CN103146482A - Tobacco flavor with sweetening function and application thereof - Google Patents
Tobacco flavor with sweetening function and application thereof Download PDFInfo
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- CN103146482A CN103146482A CN2013100925559A CN201310092555A CN103146482A CN 103146482 A CN103146482 A CN 103146482A CN 2013100925559 A CN2013100925559 A CN 2013100925559A CN 201310092555 A CN201310092555 A CN 201310092555A CN 103146482 A CN103146482 A CN 103146482A
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- cigarette
- tobacco aromatics
- tobacco
- herba lysimachiae
- extraction
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- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 37
- 239000000796 flavoring agent Substances 0.000 title abstract description 5
- 235000019634 flavors Nutrition 0.000 title abstract description 5
- 244000061176 Nicotiana tabacum Species 0.000 title abstract 3
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 50
- 238000000605 extraction Methods 0.000 claims abstract description 20
- 235000009508 confectionery Nutrition 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 238000000199 molecular distillation Methods 0.000 claims abstract description 7
- 241000208125 Nicotiana Species 0.000 claims description 34
- 239000000284 extract Substances 0.000 claims description 21
- 239000000341 volatile oil Substances 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 14
- 238000004821 distillation Methods 0.000 claims description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 6
- 238000010790 dilution Methods 0.000 claims description 5
- 239000012895 dilution Substances 0.000 claims description 5
- 239000012530 fluid Substances 0.000 claims description 5
- 239000003205 fragrance Substances 0.000 abstract description 12
- 230000000694 effects Effects 0.000 abstract description 9
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 abstract description 5
- JSNRRGGBADWTMC-UHFFFAOYSA-N (6E)-7,11-dimethyl-3-methylene-1,6,10-dodecatriene Chemical compound CC(C)=CCCC(C)=CCCC(=C)C=C JSNRRGGBADWTMC-UHFFFAOYSA-N 0.000 abstract description 4
- 244000180308 Ocimum basilicum Species 0.000 abstract description 4
- 235000010676 Ocimum basilicum Nutrition 0.000 abstract description 4
- 239000000654 additive Substances 0.000 abstract description 4
- 230000000996 additive effect Effects 0.000 abstract description 4
- 230000000638 stimulation Effects 0.000 abstract description 4
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 abstract description 3
- 241000723346 Cinnamomum camphora Species 0.000 abstract description 3
- 229930008380 camphor Natural products 0.000 abstract description 3
- 229960000846 camphor Drugs 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 3
- 235000013311 vegetables Nutrition 0.000 abstract description 3
- CXENHBSYCFFKJS-UHFFFAOYSA-N (3E,6E)-3,7,11-Trimethyl-1,3,6,10-dodecatetraene Natural products CC(C)=CCCC(C)=CCC=C(C)C=C CXENHBSYCFFKJS-UHFFFAOYSA-N 0.000 abstract description 2
- 229930009668 farnesene Natural products 0.000 abstract description 2
- 150000007823 ocimene derivatives Chemical class 0.000 abstract description 2
- -1 pinene Chemical compound 0.000 abstract description 2
- XJPBRODHZKDRCB-UHFFFAOYSA-N trans-alpha-ocimene Natural products CC(=C)CCC=C(C)C=C XJPBRODHZKDRCB-UHFFFAOYSA-N 0.000 abstract description 2
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 abstract 2
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 abstract 2
- CRPUJAZIXJMDBK-UHFFFAOYSA-N camphene Chemical compound C1CC2C(=C)C(C)(C)C1C2 CRPUJAZIXJMDBK-UHFFFAOYSA-N 0.000 abstract 2
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 abstract 2
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 abstract 2
- 229930007744 linalool Natural products 0.000 abstract 2
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 abstract 1
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 abstract 1
- 239000005770 Eugenol Substances 0.000 abstract 1
- PXRCIOIWVGAZEP-UHFFFAOYSA-N Primaeres Camphenhydrat Natural products C1CC2C(O)(C)C(C)(C)C1C2 PXRCIOIWVGAZEP-UHFFFAOYSA-N 0.000 abstract 1
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 abstract 1
- XCPQUQHBVVXMRQ-UHFFFAOYSA-N alpha-Fenchene Natural products C1CC2C(=C)CC1C2(C)C XCPQUQHBVVXMRQ-UHFFFAOYSA-N 0.000 abstract 1
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 abstract 1
- 229930006739 camphene Natural products 0.000 abstract 1
- ZYPYEBYNXWUCEA-UHFFFAOYSA-N camphenilone Natural products C1CC2C(=O)C(C)(C)C1C2 ZYPYEBYNXWUCEA-UHFFFAOYSA-N 0.000 abstract 1
- 235000000484 citronellol Nutrition 0.000 abstract 1
- SQIFACVGCPWBQZ-UHFFFAOYSA-N delta-terpineol Natural products CC(C)(O)C1CCC(=C)CC1 SQIFACVGCPWBQZ-UHFFFAOYSA-N 0.000 abstract 1
- 229960002217 eugenol Drugs 0.000 abstract 1
- 229940116411 terpineol Drugs 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 14
- 235000013599 spices Nutrition 0.000 description 11
- 238000002360 preparation method Methods 0.000 description 10
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 9
- 239000002304 perfume Substances 0.000 description 9
- 238000002474 experimental method Methods 0.000 description 8
- 230000006870 function Effects 0.000 description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- 239000000419 plant extract Substances 0.000 description 6
- 239000007789 gas Substances 0.000 description 5
- 239000003906 humectant Substances 0.000 description 4
- 235000019633 pungent taste Nutrition 0.000 description 4
- 230000001953 sensory effect Effects 0.000 description 4
- 230000000391 smoking effect Effects 0.000 description 4
- MEIRRNXMZYDVDW-MQQKCMAXSA-N (2E,4E)-2,4-hexadien-1-ol Chemical compound C\C=C\C=C\CO MEIRRNXMZYDVDW-MQQKCMAXSA-N 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 238000000855 fermentation Methods 0.000 description 3
- 230000004151 fermentation Effects 0.000 description 3
- 239000003546 flue gas Substances 0.000 description 3
- 235000011187 glycerol Nutrition 0.000 description 3
- 235000012907 honey Nutrition 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000012797 qualification Methods 0.000 description 3
- 230000033764 rhythmic process Effects 0.000 description 3
- GRWFGVWFFZKLTI-IUCAKERBSA-N (-)-α-pinene Chemical compound CC1=CC[C@@H]2C(C)(C)[C@H]1C2 GRWFGVWFFZKLTI-IUCAKERBSA-N 0.000 description 2
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 2
- 235000015164 Iris germanica var. florentina Nutrition 0.000 description 2
- 235000015265 Iris pallida Nutrition 0.000 description 2
- 244000050403 Iris x germanica Species 0.000 description 2
- 241001530121 Trollius Species 0.000 description 2
- 239000003595 mist Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- LFJQCDVYDGGFCH-JTQLQIEISA-N (+)-β-phellandrene Chemical compound CC(C)[C@@H]1CCC(=C)C=C1 LFJQCDVYDGGFCH-JTQLQIEISA-N 0.000 description 1
- LFJQCDVYDGGFCH-SNVBAGLBSA-N (+/-)-beta-Phellandrene Natural products CC(C)[C@H]1CCC(=C)C=C1 LFJQCDVYDGGFCH-SNVBAGLBSA-N 0.000 description 1
- CRDAMVZIKSXKFV-FBXUGWQNSA-N (2-cis,6-cis)-farnesol Chemical compound CC(C)=CCC\C(C)=C/CC\C(C)=C/CO CRDAMVZIKSXKFV-FBXUGWQNSA-N 0.000 description 1
- 239000000260 (2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-ol Substances 0.000 description 1
- YZFQMOQVNWBTMZ-UHFFFAOYSA-N Actinidialactone Natural products CC1C2CC=C(C)C2(C)CC1=O YZFQMOQVNWBTMZ-UHFFFAOYSA-N 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 241000790917 Dioxys <bee> Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 description 1
- 239000005792 Geraniol Substances 0.000 description 1
- VPXAKEICIWYNGX-UHFFFAOYSA-N Isoactinidialactone Natural products CC1C2CC=C(C)C2(O)CC1=O VPXAKEICIWYNGX-UHFFFAOYSA-N 0.000 description 1
- 241000207923 Lamiaceae Species 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- UZFLPKAIBPNNCA-BQYQJAHWSA-N alpha-ionone Chemical compound CC(=O)\C=C\C1C(C)=CCCC1(C)C UZFLPKAIBPNNCA-BQYQJAHWSA-N 0.000 description 1
- MVNCAPSFBDBCGF-UHFFFAOYSA-N alpha-pinene Natural products CC1=CCC23C1CC2C3(C)C MVNCAPSFBDBCGF-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- LFJQCDVYDGGFCH-UHFFFAOYSA-N beta-phellandrene Natural products CC(C)C1CCC(=C)C=C1 LFJQCDVYDGGFCH-UHFFFAOYSA-N 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 235000019751 broiler diet Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 229930002886 farnesol Natural products 0.000 description 1
- 229940043259 farnesol Drugs 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- 229940113087 geraniol Drugs 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- GRWFGVWFFZKLTI-UHFFFAOYSA-N rac-alpha-Pinene Natural products CC1=CCC2C(C)(C)C1C2 GRWFGVWFFZKLTI-UHFFFAOYSA-N 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 239000011269 tar Substances 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- CRDAMVZIKSXKFV-UHFFFAOYSA-N trans-Farnesol Natural products CC(C)=CCCC(C)=CCCC(C)=CCO CRDAMVZIKSXKFV-UHFFFAOYSA-N 0.000 description 1
- RBNWAMSGVWEHFP-UHFFFAOYSA-N trans-p-Menthane-1,8-diol Chemical compound CC(C)(O)C1CCC(C)(O)CC1 RBNWAMSGVWEHFP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a tobacco flavor with a sweetening function and application thereof. Sweet basil (Ocimum basilicum L.) which is an aromatic vegetable is used as a raw material, and a supercritical CO2 extraction technology and a molecular distillation technology are combined for extraction to prepare the additive for cigarettes. The tobacco flavor mainly comprises the following components: linalool, farnesene, linalool, camphor, pinene, camphene, ocimene, terpineol, citronellol, eugenol, and the like. After the additive is added into cigarettes, the additive has the effects of enriching the cigarette fragrance, increasing the sweet feeling and the fine and greasy feeling, improving the fragrance quality, reducing the stimulation, enabling the cigarette fragrance to be more permeable and improving the comfort.
Description
Technical field
The invention belongs to the cigarette additive technical field, be specifically related to a kind of preparation method with the tobacco aromatics using that increases sweet function, simultaneously, the invention still further relates to the application of described tobacco aromatics using in Cigarette processing.
Background technology
In tobacco product, the fragrance of tobacco and jealous be vital, along with the reduction of tar content in cigarette in recent years, low-coke tar cigarette exists smoke thin out, fragrance weakens, cigarette product loses original style, is difficult to the problem of being accepted by the human consumer.So when Jiao fell in Harm reduction techniques, cigarette flavouring and raising flue gas concentration were key issues.Perfuming cigarette is reinforced is one of core technology of tobacco industry.Mode by flavoring and casing can make up the insufficient fragrance on cigarette tobacco leaf formulation, eliminates assorted gas, makes the cigarette perfume (or spice) of cigarette product more abundant, sufficient, thereby inhaling flavor, smelling and have individual style on perfume (or spice), strengthens the feature of cigarette product.
Preparing by different way essence spice for cigarette makes an addition to and reaches the method that promotes cigarette smoking quality in cigarette and appear in the newspapers.The people such as Yang Lihua are take natural mushroom mushroom as raw material, adopt conventional extraction method, enzymolysis process and Maillard reaction method development of new tobacco aromatics using, and carry out perfuming cigarette experiment, result shows that enzyme process gained spices gives cigarette special note, has the effect that improves the flue gas comfort level.Deng state guests etc. utilize the microorganism aroma former to make the fresh iris spices of fresh iris preparation fermentation, and the absolute oil of preparation is carried out perfuming cigarette for kinds of cigarettes leaf group, experimental result shows that the fresh orris absolute of fermentation is better than without adding of the fresh orris absolute of biological fermentation of fragrant effect at the perfuming successful aspect fragrance, assorted gas and comfortableness.Zhu Baokun etc. have analyzed the impact of the humectants such as glycerine, propylene glycol, sorbyl alcohol, honey on cigarette Oranoleptic indicators such as stimulation, pleasant impression, dry sensations, result shows, the humectant consumption promotes " cloud and mist " product sensory remarkably influenced, and has determined the broiler diets of four kinds of humectants; The different humectants such as glycerine, propylene glycol, sorbyl alcohol, honey have remarkably influenced to the pungency of " cloud and mist " product, and the propylene glycol consumption is its pungency of cigarette of 0.4% less than the cigarette that has added 0.7% glycerine, 0.7% sorbyl alcohol, 0.7% honey.Ji Xiaoming etc. extract volatile oil take Flower of Chinese Globeflower as raw material, use GC-MS to analyze volatile oil component, and carry out perfuming cigarette and test, result shows the appropriate Flower of Chinese Globeflower volatile oil of interpolation in pipe tobacco, can improve fragrance matter and the perfume quantity of cigarette smoke, reduce pungency, improve pleasant impression, its main aroma component is alpha, beta-lonone, dioxy actinidia lactone etc.The reports such as Duan Binbin, carry out the perfuming experiment as material extraction volatile oil and in cigarette take the bosom chrysanthemum, result shows, this volatile oil can be modified cigarette flavor, improve that flue gas is submissive, fine and smooth degree, reduce pungency and improve pleasant impression, its key odorant composition is p-ymene, α-pinene, β-phellandrene, farnesol etc.
Herba Lysimachiae foenumgraeci (Ocimum basilicum L.) is Labiatae annual herb plant, the characteristic Fragrant vegetables, and using part is its over-ground part.Because it has unique sweet note, nuisanceless, can annual cultivate, have the bright prospects of production ﹠ marketing development.At present, the research of Herba Lysimachiae foenumgraeci is focused mostly at the cultivating and growing of Herba Lysimachiae foenumgraeci, the factors vary such as environment are on the impact of Herba Lysimachiae foenumgraeci essential oil, the research of sweet basil essential oil volatile component etc., and the method for extraction of essential oil of Herba Lysimachiae foenumgraeci mostly is wet distillation, adopts supercritical CO
2The method that abstraction technique and molecular distillation technique coupling prepare the Herba Lysimachiae foenumgraeci extract and be used for the tobacco aromatics using aspect there is not yet report.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide a kind of take Herba Lysimachiae foenumgraeci as main component preparation have a tobacco aromatics using that increases sweet function.
The present invention also aims to provide the concrete application of described tobacco aromatics using in cigarette.
Purpose of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage ratio that adopts in the present invention is mass percent.
A kind of have a tobacco aromatics using that increases sweet function, prepared by following method:
(1) the Herba Lysimachiae foenumgraeci raw material is packed in extraction kettle, add 10% to carry agent, described to carry agent be 95% ethanol, with the CO of supercritical state
2Injecting extraction kettle, is 20～40MPa in extracting pressure, extracts 1～3h under the condition that extraction temperature is 30～50 ℃, is dissolved with the CO of aroma component
2Fluid enters separating still, heats up by step-down the aroma component of Herba Lysimachiae foenumgraeci is separated;
(2) with supercritical CO
2The material that extracts carries out molecular distillation, is that 150～200g/h, knifing speed are that 200～300r/min, distillation temperature are that 40～60 ℃, distillation pressure are to separate under 250～350Pa condition to obtain volatile oil in input speed;
(3) with after 50 times of volatile oil dilutions, obtain the tobacco aromatics using that required having increases sweet function.
The Herba Lysimachiae foenumgraeci tobacco aromatics using that makes with aforesaid method is the transparent oily liquids of a kind of pistac, has unique fragrant and sweet fragrance, have simultaneously peppermint and camphor note, makings is used in conjunction chromatographic instrument and analyzes to such an extent that its main component is: phantol, farnesene, Linaool, camphor, firpene, amphene, ocimene, terpinol, geraniol and oxymethoxyallylbenzene etc.
The concrete application of described tobacco aromatics using in cigarette: this tobacco aromatics using is added in cigarette shreds with 0.25%～0.75% mass ratio, then technique rolls into cigarette routinely.
Show by the experimental result of smokeing panel test, add the cigarette of this tobacco aromatics using compared with the control, have and enrich cigarette perfume (or spice), increase sweet sense and fine and smooth sense, promote fragrance matter, reduce and stimulate, make cigarette perfume (or spice) more thoroughly send out, promote the effect of comfortableness.
Compared with prior art, the present invention has following beneficial effect:
1, select the Fragrant vegetables Herba Lysimachiae foenumgraeci to be prepared as raw material, be conducive to improve the economic use value of Special plant;
2, the interpolation of this tobacco aromatics using in cigarette when obviously increasing sweet sense, has the effect of enriching cigarette perfume (or spice), reducing to stimulate, promote comfortableness;
3, production technique operability and standardization are strong, can realize suitability for industrialized production, have good development prospect.
Embodiment
The present invention is described in further detail by the following examples.Should be appreciated that specific embodiment described herein is only in order to explain the present invention, the protection domain that is not intended to limit the present invention.
Embodiment 1
---have the preparation that increases sweet function tobacco aromatics using and use 1
1. the preparation of extract
(1) the Herba Lysimachiae foenumgraeci raw material is packed in extraction kettle, add 10% to carry agent (95% ethanol), with the CO of supercritical state
2Injecting extraction kettle, is 20 MPa in extracting pressure, extracts 3 h under the condition that extraction temperature is 30 ℃, is dissolved with the CO of aroma component
2Fluid enters separating still, heats up by step-down the aroma component of Herba Lysimachiae foenumgraeci is separated;
(2) with supercritical CO
2The material that extracts carries out molecular distillation, is that 150 g/h, knifing speed are that 200 r/min, distillation temperature are that 40 ℃, distillation pressure are that the light constituent that separates under 250 Pa conditions to obtain is as the volatile oil that uses in input speed.
(3) with after 50 times of volatile oil dilutions, obtain the perfuming extract.
2. perfuming cigarette experiment
The natural plant extracts that utilization prepares is processed tobacco leaf leaf group, and the adding proportion according to 0.75% makes an addition to the leaf group as treatment group, and with the leaf group of not adding extract as a control group.
3. the experiment of smokeing panel test
After the pipe tobacco for the treatment of group and control group is put into climatic chamber inner equilibrium 24 h, make cigarette, sample and contrast random number, the group of smokeing panel test that is comprised of the expert who possesses the qualification of smokeing panel test carries out the sensory evaluating smoking.
4. effect evaluation
Add the experimental result of smokeing panel test and show in pipe tobacco, compared with the control, the interpolation of this natural plant extracts has increases sweet rhythm, enrich cigarette perfume (or spice), reduce the effect that stimulates, covers assorted gas, promotes comfortableness.
Embodiment 2
---have the preparation that increases sweet function tobacco aromatics using and use 2
1. the preparation of extract
(1) the Herba Lysimachiae foenumgraeci raw material is packed in extraction kettle, add 10% to carry agent (95% ethanol), with the CO of supercritical state
2Injecting extraction kettle, is 40 MPa in extracting pressure, extracts 1 h under the condition that the extraction temperature is 50 ℃, is dissolved with the CO of aroma component
2Fluid enters separating still, heats up by step-down the aroma component of Herba Lysimachiae foenumgraeci is separated;
(2) with supercritical CO
2The material that extracts carries out molecular distillation, is that 200 g/h, knifing speed are that 300 r/min, distillation temperature are that 60 ℃, distillation pressure are that the light constituent that separates under 350 Pa conditions to obtain is as the volatile oil that uses in input speed.
(3) with after 50 times of volatile oil dilutions, obtain the perfuming extract.
2. perfuming cigarette experiment
The natural plant extracts that utilization prepares is processed tobacco leaf leaf group, makes an addition to the leaf group as treatment group according to the adding proportion of 0.25 %, and with the leaf group of not adding extract as a control group.
3. the experiment of smokeing panel test
After the pipe tobacco for the treatment of group and control group is put into climatic chamber inner equilibrium 24 h, make cigarette, sample and contrast random number, the group of smokeing panel test that is comprised of the expert who possesses the qualification of smokeing panel test carries out the sensory evaluating smoking.
4. effect evaluation
Add the experimental result of smokeing panel test and show in pipe tobacco, compared with the control, the interpolation of this natural plant extracts can be enriched cigarette perfume (or spice), promotes fragrance matter, reduces stimulation, cover assorted gas, can increase sweet rhythm simultaneously.
Embodiment 3
---have the preparation that increases sweet function tobacco aromatics using and use 3
1. the preparation of extract
(1) the Herba Lysimachiae foenumgraeci raw material is packed in extraction kettle, add 10% to carry agent (95% ethanol), with the CO of supercritical state
2Injecting extraction kettle, is 30 MPa in extracting pressure, extracts 2 h under the condition that extraction temperature is 40 ℃, is dissolved with the CO of aroma component
2Fluid enters separating still, heats up by step-down the aroma component of Herba Lysimachiae foenumgraeci is separated;
(2) with supercritical CO
2The material that extracts carries out molecular distillation, is that 150 g/h, knifing speed are that 200 r/min, distillation temperature are that 50 ℃, distillation pressure are that the light constituent that separates under 300 Pa conditions to obtain is as the volatile oil that uses in input speed.
(3) with after 50 times of volatile oil dilutions, obtain the perfuming extract.
2. perfuming cigarette experiment
The natural plant extracts that utilization prepares is processed tobacco leaf leaf group, and the adding proportion according to 0.50% makes an addition to the leaf group as treatment group, and with the leaf group of not adding extract as a control group.
3. the experiment of smokeing panel test
After the pipe tobacco for the treatment of group and control group is put into climatic chamber inner equilibrium 24 h, make cigarette, sample and contrast random number, the group of smokeing panel test that is comprised of the expert who possesses the qualification of smokeing panel test carries out the sensory evaluating smoking.
4. effect evaluation
Add the experimental result of smokeing panel test and show in pipe tobacco, compared with the control, the interpolation of this natural plant extracts can be enriched cigarette perfume (or spice), reduces stimulation, covers assorted gas, promote comfortableness, increases simultaneously sweet rhythm.
The above is only preferred embodiment of the present invention, not in order to limiting the present invention, all any modifications of doing within the spirit and principles in the present invention, is equal to and replaces and improvement etc., within all should being included in protection scope of the present invention.
Claims (2)
1. one kind has the tobacco aromatics using that increases sweet function, is prepared by following method:
(1) the Herba Lysimachiae foenumgraeci raw material is packed in extraction kettle, add 10% to carry agent, described to carry agent be 95% ethanol, with the CO of supercritical state
2Injecting extraction kettle, is 20～40MPa in extracting pressure, extracts 1～3h under the condition that extraction temperature is 30～50 ℃, is dissolved with the CO of aroma component
2Fluid enters separating still, heats up by step-down the aroma component of Herba Lysimachiae foenumgraeci is separated;
(2) with supercritical CO
2The material that extracts carries out molecular distillation, is that 150～200g/h, knifing speed are that 200～300r/min, distillation temperature are that 40～60 ℃, distillation pressure are to separate under 250～350Pa condition to obtain volatile oil in input speed;
(3) with after 50 times of volatile oil dilutions, obtain the tobacco aromatics using that required having increases sweet function.
2. claim 1 is described has the concrete application of tobacco aromatics using in cigarette that increases sweet function: this tobacco aromatics using is added in cigarette shreds with 0.25%～0.75% mass ratio, then technique rolls into cigarette routinely.
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| CN105146714A (en) * | 2015-09-02 | 2015-12-16 | 云南中烟工业有限责任公司 | Method for improving cigarette moisturizing and aroma-improving effects by utilizing sweet basil |
| CN110684599A (en) * | 2019-10-24 | 2020-01-14 | 江西中烟工业有限责任公司 | Preparation method of azalea absolute oil suitable for cigarettes |
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| CN110684599A (en) * | 2019-10-24 | 2020-01-14 | 江西中烟工业有限责任公司 | Preparation method of azalea absolute oil suitable for cigarettes |
| CN111876256A (en) * | 2020-07-16 | 2020-11-03 | 云南中烟工业有限责任公司 | Fresh and sweet flavor type tobacco essence and preparation method and application thereof |
| CN115820341A (en) * | 2022-10-28 | 2023-03-21 | 延边天翊科技有限公司 | Essence for costustoot rhyme, preparation method and application thereof |
| CN115820341B (en) * | 2022-10-28 | 2024-02-02 | 延边天翊科技有限公司 | Essence for costustoot charm cigarettes, and preparation method and application thereof |
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