Syringa pubescens, originates from Henan, Hebei, Shaanxi etc. and economizes ground.In Henan Province, be mainly distributed in Funiu Shan Mountain district and Wild jujube in Taihang Mountain Area, in 800～2000 meters of mountain region ditches of raw height above sea level or on cliffstone, they are all to bloom in annual 4 ~ May conventionally, about more than 10 days florescence.
Sytingamicrophylla (
syringa pubescens,turca), extensively, the flowers are in blossom, and time fragrance is attacked people to China's cultivation, and fragrance is pure.The fragrance of flowers is strong for Sytingamicrophylla, find after deliberation, can extract aromatic oil and prepare natural essence, in the Sytingamicrophylla volatile oil component of its extraction by steam distillation, contain 2-methylol-5-methyl-5-vinyl-oxolane, flavorant composition phenylethyl acetate and 3,7-dimethyl-1, the multiple natural perfume material compositions such as 6-octadiene-3-alcohol, also contain in addition benzaldehyde, the a-terpinol compound etc. of antiinflammatory, antibacterial and pain relieving active ingredient, therefore Sytingamicrophylla is applicable to the exploitation for fine chemicals as spice and essence.Current single floral type perfume is mostly the common fragrance of a flower such as Flos Rosae Rugosae, jasmine perfume, and natural single floral type perfume taking Sytingamicrophylla as main note is so far there are no report.
Summary of the invention
Object of the present invention is just to provide a kind of taking the Sytingamicrophylla fragrance of a flower as main note, is equipped with the natural single floral type perfume of other auxiliary spice, and perfume fragrance exquisiteness is soft, each spice fragrance distribute harmony, stable, protect the fragrant time longer.
To achieve these goals, technical scheme of the present invention is: a kind of native leaflet Flos Caryophylli perfume, by volume umber meter its consist of: 93.66 ~ 98.79 parts of the ethanol that 0.09 ~ 0.45 part of 0.9 ~ 4.5 part of Sytingamicrophylla natural essential oil, 0.07 ~ 0.4 part of oleum Citri sinensis, 0.05 ~ 0.33 part of Flos Pelargonii quintessence oil, 0.05 ~ 0.33 part of rosemary ethereal oil, 0.05 ~ 0.33 part of tea tree oil, Lignum Santali Albi quintessence oil and volumetric concentration are 95%.
As preferably, 97.91 parts of the ethanol that 1.5 parts of Sytingamicrophylla natural essential oils, 0.13 part of oleum Citri sinensis, 0.11 part of Flos Pelargonii quintessence oil, 0.11 part of rosemary ethereal oil, 0.11 part of tea tree oil, 0.13 part of Lignum Santali Albi quintessence oil and volumetric concentration are 95%.
Described Sytingamicrophylla natural essential oil is to adopt steam distillation extraction from the spending of Sytingamicrophylla to obtain, and its extracting method is as follows:
(1), get the flower of Sytingamicrophylla, after naturally drying in the shade, pulverize, to taking after pulverizing, to spray mass fraction be 0.9% that saline makes its surface moisture;
(2), Sytingamicrophylla that step (1) was processed puts into alembic, vapor distillation 3-5 hour, distillation speed is 1 ~ 2 per second, obtains distillate;
(3), be extracted with ethyl acetate distillate obtained above, isolate after upper layer of extraction liquid, in extract, add anhydrous sodium sulfate drying, and leave standstill 12 ~ 30 hours;
(4) mixed liquor, after step (3) is left standstill filters and obtains filtrate, and filtrate, after rotary evaporation removes desolventizing, obtains Sytingamicrophylla natural essential oil.
In the rotary evaporation process of step (4), adopt water pump distilling under reduced pressure, the rotating speed of controlling distilling flask is 80 ~ 85r/min, and in bottle, vacuum is 0.090-0.095Mpa, and bath temperature is 45 ~ 55 DEG C.
Beneficial effect: the native leaflet Flos Caryophylli perfume transparent color and luster of the present invention preparation is limpid, fragrance is fine and smooth soft, wherein each spice fragrance distribute harmony, stable, and given prominence to the main note taste of single floral type perfume Sytingamicrophylla, fragrance remaining time can reach 3 ~ 5 days.Wherein select oleum Citri sinensis as head perfume (or spice), Sytingamicrophylla is as the body note that embodies main body odor type, and come to be in harmonious proportion body note with Flos Pelargonii and Herba Rosmarini Officinalis, to give prominence to the main note taste of Sytingamicrophylla, Herba Rosmarini Officinalis also plays antiseptical function simultaneously, the Lignum Santali Albi that bottom note selects the Radix Aucklandiae to adjust, and play the effect of slow-release fragrance together with tea tree oil, to coordinate the volatility of each spice, make each spice fragrance emission become slowly, harmonious stable, make perfume fragrance more lasting simultaneously, extend fragrance remaining time.And Flos Pelargonii quintessence oil and tea tree oil all have effect antibacterial, antiinflammatory, can increase this effect together with benzaldehyde in Sytingamicrophylla quintessence oil, a-terpinol composition.
What the extraction of the Sytingamicrophylla natural essential oil in perfume of the present invention adopted is steam distillation, compared with existing super critical extraction, there is cost low, the advantage that extraction ratio is stable, and the Sytingamicrophylla natural essential oil that extracts of this process has effectively retained the fragrance component of the oxygenatedchemicalss such as the alcohol, esters and the ketone that wherein contain.In addition, in this law, select ethyl acetate to replace conventional ether, cyclohexane solvent as extractant, not only safety non-toxic, environmentally friendly, and according to the principle of similar compatibility, ethyl acetate extractant can make the essence extracting retain esters and the Flos Caryophylli phenols fragrance component in Sytingamicrophylla compared with highland.
Detailed description of the invention
A kind of native leaflet Flos Caryophylli perfume, by volume umber meter its consist of: 93.66 ~ 98.79 parts of the ethanol that 0.9 ~ 4.5 part of Sytingamicrophylla natural essential oil, 0.07 ~ 0.4 part of oleum Citri sinensis, 0.05 ~ 0.33 part of Flos Pelargonii quintessence oil, 0.05 ~ 0.33 part of rosemary ethereal oil, 0.05 ~ 0.33 part of tea tree oil, 0.09 ~ 0.45 part of Lignum Santali Albi quintessence oil and volumetric concentration are 95%.
Described Sytingamicrophylla natural essential oil is to adopt steam distillation extraction from the spending of Sytingamicrophylla to obtain, and its extracting method is as follows:
(1), get the flower of Sytingamicrophylla, after naturally drying in the shade, pulverize, to taking after pulverizing, to spray mass fraction be 0.9% that saline makes its surface moisture;
(2), Sytingamicrophylla that step (1) was processed puts into alembic, vapor distillation 3-5 hour, distillation speed is 1 ~ 2 per second, obtains distillate;
(3), be extracted with ethyl acetate distillate obtained above, isolate after upper layer of extraction liquid, in extract, add anhydrous sodium sulfate drying, and leave standstill 12 ~ 30 hours;
(4) mixed liquor, after step (3) is left standstill filters and obtains filtrate, and filtrate, after rotary evaporation removes desolventizing, obtains Sytingamicrophylla natural essential oil.
In the rotary evaporation process of step (4), adopt water pump distilling under reduced pressure, the rotating speed of controlling distilling flask is 80 ~ 85r/min, and in bottle, vacuum is 0.090-0.095Mpa, and bath temperature is 45 ~ 55 DEG C.
Embodiment 1
A kind of native leaflet Flos Caryophylli perfume, by volume umber meter its consist of: 98.79 parts of the ethanol of 0.9 part of Sytingamicrophylla natural essential oil, 0.07 part of oleum Citri sinensis, 0.05 part of Flos Pelargonii quintessence oil, 0.05 part of rosemary ethereal oil, 0.05 part of tea tree oil, 0.09 part of Lignum Santali Albi quintessence oil and volumetric concentration 95%.
Embodiment 2
A kind of native leaflet Flos Caryophylli perfume, by volume umber meter its consist of: 97.91 parts of the ethanol of 1.5 parts of Sytingamicrophylla natural essential oils, 0.13 part of oleum Citri sinensis, 0.11 part of Flos Pelargonii quintessence oil, 0.11 part of rosemary ethereal oil, 0.11 part of tea tree oil, 0.13 part of Lignum Santali Albi quintessence oil and volumetric concentration 95%.
Embodiment 3
A kind of native leaflet Flos Caryophylli perfume, by volume umber meter its consist of: 93.66 parts of the ethanol of 4.5 parts of Sytingamicrophylla natural essential oils, 0.4 part of oleum Citri sinensis, 0.33 part of Flos Pelargonii quintessence oil, 0.33 part of rosemary ethereal oil, 0.33 part of tea tree oil, 0.45 part of Lignum Santali Albi quintessence oil and volumetric concentration 95%.
Embodiment 4
A kind of native leaflet Flos Caryophylli perfume, by volume umber meter its consist of: alcohol 95 .95 part of 3.0 parts of Sytingamicrophylla natural essential oils, 0.2 part of oleum Citri sinensis, 0.2 part of Flos Pelargonii quintessence oil, 0.2 part of rosemary ethereal oil, 0.2 part of tea tree oil, 0.25 part of Lignum Santali Albi quintessence oil and volumetric concentration 95%.
Native leaflet Flos Caryophylli perfume fragrance of the present invention all fine and smooth soft, each spice fragrance emissions is coordinated, is stablized and outstanding Sytingamicrophylla main note taste, in perfume recipe, the amount of each spice used is compared and is wanted much less with similar perfume, but fragrance is strong, nature still, and fragrance remaining time can reach 3 ~ 5 days, and lasting is lasting.
Claims (3)
1. a native leaflet Flos Caryophylli perfume, is characterized in that: by volume umber meter its consist of: 93.66 ~ 98.79 parts of the ethanol that 0.09 ~ 0.45 part of 0.9 ~ 4.5 part of Sytingamicrophylla natural essential oil, 0.07 ~ 0.4 part of oleum Citri sinensis, 0.05 ~ 0.33 part of Flos Pelargonii quintessence oil, 0.05 ~ 0.33 part of rosemary ethereal oil, 0.05 ~ 0.33 part of tea tree oil, Lignum Santali Albi quintessence oil and volumetric concentration are 95%;
Described Sytingamicrophylla natural essential oil is to adopt steam distillation extraction from the spending of Sytingamicrophylla to obtain, and its extracting method is as follows:
(1), get the flower of Sytingamicrophylla, after naturally drying in the shade, pulverize, to taking after pulverizing, to spray mass fraction be 0.9% that saline makes its surface moisture;
(2), Sytingamicrophylla that step (1) was processed puts into alembic, vapor distillation 3-5 hour, distillation speed is 1 ~ 2 per second, obtains distillate;
(3), be extracted with ethyl acetate distillate obtained above, isolate after upper layer of extraction liquid, in extract, add anhydrous sodium sulfate drying, and leave standstill 12 ~ 30 hours;
(4) mixed liquor, after step (3) is left standstill filters and obtains filtrate, and filtrate, after rotary evaporation removes desolventizing, obtains Sytingamicrophylla natural essential oil.
2. a kind of native leaflet Flos Caryophylli perfume as claimed in claim 1, is characterized in that: by volume umber meter its consist of: 97.91 parts of the ethanol that 1.5 parts of Sytingamicrophylla natural essential oils, 0.13 part of oleum Citri sinensis, 0.11 part of Flos Pelargonii quintessence oil, 0.11 part of rosemary ethereal oil, 0.11 part of tea tree oil, 0.13 part of Lignum Santali Albi quintessence oil and volumetric concentration are 95%.
3. a kind of native leaflet Flos Caryophylli perfume as claimed in claim 1, it is characterized in that: in the rotary evaporation process of described step (4), adopt water pump distilling under reduced pressure, the rotating speed of controlling distilling flask is 80 ~ 85r/min, in bottle, vacuum is 0.090-0.095Mpa, and bath temperature is 45 ~ 55 DEG C.
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| CN201310297440.3A CN103405360B (en) | 2013-07-16 | 2013-07-16 | Natural syringa microphylla flower perfume |
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| CN201310297440.3A CN103405360B (en) | 2013-07-16 | 2013-07-16 | Natural syringa microphylla flower perfume |
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| CN103405360B true CN103405360B (en) | 2014-09-03 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104161696A (en) * | 2013-12-13 | 2014-11-26 | 金玛瑙香水（明光）有限公司 | Long acting perfume |
| CN106109273A (en) * | 2016-07-06 | 2016-11-16 | 唐虎 | Natural syringa microphylla flower perfume |
| CN106176343A (en) * | 2016-07-08 | 2016-12-07 | 唐虎 | The natural syringa microphylla flower perfume that lasting is long |
| CN106039370A (en) * | 2016-07-28 | 2016-10-26 | 河南科技大学 | Preparation method for rosmarinus officialis L. plant air freshener with dual effects |
| CN108589279A (en) * | 2018-04-30 | 2018-09-28 | 安徽恒益纺织科技有限公司 | A kind of fumet for textile fabric |
| CN108642876A (en) * | 2018-04-30 | 2018-10-12 | 安徽恒益纺织科技有限公司 | A kind of fragrant softening agent for textile fabric |
| CN108755114A (en) * | 2018-04-30 | 2018-11-06 | 安徽恒益纺织科技有限公司 | A kind of care agent for textile fabric |
| CN108755113A (en) * | 2018-04-30 | 2018-11-06 | 安徽恒益纺织科技有限公司 | A kind of fragrant care agent for textile fabric |
| CN108589278A (en) * | 2018-04-30 | 2018-09-28 | 安徽恒益纺织科技有限公司 | A kind of aromatic for textile fabric |
| CN109021762A (en) * | 2018-06-04 | 2018-12-18 | 安徽索立德铸业有限公司 | A kind of fragrant coating for hot investment casting part |
| CN109123938B (en) * | 2018-10-19 | 2021-07-27 | 魏佳 | Functional jewelry with effects of calming, relieving and dredging emotion congestion and use method thereof |
| CN109199929A (en) * | 2018-11-07 | 2019-01-15 | 上海芬尚生物科技有限公司 | perfume and preparation method thereof |
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| CN1895215A (en) * | 2006-06-15 | 2007-01-17 | 马凯宏 | Essential-oil cosmetic for color therapy |
| CN101897787A (en) * | 2010-07-20 | 2010-12-01 | 吴静 | Essential oil for giving up smoking |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1895215A (en) * | 2006-06-15 | 2007-01-17 | 马凯宏 | Essential-oil cosmetic for color therapy |
| CN101897787A (en) * | 2010-07-20 | 2010-12-01 | 吴静 | Essential oil for giving up smoking |
Non-Patent Citations (2)
| Title |
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| 王鹏等.野丁香的重新评价及利用.《香料香精化妆品》.1987,(第3期),第66-68页. |
| 野丁香的重新评价及利用;王鹏等;《香料香精化妆品》;19871001(第3期);第66-68页 * |
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