CN106039370A - Preparation method for rosmarinus officialis L. plant air freshener with dual effects - Google Patents
Preparation method for rosmarinus officialis L. plant air freshener with dual effects Download PDFInfo
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- CN106039370A CN106039370A CN201610604008.8A CN201610604008A CN106039370A CN 106039370 A CN106039370 A CN 106039370A CN 201610604008 A CN201610604008 A CN 201610604008A CN 106039370 A CN106039370 A CN 106039370A
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- air freshener
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- Fats And Perfumes (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention discloses a preparation method for a rosmarinus officialis L. plant air freshener with dual effects. The preparation method comprises the following steps: dissolving 1.0 to 1.5 parts by weight of natural rosmarinus officialis L. essential oil and 0.4 to 0.6 part by weight of lemon essential oil in 6.0 to 8.0 parts by weight of absolute ethyl alcohol, performing uniform mixing to obtain a mixed solution, adding an ethanol solution at a volumetric concentration of 75 percent into the mixed solution, performing dilution to 100 parts, and performing ultrasonic mixing and standing to obtain the rosmarinus officialis L. plant air freshener. The air freshener prepared by the preparation method is transparent, clear, fresh, fragrant, low in cost and environment-friendly, has good mosquito repellent and bacterium inhibition effects, and smells fresh, the dual effects of environment cleaning and bacterium inhibition are integrated, and 57 active ingredients in the natural rosmarinus officialis L. essential oil can be identified.
Description
Technical field
The invention belongs to natural prodcuts production technical field, be specifically related to a kind of rosemary plant sky with double effects
The preparation method of gas freshener.
Background technology
Herba Rosmarini Officinalis (Rosmarinus officialis L.), is Labiatae Rosmarinus plant, is the tool generally acknowledged at present
There is a kind of plant of relatively high anti-oxidation effect.Originating in Mediterranean one band country, document report is planted for 1981 by the Chinese Academy of Sciences
Thing institute is introduced a fine variety to China, and cultivates successfully.The most extensively plant.Because Herba Rosmarini Officinalis is not only a kind of sight
Reward plant, a kind of important natural perfume plant, it is widely used in daily-use chemical industry, food interpolation and medicines and health protection always
Deng field ［ 1 ］.Modern study shows, effective ingredient main in Herba Rosmarini Officinalis has two classes: one is quintessence oil, i.e. volatile ingredient,
Mainly include the ter penoids such as monoterpene, sesquiterpene；Another is antioxidant composition, i.e. involatile constituent, predominantly diterpene
Class (carnosic acid, carnosol, rosmanol, ursolic acid, rosmarinic acid) etc. ［ 2 ］.Rosemary ethereal oil is present in Herba Rosmarini Officinalis more
In leaf and stalk, lot of documents report rosemary plant has the pharmacology such as the most antibacterial, antioxidation, appetite strengthening, anti-inflammatory analgesic to make
There is strong treatment acne effect with, the most obvious anti-propionibacterium.In addition can also be by suppression bacterial reproduction
Effectively suppress the various bacteria ［ 3 ］ such as escherichia coli, staphylococcus aureus and vibrio cholera.Further with regards to Herba Rosmarini Officinalis quintessence oil carry
Access method has a lot, mainly includes machine solvent extraction method, steam distillation, microwave-assisted extraction, absorption method, squeezing
Method, ultrasonic extraction, moment voltage drop method, enzyme process assisted extraction method and supercritical CO2 Extraction etc..Different extracting method is each
There are pluses and minuses.
Summary of the invention
For solving above-mentioned technical problem, the present invention provides a kind of rosemary plant air freshener with double effects
Preparation method, the air freshener that this preparation method prepares is transparent limpid, and novel aroma overflows, and collection environment purification is with antibacterial
Double effects is in one, and with low cost, anophelifuge fungistatic effect is excellent, and abnormal smells from the patient is pure and fresh, environmental friendliness, and can be from rosemary natural essence
Oil identifies 57 kinds of effective ingredient.
The technical solution adopted in the present invention is: the preparation of a kind of rosemary plant air freshener with double effects
Method, takes rosemary natural quintessence oil 1.0-1.5 part and Fructus Citri Limoniae quintessence oil 0.4-0.6 part respectively, is dissolved in 6.0-8.0 according to parts by weight
In the dehydrated alcohol of part, obtaining mixed liquor after mix homogeneously, then adding volumetric concentration in mixed liquor is the ethanol solution of 75%
Be diluted to 100 parts, ultrasonic miscible, static after i.e. obtain rosemary plant air freshener.
Preparation method the most excellent as a kind of rosemary plant air freshener with double effects of the present invention
Change, described ultrasonic miscible static after, use preservative film seal In Shade ageing 20-40 days, obtain rosemary plant air
Freshener.
Preparation method the most excellent as a kind of rosemary plant air freshener with double effects of the present invention
Changing, the extracting method of described rosemary natural quintessence oil comprises the following steps:
Step one, the stem weighing Herba Rosmarini Officinalis aerial parts through drying in the shade and leaf, as Herba Rosmarini Officinalis raw material, use fiber after pulverizing
Element enzyme aqueous solution is sprayed on Herba Rosmarini Officinalis raw material；
Step 2, Herba Rosmarini Officinalis raw material step one processed are placed in alembic, vapor distillation 3-5 hour, distillation speed
Degree drips for 1-2 per second, obtains Herba Rosmarini Officinalis volatile oil, standby；
Step 3, Herba Rosmarini Officinalis volatile oil step 2 obtained are adopted and are extracted with ethyl acetate, and collect upper layer of extraction liquid, are subsequently adding
Anhydrous sodium sulfate is dried, and stands 12-30 hour to anhydrous sodium sulfate dried cake, filters, collects filtrate, and filtrate is through decompression
After solvent is evaporated off, i.e. obtain rosemary natural quintessence oil.
Preparation method the most excellent as a kind of rosemary plant air freshener with double effects of the present invention
Changing, the mass concentration of the cellulase aqueous solution described in step one is 0.15%.
Preparation method the most excellent as a kind of rosemary plant air freshener with double effects of the present invention
Changing, the vacuum of the decompression distillation described in step 3 is 0.090-0.095Mpa, and bath temperature is 45-52 DEG C.
Preparation method the most excellent as a kind of rosemary plant air freshener with double effects of the present invention
Change, consumption is Herba Rosmarini Officinalis volatile oil weight 1/3 of ethyl acetate described in step 3.
Compared with prior art, the present invention at least has and has the advantage that and beneficial effect:
One, the air that the preparation method of the rosemary plant air freshener with double effects that the present invention provides prepares
Freshener is transparent limpid, and novel aroma overflows, and integrates environment purification and antibacterial double effects, and with low cost, anophelifuge is antibacterial
Excellent effect, abnormal smells from the patient is pure and fresh, environmental friendliness.
Two, the extracting method oil yield using the rosemary natural quintessence oil of present invention offer is 1.58%, the Herba Rosmarini Officinalis obtained
Essential oil content is 92.73%, and can identify 57 kinds of effective ingredient from rosemary natural quintessence oil, and significantly larger than document is reported
35 kinds.The present invention provides fundamental basis for research rosemary ethereal oil effect further, for it in medicine and the exploitation of perfume industry
Utilize and science and technology and foundation are provided.
Accompanying drawing explanation
Fig. 1 is the total ions chromatogram that the present invention extracts the rosemary natural quintessence oil obtained；
Fig. 2 present invention extracts the component content catalog of the rosemary natural quintessence oil obtained.
Detailed description of the invention
For making present disclosure become apparent, below in conjunction with specific embodiment, describe the present invention.
The preparation method of a kind of rosemary plant air freshener with double effects, takes fan respectively according to parts by weight
The most fragrant natural essential oil 1.0-1.5 part and Fructus Citri Limoniae quintessence oil 0.4-0.6 part, be dissolved in the dehydrated alcohol of 6.0-8.0 part, after mix homogeneously
Obtain mixed liquor, in mixed liquor, then add the ethanol solution that volumetric concentration is 75% be diluted to 100 parts, ultrasonic miscible static
After, use preservative film to seal In Shade ageing 20-40 days, i.e. obtain rosemary plant air freshener；
The extracting method of described rosemary natural quintessence oil comprises the following steps:
Step one, the stem weighing Herba Rosmarini Officinalis aerial parts through drying in the shade and leaf, as Herba Rosmarini Officinalis raw material, use quality after pulverizing
Concentration is that 0.15% cellulase aqueous solution is sprayed on Herba Rosmarini Officinalis raw material；
Step 2, Herba Rosmarini Officinalis raw material step one processed are placed in alembic, vapor distillation 3-5 hour, distillation speed
Degree drips for 1-2 per second, obtains Herba Rosmarini Officinalis volatile oil, standby；
Step 3, Herba Rosmarini Officinalis volatile oil step 2 obtained are adopted and are extracted with ethyl acetate, and the consumption of ethyl acetate is Herba Rosmarini Officinalis
The 1/3 of volatile oil weight, collects upper layer of extraction liquid, is subsequently adding anhydrous sodium sulfate and is dried, and stands 12-30 hour to anhydrous
Sodium sulfate dried cake, filters, and collects filtrate, and filtrate is after removing solvent under reduced pressure, and the vacuum of decompression distillation is 0.090-
0.095Mpa, bath temperature is 45-52 DEG C, i.e. obtains rosemary natural quintessence oil.
Embodiment 1:
The preparation method of a kind of rosemary plant air freshener with double effects, takes Herba Rosmarini Officinalis respectively according to parts by weight
Natural essential oil 1.0 parts and Fructus Citri Limoniae quintessence oil 0.4 part, be dissolved in the dehydrated alcohol of 6.0 parts, obtain mixed liquor, then after mix homogeneously
In mixed liquor add volumetric concentration be 75% ethanol solution be diluted to 100 parts, ultrasonic miscible static after, use preservative film close
It is sealed and placed at cool place and is aged 20 days, i.e. obtain rosemary plant air freshener；
The extracting method of described rosemary natural quintessence oil comprises the following steps:
Step one, the stem weighing Herba Rosmarini Officinalis aerial parts through drying in the shade and leaf, as Herba Rosmarini Officinalis raw material, use quality after pulverizing
Concentration is that 0.15% cellulase aqueous solution is sprayed on Herba Rosmarini Officinalis raw material；
Step 2, Herba Rosmarini Officinalis raw material step one processed are placed in alembic, vapor distillation 3 hours, distillation speed
For 1 per second, obtain Herba Rosmarini Officinalis volatile oil, standby；
Step 3, Herba Rosmarini Officinalis volatile oil step 2 obtained are adopted and are extracted with ethyl acetate, and the consumption of ethyl acetate is Herba Rosmarini Officinalis
The 1/3 of volatile oil weight, collects upper layer of extraction liquid, is subsequently adding anhydrous sodium sulfate and is dried, and stands 12 hours to anhydrous sulfur
Acid sodium dried cake, filters, and collects filtrate, and filtrate is after removing solvent under reduced pressure, and the vacuum of decompression distillation is 0.090-
0.095Mpa, bath temperature is 45-52 DEG C, i.e. obtains rosemary natural quintessence oil.
Embodiment 2:
The preparation method of a kind of rosemary plant air freshener with double effects, takes Herba Rosmarini Officinalis respectively according to parts by weight
Natural essential oil 1.5 parts and Fructus Citri Limoniae quintessence oil 0.5 part, be dissolved in the dehydrated alcohol of 8.0 parts, obtain mixed liquor, then after mix homogeneously
In mixed liquor add volumetric concentration be 75% ethanol solution be diluted to 100 parts, ultrasonic miscible static after, use preservative film close
It is sealed and placed at cool place and is aged 40 days, i.e. obtain rosemary plant air freshener；
The extracting method of described rosemary natural quintessence oil comprises the following steps:
Step one, the stem weighing Herba Rosmarini Officinalis aerial parts through drying in the shade and leaf, as Herba Rosmarini Officinalis raw material, use quality after pulverizing
Concentration is that 0.15% cellulase aqueous solution is sprayed on Herba Rosmarini Officinalis raw material；
Step 2, Herba Rosmarini Officinalis raw material step one processed are placed in alembic, vapor distillation 5 hours, distillation speed
For 2 per second, obtain Herba Rosmarini Officinalis volatile oil, standby；
Step 3, Herba Rosmarini Officinalis volatile oil step 2 obtained are adopted and are extracted with ethyl acetate, and the consumption of ethyl acetate is Herba Rosmarini Officinalis
The 1/3 of volatile oil weight, collects upper layer of extraction liquid, is subsequently adding anhydrous sodium sulfate and is dried, and stands 30 hours to anhydrous sulfur
Acid sodium dried cake, filters, and collects filtrate, and filtrate is after removing solvent under reduced pressure, and the vacuum of decompression distillation is 0.090-
0.095Mpa, bath temperature is 45-52 DEG C, i.e. obtains rosemary natural quintessence oil.
Embodiment 3:
The preparation method of a kind of rosemary plant air freshener with double effects, takes Herba Rosmarini Officinalis respectively according to parts by weight
Natural essential oil 1.2 parts and Fructus Citri Limoniae quintessence oil 0.6 part, be dissolved in the dehydrated alcohol of 7.0 parts, obtain mixed liquor, then after mix homogeneously
In mixed liquor add volumetric concentration be 75% ethanol solution be diluted to 100 parts, ultrasonic miscible static after, use preservative film close
It is sealed and placed at cool place and is aged 30 days, i.e. obtain rosemary plant air freshener；
The extracting method of described rosemary natural quintessence oil comprises the following steps:
Step one, the stem weighing Herba Rosmarini Officinalis aerial parts through drying in the shade and leaf, as Herba Rosmarini Officinalis raw material, use quality after pulverizing
Concentration is that 0.15% cellulase aqueous solution is sprayed on Herba Rosmarini Officinalis raw material；
Step 2, Herba Rosmarini Officinalis raw material step one processed are placed in alembic, vapor distillation 4 hours, distillation speed
For 2 per second, obtain Herba Rosmarini Officinalis volatile oil, standby；
Step 3, Herba Rosmarini Officinalis volatile oil step 2 obtained are adopted and are extracted with ethyl acetate, and the consumption of ethyl acetate is Herba Rosmarini Officinalis
The 1/3 of volatile oil weight, collects upper layer of extraction liquid, is subsequently adding anhydrous sodium sulfate and is dried, and stands 21 hours to anhydrous sulfur
Acid sodium dried cake, filters, and collects filtrate, and filtrate is after removing solvent under reduced pressure, and the vacuum of decompression distillation is 0.090-
0.095Mpa, bath temperature is 45-52 DEG C, i.e. obtains rosemary natural quintessence oil.
Experimental study data
Rosemary natural quintessence oil embodiment prepared carries out chromatograph qualification, and the total ions chromatogram and the composition that obtain contain
Amount catalog is shown in Fig. 1 and Fig. 2.
Result and characteristic discussion: identified, leaf of Herba Rosmarini Officinalis adds cellulase and obtains transparent liquid after distillation, dehydration
Body, identifies 57 kinds of compositions of composition, significantly larger than 35 kinds of document report altogether.Oil yield is the 1.5% of 1.58%(＞ report), relatively
Density is 0.873, and index of refraction is Isosorbide-5-Nitrae 72.
This analysis result shows, main component 4,6,6-trimethyl bicyclo-[3.1.1] the hept-3-alkene in rosemary ethereal oil-
2-ketone content is 24.121%；Isobornyl formate content is 18.202%；Levo-camphor content is 13.658%；Eudesmol contains
Amount is 9.2796%；Terpinen-4-ols content is 4.4557%.
Contrast and find: the content difference of cineole, Camphora in the rosemary natural quintessence oil that the Funiu Shan Mountain that experiment is extracted produces
Be 9.2796% and 13.658%, with document report 11.88% and 11.84% have notable difference, according to classification should be " low by 1,8-eucalyptus globulus
Foline/pinene and homocamphor " type (also known as Tunisia/Morocco's type).Different from document report, Funiu Shan Mountain produces Herba Rosmarini Officinalis composition
The fragrance components such as peculiar terpinen-4-ols, isobornyl formate, 4,6,6-trimethyl bicyclo-[3,1,1]-hept-3-alkene-2-ketone,
The most there is not limonene, camphene, 1R-australene and the α in document report, α, 4-trimethyl-3-cyclohexene-1-methanol etc. becomes
Point.Obviously these component differences may by Herba Rosmarini Officinalis the factors such as growing environment, planting area and kind cause.
Claims (6)
1. the preparation method of a rosemary plant air freshener with double effects, it is characterised in that: according to weight portion
Number takes rosemary natural quintessence oil 1.0-1.5 part and Fructus Citri Limoniae quintessence oil 0.4-0.6 part respectively, is dissolved in the dehydrated alcohol of 6.0-8.0 part,
Obtain mixed liquor after mix homogeneously, in mixed liquor, then add the ethanol solution that volumetric concentration is 75% be diluted to 100 parts, super
Sound is miscible, static after i.e. obtain rosemary plant air freshener.
The preparation method of a kind of rosemary plant air freshener with double effects, it is special
Levy and be: described ultrasonic miscible static after, use preservative film seal In Shade ageing 20-40 days, obtain rosemary plant
Air freshener.
The preparation method of a kind of rosemary plant air freshener with double effects, it is special
Levy and be: the extracting method of described rosemary natural quintessence oil comprises the following steps:
Step one, the stem weighing Herba Rosmarini Officinalis aerial parts through drying in the shade and leaf, as Herba Rosmarini Officinalis raw material, use fiber after pulverizing
Element enzyme aqueous solution is sprayed on Herba Rosmarini Officinalis raw material；
Step 2, Herba Rosmarini Officinalis raw material step one processed are placed in alembic, vapor distillation 3-5 hour, distillation speed
Degree drips for 1-2 per second, obtains Herba Rosmarini Officinalis volatile oil, standby；
Step 3, Herba Rosmarini Officinalis volatile oil step 2 obtained are adopted and are extracted with ethyl acetate, and collect upper layer of extraction liquid, are subsequently adding
Anhydrous sodium sulfate is dried, and stands 12-30 hour to anhydrous sodium sulfate dried cake, filters, collects filtrate, and filtrate is through decompression
After solvent is evaporated off, i.e. obtain rosemary natural quintessence oil.
The preparation method of a kind of rosemary plant air freshener with double effects, it is special
Levy and be: the mass concentration of the cellulase aqueous solution described in step one is 0.15%.
The preparation method of a kind of rosemary plant air freshener with double effects, it is special
Levy and be: the vacuum of the decompression distillation described in step 3 is 0.090-0.095Mpa, and bath temperature is 45-52 DEG C.
The preparation method of a kind of rosemary plant air freshener with double effects, it is special
Levy and be: the consumption of ethyl acetate described in step 3 is the 1/3 of Herba Rosmarini Officinalis volatile oil weight.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112956497A (en) * | 2021-03-22 | 2021-06-15 | 王立强 | Compound natural essential oil disinfection bacteriostat and preparation method thereof |
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